CN102429896A - Preparation method of aquatic animal pesticide - Google Patents
Preparation method of aquatic animal pesticide Download PDFInfo
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- CN102429896A CN102429896A CN2011103283225A CN201110328322A CN102429896A CN 102429896 A CN102429896 A CN 102429896A CN 2011103283225 A CN2011103283225 A CN 2011103283225A CN 201110328322 A CN201110328322 A CN 201110328322A CN 102429896 A CN102429896 A CN 102429896A
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- cypermethrin
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- dimethyl formamide
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- 241001465754 Metazoa Species 0.000 title claims abstract description 15
- 238000002360 preparation method Methods 0.000 title abstract description 7
- 239000000575 pesticide Substances 0.000 title abstract description 5
- ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 claims abstract description 57
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 claims abstract description 42
- 239000003814 drug Substances 0.000 claims abstract description 19
- 239000000284 extract Substances 0.000 claims abstract description 14
- 238000005303 weighing Methods 0.000 claims abstract description 14
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 claims abstract description 13
- 239000003995 emulsifying agent Substances 0.000 claims abstract description 13
- 239000008096 xylene Substances 0.000 claims abstract description 13
- 229910052801 chlorine Inorganic materials 0.000 claims abstract description 12
- 239000000460 chlorine Substances 0.000 claims abstract description 12
- 238000003756 stirring Methods 0.000 claims abstract description 12
- 229940079593 drug Drugs 0.000 claims abstract description 9
- 239000000203 mixture Substances 0.000 claims abstract description 8
- 239000002917 insecticide Substances 0.000 claims description 19
- 239000005946 Cypermethrin Substances 0.000 claims description 15
- KAATUXNTWXVJKI-UHFFFAOYSA-N cypermethrin Chemical compound CC1(C)C(C=C(Cl)Cl)C1C(=O)OC(C#N)C1=CC=CC(OC=2C=CC=CC=2)=C1 KAATUXNTWXVJKI-UHFFFAOYSA-N 0.000 claims description 15
- 229960005424 cypermethrin Drugs 0.000 claims description 15
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims description 10
- 238000004519 manufacturing process Methods 0.000 claims description 8
- 230000000694 effects Effects 0.000 abstract description 11
- 241000251468 Actinopterygii Species 0.000 abstract description 10
- KAATUXNTWXVJKI-NSHGMRRFSA-N (1R)-cis-(alphaS)-cypermethrin Chemical compound CC1(C)[C@@H](C=C(Cl)Cl)[C@H]1C(=O)O[C@H](C#N)C1=CC=CC(OC=2C=CC=CC=2)=C1 KAATUXNTWXVJKI-NSHGMRRFSA-N 0.000 abstract description 5
- 230000002265 prevention Effects 0.000 abstract description 3
- 239000005878 Azadirachtin Substances 0.000 abstract 3
- VEHPJKVTJQSSKL-UHFFFAOYSA-N azadirachtin Natural products O1C2(C)C(C3(C=COC3O3)O)CC3C21C1(C)C(O)C(OCC2(OC(C)=O)C(CC3OC(=O)C(C)=CC)OC(C)=O)C2C32COC(C(=O)OC)(O)C12 VEHPJKVTJQSSKL-UHFFFAOYSA-N 0.000 abstract 3
- FTNJWQUOZFUQQJ-IRYYUVNJSA-N azadirachtin A Natural products C([C@@H]([C@]1(C=CO[C@H]1O1)O)[C@]2(C)O3)[C@H]1[C@]23[C@]1(C)[C@H](O)[C@H](OC[C@@]2([C@@H](C[C@@H]3OC(=O)C(\C)=C/C)OC(C)=O)C(=O)OC)[C@@H]2[C@]32CO[C@@](C(=O)OC)(O)[C@@H]12 FTNJWQUOZFUQQJ-IRYYUVNJSA-N 0.000 abstract 3
- FTNJWQUOZFUQQJ-NDAWSKJSSA-N azadirachtin A Chemical compound C([C@@H]([C@]1(C=CO[C@H]1O1)O)[C@]2(C)O3)[C@H]1[C@]23[C@]1(C)[C@H](O)[C@H](OC[C@@]2([C@@H](C[C@@H]3OC(=O)C(\C)=C\C)OC(C)=O)C(=O)OC)[C@@H]2[C@]32CO[C@@](C(=O)OC)(O)[C@@H]12 FTNJWQUOZFUQQJ-NDAWSKJSSA-N 0.000 abstract 3
- 241000143060 Americamysis bahia Species 0.000 abstract 1
