CN102294045B - Air freshener containing Zingiber corallinum Hance essential oil and its preparation method - Google Patents
Air freshener containing Zingiber corallinum Hance essential oil and its preparation method Download PDFInfo
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- CN102294045B CN102294045B CN2011102149214A CN201110214921A CN102294045B CN 102294045 B CN102294045 B CN 102294045B CN 2011102149214 A CN2011102149214 A CN 2011102149214A CN 201110214921 A CN201110214921 A CN 201110214921A CN 102294045 B CN102294045 B CN 102294045B
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- 239000002386 air freshener Substances 0.000 title claims abstract description 45
- 239000000341 volatile oil Substances 0.000 title claims abstract description 19
- 238000002360 preparation method Methods 0.000 title claims abstract description 13
- 241000146412 Zingiber corallinum Species 0.000 title abstract description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 38
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 17
- 239000003921 oil Substances 0.000 claims description 80
- 239000000203 mixture Substances 0.000 claims description 29
- ZORQXIQZAOLNGE-UHFFFAOYSA-N 1,1-difluorocyclohexane Chemical compound FC1(F)CCCCC1 ZORQXIQZAOLNGE-UHFFFAOYSA-N 0.000 claims description 16
- 229920001214 Polysorbate 60 Polymers 0.000 claims description 16
- 239000001593 sorbitan monooleate Substances 0.000 claims description 16
- 229940035049 sorbitan monooleate Drugs 0.000 claims description 16
- 235000011069 sorbitan monooleate Nutrition 0.000 claims description 16
- 238000003756 stirring Methods 0.000 claims description 15
- 239000004744 fabric Substances 0.000 claims description 6
- 238000012856 packing Methods 0.000 claims description 6
- 239000012736 aqueous medium Substances 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 11
- 230000001954 sterilising effect Effects 0.000 abstract description 10
- 238000004659 sterilization and disinfection Methods 0.000 abstract description 8
- 210000004556 brain Anatomy 0.000 abstract description 4
- 201000003152 motion sickness Diseases 0.000 abstract description 4
- 241000588724 Escherichia coli Species 0.000 abstract description 3
- 238000002156 mixing Methods 0.000 abstract description 3
- 238000001514 detection method Methods 0.000 abstract description 2
- 235000005979 Citrus limon Nutrition 0.000 abstract 1
- 244000131522 Citrus pyriformis Species 0.000 abstract 1
- 244000166675 Cymbopogon nardus Species 0.000 abstract 1
- 235000018791 Cymbopogon nardus Nutrition 0.000 abstract 1
- 241000255925 Diptera Species 0.000 abstract 1
- 235000006679 Mentha X verticillata Nutrition 0.000 abstract 1
- 235000002899 Mentha suaveolens Nutrition 0.000 abstract 1
- 235000001636 Mentha x rotundifolia Nutrition 0.000 abstract 1
- 241000191967 Staphylococcus aureus Species 0.000 abstract 1
- 244000269722 Thea sinensis Species 0.000 abstract 1
- 235000010482 polyoxyethylene sorbitan monooleate Nutrition 0.000 abstract 1
- 239000000244 polyoxyethylene sorbitan monooleate Substances 0.000 abstract 1
- 229920000053 polysorbate 80 Polymers 0.000 abstract 1
- 230000001846 repelling effect Effects 0.000 abstract 1
- 235000019198 oils Nutrition 0.000 description 60
- 229960004756 ethanol Drugs 0.000 description 11
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 10
- 238000012360 testing method Methods 0.000 description 10
- 230000002159 abnormal effect Effects 0.000 description 7
- 230000000844 anti-bacterial effect Effects 0.000 description 7
- 239000007921 spray Substances 0.000 description 7
- 241000196324 Embryophyta Species 0.000 description 6
- 229910021529 ammonia Inorganic materials 0.000 description 5
- 239000000796 flavoring agent Substances 0.000 description 5
- 235000019634 flavors Nutrition 0.000 description 5
- 241000894006 Bacteria Species 0.000 description 4
- 239000004215 Carbon black (E152) Substances 0.000 description 4
- ATUOYWHBWRKTHZ-UHFFFAOYSA-N Propane Chemical compound CCC ATUOYWHBWRKTHZ-UHFFFAOYSA-N 0.000 description 4
- 239000003205 fragrance Substances 0.000 description 4
- 229930195733 hydrocarbon Natural products 0.000 description 4
- 150000002430 hydrocarbons Chemical class 0.000 description 4
