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CN102607929A - Pneumatic type sample loader - Google Patents

Pneumatic type sample loader Download PDF

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Publication number
CN102607929A
CN102607929A CN2012100558146A CN201210055814A CN102607929A CN 102607929 A CN102607929 A CN 102607929A CN 2012100558146 A CN2012100558146 A CN 2012100558146A CN 201210055814 A CN201210055814 A CN 201210055814A CN 102607929 A CN102607929 A CN 102607929A
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air
pressure chamber
pressure
groove
storage room
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CN102607929B (en
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杨伟
伍向阳
郝召兵
黄卫清
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Institute of Geology and Geophysics of CAS
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Abstract

一种气压式样品装样器:一气压室,内部装有活塞块,该活塞块上方连接一活塞杆,由活塞杆带动活塞块在气压室内做向下和向上的往复运动;该气压室的下端连接第一固定压帽,该第一固定压帽的下方连接储物室;第一固定压帽设有第一锥度槽和第二锥度槽,其中第一个锥度槽贯通气压室和储物室,所述第一锥度槽的锥度口朝向气压室;第二锥度槽连接一气道,所述第二锥度槽的锥度口朝向储物室;第一锥度槽和第二锥度槽内均设有一弹簧,其中第一锥度槽内的弹簧上方抵顶一钢珠,形成由气压室至储物室的单向气阀;第二锥度槽内的弹簧下方抵顶一钢珠,形成气压室至大气的单向气阀;储物室的下端口设有第二固定压帽,该第二固定压帽与储物室之间夹持一橡皮套。

Figure 201210055814

A pneumatic sample loader: an air pressure chamber with a piston block inside, a piston rod connected above the piston block, and the piston rod drives the piston block to reciprocate downward and upward in the air pressure chamber; the air pressure chamber The lower end is connected to the first fixed pressure cap, and the bottom of the first fixed pressure cap is connected to the storage room; the first fixed pressure cap is provided with a first tapered groove and a second tapered groove, wherein the first tapered groove penetrates the air pressure chamber and the storage chamber, the taper mouth of the first taper groove is facing the air pressure chamber; the second taper groove is connected to an air passage, and the taper mouth of the second taper groove is facing the storage chamber; a Spring, wherein the top of the spring in the first tapered groove is against a steel ball to form a one-way air valve from the air pressure chamber to the storage chamber; the bottom of the spring in the second tapered groove is against a steel ball to form a one-way air valve from the air pressure chamber to the atmosphere. Air valve; the lower port of the storage chamber is provided with a second fixed pressure cap, and a rubber sleeve is clamped between the second fixed pressure cap and the storage chamber.

Figure 201210055814

Description

一种气压式样品装样器A pneumatic sample loader

技术领域 technical field

本发明涉及一种用于测定岩石样品的物理和力学参数的工具,更具体地涉及一种气压式样品装样器,以方便岩石样品的物理和力学参数测试中橡皮套密封样品的装配。The invention relates to a tool for measuring physical and mechanical parameters of rock samples, and more particularly relates to a pneumatic sample loader to facilitate the assembly of rubber-sealed samples in the testing of physical and mechanical parameters of rock samples.

背景技术 Background technique

在工程、能源应用及地球科学研究等领域常常需要测定岩石样品的物理和力学参数。在具有压力环境下岩石样品的物理和力学参数测试实验中,样品需要用密封材料紧密包裹,以防止传压介质进入样品。从方便和经济角度常选用橡皮套为密封材料,实际中使用橡皮套包裹样品时,要碰到以下问题:In the fields of engineering, energy application and earth science research, it is often necessary to determine the physical and mechanical parameters of rock samples. In the physical and mechanical parameter testing experiments of rock samples under pressure, the samples need to be tightly wrapped with sealing materials to prevent the pressure transmission medium from entering the samples. From the perspective of convenience and economy, rubber sleeves are often used as sealing materials. In practice, when using rubber sleeves to wrap samples, the following problems must be encountered:

