CN102740580B - A kind of Small-power microwave microplasma integration source - Google Patents
A kind of Small-power microwave microplasma integration source Download PDFInfo
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Abstract
本发明公开了一种小功率集成微波微等离子体源,包括锁相环频率合成器;可调衰减器,与锁相环频率合成器连接;宽带功率放大器,与可调衰减器连接;环行器,与宽带功率放大器连接;平面微带渐变螺旋电感耦合线圈,与环行器连接。工作时小功率微波输入到平面微带渐变螺旋电感耦合线圈而激励起微波微等离子体。本发明具有频率可调、功率可调、功率源保护以及小型便携等优点。
The invention discloses a low-power integrated microwave micro-plasma source, which comprises a phase-locked loop frequency synthesizer; an adjustable attenuator connected with the phase-locked loop frequency synthesizer; a broadband power amplifier connected with the adjustable attenuator; a circulator , connected with broadband power amplifier; planar microstrip gradient spiral inductively coupled coil, connected with circulator. When working, low-power microwaves are input to the planar microstrip gradient spiral inductively coupled coil to excite microwave microplasma. The invention has the advantages of adjustable frequency, adjustable power, power source protection, small size and portability.
Description
技术领域technical field
本发明涉及微波等离子体源的技术领域,尤其涉及一种小功率集成微波微等离子体源。The invention relates to the technical field of microwave plasma sources, in particular to a low-power integrated microwave micro-plasma source.
背景技术Background technique
小功率微波微等离子体技术是一项近几年发展起来的集微电子技术、微波技术和等离子体技术于一体的高新技术,它是随着MEMS技术的发展而发展起来的。微等离子体包括直流微等离子体、射频微等离子体和微波微等离子体。当放电空间进一步减小到纳米尺寸时,就成为纳等离子体。由于微电子机械系统(MEMS)具有低损耗、高隔离、体积小、制造成本低、易与IC、MMIC电路集成等特点,通过MEMS工艺可以实现微波等离子体的小功率封装和有源集成。因此将微波等离子体结合MEMS工艺可使等离子体的结构和特性发生巨大的改变。Low-power microwave micro-plasma technology is a high-tech developed in recent years that integrates microelectronics technology, microwave technology and plasma technology. It develops along with the development of MEMS technology. Micro plasmas include direct current micro plasmas, radio frequency micro plasmas and microwave micro plasmas. When the discharge space is further reduced to a nanometer size, it becomes a nanoplasma. Because microelectromechanical systems (MEMS) have the characteristics of low loss, high isolation, small size, low manufacturing cost, and easy integration with IC and MMIC circuits, low-power packaging and active integration of microwave plasma can be realized through MEMS technology. Therefore, combining microwave plasma with MEMS technology can greatly change the structure and characteristics of plasma.
微波等离子体可广泛应用于新材料、微电子和化学等高科技领域,随着微波等离子体的小型化发展,电路尺寸要求在毫米级、微米级甚至纳米级,以前那种厘米甚至米级的大面积的微波等离子体已不再适用。在微波微等离子体的研究中,小功率微波微等离子体源的结构封装和系统集成是非常重要的两个环节。小功率平面螺旋电感耦合微波微等离子体源就是采用MEMS工艺通过微小功率微波激励起微小尺寸的等离子体,如用不超过1~3瓦的微波功率使气体电离,产生10毫米甚至0.2毫米尺寸的等离子体。由于此项技术在生物MEMS的杀菌消毒、小尺寸材料的处理、微化学分析系统、微型推进器等领域具有良好的应用前景,因而受到越来越广泛的关注。Microwave plasma can be widely used in high-tech fields such as new materials, microelectronics and chemistry. With the development of miniaturization of microwave plasma, the circuit size is required to be at the millimeter level, micron level or even nanometer level. The previous centimeter or even meter level Large-area microwave plasmas are no longer applicable. In the research of microwave microplasma, the structural packaging and system integration of low-power microwave microplasma source are two very important links. The low-power planar spiral inductively coupled microwave micro-plasma source uses MEMS technology to excite micro-sized plasma through micro-power microwaves. For example, the gas is ionized with a microwave power of no more than 1 to 3 watts, and a 10 mm or even 0.2 mm size plasma is generated. plasma. Because this technology has good application prospects in the fields of sterilization and disinfection of biological MEMS, processing of small-sized materials, microchemical analysis systems, and micro propulsion, it has received more and more attention.
