CN102552092A - A vine tea mask capsule and a method of preparing the same - Google Patents
A vine tea mask capsule and a method of preparing the same Download PDFInfo
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- CN102552092A CN102552092A CN2012100394729A CN201210039472A CN102552092A CN 102552092 A CN102552092 A CN 102552092A CN 2012100394729 A CN2012100394729 A CN 2012100394729A CN 201210039472 A CN201210039472 A CN 201210039472A CN 102552092 A CN102552092 A CN 102552092A
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- powder
- vine tea
- ampelopsis grossedentata
- facial film
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- POJWUDADGALRAB-PVQJCKRUSA-N Allantoin Natural products NC(=O)N[C@@H]1NC(=O)NC1=O POJWUDADGALRAB-PVQJCKRUSA-N 0.000 claims description 5
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Landscapes
- Medicines Containing Plant Substances (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Abstract
本发明的一种藤茶面膜胶囊的制备方法，包括藤茶粉的制备、脱脂处理、提取藤茶黄酮类化合物、结晶除杂、粉碎并灭菌、面膜胶囊粉的配制、装入胶囊。本发明的藤茶面膜胶囊为纯植物成分，无防腐剂、添加剂，对皮肤无刺激和伤害。使用时打开胶囊，取80ML80℃的热水，边搅拌，边把胶囊中的粉末缓慢均匀的倒入热水中。搅拌胶囊粉使其充分溶解后倒入膜板，冷却成型即为面膜，将面膜敷帖于面部，停留20-30分钟即可。藤茶面膜由纯天然魔芋胶与黄原胶配制而成，面膜外形晶莹剔透，渗透快、吸收好。不需无纺布做介质，不会因面膜纸而吸去大部分精华。还能根据自身肌肤美白、去黄、红润、祛痘排毒等需要配制多种美容功效面膜。The preparation method of a vine tea facial mask capsule of the present invention comprises the preparation of vine tea powder, degreasing treatment, extraction of vine tea flavonoids, crystallization and impurity removal, crushing and sterilization, preparation of mask capsule powder, and filling into capsules. The rattan tea facial mask capsule of the present invention is pure plant components, without preservatives and additives, and has no stimulation and damage to the skin. When using, open the capsule, take 80ML hot water at 80°C, and pour the powder in the capsule into the hot water slowly and evenly while stirring. Stir the capsule powder to make it fully dissolve, pour it into the film plate, cool and form it into a mask, apply the mask on the face, and leave it for 20-30 minutes. The vine tea mask is made of pure natural konjac gum and xanthan gum. The mask has a crystal clear appearance, fast penetration and good absorption. There is no need for non-woven fabric as a medium, and most of the essence will not be absorbed by the mask paper. It can also prepare a variety of cosmetic masks according to the needs of skin whitening, yellowing, redness, acne and detoxification.
Description
Technical field
The present invention relates to a kind of cosmetics and preparation method thereof, be specifically related to a kind of Ampelopsis grossedentata facial film capsule and preparation method thereof.
Background technology
Step into aging gradually and diet is unhealthy, Exposure to Sunlight, pressure, environmental pollution etc. along with Chinese society, the anti-aging beauty-care skin care item more and more receive people's attention.The data of China spices and essence cosmetics industry association issue show that defying age is the problem that present women is concerned about most.One of main factor of skin aging is that the skin photosensitiveness that caused by ultraviolet radiation is old and feeble; Because ultraviolet is after infiltrating skin; Can produce harmful free radicals, these free radicals can destroy elastic fibers of skin, and the stimulation melanin cell increases secretion; Thereby cause xerosis cutis lax, quicken old and feeble.So need help reduce the generation of free radical through replenishing antioxidant.Present antioxidant has two types of enzyme and non-enzymes, and because of its poor stability, and molecular weight is bigger, infiltrates skin and is restricted, and has limited its application in cosmetics.Recently the micromolecule antioxidant that discovery is extracted from plant has very strong antioxidation, and more is prone to infiltrate skin, and is more stable.Plant flavonoids has very strong oxidation resistance, has free radical in the skin of removing, promotion skin metabolism, reduces effects such as pigmentation, moist skin.Because flavones content is high in the Ampelopsis grossedentata, extract simple, can be developed into for safely, natural material in the green cosmetic field that has no side effect.
