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CN102337191B - Preparation method of low-alcohol foxnut wine - Google Patents

Preparation method of low-alcohol foxnut wine Download PDF

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CN102337191B
CN102337191B CN 201110290305 CN201110290305A CN102337191B CN 102337191 B CN102337191 B CN 102337191B CN 201110290305 CN201110290305 CN 201110290305 CN 201110290305 A CN201110290305 A CN 201110290305A CN 102337191 B CN102337191 B CN 102337191B
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CN102337191A (en
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张汆
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Anhui Jinshang Real Estate Development Co Ltd
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Chuzhou University
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Abstract

The invention provides a preparation method of a low-alcohol foxnut wine. According to the technical scheme of the invention, the obtained wine body is amber, is clear and transparent, has faint scent taste and pure flavor, and the content of alcohol in the wine is about 15% (v/v). According to the results of tests, the foxnut wine contains rich polyphenol substances and the content of total phenol is 120mg/L (Folin-Ciocalteus reagent method). Thus, the wine has strong anti-oxidation and removing free radical activity.

Description

一种低度芡实酒的制备方法A kind of preparation method of low-alcohol Gorgon fruit wine

技术领域 technical field

本发明涉及一种低度芡实酒的配方、酿造工艺和产品理化功能性质描述。  The invention relates to a formula, a brewing process and a description of the physical and chemical functional properties of a low-alcohol Gorgon fruit wine. the

背景技术 Background technique

芡实是一种水生植物芡的成熟种仁,俗称芡米,是我国传统中药材之一,也是我国卫生部首批颁布的“药食兼用”材料之一。芡实具有多种保健功能,如“芡能止渴益肾,治小便不禁、遗精、白浊、带下”(《本草纲目》)、芡实具有“补脾、利湿、固肾”功效(《本草求真》)。因芡实是水生植物,所以其分布具有明显的地域特色,在中国,芡实多分布与湖泊、池塘、水系发达的浙江、江苏、安徽、广东、山东、湖北等地。年产干芡实米10000吨左右,其中约1500-2000吨用于中药材,其余用作滋补食材或食品加工。  Gorgon fruit is the mature seed kernel of a kind of aquatic plant Gorgon, commonly known as Gorgon rice. It is one of the traditional Chinese medicinal materials in my country and one of the first batch of "both medicine and food" materials promulgated by the Ministry of Health of my country. Gorgon has a variety of health care functions, such as "Gorgon can quench thirst and nourish the kidney, treat incontinence, nocturnal emission, white turbidity, and leukorrhea" ("Compendium of Materia Medica"), and Gorgon has the effects of "tonifying the spleen, dampness, and strengthening the kidney" ("Compendium of Materia Medica"). Materia Medica Seeking Truth"). Because Gorgon is an aquatic plant, its distribution has obvious regional characteristics. In China, Gorgon is mostly distributed in lakes, ponds, and Zhejiang, Jiangsu, Anhui, Guangdong, Shandong, Hubei and other places with developed water systems. The annual output of dried gorgon rice is about 10,000 tons, of which about 1,500-2,000 tons are used for Chinese medicinal materials, and the rest are used as nourishing ingredients or food processing. the

目前,国内外对芡实深加工领域的文献报道很少。在芡实产区,芡实加工以速冻鲜芡实、芡米或干制芡米等初加工产品为主,产品种类单一,应用范围窄,经济效益低下,致使我国芡实产业长期处于低水平、低效益的徘徊阶段。因此,研究开发新的芡实食品和工艺技术是促进芡实产业快速发展,提升产业效益和技术水平的当务之急。  At present, there are few literature reports on the deep processing of Gorgon fruit at home and abroad. In the Gorgon fruit production area, Gorgon fruit processing is mainly based on primary processed products such as quick-frozen fresh Gorgon fruit, Gorgon rice or dried Gorgon rice. The product category is single, the application range is narrow, and the economic benefit is low, which has caused my country's Gorgon fruit industry to remain at a low level and low benefit for a long time. wandering stage. Therefore, it is imperative to research and develop new Gorgon fruit food and technology to promote the rapid development of Gorgon fruit industry and improve industrial efficiency and technical level. the