1)装样困难,实验测试要求橡皮套与样品紧贴,所以橡皮套的内径要小于样品的外径,以利用橡皮套的弹性紧密包裹样品。这导致把样品放入橡皮套时需要把橡皮套撑开,常常通过用力挤入的方式,但这种方式是比较费力的。实际中使用的橡皮套常需要一定的厚度,以达到在温度压力下保持一定物理机械性能的要求,这样把样品用力挤入厚的橡皮套中将更加费力;1) It is difficult to load the sample. The experimental test requires the rubber sleeve to be close to the sample, so the inner diameter of the rubber sleeve should be smaller than the outer diameter of the sample, so as to use the elasticity of the rubber sleeve to tightly wrap the sample. This leads to the need to stretch the rubber sheath when putting the sample into the rubber sheath, often by forcing it in, but this method is relatively laborious. The rubber sleeve used in practice often needs a certain thickness to meet the requirements of maintaining certain physical and mechanical properties under temperature and pressure, so it will be more laborious to squeeze the sample into a thick rubber sleeve;

2)如果样品的结构比较软弱,装样时施加压力过大就容易把样品压坏。2) If the structure of the sample is relatively weak, it is easy to crush the sample if the pressure is too large when loading the sample.

发明内容 Contents of the invention

本发明的目的在于提供一种气压式样品装样器,以改进公知技术中存在的缺陷。The object of the present invention is to provide a pneumatic sample loader to improve the defects in the known technology.

为实现上述目的,本发明提供的气压式样品装样器,主要包括有:In order to achieve the above object, the pneumatic sample loader provided by the present invention mainly includes:

一气压室,内部装有活塞块,该活塞块上方连接一活塞杆,由活塞杆带动活塞块在气压室内做向下和向上的往复运动;A pneumatic chamber with a piston block inside, a piston rod is connected above the piston block, and the piston rod drives the piston block to reciprocate downward and upward in the air pressure chamber;

该气压室的下端连接第一固定压帽,该第一固定压帽的下方连接储物室;The lower end of the air pressure chamber is connected to the first fixed pressure cap, and the bottom of the first fixed pressure cap is connected to the storage chamber;

第一固定压帽设有第一锥度槽和第二锥度槽,其中第一个锥度槽贯通气压室和储物室,所述第一锥度槽的锥度口朝向气压室;第二锥度槽连接一气道,所述第二锥度槽的锥度口朝向储物室;The first fixed pressure cap is provided with a first taper groove and a second taper groove, wherein the first taper groove passes through the air pressure chamber and the storage chamber, and the taper opening of the first taper groove faces the air pressure chamber; the second taper groove connects an air Road, the tapered opening of the second tapered groove faces the storage chamber;

第一锥度槽和第二锥度槽内均设有一弹簧,其中第一锥度槽内的弹簧上方抵顶一钢珠,形成由气压室至储物室的单向气阀;A spring is provided in both the first tapered groove and the second tapered groove, wherein the upper part of the spring in the first tapered groove bears against a steel ball to form a one-way air valve from the air pressure chamber to the storage chamber;

第二锥度槽内的弹簧下方抵顶一钢珠,形成气压室至大气的单向气阀;The bottom of the spring in the second taper groove is against a steel ball to form a one-way air valve from the air pressure chamber to the atmosphere;

储物室的下端口设有第二固定压帽,该第二固定压帽与储物室之间夹持一橡皮套。The lower port of the storage chamber is provided with a second fixed pressure cap, and a rubber sleeve is sandwiched between the second fixed pressure cap and the storage chamber.

所述的气压式样品装样器,其中,气压室的上端固定有一上压盖,防止活塞块向上运动而从气压室脱离,活塞杆伸延出该上压盖。In the pneumatic sample loader, an upper gland is fixed on the upper end of the air pressure chamber to prevent the piston block from moving upwards and detaching from the air pressure chamber, and the piston rod extends out of the upper gland.

所述的气压式样品装样器,其中,活塞块的上下两面均设有密封圈,与活塞块一起和活塞杆连接形成一整体。In the pneumatic sample loader, the upper and lower surfaces of the piston block are provided with sealing rings, which are connected with the piston rod together with the piston block to form an integral body.

所述的气压式样品装样器,其中,储物室与第一固定压帽之间设有密封圈,使储物室的端面与第一固定压帽之间为密封状态。In the pneumatic sample loader, a sealing ring is provided between the storage chamber and the first fixed pressure cap, so that the end surface of the storage chamber and the first fixed pressure cap are in a sealed state.

所述的气压式样品装样器,其中,第一固定压帽中第一锥度槽和第二锥度槽的弹簧由固定透气螺母固定。In the pneumatic sample loader, the springs of the first tapered groove and the second tapered groove in the first fixed pressure cap are fixed by fixed air-permeable nuts.