- NNPPMTNAJDCUHE-UHFFFAOYSA-N isobutane Chemical compound CC(C)C NNPPMTNAJDCUHE-UHFFFAOYSA-N 0.000 description 4
- 239000003380 propellant Substances 0.000 description 4
- 239000012752 auxiliary agent Substances 0.000 description 3
- 238000000034 method Methods 0.000 description 3
- 230000035943 smell Effects 0.000 description 3
- SBASXUCJHJRPEV-UHFFFAOYSA-N 2-(2-methoxyethoxy)ethanol Chemical compound COCCOCCO SBASXUCJHJRPEV-UHFFFAOYSA-N 0.000 description 2
- RPWFJAMTCNSJKK-UHFFFAOYSA-N Dodecyl gallate Chemical compound CCCCCCCCCCCCOC(=O)C1=CC(O)=C(O)C(O)=C1 RPWFJAMTCNSJKK-UHFFFAOYSA-N 0.000 description 2
- 235000018958 Gardenia augusta Nutrition 0.000 description 2
- IGFHQQFPSIBGKE-UHFFFAOYSA-N Nonylphenol Natural products CCCCCCCCCC1=CC=C(O)C=C1 IGFHQQFPSIBGKE-UHFFFAOYSA-N 0.000 description 2
- 241000295644 Staphylococcaceae Species 0.000 description 2
- 230000003115 biocidal effect Effects 0.000 description 2
- 239000006071 cream Substances 0.000 description 2
- 229960000935 dehydrated alcohol Drugs 0.000 description 2
- 238000010790 dilution Methods 0.000 description 2
- 239000012895 dilution Substances 0.000 description 2
- 229940080643 dodecyl gallate Drugs 0.000 description 2
- 235000010386 dodecyl gallate Nutrition 0.000 description 2
- 239000000555 dodecyl gallate Substances 0.000 description 2
- 239000003814 drug Substances 0.000 description 2
- 238000011156 evaluation Methods 0.000 description 2
- 239000001282 iso-butane Substances 0.000 description 2
- 235000013847 iso-butane Nutrition 0.000 description 2
- 238000011031 large-scale manufacturing process Methods 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- SNQQPOLDUKLAAF-UHFFFAOYSA-N nonylphenol Chemical compound CCCCCCCCCC1=CC=CC=C1O SNQQPOLDUKLAAF-UHFFFAOYSA-N 0.000 description 2
- 239000001294 propane Substances 0.000 description 2
- 239000013558 reference substance Substances 0.000 description 2
- 238000011160 research Methods 0.000 description 2
- 230000001953 sensory effect Effects 0.000 description 2
- 239000000725 suspension Substances 0.000 description 2
- 229920001817 Agar Polymers 0.000 description 1
- 241000144210 Culex pipiens pallens Species 0.000 description 1
- 241000256113 Culicidae Species 0.000 description 1
- 206010012374 Depressed mood Diseases 0.000 description 1
- 235000010254 Jasminum officinale Nutrition 0.000 description 1
- 240000005385 Jasminum sambac Species 0.000 description 1
- 244000246386 Mentha pulegium Species 0.000 description 1
- 235000016257 Mentha pulegium Nutrition 0.000 description 1
- 235000004357 Mentha x piperita Nutrition 0.000 description 1
- 241000234314 Zingiber Species 0.000 description 1
- 239000000443 aerosol Substances 0.000 description 1
- 239000008272 agar Substances 0.000 description 1
- 230000000202 analgesic effect Effects 0.000 description 1
- 239000003242 anti bacterial agent Substances 0.000 description 1
- 230000003110 anti-inflammatory effect Effects 0.000 description 1
- 229940088710 antibiotic agent Drugs 0.000 description 1
- 235000019568 aromas Nutrition 0.000 description 1
- 238000003556 assay Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000000975 bioactive effect Effects 0.000 description 1
- 230000017531 blood circulation Effects 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- 239000008367 deionised water Substances 0.000 description 1
- 229910021641 deionized water Inorganic materials 0.000 description 1
- 230000001877 deodorizing effect Effects 0.000 description 1
- 230000008451 emotion Effects 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 235000001050 hortel pimenta Nutrition 0.000 description 1
- 238000000338 in vitro Methods 0.000 description 1
- 229940040145 liniment Drugs 0.000 description 1
- 239000000865 liniment Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 230000003340 mental effect Effects 0.000 description 1
- 239000006916 nutrient agar Substances 0.000 description 1
- 239000002674 ointment Substances 0.000 description 1
- 239000002304 perfume Substances 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000003507 refrigerant Substances 0.000 description 1
- 239000008159 sesame oil Substances 0.000 description 1
- 235000011803 sesame oil Nutrition 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 230000000475 sunscreen effect Effects 0.000 description 1