Application number is 01104418.7 patent of invention " a kind of biological anti-senility cosmetics " (applying date: 2001/02/26), introduced the crease-resistant emulsion of a kind of skin moistening.Though the main defying age composition cucumber extract of these cosmetics, Aloe extraction solution also are biotypes; But added Polyethylene Glycol as o/w type emulsifying agent and stabilizing agent; Show that it has side effect to skin though go back no evidence; But it is influential to gastric secretion and gastric acid secretory volume during as solvent in the pharmaceutical preparation or substrate that existing report shows when it, explains that it still has certain toxicity.
Application number is 200810030279.2 patent of invention " interpolation biological micro crystal freeze-dried powder the anti-aging cosmetics " (applying date: 2008/08/20); Introduced a kind of biomedical high nutritional type lyophilized powder; It adopts nanotechnology with the technical finesse of effective collagenic protein through lyophilized powder, uses the effective defying age composition of active ingredient transmission.Though this cosmetics absorbance is high, need to add antiseptic, and troublesome poeration, cost is also higher.
Application number is 01135113.6 patent of invention " the natural plant beauty skin-protection mask " (applying date: 2001/11/19), introduced a kind of powder face pack.Though this formula for a product also has the effect of anti-ageing wrinkle removal, can only its furnishing paste be smeared after adding water, and paste typing effect is not good enough, and is unfavorable for cleaning, use comparatively trouble.
Application number is patent of invention " a kind of Rhizoma amorphophalli facial film " (applying date: 2008/11/24), introduced a kind of Rhizoma amorphophalli facial film of 200810158986.x.Though this product also has certain anti-ageing effect, this type of facial mask needs packing cost, and storage life or corrosion-resistant problem are arranged, and price is higher, not environmental protection, and variability is little simultaneously, can't fill a prescription according to the demand adjustment voluntarily, thereby cause using inconvenience.
Summary of the invention
Deficiency in view of prior art; Film property after the objective of the invention is to utilize anti-oxidation characteristics and Konjac glucomannan and the xanthan gum of flavone compound in the Ampelopsis grossedentata composite, provide a kind of with low cost, safely, have no side effect, can be by Ampelopsis grossedentata facial film capsule of skin fast Absorption and preparation method thereof.
The capsular method for preparing of a kind of Ampelopsis grossedentata facial film of the present invention is characterized in that operating procedure is following:
(1) preparation of Ampelopsis grossedentata powder: the chopping of Ampelopsis grossedentata tender leaf is placed in the baking oven, under 50～100 ℃ of conditions, toasted 48～60 hours, take out pulverizing and cross 60～80 mesh sieves, process the Ampelopsis grossedentata powder;
(2) ungrease treatment: the Ampelopsis grossedentata powder that step (1) is made; Using quality is to carry out ungrease treatment under 50～70 ℃ of reflux states as 10-30 ethyl acetate doubly in temperature; The defat response time is 1.6～2 hours; Filter then, vacuum drying is 1～2 hour under 70～80 ℃ of conditions, removes ethyl acetate;
(3) extract the vine tea flavone compounds: (W/V) is 1:20～35 by the mass volume ratio of feed liquid; In extraction vessel, add Ampelopsis grossedentata powder and distilled water after step (2) ungrease treatment; Reflux is 2～4 hours under 80～90 ℃ of conditions, is cooled to room temperature, with 3000～4000rpm centrifugalize; Collect supernatant, be the vine tea flavone crude extract;
(4) crystallization remove impurity: under 50 ℃ of conditions of vine tea flavone crude extract that step (3) is made 1/10～1/20 of vacuum concentration to initial volume; The deionized water and stirring that adds 1～2 times of concentrated solution volume is even, in boiling water bath, heats 20～30 minutes, leaves standstill crystalline deposit; Filter; Get crystal, drying obtains vine tea flavone;
(5) pulverize and sterilization: the vine tea flavone that step (4) is made is pulverized and is crossed 1000～1200 mesh sieves, in 100～110 ℃ of following sterilization treatment, can not check pathogenic bacterium to inspection, makes the vine tea flavone powder;
(6) preparation of facial film capsule powder: facial film capsule powder comprises following each raw material, and the percentage rate that each raw material accounts for facial film capsule powder gross mass is: vine tea flavone powder 20～26%, Konjac glucomannan 15～18%, xanthan gum 15～18%, soybean protein isolate 10～14%, arbutin 5～8%, hyaluronic acid (HA) 5～10%, Radix Scutellariae 4～8%, left-handed VC6～8%, allantoin 4～5%;
(7) incapsulate: incapsulate behind the facial film capsule powder mix homogeneously with step (6) preparation.