- 239000011259 mixed solution Substances 0.000 abstract 1
- 239000002994 raw material Substances 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 9
- 239000000243 solution Substances 0.000 description 8
- 240000005343 Azadirachta indica Species 0.000 description 5
- 235000013500 Melia azadirachta Nutrition 0.000 description 5
- 239000000047 product Substances 0.000 description 5
- 244000045947 parasite Species 0.000 description 4
- 238000009987 spinning Methods 0.000 description 4
- 239000000126 substance Substances 0.000 description 4
- 239000006184 cosolvent Substances 0.000 description 3
- 201000010099 disease Diseases 0.000 description 3
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 3
- 238000001228 spectrum Methods 0.000 description 3
- KAATUXNTWXVJKI-GGPKGHCWSA-N (1R)-trans-(alphaS)-cypermethrin Chemical compound CC1(C)[C@H](C=C(Cl)Cl)[C@H]1C(=O)O[C@H](C#N)C1=CC=CC(OC=2C=CC=CC=2)=C1 KAATUXNTWXVJKI-GGPKGHCWSA-N 0.000 description 2
- 239000005877 Alpha-Cypermethrin Substances 0.000 description 2
- 241000252230 Ctenopharyngodon idella Species 0.000 description 2
- 241000196324 Embryophyta Species 0.000 description 2
- 241000607479 Yersinia pestis Species 0.000 description 2
- 238000009360 aquaculture Methods 0.000 description 2
- 244000144974 aquaculture Species 0.000 description 2
- 230000008859 change Effects 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 230000007613 environmental effect Effects 0.000 description 2
- 238000003912 environmental pollution Methods 0.000 description 2
- 230000006872 improvement Effects 0.000 description 2
- 231100000053 low toxicity Toxicity 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 230000007246 mechanism Effects 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- NHOIBRJOQAYBJT-IMGVWCFESA-N nimbin Chemical compound C=1([C@@H]2C[C@H]3O[C@H]4[C@](C3=C2C)(C)[C@@H]([C@]2(C(=O)C=C[C@](C)([C@@H]2[C@H]4OC(C)=O)C(=O)OC)C)CC(=O)OC)C=COC=1 NHOIBRJOQAYBJT-IMGVWCFESA-N 0.000 description 2
- ZQIYJHBQRBBBRZ-UHFFFAOYSA-N nimbin Natural products COC(=O)CC1C2C(C(OC(=O)C)C3OC4CC(C(=C4C13C)C)c5cocc5)C(C)(C=CC2=O)C(=O)OC ZQIYJHBQRBBBRZ-UHFFFAOYSA-N 0.000 description 2
- 235000013311 vegetables Nutrition 0.000 description 2
- 241000238557 Decapoda Species 0.000 description 1
- 206010059866 Drug resistance Diseases 0.000 description 1
- 241000371997 Eriocheir sinensis Species 0.000 description 1
- 241000252234 Hypophthalmichthys nobilis Species 0.000 description 1
- 208000030852 Parasitic disease Diseases 0.000 description 1
- 241001500087 Trichodina Species 0.000 description 1
- SYKNUAWMBRIEKB-UHFFFAOYSA-N [Cl].[Br] Chemical compound [Cl].[Br] SYKNUAWMBRIEKB-UHFFFAOYSA-N 0.000 description 1
- 230000002159 abnormal effect Effects 0.000 description 1
- 238000009825 accumulation Methods 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 238000012258 culturing Methods 0.000 description 1
- 238000006731 degradation reaction Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 238000003933 environmental pollution control Methods 0.000 description 1
- 210000002615 epidermis Anatomy 0.000 description 1
- 208000010824 fish disease Diseases 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 239000007952 growth promoter Substances 0.000 description 1
- WJRBRSLFGCUECM-UHFFFAOYSA-N hydantoin Chemical compound O=C1CNC(=O)N1 WJRBRSLFGCUECM-UHFFFAOYSA-N 0.000 description 1
- 229940091173 hydantoin Drugs 0.000 description 1
- 230000000749 insecticidal effect Effects 0.000 description 1
- 230000005923 long-lasting effect Effects 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 231100001225 mammalian toxicity Toxicity 0.000 description 1
