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CN102423680A - Catalyst random packing - Google Patents

Catalyst random packing Download PDF

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Publication number
CN102423680A
CN102423680A CN201110253785XA CN201110253785A CN102423680A CN 102423680 A CN102423680 A CN 102423680A CN 201110253785X A CN201110253785X A CN 201110253785XA CN 201110253785 A CN201110253785 A CN 201110253785A CN 102423680 A CN102423680 A CN 102423680A
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catalyst
cylinder
packing
end cover
shell
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CN201110253785XA
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CN102423680B (en
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马晓迅
褚雅宏
王领
高中强
桂凯
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NORTHWEST UNIVERSITY
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NORTHWEST UNIVERSITY
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Abstract

The invention relates to a catalyst random packing. The catalyst random packing comprises a packing shell and a catalyst packet placed inside the packing shell. The packing shell is provided with a cylinder. One end of the cylinder is provided with a block end cover. The cylinder wall of the cylinder is provided with at least a circle of inner oblique tongue pieces, wherein the inner oblique tongue pieces are uniformly arranged along the circumference of the cylinder wall. The inner oblique tongue pieces extend to the cylinder, and the tongue tips are toward the direction of the block end cover. According to the present invention, one end of the catalyst packet is blocked by the block end cover, and the other end of the catalyst packet is hooked by the barbs formed by the inner oblique tongue pieces, such that the catalyst packet is suspended and fixed in the packing shell, and can not prolapse due to the gas surging and the liquid surging, the problems of suspension and fixation of the catalyst and the packing shell are solved; due to the random characteristic of the packing of the present invention, the gas short circuit phenomenon of the whole bundle of the catalyst filler packet can be overcome, the specific surface area of the gas-liquid contact can be increased, the effect of the catalytic reaction can be improved, and the reactive rectification process is achieved well.

Description

一种催化剂散堆填料A catalyst random packing

技术领域 technical field

本发明涉及一种化工催化剂填料,尤其是一种催化剂散堆填料,主要应用于化工催化精馏过程。The invention relates to a chemical catalyst packing, in particular to a catalyst random packing, which is mainly used in the catalytic rectification process of the chemical industry.

背景技术 Background technique

在已有技术中,化工催化精馏过程所用的催化剂大都是以规整填料的形式设置在精馏塔中,最常用的是一种催化剂丝网规整填料,俗称捆包催化剂,它是将催化剂装袋附载在两层丝网之间,然后卷成卷,形成一个圆柱体。用于催化精馏时,填料竖立码放在填料支撑格栅上,形成催化剂床层。这种规整填料存在的缺点是:填料的卷与卷之间存着较大空间,实验发现气体从该空间直通而上形成气体短路,没有很好的气液接触,所以不能很好的传质。为此,有人也想用散堆填料来克服规整填料的这一缺点,但因催化剂与填料壳难以悬浮固定,导致制作复杂、成本较高,都未能实现。In the prior art, most of the catalysts used in the chemical catalytic rectification process are arranged in the rectification tower in the form of structured packing. The bag is loaded between two layers of wire mesh and then rolled into a roll to form a cylinder. When used for catalytic rectification, the filler is vertically stacked on the filler support grid to form a catalyst bed. The disadvantage of this kind of structured packing is: there is a large space between the packing rolls, and the experiment found that the gas passes through this space to form a gas short circuit, and there is no good gas-liquid contact, so it cannot transfer mass well. . For this reason, some people also want to use random packing to overcome this shortcoming of structured packing, but because the catalyst and packing shell are difficult to suspend and fix, resulting in complicated production and high cost, they have not been realized.

发明内容 Contents of the invention

本发明的目的是针对已有技术中的问题,提供一种催化剂散堆填料,它较好地解决了催化剂与填料体的悬浮固定问题,使本催化剂散堆填料能够代替规整填料,消除规整填料中的气体短路,增加气、液及液体与催化剂的接触机会和时间,提高气液传质效率和催化反应转化率。The purpose of the present invention is to solve the problems in the prior art by providing a catalyst random packing, which better solves the problem of suspension and fixation of the catalyst and the packing body, so that the random packing of the catalyst can replace the structured packing and eliminate the structured packing. The short circuit of the gas in the catalyst increases the contact opportunity and time of gas, liquid and liquid with the catalyst, and improves the gas-liquid mass transfer efficiency and catalytic reaction conversion rate.