目前国外使用的小功率微波微等离子体源主要采用900MHz的频段,输出功率为4瓦,虽然结构简单,但只能工作在单一频点和单一功率,即频率和功率都不可调。如果微带平面渐变螺旋电感线圈的结构和频率发生变化,则需要重新设计功率源的硬件电路。At present, the low-power microwave micro-plasma source used abroad mainly adopts the frequency band of 900MHz, and the output power is 4 watts. Although the structure is simple, it can only work at a single frequency point and single power, that is, neither frequency nor power can be adjusted. If the structure and frequency of the microstrip planar gradient spiral inductance coil change, the hardware circuit of the power source needs to be redesigned.
发明内容Contents of the invention
本发明克服了上述功率源的缺陷,较好实现了小功率微波微等离子体源的频率可调、功率可调、功率源保护以及小型便携。The invention overcomes the above-mentioned defects of the power source, and preferably realizes adjustable frequency, adjustable power, power source protection and small-scale portability of the low-power microwave micro-plasma source.
根据微波电路理论,采用锁相环频率合成器、可调衰减器、宽带功率放大器、环行器等的系统集成可满足辐射单元激励微波微等离子体的要求。小功率集成微波微等离子体源通过上位机程序调节频率,锁相环频率合成器产生微波信号,电位器调节衰减量,宽带功率放大器放大后的微波功率经过环行器输入到微带平面渐变螺旋电感线圈上,在常压或低压条件下激励起微波微等离子体。According to microwave circuit theory, the system integration using phase-locked loop frequency synthesizer, adjustable attenuator, broadband power amplifier, circulator, etc. can meet the requirements of the radiation unit to excite microwave micro-plasma. The low-power integrated microwave micro-plasma source adjusts the frequency through the host computer program, the phase-locked loop frequency synthesizer generates microwave signals, the potentiometer adjusts the attenuation, and the microwave power amplified by the broadband power amplifier is input to the microstrip plane gradient spiral inductor through the circulator On the coil, microwave micro-plasma is excited under the condition of normal pressure or low pressure.
本发明提出了一种小功率集成微波微等离子体源,包括:The present invention proposes a low-power integrated microwave micro-plasma source, comprising:
锁相环频率合成器,用于产生性能优良的微波频率振荡信号;A phase-locked loop frequency synthesizer, used to generate microwave frequency oscillation signals with excellent performance;
可调衰减器,与所述锁相环频率合成器连接,用于增大所述微波频率振荡信号功率的可调范围;An adjustable attenuator, connected to the phase-locked loop frequency synthesizer, is used to increase the adjustable range of the power of the microwave frequency oscillation signal;
宽带功率放大器,与所述可调衰减器连接,用于放大所述微波频率振荡信号;a broadband power amplifier, connected to the adjustable attenuator, for amplifying the microwave frequency oscillation signal;
环行器,与所述宽带功率放大器连接,用于减小微波微等离子体的激励所带来的阻抗不匹配对小型微波功率源的影响;A circulator, connected to the broadband power amplifier, is used to reduce the impact of the impedance mismatch caused by the excitation of microwave micro-plasma on the small microwave power source;
平面微带渐变螺旋电感耦合线圈,与所述环行器连接,用于激励微波微等离子体。A planar microstrip tapered spiral inductively coupled coil is connected with the circulator and used to excite microwave microplasma.
其中,所述锁相环频率合成器的频率输出范围为2.3GHz至2.6GHz。Wherein, the frequency output range of the phase-locked loop frequency synthesizer is 2.3GHz to 2.6GHz.
其中,所述可调衰减器的衰减范围在-2dB至-17dB。Wherein, the attenuation range of the adjustable attenuator is -2dB to -17dB.