发明内容 Contents of the invention

本发明利用芡实的生理保健功能,结合相关中医药研究理论,复配以一定比例的山药和糯米,采用由糖化菌种和酿酒酵母组成的复合菌种进行同时发酵,在对原料配方、酿造工艺分析优化的基础上,得到该低度芡实酒的配方、酿造工艺,并对该产品的主要理化功能特性进行了分析检测和描述。在国内,类似于本发明的相关研究和专利还未见有文献报道。  The present invention utilizes the physiological and health-care function of Gorgon fruit, combines relevant Chinese medicine research theories, mixes Chinese yam and glutinous rice in a certain proportion, and adopts the compound strains composed of saccharification strains and Saccharomyces cerevisiae to carry out simultaneous fermentation. On the basis of analysis and optimization, the formula and brewing process of the low-alcohol Gorgon wine were obtained, and the main physical and chemical functional characteristics of the product were analyzed, detected and described. At home, there are no literature reports similar to related research and patents of the present invention. the

本发明是通过以下技术方案实现的:  The present invention is achieved through the following technical solutions:

一种低度芡实酒的制造方法,所述工艺包括:  A kind of manufacture method of low-alcohol Gorgon fruit wine, described technology comprises:

1)原料配方为芡实、山药干和糯米,三种原料的质量比为20∶10∶70;  1) The raw material formula is Gorgon fruit, dried yam and glutinous rice, and the mass ratio of the three raw materials is 20:10:70;

2)将三种原料混合后,加入原料总质量1.2-1.5倍的水,浸泡后,上笼蒸煮;  2) After mixing the three raw materials, add water 1.2-1.5 times the total mass of the raw materials, after soaking, steam in a basket;

3)蒸煮后的原料经摊晾后,接种由糖化菌种和酿酒酵母菌组成的混合菌种,进行复合发 酵,其中菌种接种量为浸泡前干原料质量的0.8%-1.0%;  3) After the boiled raw materials are spread out to air, inoculate the mixed strains composed of saccharification strains and Saccharomyces cerevisiae for compound fermentation, wherein the inoculum amount of the strains is 0.8%-1.0% of the mass of the dry raw materials before soaking;

4)将原料和复合菌种混合均匀后,放入发酵罐于30℃下发酵10-15天;  4) After mixing the raw materials and the compound strains evenly, put them into a fermenter and ferment at 30°C for 10-15 days;

5)对步骤4的发酵产物采用压滤法进行液固分离,收集滤液即得到初滤酒;  5) The fermentation product of step 4 is separated from liquid to solid by pressure filtration, and the filtrate is collected to obtain the primary filtered wine;

6)将初滤酒装入瓶中密封,在室温、避光条件下,进行后发酵和自然澄清;  6) Put the first-filtered wine into a bottle and seal it, and carry out post-fermentation and natural clarification at room temperature and under dark conditions;

7)待步骤6的酒体澄清后,采用虹吸法得到上层澄清酒液,加盖密封,在室温、避光条件下继续陈酿2-3个月;  7) After the wine body in step 6 is clarified, use the siphon method to obtain the clarified wine liquid in the upper layer, cover and seal, and continue aging for 2-3 months at room temperature and under dark conditions;

8)步骤7经陈酿的酒液经老化和熟化处理,即可形成低度芡实酒。  8) The aged wine liquid in step 7 can be aged and matured to form low-alcohol Gorgon fruit wine. the

所述步骤1中芡实原料粒径为0.5-1.0mm。  The particle size of Gorgon fruit raw material in the step 1 is 0.5-1.0mm. the

所述步骤1山药干原料粒径为1-2mm。  The particle size of the dried yam raw material in step 1 is 1-2 mm. the

所述步骤2中浸泡时长为30min,蒸煮时间为30min。  The soaking time in the step 2 is 30min, and the cooking time is 30min. the