为了实现上述目的,本发明的技术方案如下:In order to achieve the above object, the technical scheme of the present invention is as follows:

它具有一个填料壳和一个放置在该填料壳中的催化剂包,所述的填料壳具有一个筒体,在该筒体的一端设有一个格档端盖,在所述筒体的筒壁上至少设有一圈沿筒壁周向均匀排布的内斜舌片,所述的内斜舌片向筒体内伸出,并且舌尖朝向格档端盖的方向。It has a stuffing shell and a catalyst package placed in the stuffing shell, the stuffing shell has a cylinder body, a grille end cap is arranged at one end of the cylinder body, and on the cylinder wall of the cylinder body There is at least one circle of inner oblique tongue pieces uniformly arranged along the circumference of the cylinder wall, the inner oblique tongue pieces protrude into the cylinder, and the tip of the tongue faces the direction of the end cover of the grille.

本发明进一步的技术方案如下:The further technical scheme of the present invention is as follows:

所述的内斜舌片沿筒壁轴向设有两圈或多圈,且圈与圈之间的内斜舌片相互错位排列。The inner oblique tongues are provided with two or more circles along the axial direction of the cylinder wall, and the inner oblique tongues between the circles are mutually misaligned.

所述的格档端盖至少由二个或多个沿筒壁周向均匀布置、并从筒壁上径向内凸的径向内弯弧环构成。The grill end cover is composed of at least two or more radially inwardly curved arc rings arranged uniformly along the circumference of the cylinder wall and projecting radially inward from the cylinder wall.

所述的格档端盖由多个沿筒壁周向均匀布置、并从筒壁伸向中心的径向舌片构成。The grill end cover is composed of a plurality of radial tongues evenly arranged along the circumference of the cylinder wall and extending from the cylinder wall to the center.

本发明的特点如下:Features of the present invention are as follows:

一、本发明较好将催化剂包装填在填料壳中,一端被格档端盖封挡,同时被内斜舌片形成的倒刺挂住,使催化剂包悬浮固定在填料壳内,不会因气、液涌动而脱出,较好地解决了催化剂与填料壳的悬浮固定问题。不但可以很好地进行反应,而且实现了散堆填料的传质功能。1. In the present invention, the catalyst package is preferably filled in the packing shell, and one end is blocked by the end cover of the grille, and at the same time, it is hung by the barb formed by the inner oblique tongue, so that the catalyst package is suspended and fixed in the packing shell, and will not be damaged due to The gas and liquid surge and come out, which better solves the problem of suspension and fixation of the catalyst and the packing shell. Not only can the reaction be carried out well, but also the mass transfer function of random packing can be realized.

二、由于本填料是一种催化剂散堆填料,当它散堆在精馏塔的催化精馏塔段时,不仅能克服了规整填料的气体短路现象,增加气、液及液体与催化剂的接触机会与时间,而且还能够在催化反应的同时进行精馏,达到一边反应、一边分离的目的,最终使气液传质效率和催化反应转化率得到有效地提高。2. Since this packing is a catalyst random packing, when it is scattered in the catalytic rectification column section of the rectification tower, it can not only overcome the gas short circuit phenomenon of the structured packing, but also increase the contact between gas, liquid and liquid and the catalyst Opportunity and time, but also can carry out rectification at the same time of catalytic reaction, achieve the purpose of separation while reacting, and finally effectively improve the efficiency of gas-liquid mass transfer and the conversion rate of catalytic reaction.

三、本填料的填料壳一端用格档端盖封挡,另一端用内斜舌片形成的倒刺挂包,使催化剂包的装填不用封盖,装填操作简单,降低了填料的制作成本。3. One end of the packing shell of this packing is sealed with a grille end cover, and the other end is a barbed hanging bag formed by an inner oblique tongue, so that the filling of the catalyst package does not need a cover, the filling operation is simple, and the production cost of the packing is reduced.

附图说明 Description of drawings

图1是本发明填料壳结构之一的主视图。Fig. 1 is a front view of one of the packing shell structures of the present invention.

图2是图1俯视图。Fig. 2 is a top view of Fig. 1 .

图3是图1的立体结构图。Fig. 3 is a three-dimensional structure diagram of Fig. 1 .

图4是催化剂包皮的结构示意图。Fig. 4 is a schematic diagram of the structure of the catalyst sheath.

图5是本发明填料壳结构之二的主视图。Fig. 5 is a front view of the second packing shell structure of the present invention.

图6是图5的俯视图。FIG. 6 is a top view of FIG. 5 .

图7是图5的立体结构图。FIG. 7 is a three-dimensional structure diagram of FIG. 5 .