其中,所述宽带功率放大器的功率输出范围为+20dBm至+40dBm,峰值功率大于43dBm。Wherein, the power output range of the broadband power amplifier is +20dBm to +40dBm, and the peak power is greater than 43dBm.
其中,所述环行器的频率范围为2.3GHz至2.5GHz,插入损耗为0.25dB至0.3dB,隔离度为20dB至25dB。Wherein, the frequency range of the circulator is 2.3GHz to 2.5GHz, the insertion loss is 0.25dB to 0.3dB, and the isolation is 20dB to 25dB.
其中,所述平面微带渐变螺旋电感耦合线圈的匝数为3;所述平面微带渐变螺旋电感耦合线圈的线圈宽度为100μm至400μm,线圈间距为100μm至400μm,所述线圈宽度与线圈间距由外圈向内圈逐渐减小。Wherein, the number of turns of the planar microstrip gradient spiral inductively coupled coil is 3; the coil width of the planar microstrip gradient spiral inductively coupled coil is 100 μm to 400 μm, and the coil spacing is 100 μm to 400 μm, and the coil width and the coil spacing It gradually decreases from the outer ring to the inner ring.
其中,进一步包括匹配负载;所述匹配负载与所述环行器连接。Wherein, a matching load is further included; the matching load is connected to the circulator.
其中,所述匹配负载的频率范围为直流至2.7GHz,回波损耗大于20dB,功率容量为150瓦。Wherein, the frequency range of the matching load is from DC to 2.7GHz, the return loss is greater than 20dB, and the power capacity is 150W.
其中,进一步包括匹配电路,所述匹配电路连接所述环行器与平面微带渐变螺旋电感耦合线圈。Wherein, a matching circuit is further included, and the matching circuit is connected to the circulator and the planar microstrip tapered spiral inductively coupled coil.
其中,所述锁相环频率合成器、可调衰减器、宽带功率放大器以及环行器设置在屏蔽盒内。Wherein, the phase-locked loop frequency synthesizer, adjustable attenuator, broadband power amplifier and circulator are arranged in the shielding box.
本发明提供的小功率集成微波微等离子体源是一种激励微波微等离子体的装置,具有频率可调、功率可调、功率源保护以及小型便携等优点。小型微波功率源与平面微带渐变螺旋电感耦合线圈的集成使整个装置小型化;调节上位机程序使锁相环频率合成器的输出频率可调;改变可调衰减器的大小使输出微波功率可调;而环行器可减小微波微等离子体的激励所带来的阻抗不匹配对小型微波功率源的影响,起到保护小型微波功率源的作用。The low-power integrated microwave micro-plasma source provided by the invention is a device for exciting microwave micro-plasma, and has the advantages of adjustable frequency, adjustable power, power source protection, small size and portability. The integration of the small microwave power source and the planar microstrip gradient spiral inductive coupling coil makes the whole device miniaturized; adjusting the host computer program makes the output frequency of the phase-locked loop frequency synthesizer adjustable; changing the size of the adjustable attenuator makes the output microwave power adjustable The circulator can reduce the impact of the impedance mismatch caused by the excitation of microwave micro-plasma on the small microwave power source, and play a role in protecting the small microwave power source.
附图说明Description of drawings
图1是本发明小功率集成微波微等离子体源的系统结构示意图。Fig. 1 is a schematic diagram of the system structure of the low-power integrated microwave micro-plasma source of the present invention.
图2是本实施例中小功率集成微波微等离子体源的电路示意图。Fig. 2 is a schematic circuit diagram of a low-power integrated microwave micro-plasma source in this embodiment.
具体实施方式Detailed ways
下面结合附图和实施例对本发明的具体实施方式做进一步详细的说明,但不应以此限制本发明的保护范围。The specific implementation manner of the present invention will be further described in detail below in conjunction with the accompanying drawings and examples, but the protection scope of the present invention should not be limited thereby.