所述步骤4中,投入发酵罐的原料占发酵罐体积的2/3。  In the step 4, the raw materials put into the fermenter account for 2/3 of the volume of the fermenter. the

所述步骤6中,后发酵和自然澄清时长为20-25天。  In said step 6, the duration of post-fermentation and natural clarification is 20-25 days. the

采用本发明制造的低度芡实酒,酒体澄清透明,呈琥珀色,风味清香、滋味甘醇,酒精含量15%(v/v)左右。据本课题组测定,所得芡实酒内含丰富的多酚类物质,总酚含量120mg/L(Folin-Ciocalteus试剂法),具有较强的抗氧化和清除自由基活性。  The low-alcohol Gorgon fruit wine produced by the invention has a clear and transparent body, amber color, delicate flavor, mellow taste, and an alcohol content of about 15% (v/v). According to the determination of our research group, the obtained Gorgon fruit wine is rich in polyphenols, with a total phenol content of 120 mg/L (Folin-Ciocalteus reagent method), and has strong antioxidant and free radical scavenging activities. the

本发明具有以下特点和创新:  The present invention has the following characteristics and innovations:

1、作为一种特色资源的利用,本发明对芡实在功能食品领域深加工进行了有益探索,并取得了较为理想的结果。  1. As a characteristic resource utilization, the present invention has carried out beneficial exploration on the deep processing of Gorgon fruit in the field of functional food, and achieved relatively ideal results. the

2、采用本发明制造的低度芡实酒,酒体澄清透明,呈琥珀色,酒精含量15%(v/v)左右,风味清香、滋味甘醇。因酒精含量较低,适宜不同年龄阶段的成年人饮用。  2. The low-alcohol Gorgon fruit wine manufactured by the present invention has a clear and transparent body, amber color, about 15% (v/v) alcohol content, delicate flavor and mellow taste. Due to the low alcohol content, it is suitable for adults of different ages to drink. the

3、采用本发明制造的低度芡实酒,采用压滤方式进行液渣分离,发酵过程中形成的功能活性组分(氨基酸、多酚、维生素等)均保留在酒液中,所得芡实酒的营养更全面,产品产率也较高。  3. Adopt the low-strength Gorgon fruit wine manufactured by the present invention, adopt the filter press mode to carry out liquid slag separation, the functional active components (amino acids, polyphenols, vitamins, etc.) formed in the fermentation process are all retained in the wine liquid, the obtained Gorgon fruit wine The nutrition is more comprehensive, and the product yield is also higher. the

4、采用发明制造的低度芡实酒,采用压滤方式进行分离,酒体经自然沉降而澄清,整个加工工程未涉及高温处理,更有利于原料中热敏感性功能活性组分的保留。  4. The low-alcohol Gorgon wine produced by the invention is separated by pressure filtration, and the wine body is clarified by natural sedimentation. The whole processing project does not involve high-temperature treatment, which is more conducive to the retention of heat-sensitive functional active components in raw materials. the

5、采用本发明制造的低度芡实酒,虽然整个加工过程中从未涉及高温处理,且所得酒体中酒精含量较低(15%,v/v),但在室温下贮藏18个月后,酒体中仍未发现任何腐败、变质现象。说明采用本发明制造的低度芡实酒酒体稳定,具有较强的自我防腐功能。  5. Although the low-alcohol Gorgon fruit wine produced by the present invention has never involved high-temperature treatment in the whole processing process, and the alcohol content in the obtained wine body is low (15%, v/v), after 18 months of storage at room temperature However, no corruption or deterioration has been found in the wine body. It shows that the low-alcohol Gorgon fruit wine produced by the invention has a stable wine body and strong self-preservation function. the

6、采用本发明制造的低度芡实酒,经室温自然陈酿3个月后,其风味即发生明显改善,新配制酒中的苦味明显减少,同时产生较强的香味,滋味也更加甘醇。  6. The flavor of the low-alcohol Gorgon fruit wine produced by the present invention is obviously improved after natural aging at room temperature for 3 months, and the bitterness in the newly prepared wine is obviously reduced, while producing stronger fragrance and more mellow taste. the