所述的气压式样品装样器,其中,储物室夹持橡皮套的一端为一锥度面。In the pneumatic sample loader, one end of the storage chamber holding the rubber sleeve is a tapered surface.

所述的气压式样品装样器,其中,橡皮套的出口设有密封卡子。The pneumatic sample loader, wherein the outlet of the rubber sheath is provided with a sealing clip.

本发明提供的气压式样品装样器,在实际操作中,通过气压把橡皮套内径撑大以方便样品进入橡皮套中,实现样品无损装配,解决橡皮套密封样品的装配问题。The air pressure sample loader provided by the present invention expands the inner diameter of the rubber sheath by air pressure in actual operation to facilitate the entry of the sample into the rubber sheath, realizes the non-destructive assembly of the sample, and solves the assembly problem of the rubber sheath sealed sample.

附图说明 Description of drawings

图1是本发明的气压式样品装样器的结构示意图。Fig. 1 is a schematic structural view of a pneumatic sample loader of the present invention.

图2是图1所示方向的左侧视图,显示了本发明的气压式样品装样器进行装样时旋转的示意图。Fig. 2 is a left side view from the direction shown in Fig. 1, showing a schematic diagram of the rotation of the pneumatic sample loader of the present invention during sample loading.

附图中组件名称说明:Explanation of component names in the attached drawings:

1上压盖,2活塞块,3、7密封圈,4、20钢珠,5、19弹簧,6、18固定透气螺母,8第一固定压帽,9、13探头,10储物室,11样品,12第二固定压帽,14橡皮套,15密封卡子,16活塞杆,17气压室,21紧固手柄,22固定螺栓,23旋转盘,24固定支架,25紧固螺栓,26气道。1 upper gland, 2 piston block, 3, 7 sealing ring, 4, 20 steel ball, 5, 19 spring, 6, 18 fixed breathable nut, 8 first fixed pressure cap, 9, 13 probe, 10 storage room, 11 Sample, 12 second fixed pressure cap, 14 rubber sleeve, 15 sealing clip, 16 piston rod, 17 air chamber, 21 fastening handle, 22 fixing bolt, 23 rotating disc, 24 fixing bracket, 25 fastening bolt, 26 air channel .

具体实施方式 Detailed ways

以下结合附图对本发明作详细描述。The present invention will be described in detail below in conjunction with the accompanying drawings.

请参阅图1,本发明的气压式样品装样器基本由气压室17和储物室10两部分组成。Please refer to FIG. 1 , the pneumatic sample loader of the present invention is basically composed of two parts: a pneumatic chamber 17 and a storage chamber 10 .

气压室17上装设有上压盖1、活塞块2、密封圈3、钢珠4、弹簧5、固定透气螺母6、第一固定压帽8、活塞杆16、固定透气螺母18、弹簧19、钢珠20。The air pressure chamber 17 is equipped with an upper gland 1, a piston block 2, a sealing ring 3, a steel ball 4, a spring 5, a fixed ventilating nut 6, a first fixed pressing cap 8, a piston rod 16, a fixed ventilating nut 18, a spring 19, a steel ball 20.