Described Konjac glucomannan, xanthan gum, soybean protein isolate, hyaluronic acid, Radix Scutellariae, left-handed VC, arbutin, allantoin are cosmetics-stage.
The capsular method for using of the present invention is: every capsules is generally 0.45g.Open capsule during use, get the hot water of 80 ℃ of 80ML, stir on the limit, and the limit is slowly poured the powder in the capsule in the hot water into uniformly.Be stirred to then and pour lamina membranacea into after capsule powders is fully dissolved, cooling forming is facial film, and facial film is applied card in face, stops to get final product in 20-30 minute.
The present invention has the following advantages: 1, the anti-ageing wrinkle removal effect of the present invention significantly and its composition be pure plant component, various chemical constituents such as preservative free, additive, non-stimulated and injury to skin.Flavone extract has good defying age, antiinflammatory, antibacterial and multiple skin-care effect such as brighten in the Ampelopsis grossedentata; Rhizoma amorphophalli glucomannan has antibiotic property, water absorption, non-oxidizability, can prevent the skin dehydration, alleviates old and feeble; Xanthan gum can promote collagen protein synthesis, and prevention is aging, reduces microgroove, desalination melanin; Soybean protein isolate contains multiple essential amino acids of human body and trace element, has very high nutritive value and health-care efficacy; Arbutin can suppress tryrosinase in the skin activity, the desalination pigment, whiten.2, can prepare multiple beauty functions facial film.Can whiten, go needs such as Huang, ruddy, anti-acne toxin expelling according to self skin, when dissolving, add natural components such as milk, red wine, lotus-seed-heart powder, green tea powder, prepare multiple facial film at any time with above-mentioned functions.And dryness, oiliness and Combination skin all should use.
3, quick permeation, good absorbing.Formulated by pure natural Konjac glucomannan and xanthan gum, the facial film profile is glittering and translucent.Do not need non-woven fabrics to do medium, can not inhale most of elite, so can real former absorption because of face paper.Nutritional labeling all condenses in the facial film, and with rapid permeability after the contact skin, and dissolving absorbs gradually.
The specific embodiment
Below in conjunction with embodiment the present invention is done further elaboration.
Embodiment: the capsular method for preparing of a kind of Ampelopsis grossedentata facial film may further comprise the steps:
(1) preparation of Ampelopsis grossedentata powder: the chopping of Ampelopsis grossedentata tender leaf is placed in the baking oven, and baking is 48 hours under 70 ℃ of conditions, takes out pulverizing and crosses 80 mesh sieves, processes the Ampelopsis grossedentata powder;
(2) ungrease treatment: the Ampelopsis grossedentata powder use quality that step (1) is made is to carry out ungrease treatment under 60 ℃ of reflux states for its ethyl acetate of 8 times in temperature; The defat response time is 1.7 hours; Filter then, vacuum drying is 2 hours under 70 ℃ of conditions, removes ethyl acetate;
(3) extract the vine tea flavone compounds: (W/V) is 1:30 by the mass volume ratio of feed liquid; In extraction vessel, add Ampelopsis grossedentata powder and distilled water after step (2) ungrease treatment; Reflux is 3 hours under 90 ℃ of conditions, is cooled to room temperature, with the 4000rpm centrifugalize; Collect supernatant, be the vine tea flavone crude extract;
(4) crystallization remove impurity: under 50 ℃ of conditions of vine tea flavone crude extract that step (3) is made 1/10 of vacuum concentration to initial volume, the deionized water and stirring that adds 2 times of concentrated solution volumes is even, and heating is 25 minutes in boiling water bath; Leave standstill crystalline deposit; Get crystallization after the filtration, with the deionized water crystallization of filtrating reuse equivalent once, filter, merge the crystal behind the secondary filter; Drying obtains vine tea flavone;
(5) pulverize and sterilization: the vine tea flavone that step (4) is made is pulverized and is crossed 1200 mesh sieves, in 100 ℃ of sterilization treatment, can not check pathogenic bacterium to inspection, makes the vine tea flavone powder;
(6) preparation of facial film capsule powder: facial film capsule powder comprises following each raw material, and the percentage rate that each raw material accounts for facial film capsule powder gross mass is: vine tea flavone powder 26%, Konjac glucomannan 17%, xanthan gum 17%, soybean protein isolate 12%, arbutin 8%, Radix Scutellariae 6%, left-handed VC 5%, hyaluronic acid (HA) 5%, allantoin 4%;
(7) incapsulate: the facial film capsule powder with step (6) preparation incapsulates every capsules 0.45g behind the mix homogeneously.