7、采用本发明制造的低度芡实酒,酒精含量15%(v/v)左右,总酚含量120mg/L (Folin-Ciocalteus试剂法),总固形物含量56.4mg/mL,总糖含量23.33mg/mL,总蛋白含量32.51mg/mL,游离氨基酸含量17.26mg/mL,游离氨基酸中必须氨基酸总量6.72mg/mL。该芡实酒具有较强的抗氧化和清除自由基活性,其总还原力和清除超氧阴离子自由基(·O- 2)活性显著高于0.1mg/mL的维生素C溶液,对亚油酸过氧化抑制率达80%以上。  7. The low-alcohol Gorgon fruit wine produced by the present invention has an alcohol content of about 15% (v/v), a total phenol content of 120 mg/L (Folin-Ciocalteus reagent method), a total solid content of 56.4 mg/mL, and a total sugar content of 23.33 mg/mL, the total protein content is 32.51mg/mL, the free amino acid content is 17.26mg/mL, and the total amount of essential amino acids in free amino acids is 6.72mg/mL. The Gorgon fruit wine has strong anti-oxidation and free radical scavenging activities, and its total reducing power and superoxide anion free radical ( O - 2 ) scavenging activity are significantly higher than 0.1mg/mL vitamin C solution, and it has a strong effect on linoleic acid. The oxidation inhibition rate is over 80%.

附图说明 Description of drawings

图1为本发明的主要制造工艺流程图。  Fig. 1 is the main manufacturing process flowchart of the present invention. the

具体实施方式 Detailed ways

以下通过低度芡实酒制造的工艺流程图,结合制造过程,对本发明内容的具体实施过程作进一步地描述:  The following process flow chart of the manufacture of low-alcohol Gorgon wine, combined with the manufacturing process, further describes the specific implementation process of the content of the present invention:

(1)原料配方:芡实、山药干和糯米3种原料的质量比为20∶10∶70,其中芡实进行粗粉碎(粒径0.5-1.0mm),山药干粗粉(粒径1-2mm),然后与糯米混合后,加入其总质量1.2-1.5倍量的水,浸泡30min后,上笼蒸30min。  (1) Raw material formula: the mass ratio of Gorgon fruit, dried yam and glutinous rice is 20:10:70, wherein Gorgon fruit is coarsely crushed (particle size 0.5-1.0mm), yam dry coarse powder (particle size 1-2mm) , and then mix it with glutinous rice, add water of 1.2-1.5 times the total mass, soak for 30 minutes, and steam in a basket for 30 minutes. the

(2)蒸煮后的原料经摊晾后,需要接入菌种进行发酵。本发明采用菌种为由糖化菌种和酿酒酵母菌组成的混合菌种,接种量为浸泡前干原料质量的0.8%-1.0%,混合均匀后,尽可放入发酵罐(原科装入量为发酵罐2/3体积为宜)于30℃下发酵10-15天。  (2) After the boiled raw materials are spread out to dry, bacteria need to be added for fermentation. The present invention adopts bacterial classification as the mixed bacterial classification that is made up of saccharification bacterial classification and Saccharomyces cerevisiae, and the inoculum amount is 0.8%-1.0% of the dry raw material quality before soaking, and after mixing evenly, can put into fermenter as far as possible (original section loads The amount is preferably 2/3 of the volume of the fermenter) and fermented at 30°C for 10-15 days. the

(3)发酵结束后,采用压滤法进行酒液和固体残渣的分离,收集滤液即得到初滤酒。将初滤酒装入瓶中,密封,在室温、避光条件下,进入后发酵和自然澄清阶段。最后死亡的微生物菌体与发酵液中其他颗粒物、胶体等微粒,自然沉降,使酒体自然澄清。此过程需20-25天。  (3) After the fermentation is finished, the wine liquid and the solid residue are separated by pressure filtration, and the filtrate is collected to obtain the primary filtered wine. Put the primary filtered wine into the bottle, seal it, and enter the stage of post-fermentation and natural clarification at room temperature and under the condition of avoiding light. Finally, the dead microbial cells and other particles, colloids and other particles in the fermentation liquid will settle naturally to make the wine body naturally clear. This process takes 20-25 days. the