上压盖1紧固在气压室17上,起到防止活塞块2向上运动而从气压室17脱离的作用。活塞块2放在气压室17内,与密封圈3和活塞杆16连接形成整体做向下和向上的往复运动,进行空气的压缩和吸气工作。第一固定压帽8内设有贯通气压室和储物室的第一个锥度槽,钢珠4放在第一固定压帽8的第一锥度槽内,该第一锥度槽的锥度口朝向气压室17,弹簧5放在第一固定压帽8的第一锥度槽内,从下面顶住钢珠4,固定透气螺母6放在第一固定压帽8的第一锥度槽内,在钢珠4和弹簧5的下面顶住弹簧5使它们成为一个整体,起到固定钢珠4和弹簧5的作用。在弹簧5和固定透气螺母6的作用下,可以使钢珠4上顶封住第一锥度槽的锥度口。当活塞块2与密封圈3及活塞杆16连接形成整体做向下压缩空气时,钢珠4在空气的压力下打开第一锥度槽的锥度口,压缩空气进入储物室10。当活塞块2与密封圈3及16活塞杆连接形成整体做向上运动时,空气压力降低,弹簧5将钢珠4重新顶住以封住第一锥度槽的锥度口,形成由气压室17至储物室10的单向气阀。The upper gland 1 is fastened on the air pressure chamber 17 to prevent the piston block 2 from moving upwards and disengaging from the air pressure chamber 17 . The piston block 2 is placed in the air pressure chamber 17, and is connected with the sealing ring 3 and the piston rod 16 to form a whole to perform downward and upward reciprocating movements to perform air compression and suction work. The first fixed pressure cap 8 is provided with a first tapered groove through the air pressure chamber and the storage chamber, the steel ball 4 is placed in the first tapered groove of the first fixed pressure cap 8, and the taper opening of the first tapered groove faces the air pressure In the chamber 17, the spring 5 is placed in the first tapered groove of the first fixed pressure cap 8 to withstand the steel ball 4 from below, and the fixed breathable nut 6 is placed in the first tapered groove of the first fixed pressure cap 8, between the steel ball 4 and The bottom of the spring 5 withstands the spring 5 and makes them into a whole, which plays the role of fixing the steel ball 4 and the spring 5. Under the action of the spring 5 and the fixed air-permeable nut 6, the steel ball 4 can be topped to seal the taper opening of the first taper groove. When the piston block 2 is connected with the sealing ring 3 and the piston rod 16 to form a whole to compress air downward, the steel ball 4 opens the taper opening of the first taper groove under the pressure of the air, and the compressed air enters the storage chamber 10 . When the piston block 2 is connected with the seal ring 3 and the 16 piston rod to move upwards as a whole, the air pressure decreases, and the spring 5 will support the steel ball 4 again to seal the taper opening of the first taper groove, forming a pressure chamber from the air pressure chamber 17 to the storage tank. The one-way air valve of object chamber 10.

第一固定压帽8还设有第二锥度槽,该第二锥度槽通过一气道26与外界大气相通,该第二锥度槽的锥度口朝向储物室10的方向,固定透气螺母18和弹簧19及钢珠20一起放在第二锥度槽内,锥度槽的底部朝下呈90度直角通过气道26与向外界贯通。钢珠20在弹簧19和固定透气螺母18作用下,向下封住第二锥度槽的锥度口,当活塞块2与密封圈3和活塞杆16连接形成整体做向下压缩空气时,钢珠4向下打开,压缩气体进入储物室10,这时钢珠20在弹簧19和固定透气螺母18作用下,封住第二锥度槽与气道26通往外部的通路,形成气压室17至大气的单向气阀。The first fixed pressure cap 8 is also provided with a second tapered groove, which communicates with the outside atmosphere through an air passage 26, and the tapered mouth of the second tapered groove faces the direction of the storage chamber 10, and fixes the breathable nut 18 and the spring. 19 and the steel ball 20 are placed together in the second tapered groove, and the bottom of the tapered groove is downward at a 90-degree right angle and passes through the air passage 26 to communicate with the outside world. Under the action of spring 19 and fixed vent nut 18, steel ball 20 seals the taper mouth of the second taper groove downwards. When piston block 2 is connected with sealing ring 3 and piston rod 16 to form a whole to compress air downward, steel ball 4 will Open down, the compressed gas enters the storage chamber 10, at this time the steel ball 20, under the action of the spring 19 and the fixed breathable nut 18, seals the second tapered groove and the passage of the air passage 26 leading to the outside, forming a single passage between the air pressure chamber 17 and the atmosphere. to the air valve.

第一固定压帽8是气压室17的基座,同时还是储物室10的固定压帽。第一固定压帽8和气压室17螺纹连接时,须用聚四氟乙烯料带缠在气压室17螺纹上起到密封作用。The first fixed pressure cap 8 is the base of the air pressure chamber 17 and also the fixed pressure cap of the storage chamber 10 . When the first fixed pressure cap 8 is threaded with the air pressure chamber 17, it must be wrapped around the air pressure chamber 17 threads with polytetrafluoroethylene tape to play a sealing effect.

储物室10装设有第一固定压帽8、探头9和13、样品11、第二固定压帽12、橡皮套14、15密封卡子。The storage chamber 10 is equipped with a first fixed pressure cap 8 , probes 9 and 13 , a sample 11 , a second fixed pressure cap 12 , rubber sleeves 14 , 15 sealing clips.