The above is merely preferred embodiment of the present invention, and all equalizations of doing according to claim of the present invention change and modify, and all should belong to covering scope of the present invention.
Claims (3)
1. capsular method for preparing of Ampelopsis grossedentata facial film is characterized in that operating procedure is following:
(1) preparation of Ampelopsis grossedentata powder: the chopping of Ampelopsis grossedentata tender leaf is placed in the baking oven, under 50～100 ℃ of conditions, toasted 48～60 hours, take out pulverizing and cross 60～80 mesh sieves, process the Ampelopsis grossedentata powder;
(2) ungrease treatment: the Ampelopsis grossedentata powder that step (1) is made; Using quality is to carry out ungrease treatment under 50～70 ℃ of reflux states as 10-30 ethyl acetate doubly in temperature; The defat response time is 1.6～2 hours; Filter then, vacuum drying is 1～2 hour under 70～80 ℃ of conditions, removes ethyl acetate;
(3) extract the vine tea flavone compounds: (W/V) is 1:20～35 by the mass volume ratio of feed liquid; In extraction vessel, add Ampelopsis grossedentata powder and distilled water after step (2) ungrease treatment; Reflux is 2～4 hours under 80～90 ℃ of conditions, is cooled to room temperature, with 3000～4000rpm centrifugalize; Collect supernatant, be the vine tea flavone crude extract;
(4) crystallization remove impurity: under 50 ℃ of conditions of vine tea flavone crude extract that step (3) is made 1/10～1/20 of vacuum concentration to initial volume; The deionized water and stirring that adds 1～2 times of concentrated solution volume is even, in boiling water bath, heats 20～30 minutes, leaves standstill crystalline deposit; Filter; Get crystal, drying obtains vine tea flavone;
(5) pulverize and sterilization: the vine tea flavone that step (4) is made is pulverized and is crossed 1000～1200 mesh sieves, in 100～110 ℃ of following sterilization treatment, can not check pathogenic bacterium to inspection, makes the vine tea flavone powder;
(6) preparation of facial film capsule powder: facial film capsule powder comprises following each raw material, and the percentage rate that each raw material accounts for facial film capsule powder gross mass is: vine tea flavone powder 20～26%, Konjac glucomannan 15～18%, xanthan gum 15～18%, soybean protein isolate 10～14%, arbutin 5～8%, hyaluronic acid 5～10%, Radix Scutellariae 4～8%, left-handed VC6～8%, allantoin 4～5%;
(7) incapsulate: the facial film capsule powder with step (6) preparation incapsulates behind the mix homogeneously.