如图1-2所示,1-锁相环频率合成器,2-可调衰减器,3-宽带功率放大器,4-环行器,5-匹配负载,6-平面微带渐变螺旋电感耦合线圈,7-匹配电路,8-接口电路,9-USB接口,10-上位机,21-PIN管,22-3dB电桥,31-驱动放大器,32-末级宽带功率放大器。As shown in Figure 1-2, 1-phase-locked loop frequency synthesizer, 2-adjustable attenuator, 3-broadband power amplifier, 4-circulator, 5-matching load, 6-plane microstrip gradient spiral inductive coupling coil , 7-matching circuit, 8-interface circuit, 9-USB interface, 10-host computer, 21-PIN tube, 22-3dB bridge, 31-drive amplifier, 32-final broadband power amplifier.
如图1所示,本发明的小功率集成微波微等离子体源,包括:As shown in Figure 1, the low-power integrated microwave micro-plasma source of the present invention includes:
锁相环频率合成器1,用于产生性能优良的微波频率振荡信号;A phase-locked loop frequency synthesizer 1, which is used to generate a microwave frequency oscillation signal with excellent performance;
可调衰减器2,与锁相环频率合成器1连接,用于增大微波频率振荡信号功率的可调范围;The adjustable attenuator 2 is connected with the phase-locked loop frequency synthesizer 1, and is used to increase the adjustable range of the power of the microwave frequency oscillation signal;
宽带功率放大器3,与可调衰减器2连接,用于放大输入的微波频率振荡信号,使之在较宽频带内达到足够的功率电平;The broadband power amplifier 3 is connected with the adjustable attenuator 2, and is used for amplifying the input microwave frequency oscillation signal to make it reach a sufficient power level in a wider frequency band;
环行器4,与宽带功率放大器3连接,用于减小微波微等离子体的激励所带来的阻抗不匹配对小型微波功率源的影响,起到保护小型微波功率源的作用;The circulator 4 is connected with the broadband power amplifier 3, and is used to reduce the impact of the impedance mismatch brought by the excitation of the microwave micro-plasma on the small microwave power source, and protect the small microwave power source;
平面微带渐变螺旋电感耦合线圈6,与环行器4连接,用于激励微波微等离子体。The planar microstrip tapered spiral inductively coupled coil 6 is connected with the circulator 4 and is used to excite microwave microplasma.
其中,锁相环频率合成器1的频率输出范围为2.3GHz至2.6GHz。Wherein, the frequency output range of the phase-locked loop frequency synthesizer 1 is 2.3GHz to 2.6GHz.
其中,可调衰减器2的衰减范围在-2dB至-17dB。Wherein, the attenuation range of the adjustable attenuator 2 is from -2dB to -17dB.
其中,宽带功率放大器3的功率输出范围为+20dBm至+40dBm,峰值功率大于43dBm。Wherein, the power output range of the broadband power amplifier 3 is +20dBm to +40dBm, and the peak power is greater than 43dBm.
其中,环行器4的频率范围为2.3GHz至2.5GHz,插入损耗为0.25dB至0.3dB,隔离度为20dB至25dB。Wherein, the frequency range of the circulator 4 is 2.3GHz to 2.5GHz, the insertion loss is 0.25dB to 0.3dB, and the isolation is 20dB to 25dB.
其中,平面微带渐变螺旋电感耦合线圈6的匝数为3;平面微带渐变螺旋电感耦合线圈6的线圈宽度为100μm至400μm,,线圈间距为100μm至400μm,线圈宽度与线圈间距由外圈向内圈逐渐减小。Among them, the number of turns of the planar microstrip gradient spiral inductively coupled coil 6 is 3; the coil width of the planar microstrip gradient spiral inductively coupled coil 6 is 100 μm to 400 μm, and the coil spacing is 100 μm to 400 μm, and the coil width and coil spacing are determined by the outer ring gradually decreases toward the inner circle.
其中,进一步包括匹配负载5;匹配负载5与环行器4连接。Wherein, a matching load 5 is further included; the matching load 5 is connected to the circulator 4 .
其中,匹配负载5的频率范围为直流至2.7GHz,回波损耗大于20dB,功率容量为150瓦。Wherein, the frequency range of the matching load 5 is from direct current to 2.7 GHz, the return loss is greater than 20 dB, and the power capacity is 150 watts.