探头9和13放在储物室10内,样品11置于两个控头9和13之间。第二固定压帽12通过自身内螺纹和储物室10下面的外螺纹连接,同时把橡皮套14压在储物室10底部的锥度面上。第二固定压帽12底部和储物室10底部的锥度相同,拧紧第二固定压帽12将套在10储物室底部锥度面上的橡皮套14压住,起到固定和密封的作用。橡皮套14的出口安装有密封卡15,密封卡15的作用是把有一定长度的橡皮套14的出口密封卡住。The probes 9 and 13 are placed in the storage chamber 10, and the sample 11 is placed between the two control heads 9 and 13. The second fixed pressure cap 12 is connected with the external thread on the bottom of the storage chamber 10 through its own internal thread, and simultaneously presses the rubber sleeve 14 on the tapered surface at the bottom of the storage chamber 10 . The taper at the bottom of the second fixed pressure cap 12 is the same as that at the bottom of the storage chamber 10. Tighten the second fixed pressure cap 12 to push down the rubber sleeve 14 that is enclosed within the tapered surface at the bottom of the storage chamber 10 to play the role of fixing and sealing. The outlet of rubber sheath 14 is equipped with sealing card 15, and the effect of sealing card 15 is to have the export sealing of rubber sheath 14 of certain length to block.

随着气压室17的压缩空气不断打进,橡皮套14的内径不断膨胀和延长,为探头9、样品11和探头13能顺利进入橡皮套14内提供了足够的空间。当探头9、样品11和探头13进入橡皮套14后,松开第二固定压帽12取下橡皮套14,完成装样过程。As the compressed air in the air pressure chamber 17 is continuously injected, the inner diameter of the rubber sheath 14 is continuously expanded and extended, providing enough space for the probe 9, the sample 11 and the probe 13 to enter the rubber sheath 14 smoothly. After the probe 9, the sample 11 and the probe 13 enter the rubber sheath 14, the second fixing cap 12 is released to take off the rubber sheath 14, and the sample loading process is completed.

本发明的气压式样品装样器还设有旋转盘23,该旋转盘23可旋转地固定在固定支架24上,由该固定支架24固定在工作台上。The pneumatic sample loader of the present invention is also provided with a rotating disk 23 , which is rotatably fixed on a fixed bracket 24 and fixed on the workbench by the fixed bracket 24 .

紧固手柄21拧在固定螺栓22上,固定螺栓22穿过固定支架24上面的槽与旋转盘23拧紧形成一个整体。旋转盘23穿过固定支架24的中心孔,旋转盘23小头的直径与储物室10的外中部位置焊接形成一个整体,当旋转储物室10时带动旋转盘23同步运动,从图2中可以看到,旋转储物室10时可以用紧固手柄21拧紧在固定支架24面板上。紧固螺栓25穿过固定支架24的底部槽,固定支架24固定在桌子上面时用紧固螺栓25旋转顶住。在进行装样时,松开固定螺栓22,旋转气压式样品装样器呈水平状,将样品装入后再旋转气压式样品装样器呈垂直状,开始加压过程。旋转方向如图2中的箭头所示。The tightening handle 21 is screwed on the fixing bolt 22, and the fixing bolt 22 passes through the groove on the fixing bracket 24 and is tightened with the rotating disk 23 to form an integral body. The rotating disk 23 passes through the central hole of the fixed bracket 24, and the diameter of the small head of the rotating disk 23 is welded with the outer middle position of the storage chamber 10 to form a whole. When the storage chamber 10 is rotated, the rotating disk 23 is driven to move synchronously, as shown in FIG. 2 As can be seen in the figure, the fastening handle 21 can be used to tighten the fastening handle 21 on the panel of the fixed bracket 24 when the storage compartment 10 is rotated. Fastening bolt 25 passes the bottom groove of fixed support 24, and fixed support 24 is supported with fastening bolt 25 rotations when being fixed on the table. When loading the sample, the fixing bolt 22 is loosened, the pneumatic sample loader is rotated to be horizontal, and after the sample is loaded, the pneumatic sample loader is rotated to be vertical, and the pressurization process starts. The direction of rotation is indicated by the arrow in Figure 2.