- 238000000386 microscopy Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 230000003071 parasitic effect Effects 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 231100000572 poisoning Toxicity 0.000 description 1
- 230000000607 poisoning effect Effects 0.000 description 1
- 244000144977 poultry Species 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 239000011265 semifinished product Substances 0.000 description 1
- 238000004659 sterilization and disinfection Methods 0.000 description 1
- 208000024891 symptom Diseases 0.000 description 1
- 210000001835 viscera Anatomy 0.000 description 1
- 238000011179 visual inspection Methods 0.000 description 1
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- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention relates to a preparation method of an aquatic animal pesticide, which comprises the following implementation steps: (1) weighing the following raw material medicines in parts by weight: 200-500 parts of azadirachtin extract, 50-150 parts of beta-cypermethrin benzene oil, 50-150 parts of high-chlorine emulsifier, 100-400 parts of dimethylformamide and 300 parts of xylene; (2) putting the weighed high-chlorine emulsifier, the xylene and the dimethyl formamide with the amount of 1/3-1/2 into a container, slowly pouring the weighed beta-cypermethrin benzene oil into the container, and stirring while adding to completely dissolve the beta-cypermethrin benzene oil; (3) weighing azadirachtin extract, adding into the uniformly mixed solution, and stirring while adding to fully mix the azadirachtin extract; then the residual amount of dimethylformamide is used for constant volume, and the mixture is subpackaged into 100 ml/bottle. The pesticide can be used as a medicine for preventing and treating the epizoonosis of cultured fishes and shrimps, has the characteristics of high efficiency, quick effect, broad spectrum, natural ecotype, multiple functions and the like, and has definite prevention and treatment effect. The traditional Chinese medicine composition has the advantages of reasonable formula, simple preparation, wide application and obvious effect.
Description
Technical field
The present invention relates to a kind of method for preparing of aquatic animal medicine, particularly a kind of aquatic animal method for producing insecticide.
Background technology
Parasitic disease is one type of common, multiple and bigger disease of control difficulty in the fishery disease.Annual the end of spring and the beginning of summer Fish dactylogyrider, the parasite disease that Trichodina causes, cause bigger economic loss to aquaculture.Parasite killing plays very important effect aspect the fish diseases preventing and treating, in occupation of the share of Aquatic product medicine about 1/3.Used the sick effect of chemical classes parasite killing control eliminating fish parasites pretty good, but along with the passing of service time, Drug resistance constantly manifest in the past.This type medicine has the residual effect of accumulating to cultivated animals simultaneously, can cause the aquatic product quality problem.The current healthy nuisanceless aquaculture pattern of wideling popularize presses for seeks a kind of novel non-environmental pollution control medicine.
The environment-friendly type natural insecticide of efficient, the low toxicity that from plant, extracts, low-residual,, non-environmental-pollution nontoxic to the person poultry safety is current vegetable insecticide of praising highly the most, can be widely used in the control agricultural pests.