其中,进一步包括匹配电路7,匹配电路7连接环行器4与平面微带渐变螺旋电感耦合线圈6。Wherein, a matching circuit 7 is further included, and the matching circuit 7 is connected to the circulator 4 and the planar microstrip tapered spiral inductively coupled coil 6 .
其中,锁相环频率合成器1、可调衰减器2、宽带功率放大器3以及环行器4设置在屏蔽盒内。Wherein, the phase-locked loop frequency synthesizer 1, the adjustable attenuator 2, the broadband power amplifier 3 and the circulator 4 are arranged in the shielding box.
实施例1Example 1
本实施例中锁相环频率合成器1的芯片为ADF4350,锁相环频率合成器1的输出频率为2.45GHz,整体相噪在频偏1kHz为-73dBc,在频偏100kHz为-87dBc/Hz。锁相环频率合成器1通过接口电路8以及USB接口9与上位机10连接。上位机10通过USB接口9向接口电路8发送数据,接口电路8由微控制器芯片CY7C68013完成USB接口9到三线串口的转换,实现上位机10与锁相环频率合成器1的数据传输。In this embodiment, the chip of PLL frequency synthesizer 1 is ADF4350, the output frequency of PLL frequency synthesizer 1 is 2.45GHz, and the overall phase noise is -73dBc at frequency deviation 1kHz, and is -87dBc/Hz at frequency deviation 100kHz . The phase-locked loop frequency synthesizer 1 is connected to a host computer 10 through an interface circuit 8 and a USB interface 9 . The host computer 10 sends data to the interface circuit 8 through the USB interface 9, and the interface circuit 8 completes the conversion from the USB interface 9 to the three-wire serial port by the microcontroller chip CY7C68013, and realizes the data transmission between the host computer 10 and the phase-locked loop frequency synthesizer 1.
本实施例中可调衰减器2包括PIN管21与3dB电桥22。可调衰减器2的PIN管21的芯片为HSMP3814,3dB电桥22的芯片为JP503S,可调衰减器2的衰减值为-10dB。In this embodiment, the adjustable attenuator 2 includes a PIN tube 21 and a 3dB bridge 22 . The chip of the PIN tube 21 of the adjustable attenuator 2 is HSMP3814, the chip of the 3dB bridge 22 is JP503S, and the attenuation value of the adjustable attenuator 2 is -10dB.
本实施例中宽带功率放大器3包括驱动放大器31与末级宽带功率放大器32。驱动放大器31的芯片为SBB-4089Z,末级宽带功率放大器32的芯片为MW7IC2725,末级宽带功率放大器32的功率输出为+32dBm。In this embodiment, the broadband power amplifier 3 includes a driving amplifier 31 and a final broadband power amplifier 32 . The chip of the driving amplifier 31 is SBB-4089Z, the chip of the final broadband power amplifier 32 is MW7IC2725, and the power output of the final broadband power amplifier 32 is +32dBm.
本实施例中环行器4的芯片为MAFR-000488,50Ω匹配负载5的芯片为E150N50X4。In this embodiment, the chip of the circulator 4 is MAFR-000488, and the chip of the 50Ω matching load 5 is E150N50X4.
本实施例中平面微带渐变螺旋电感耦合线圈6的匝数为3,线圈宽度和线圈间距由外向内逐渐减小,而且最内圈终端开路。平面微带渐变螺旋电感耦合线圈6的输入端使用SMA接头。In this embodiment, the number of turns of the planar microstrip gradient spiral inductively coupled coil 6 is 3, the coil width and coil spacing gradually decrease from outside to inside, and the innermost coil terminal is open. The input end of the planar microstrip tapered spiral inductively coupled coil 6 uses an SMA connector.
本实施例中平面微带渐变螺旋电感耦合线圈6中的线圈部分采用高导电率的金属材料,该高导电率的金属材料是金。In this embodiment, the coil part of the planar microstrip tapered spiral inductively coupled coil 6 is made of high-conductivity metal material, and the high-conductivity metal material is gold.