(4)待酒体澄清后,采用虹吸法,将上层澄清酒液转移至另一干净容器内,并尽量装满,加盖密封。室温、避光条件下继续陈酿约2-3个月,再经老化和熟化处理,即可形成风味浓郁的低度芡实酒。  (4) After the wine body is clarified, use the siphon method to transfer the clarified wine liquid on the upper layer to another clean container, fill it as much as possible, and seal it with a cover. Continue to age for about 2-3 months at room temperature and in the dark, and then undergo aging and aging treatments to form a low-alcohol Gorgon wine with strong flavor. the

(5)贮藏试验结果表明,采用本发明制备的低度芡实酒在室温(15-25℃)、避光条件下贮藏18个月,酒体保持澄清、透明状态,色泽金黄、风味浓郁,无任何变质现象。  (5) The storage test results show that the low-alcohol Gorgon fruit wine prepared by the present invention is stored for 18 months at room temperature (15-25° C.) and under light-proof conditions, and the wine body remains clear and transparent, with golden color and strong flavor. any deterioration. the

Claims (7)

1. the manufacture method of a low-alcohol foxnut wine is characterized in that described technique comprises:
1) composition of raw materials is Gorgon fruit, Dry Rhizoma Dioscoreae and glutinous rice, and the mass ratio of three kinds of raw materials is 20: 10: 70;
2) with after three kinds of raw materials mixing, add raw material total mass 1.2-1.5 water doubly, after the immersion, upper cage boiling;
3) after the raw material airing after the boiling, access is carried out complex ferment by the mixed strains that saccharification bacterial classification and S. cervisiae form, and wherein the bacterial classification inoculation amount is 0.8%-1.0%;
4) raw material and composite bacteria are mixed after, put into fermentor tank in 30 ℃ of bottom fermentation 10-15 days;
5) adopt filter press technique to carry out liquid-solid separation to the tunning of step 4, collect filtrate and namely obtain initial filter wine;
6) initial filter wine is packed into seal in the bottle, under room temperature, lucifuge condition, carry out secondary fermentation and naturally clarify;
7) after the wine body clarification of step 6, adopt siphonage to obtain upper strata clarification wine liquid, seal, under room temperature, lucifuge condition, continued ageing 2-3 month;
8) step 7 again after aging and maturation process, can form low-alcohol foxnut wine through the wine liquid of ageing.
2. the manufacture method of low-alcohol foxnut wine according to claim 1 is characterized in that the Gorgon fruit raw material particle size is 0.5-1.0mm in the described step 1.
3. the manufacture method of low-alcohol foxnut wine according to claim 1 is characterized in that described step 1 Dry Rhizoma Dioscoreae raw material particle size is 1-2mm.
4. the manufacture method of low-alcohol foxnut wine according to claim 1 is characterized in that adding in the described step 1 the total water soaking of expecting 1.5 times of raw material.
5. the manufacture method of low-alcohol foxnut wine according to claim 1 is characterized in that soaking duration in the described step 2 is 30min, and the boiling duration is 30min.
6. the manufacture method of low-alcohol foxnut wine according to claim 1 is characterized in that in the described step 4, and the raw material that drops into fermentor tank accounts for 2/3 of fermentor tank volume.
7. the manufacture method of low-alcohol foxnut wine according to claim 1 is characterized in that in the described step 6, and secondary fermentation and natural settling time are 20-25 days.
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CN103952265A (en) * 2014-05-26 2014-07-30 济宁学院 Gorgon fruit wine and preparation method thereof
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CN101544936A (en) * 2009-04-30 2009-09-30 山东社汇酒业有限公司 Strongly-aromatic white wine produced by using lake plants such as water caltrop, gordon euryale seed, lotus seed, and the like as raw materials and preparation method thereof
CN102161952A (en) * 2011-02-23 2011-08-24 陕西科技大学 Method for preparing coix seed health-care wine

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