2. the capsular method for preparing of a kind of Ampelopsis grossedentata facial film according to claim 1 is characterized in that operating procedure is following:
(1) preparation of Ampelopsis grossedentata powder: the chopping of Ampelopsis grossedentata tender leaf is placed in the baking oven, and baking is 48 hours under 70 ℃ of conditions, takes out pulverizing and crosses 80 mesh sieves, processes the Ampelopsis grossedentata powder;
(2) ungrease treatment: the Ampelopsis grossedentata powder use quality that step (1) is made is to carry out ungrease treatment under 60 ℃ of reflux states for its ethyl acetate of 8 times in temperature; The defat response time is 1.7 hours; Filter then, vacuum drying is 2 hours under 70 ℃ of conditions, removes ethyl acetate;
(3) extract the vine tea flavone compounds: (W/V) is 1:30 by the mass volume ratio of feed liquid; In extraction vessel, add Ampelopsis grossedentata powder and distilled water after step (2) ungrease treatment; Reflux is 3 hours under 90 ℃ of conditions, is cooled to room temperature, with the 4000rpm centrifugalize; Collect supernatant, be the vine tea flavone crude extract;
(4) crystallization remove impurity: under 50 ℃ of conditions of vine tea flavone crude extract that step (3) is made 1/10 of vacuum concentration to initial volume, the deionized water and stirring that adds 2 times of concentrated solution volumes is even, and heating is 25 minutes in boiling water bath; Leave standstill crystalline deposit; Get crystallization after the filtration, with the deionized water crystallization of filtrating reuse equivalent once, filter, merge the crystal behind the secondary filter; Drying obtains vine tea flavone;
(5) pulverize and sterilization: the vine tea flavone that step (4) is made is pulverized and is crossed 1200 mesh sieves, in 100 ℃ of sterilization treatment, can not check pathogenic bacterium to inspection, makes the vine tea flavone powder;
(6) preparation of facial film capsule powder: facial film capsule powder comprises following each raw material, and the percentage rate that each raw material accounts for facial film capsule powder gross mass is: vine tea flavone powder 26%, Konjac glucomannan 17%, xanthan gum 17%, soybean protein isolate 12%, arbutin 8%, Radix Scutellariae 6%, left-handed VC 5%, hyaluronic acid 5%, allantoin 4%;
(7) incapsulate: the facial film capsule powder with step (6) preparation incapsulates every capsules 0.45g behind the mix homogeneously.
3. by the Ampelopsis grossedentata facial film capsule of the method for claim 1 or 2 preparation.
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| CN104706551A (en) * | 2013-12-13 | 2015-06-17 | 江南大学 | Facial cleanser containing ampelopsin grossedentata extract |
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| CN104873422A (en) * | 2015-05-22 | 2015-09-02 | 周维新 | Whitening mask capsule |
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| CN105213248A (en) * | 2015-08-07 | 2016-01-06 | 袁朝宁 | A kind of ecosystem fruit-vegetable facial mask pastes |
| WO2017030898A1 (en) * | 2015-08-14 | 2017-02-23 | Johnson & Johnson Consumer Inc. | Compositions including ampelopsis grossedentata and albizia julibrissin extracts and methods of use |
| US9827188B2 (en) | 2015-08-14 | 2017-11-28 | Johnson & Johnson Consumer Inc. | Compositions comprising ampelopsis grossedentata and albizia julibrissin extracts |
| US9925136B2 (en) | 2015-08-14 | 2018-03-27 | Johnson & Johnson Consumer Inc. | Methods of reducing signs of skin aging using compositions comprising ampelopsis grossedentata and albizia julibrissin extracts |
| US10004677B2 (en) | 2015-08-14 | 2018-06-26 | Johnson & Johnson Consumer Inc. | Methods of reducing skin inflammation using compositions comprising Ampelopsis grossedentata and Albizia julibrissin extracts |
| RU2731561C2 (en) * | 2015-08-14 | 2020-09-04 | Джонсон энд Джонсон Консьюмер Инк. | Compositions containing ampelopsis grossedentata extracts and albizia julibrissin extracts, and methods of using them |
| AU2016307932B2 (en) * | 2015-08-14 | 2021-08-19 | Kenvue Brands Llc | Compositions including Ampelopsis grossedentata and Albizia julibrissin extracts and methods of use |
| CN106811343A (en) * | 2016-12-28 | 2017-06-09 | 贵阳中医学院 | Whitening anti-inflammatory antibacterial toilet soap containing vine tea general flavone and its preparation method and application |
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| CN108938533A (en) * | 2018-07-31 | 2018-12-07 | 北京东方淼森生物科技有限公司 | A kind of ageing-resistant skin care composition and its preparation method and application |
| CN114405625A (en) * | 2022-01-07 | 2022-04-29 | 江西富牛生态农业发展有限公司 | A extraction element for preparing ampelopsis grossedentata |
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