Therefore, providing a kind of preparation simple, obvious results aquatic animal method for producing insecticide, is one of this field scientific research technical staff important difficult problem of being badly in need of solving.
Summary of the invention
The objective of the invention is to overcome above-mentioned weak point, a kind of reasonable recipe, simple, easy to use, the obvious results aquatic animal method for producing insecticide of preparation are provided.
For realizing that the technical scheme that above-mentioned purpose the present invention is adopted is:
A kind of aquatic animal method for producing insecticide is characterized in that implementation step is following:
(1) takes by weighing following various crude drug by weight: mimbin extract 200-500 part, effective cypermethrin benzene oil (mass concentration 27%) 50-150 part, high chlorine emulsifying agent (mass concentration 4.5%) 50-150 part, dimethyl formamide 100-400 part, xylene 100-300 part;
The dimethyl formamide that (2) will take by weighing high chlorine emulsifying agent, xylene and the 1/3-1/2 amount of said amount is put into the container mixing, slowly pours load weighted effective cypermethrin benzene oil into said vesse then, and the limit edged stirs, and it is dissolved fully;
(3) take by weighing mimbin extract according to quantity, join in the solution of above-mentioned mix homogeneously, the limit edged stirs, and it is fully mixed; The dimethyl formamide standardize solution of reuse surplus is packed as the 100ml/ bottle.
When using product of the present invention, culture the consumption that product 20ml of the present invention is used in the pond, full pool spilling head for every mu of 1 meter of the depth of water.
The characteristic of each crude drug and effect in the product of the present invention:
The nimbin insecticide is maximum, the universally acknowledged wide spectrum of our times various countries research, the novel insecticide of environmental friendliness efficiently.The Azadirachta Indica A. insecticide can satisfy the requirement of present pesticide developing preferably, and is good etc. like efficient, low toxicity, noresidue, selectivity.Active component is the material that nature exists in the Azadirachta Indica A.; With natural long-term evolution process in; Nature has formed perfect degradation mechanism already to the various chemical constituents in the Azadirachta Indica A., and its active component does not have accumulation at occurring in nature, and is environmentally safe; Be specially adapted to directly edible crop and animal such as vegetable, fruit, Folium Camelliae sinensis, aquatic animal, and it is not produced poisoning.The Azadirachta Indica A. insecticide mainly has and suppresses growth promoter, refusing to eat, avoids and keep away and model of action such as sterile, and widely different with the insecticidal action mechanism of conventional pesticide, active component is complicated; Help overcoming pest resistance to insecticide; To non-target organism safety, low to mammalian toxicity, and obvious selectivity is arranged.Nimbin and Azadirachta Indica A. insecticide have good Environmental compatibility, and have environmental pollution improvement's function.
Effective cypermethrin has another name called second body cypermethrin, chemical name be (R, S)-alpha-cyano-3-phenoxy benzyl (1R; 3R)-and 3-(2, the 2-dichloroethylene)-2,2-dimethyl cyclopropane carboxylic acid ester; Be to obtain 2 pairs of enantiomer that activity is higher through epimerism from cypermethrin; Be alphamethrin (alpha-cypermethrin) and theta-cypermethrin (theta-cypermethrin), the specific activity cypermethrin is high 1 times, and is stable to light; Having long lasting effect, is a kind of more efficient, wide spectrum, fast-acting insecticide.Effective cypermethrin benzene oil is that this material content is 27% semi-finished product medicine.
Cosolvent: emulsifying agent, dimethyl formamide, xylene are cosolvent.Cosolvent can be used for dissolving former medicine on the one hand, and the physical property that can improve preparation on the other hand is like flowability, appearance stability, dilution stability etc.
The invention has the beneficial effects as follows: insecticide of the present invention is the aquatic animal insecticide that a kind of natural plant and chemicals are mixed and made into; Can be used as the ectozoal control medicine of culturing fish and shrimp; Have efficient, wide spectrum, quick-acting, natural sex, the ecotype; Characteristics such as multi-functional, prevention effect is definite.Reasonable recipe of the present invention complements each other, and preparation is simple, is widely used, and prevention effect is very obvious.