具体实施方式 Detailed ways

实施例1Example 1

参见图1~3,它具有一个填料壳和一个放置在该填料壳中的催化剂包(图中未画出催化剂包),所述的填料壳具有一个筒体1,在该筒体的一端设有一个格档端盖,在所述筒体的筒壁上至少设有一圈沿筒壁周向均匀排布的内斜舌片2,所述的内斜舌片2向筒体内伸出,并且其舌尖朝向格档端盖的方向,从而形成挂包倒刺;所述内斜舌片的轴与筒壁有一个夹角,该夹角可以在大于0°和小于90°之间调整,从而使该内斜舌片具有较好的弹性。为了使本填料更好地进行气液接触,所述的内斜舌片2沿筒壁轴向设有两圈或多圈,本例给出两圈的结构,且圈与圈之间的内斜舌片错位排列。所述的筒体1可以由一块金属板材卷曲构成,其筒壁上的内斜舌片2可以在该金属板材上裁切、模具冲压构成,并且卷曲对接边4轴向错位对接,以实现对接部位内斜舌片2的错位排列;所述的格档端盖可以是一个单独的端盖件,然后再与所述的筒体1固联在一起;也可以是在筒体上直接形成的连体端盖;本例采用连体端盖,它至少由二个或多个沿筒壁周向均匀布置、并从筒壁上径向内凸的径向弯弧环3构成。这样的连体端盖可以在卷曲筒体的板材上直接裁切、模具冲压成型,故具有制作简单的优点。Referring to Fig. 1~3, it has a stuffing shell and a catalyst bag (not drawing catalyst bag among the figure) that is placed in this stuffing shell, described stuffing shell has a cylinder body 1, is set at one end of this cylinder body There is a grill end cover, and at least a circle of inner oblique tongue pieces 2 arranged uniformly along the circumference of the cylinder wall is provided on the cylinder wall of the cylinder body, and the inner oblique tongue pieces 2 protrude into the cylinder, and The tip of the tongue is facing the direction of the grille end cap, thereby forming a hanging bag barb; the shaft of the inner oblique tongue has an included angle with the cylinder wall, and the included angle can be adjusted between greater than 0° and less than 90°, so that The inner oblique tongue piece has better elasticity. In order to make the packing better in gas-liquid contact, the inner oblique tongue piece 2 is provided with two or more turns along the axial direction of the cylinder wall. The oblique tongue pieces are misaligned. The cylinder body 1 can be formed by curling a piece of metal plate, the inner oblique tongue piece 2 on the cylinder wall can be formed by cutting and die stamping on the metal plate, and the curled butt joint edge 4 is axially dislocated butted to realize the butt joint The dislocation arrangement of the oblique tongue pieces 2 in the position; the grill end cover can be a separate end cover, and then fixedly connected with the cylinder 1; it can also be formed directly on the cylinder One-piece end cap; this example adopts one-piece end cap, which is composed of at least two or more radial curved arc rings 3 that are evenly arranged along the circumference of the cylinder wall and radially protrude from the cylinder wall. Such one-piece end caps can be directly cut and formed by die stamping on the plate of the curled cylinder, so it has the advantage of simple manufacture.

参见图4,所述的催化剂包做成与筒体1的体积相配合的形状,可以先做一个如图5所示网套,装入催化剂后,两端扎住或缝在一起,形成一个圆柱形催化剂包,然后装入填料壳1内,最终形成一个催化剂散堆填料。Referring to Fig. 4, the catalyst package is made into a shape that matches the volume of cylinder body 1. A mesh cover as shown in Fig. 5 can be made earlier, and after the catalyst is loaded, the two ends are tied or sewn together to form a The cylindrical catalyst package is then loaded into the packing shell 1 to finally form a catalyst random packing.

实施例2Example 2

本例在实施例1的结构基础上,其格档端盖采用另一种结构形式的连体端盖,它由多个沿筒壁周向均匀布置、并从筒壁上伸向中心的径向舌片5构成。这种格档端盖也适于采用在卷曲筒体的板材上直接裁切、模具冲压成型,同样具有制作简单的优点。本例的其它结构与实施例1相同。In this example, on the basis of the structure of Example 1, the grid end cover adopts another structural form of one-piece end cover. Formed towards the tongue 5. This lattice end cover is also suitable for direct cutting and die stamping on the plate of the curled cylinder, and also has the advantage of simple manufacture. The other structures of this example are the same as in Embodiment 1.