Claims (7)

1. vapour-pressure type sample sample charging device mainly includes:
One air-pressure chamber, piston block is equipped with in inside, and this piston block top connects a piston rod, drives piston block by piston rod and in air-pressure chamber, does downwards and the to-and-fro movement that makes progress;
The lower end of this air-pressure chamber connects the first fixing pressure cap, this first fixing below connection material storage room of pressure cap;
First fixedly pressure cap be provided with the first tapering groove and the second tapering groove, wherein first tapering groove connects air-pressure chamber and material storage room, the tapering mouth of the said first tapering groove is towards air-pressure chamber; The second tapering groove connects an air flue, and the tapering mouth of the said second tapering groove is towards material storage room;
Be equipped with a spring in the first tapering groove and the second tapering groove, wherein a steel ball is replaced in the top of the spring in the first tapering groove, forms the Non-return air valve by air-pressure chamber to material storage room;
A steel ball is replaced in spring below in the second tapering groove, forms the Non-return air valve of air-pressure chamber to atmosphere;
The lower port of material storage room is provided with the second fixing pressure cap, this second fixing clamping one rubber case between pressure cap and the material storage room.
2. vapour-pressure type sample sample charging device according to claim 1, wherein, the upper end of air-pressure chamber is fixed with a upper press cover, prevents that piston block from moving upward and breaks away from from air-pressure chamber, and piston rod extends this upper press cover.
3. vapour-pressure type sample sample charging device according to claim 1, wherein, the upper and lower surface of piston block is equipped with O-ring seal, is connected to form an integral body with piston block and piston rod.
4. vapour-pressure type sample sample charging device according to claim 1, wherein, material storage room and first fixedly is provided with O-ring seal between the pressure cap, makes the end face and first of material storage room fixedly be sealing state between the pressure cap.
5. vapour-pressure type sample sample charging device according to claim 1, wherein, first fixedly in the pressure cap spring of the first tapering groove and the second tapering groove fix by the fixed ventilation nut.
6. vapour-pressure type sample sample charging device according to claim 1, wherein, an end of material storage room's clamping rubber case is a tapering face.
7. vapour-pressure type sample sample charging device according to claim 1, wherein, the outlet of rubber case is provided with the sealing clamp.
CN 201210055814 2012-03-05 2012-03-05 Pneumatic type sample loader Expired - Fee Related CN102607929B (en)

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Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS4847394U (en) * 1971-10-05 1973-06-21
JPH03229126A (en) * 1990-02-02 1991-10-11 Nkk Corp Pressure holding container
CN2188205Y (en) * 1993-10-22 1995-01-25 西南石油学院 Rock physical property parameter testing device
CN1242520A (en) * 1998-07-20 2000-01-26 丁天惠 Automatic air pressure sample feeding device for capillary electrophoretic instrument
CN2533463Y (en) * 2001-12-24 2003-01-29 中国科学院安徽光学精密机械研究所 Quick sample feeding device for analyzing solid sample in high vacuum
CN101143270A (en) * 2006-09-15 2008-03-19 中国科学院大连化学物理研究所 A sleeve type high temperature and high pressure resistant extraction cell and kit for solvent extraction
CN201159738Y (en) * 2008-02-21 2008-12-03 宝山钢铁股份有限公司 Sample orienting and locating transmission device for pneumatic sampling machine
CN101525742A (en) * 2009-04-20 2009-09-09 南京大学 Method for sample loading, sampling and sample transferring of chemical vapor deposition material growing equipment

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS4847394U (en) * 1971-10-05 1973-06-21
JPH03229126A (en) * 1990-02-02 1991-10-11 Nkk Corp Pressure holding container
CN2188205Y (en) * 1993-10-22 1995-01-25 西南石油学院 Rock physical property parameter testing device
CN1242520A (en) * 1998-07-20 2000-01-26 丁天惠 Automatic air pressure sample feeding device for capillary electrophoretic instrument
CN2533463Y (en) * 2001-12-24 2003-01-29 中国科学院安徽光学精密机械研究所 Quick sample feeding device for analyzing solid sample in high vacuum
CN101143270A (en) * 2006-09-15 2008-03-19 中国科学院大连化学物理研究所 A sleeve type high temperature and high pressure resistant extraction cell and kit for solvent extraction
CN201159738Y (en) * 2008-02-21 2008-12-03 宝山钢铁股份有限公司 Sample orienting and locating transmission device for pneumatic sampling machine
CN101525742A (en) * 2009-04-20 2009-09-09 南京大学 Method for sample loading, sampling and sample transferring of chemical vapor deposition material growing equipment

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