The specific embodiment
Below in conjunction with specific embodiment technology contents of the present invention is made detailed explanation:
Embodiment 1 (every part by 1g)
A kind of aquatic animal method for producing insecticide, implementation step is following:
(1) takes by weighing following various crude drug by weight: mimbin extract 200g, effective cypermethrin benzene oil (mass concentration 27%) 50g, high chlorine emulsifying agent (mass concentration 4.5%) 50g, dimethyl formamide 300g, xylene 300g.
Dimethyl formamide (100g), the xylene that (2) will take by weighing high chlorine emulsifying agent (mass concentration 4.5%), the 1/3-1/2 amount of said amount are put into container; Slowly pour load weighted effective cypermethrin benzene oil (mass concentration 27%) into said vesse then, the limit edged stirs, and it is dissolved fully.
(3) measure mimbin extract, join in the solution of above-mentioned mix homogeneously, the limit edged stirs, and it is fully mixed; The dimethyl formamide of reuse surplus (200g) standardize solution is packed as the 100ml/ bottle.
The various crude drug that the present invention adopts etc. are the commercially available prod.
Embodiment 2
(1) takes by weighing following various crude drug by weight: mimbin extract 500g, effective cypermethrin benzene oil (27%) 150g, high chlorine emulsifying agent (4.5%) 150g, dimethyl formamide 100 g, xylene 100g.
Dimethyl formamide (150g), the xylene that (2) will take by weighing high chlorine emulsifying agent (4.5%), the 1/3-1/2 amount of said amount are put into container; Slowly pour load weighted effective cypermethrin benzene oil (27%) into said vesse then, the limit edged stirs, and it is dissolved fully.
(3) measure mimbin extract, join in the solution of above-mentioned mix homogeneously, the limit edged stirs, and it is fully mixed; The dimethyl formamide of reuse surplus (150g) standardize solution is packed as the 100ml/ bottle.
Other is with embodiment 1.
Embodiment 3
(1) takes by weighing following various crude drug by weight: mimbin extract 300g, effective cypermethrin benzene oil (27%) 100g, high chlorine emulsifying agent (4.5%) 100g, dimethyl formamide 300 g, xylene 200g.
Dimethyl formamide (120g), the xylene that (2) will take by weighing high chlorine emulsifying agent (4.5%), the 1/3-1/2 amount of said amount are put into container; Slowly pour load weighted effective cypermethrin benzene oil (27%) into said vesse then, the limit edged stirs, and it is dissolved fully.
(3) measure mimbin extract, join in the solution of above-mentioned mix homogeneously, the limit edged stirs, and it is fully mixed; The dimethyl formamide of reuse surplus (180g) standardize solution is packed as the 100ml/ bottle.
It is with embodiment 1.
The clinical practice instance:
The a certain raiser in Yancheng, Jiangsu has 6 mu of areas to culture Ctenopharyngodon idellus to raise together with the pond, and from May 7th, 2010, the fish abundance of food of ingesting reduced, and finding has a small amount of Ctenopharyngodon idellus and silver carp on the water surface, to spin, and constantly has fish on the water surface, to jump; May 8, whole daytime on the 9th, there is in groups fish on the water surface, slowly to move about and constantly breaks the water the dead fish of continual discovery.Fish for fish 10 tails that the water surface slowly moves about, get its epidermis respectively, cheek silk is examined under a microscope, all find to have a large amount of dactylogyriders parasitic, dissect back visual inspection, all no abnormal symptom of the sick fish internal organs of microscopy, confirm as doctylogyrosis.Under technical staff's suggestion, May 10 began to heal with medicine.Used the fine worm of shrimp Eriocheir sinensis clean in first day, found that the fish phenomenon of spinning was also relatively more serious in second day when throwing something and feeding feedstuff, ingest that there is a change for the better, continued medication once on the 3rd day, the phenomenon of spinning alleviates, and to the improvement of ingesting in the 4th day, the phenomenon of spinning was few.Use bromine chlorine hydantoin to carry out water body disinfection after the 6th day, one week the back pondfish ingest normally, nothing is in the water surface situation of spinning, water colour does not have significant change.