Claims (4)

1.一种催化剂散堆填料,其特征是:它具有一个填料壳和一个放置在该填料壳中的催化剂包,所述的填料壳具有一个筒体(1),在该筒体的一端设有一个格档端盖,在所述筒体的筒壁上至少设有一圈沿筒壁周向均匀排布的内斜舌片(2),所述的内斜舌片(2)向筒体内伸出,并且舌尖朝向格档端盖的方向。1. A catalyst random packing is characterized in that: it has a packing shell and a catalyst bag placed in the packing shell, the packing shell has a cylinder (1), and an end of the cylinder is provided There is a grille end cover, and at least one circle of inner oblique tongues (2) arranged uniformly along the circumference of the cylinder wall is provided on the cylinder wall of the cylinder, and the inner oblique tongues (2) are directed toward the cylinder. Stretch out with the tip of your tongue facing the direction of the grill end cap. 2.根据权利要求1所述的催化剂散堆填料,其特征是:所述的内斜舌片(2)沿筒壁轴向设有两圈或多圈,且圈与圈之间的内斜舌片(2)相互错位排列。2. Catalyst random packing according to claim 1, characterized in that: said inner slant tongue (2) is provided with two or more turns along the axial direction of the cylinder wall, and the inner slant between the turns The tongue pieces (2) are mutually misaligned and arranged. 3.根据权利要求1所述的催化剂散堆填料,其特征是:所述的格档端盖至少由二个或多个沿筒壁周向均匀布置、并从筒壁上径向内凸的径向内弯弧环(3)构成。3. Catalyst random packing according to claim 1, characterized in that: the grill end cover is composed of at least two or more uniformly arranged along the circumference of the cylinder wall and protruding radially from the cylinder wall. The radial inner curved arc ring (3) is formed. 4.根据权利要求1所述的催化剂散堆填料,其特征是:所述的格档端盖由多个沿筒壁周向均匀布置、并从筒壁伸向中心的径向舌片(5)构成。4. Catalyst random packing according to claim 1, characterized in that: the grille end cover is composed of a plurality of radial tongues (5 )constitute.
CN 201110253785 2011-08-31 2011-08-31 A catalyst random packing Expired - Fee Related CN102423680B (en)

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104587908A (en) * 2015-01-24 2015-05-06 福州大学 Catalyst filling structure applicable to large-tower-diameter catalytic rectifying column and usage thereof
CN106732319A (en) * 2016-12-19 2017-05-31 海盐得胜化工设备有限公司 A kind of filler being connected with each other
CN108347900A (en) * 2015-10-23 2018-07-31 佩特斯兰得堡机械有限公司 Mixing feed device
CN113164908A (en) * 2018-12-13 2021-07-23 西格里碳素欧洲公司 Filling body

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4376081A (en) * 1980-05-16 1983-03-08 Max Leva Tower packing
US4496498A (en) * 1981-07-30 1985-01-29 Sulzer Brothers Limited Statistical packing
CN2547393Y (en) * 2002-04-27 2003-04-30 朱恩来 Metal ring Intalox saddle packing with reinforced outer-ring corrugated inner saddle arc
CN201815312U (en) * 2010-09-11 2011-05-04 兰州瑞玛化机有限公司 Ceramic filler for gear ring

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4376081A (en) * 1980-05-16 1983-03-08 Max Leva Tower packing
US4496498A (en) * 1981-07-30 1985-01-29 Sulzer Brothers Limited Statistical packing
CN2547393Y (en) * 2002-04-27 2003-04-30 朱恩来 Metal ring Intalox saddle packing with reinforced outer-ring corrugated inner saddle arc
CN201815312U (en) * 2010-09-11 2011-05-04 兰州瑞玛化机有限公司 Ceramic filler for gear ring

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* Cited by examiner, † Cited by third party
Title
张雯: "高效填料介绍", 《医药工程设计》 *

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104587908A (en) * 2015-01-24 2015-05-06 福州大学 Catalyst filling structure applicable to large-tower-diameter catalytic rectifying column and usage thereof
CN108347900A (en) * 2015-10-23 2018-07-31 佩特斯兰得堡机械有限公司 Mixing feed device
CN106732319A (en) * 2016-12-19 2017-05-31 海盐得胜化工设备有限公司 A kind of filler being connected with each other
CN106732319B (en) * 2016-12-19 2019-04-09 海盐得胜化工设备有限公司 One kind can filler interconnected
CN113164908A (en) * 2018-12-13 2021-07-23 西格里碳素欧洲公司 Filling body

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