本实施例中平面微带渐变螺旋电感耦合线圈6的基片部分采用耐高温、耐腐蚀的低损耗介质基片,该低损耗介质基片为氧化铝陶瓷。In this embodiment, the substrate part of the planar microstrip tapered spiral inductive coupling coil 6 adopts a high-temperature-resistant, corrosion-resistant low-loss dielectric substrate, and the low-loss dielectric substrate is alumina ceramics.
如图2所示,本实施例中的提供一种小功率集成微波微等离子体源,包括频率源合成器1、可调衰减器2、宽带功率放大器3、环行器4、匹配电路7和平面微带渐变螺旋电感耦合线圈6,上述各部件依次连接。锁相环频率合成器1、可调衰减器2、宽带功率放大器3以及环行器4设置在屏蔽盒内。50Ω匹配负载5与环行器4连接。As shown in Figure 2, a low-power integrated microwave micro-plasma source is provided in this embodiment, including a frequency source synthesizer 1, an adjustable attenuator 2, a broadband power amplifier 3, a circulator 4, a matching circuit 7 and a plane The microstrip tapered spiral inductively coupled coil 6, the above-mentioned components are connected in sequence. A phase-locked loop frequency synthesizer 1, an adjustable attenuator 2, a broadband power amplifier 3 and a circulator 4 are arranged in the shielding box. The 50Ω matching load 5 is connected to the circulator 4 .
工作时,将锁相环频率合成器1依次通过接口电路8、USB接口9与上位机10进行连接。由上位机10控制锁相环频率合成器1产生2.45GHz的微波频率振荡信号,通过可调衰减器2调节微波频率振荡信号的幅度,使可调衰减器2的衰减量为-8dB,微波频率振荡信号依次输入到宽带功率放大器3的驱动放大器31与末级宽带功率放大器32进行功率放大,经过放大后该微波频率振荡信号的功率为+32dBm。微波频率振荡信号经过微波功率放大后经过环行器4馈入平面微带渐变螺旋电感耦合线圈6,在0.04Torr至10Torr的气压条件下激励起微波微等离子体,从而实现小功率微波微等离子体源。When working, the phase-locked loop frequency synthesizer 1 is connected to the host computer 10 through the interface circuit 8 and the USB interface 9 in sequence. The host computer 10 controls the phase-locked loop frequency synthesizer 1 to generate a microwave frequency oscillating signal of 2.45GHz, and adjusts the amplitude of the microwave frequency oscillating signal through the adjustable attenuator 2, so that the attenuation of the adjustable attenuator 2 is -8dB, and the microwave frequency The oscillating signal is sequentially input to the drive amplifier 31 of the broadband power amplifier 3 and the final broadband power amplifier 32 for power amplification, and the power of the microwave frequency oscillating signal after amplification is +32dBm. The microwave frequency oscillating signal is amplified by the microwave power and fed into the planar microstrip gradient spiral inductively coupled coil 6 through the circulator 4, and the microwave micro-plasma is excited under the pressure condition of 0.04Torr to 10Torr, so as to realize the low-power microwave micro-plasma source .
匹配电路7采用自谐振结构匹配电路或叉指电容结构匹配电路,用于对平面微带渐变螺旋电感耦合线圈6进行调配,使匹配电路7左端看进去的输入阻抗为50Ω。The matching circuit 7 adopts a self-resonant structure matching circuit or an interdigitated capacitor structure matching circuit, which is used to adjust the planar microstrip gradient spiral inductive coupling coil 6, so that the input impedance seen from the left end of the matching circuit 7 is 50Ω.
以上所述仅为本发明的较佳实施例,并非用来限定本发明的实施范围。任何所属技术领域中具有通常知识者,在不脱离本发明的精神和范围内,当可作各种变动与润饰,本发明保护范围应以权利要求书所界定的保护范围为准。The above descriptions are only preferred embodiments of the present invention, and are not intended to limit the implementation scope of the present invention. Anyone with ordinary knowledge in the technical field may make various changes and modifications without departing from the spirit and scope of the present invention, and the protection scope of the present invention shall be determined by the protection scope defined in the claims.
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