Above-mentioned detailed description of the aquatic animal method for producing insecticide being carried out with reference to embodiment; Be illustrative rather than determinate; Can be according to institute's limited range several embodiment that give an example out; Therefore in the variation and the modification that do not break away under the general plotting of the present invention, should belong within protection scope of the present invention.
Claims (1)
1. aquatic animal method for producing insecticide is characterized in that implementation step is following:
(1) takes by weighing following various crude drug by weight: mimbin extract 200-500 part, effective cypermethrin benzene oil 50-150 part, high chlorine emulsifying agent 50-150 part, dimethyl formamide 100-400 part, xylene 100-300 part;
The dimethyl formamide that (2) will take by weighing high chlorine emulsifying agent, xylene and the 1/3-1/2 amount of said amount is put into the container mixing, slowly pours load weighted effective cypermethrin benzene oil into said vesse then, and the limit edged stirs, and it is dissolved fully;
(3) take by weighing mimbin extract according to quantity, join in the solution of above-mentioned mix homogeneously, the limit edged stirs, and it is fully mixed; The dimethyl formamide standardize solution of reuse surplus is packed as the 100ml/ bottle.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2011103283225A CN102429896A (en) | 2011-10-26 | 2011-10-26 | Preparation method of aquatic animal pesticide |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2011103283225A CN102429896A (en) | 2011-10-26 | 2011-10-26 | Preparation method of aquatic animal pesticide |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN102429896A true CN102429896A (en) | 2012-05-02 |
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| CN2011103283225A Pending CN102429896A (en) | 2011-10-26 | 2011-10-26 | Preparation method of aquatic animal pesticide |
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| Country | Link |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2015021534A1 (en) * | 2013-08-15 | 2015-02-19 | Sylleta Inc. | Compositions and methods for control of marine ectoparasites |
| US20160029669A1 (en) * | 2013-03-15 | 2016-02-04 | Neemco Limited | Supplemented fish feed |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1555708A (en) * | 2003-12-30 | 2004-12-22 | 成都柯邦药业有限公司 | Nimbin composite plant source micro emulsion pesticide and its manufacturing method and use in aquatic product cultivation |
-
2011
- 2011-10-26 CN CN2011103283225A patent/CN102429896A/en active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1555708A (en) * | 2003-12-30 | 2004-12-22 | 成都柯邦药业有限公司 | Nimbin composite plant source micro emulsion pesticide and its manufacturing method and use in aquatic product cultivation |
Non-Patent Citations (3)
| Title |
|---|
| 宋仲容等: "印楝素、高效氯氰菊酯及其混剂对菜青虫的毒力与药效", 《长江蔬菜（学术版）》 * |
| 尹伦甫: "植物精油在水产杀虫剂中的应用", 《科学养鱼》 * |
| 王江柱等: "《无公害果蔬农药选择与使用教材》", 30 April 2005 * |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20160029669A1 (en) * | 2013-03-15 | 2016-02-04 | Neemco Limited | Supplemented fish feed |
| US11096404B2 (en) * | 2013-03-15 | 2021-08-24 | Can Technologies, Inc. | Supplemented fish feed |
| US12082597B2 (en) | 2013-03-15 | 2024-09-10 | Can Technologies, Inc. | Supplemented fish feed |
| WO2015021534A1 (en) * | 2013-08-15 | 2015-02-19 | Sylleta Inc. | Compositions and methods for control of marine ectoparasites |
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Application publication date: 20120502 |