- 239000000516 sunscreening agent Substances 0.000 description 1
- 230000008961 swelling Effects 0.000 description 1
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
Landscapes
- Cosmetics (AREA)
- Disinfection, Sterilisation Or Deodorisation Of Air (AREA)
Abstract
The invention relates to an air freshener and a preparation method thereof, wherein the air freshener consists of 1-4 parts of Zingiber corallinum Hance essential oil, 1-4 parts of lemon essential oil, 1-3 parts of mint essential oil, 0.5-2.5 parts of citronella essential oil, 0.5-2 parts of polyoxyethylene sorbitan monooleate, 20-30 parts of water and 60-70 parts of ethanol with the volume fraction of 95%; mixing the essential oil according to the formula amount uniformly, then sequentially adding ethanol and water, and uniformly mixing; the air freshener has the functions of refreshing air, sterilizing, refreshing, removing peculiar smell, preventing carsickness, repelling mosquitoes and the like, and can comprehensively improve the air quality; the freshener has an obvious sterilization effect, and the detection shows that the killing rate of escherichia coli and staphylococcus aureus is 95.0%; the natural essential oil contained in the tea can revivify, refresh the mind, refresh the brain, improve the learning and working efficiency, and can react with peculiar smell molecules to decompose and eliminate peculiar smell; the air freshener disclosed by the invention is cool and fragrant in smell, and is suitable for being used in rooms, offices, vehicles, hotels and the like.
Description
Technical field
The present invention relates to filed of daily-use chemical industry, particularly air freshener and preparation method thereof.
Background technology
Along with the raising of people's living standard, air freshener has become articles for daily use.Traditional air freshener is mainly used in improving air quality as " environment perfume ".They are the chemical reagent that utilizes synthetic mostly, though play the effect of covering smell, health and environment are threatened.At present, also rarely have the air freshener that adopts the natural extract preparation on the market, particularly be applicable to the personalized air freshener of varying environment.
Rhizoma Zingiberis corallini is commonly called as cloudy Rhizoma Zingiberis Recens, is zingiberaceous plant, and its rhizome is used as medicine, and the subduing swelling and detoxicating function is arranged.Recent research shows that Rhizoma Zingiberis corallini quintessence oil is a kind of natural plants antibacterial, and very strong sterilization and bacteriostasis are arranged; Sunscreen cream, ZHICHUANG GAO and anti-inflammatory analgesic cream etc. have been used to prepare.Application number is that 200810070117.1 Chinese patent application discloses a kind of osmidrosis dispelling liniment that contains natural Zingiber corallinum Hance essential oil, application number is that 200810070369.4 Chinese patent application discloses the kibe ointment that contains natural zingiber oil, and application number is that 201010102989.9 Chinese patent application discloses the ZHICHUANG GAO that contains Rhizoma Zingiberis corallini quintessence oil.What these patent applications only related to is the human body skin product, and mainly is the antibacterial functions that utilizes the single raw material of Rhizoma Zingiberis corallini quintessence oil.Utilize the antibacterial characteristics of Rhizoma Zingiberis corallini quintessence oil, and adapted other have the natural plant essential oils of antibiotic isoreactivity, the exploitation air freshener, be expected to reach efficient, natural safe ideal effect.This type of research at present there is no report in all kinds of documents.
Summary of the invention
The object of the present invention is to provide a kind of essential oil composition, it has sterilization, refreshment, removes the function of abnormal flavour.
For achieving the above object, technical scheme of the present invention is:
Essential oil composition, composed of the following components by weight:
Rhizoma Zingiberis corallini quintessence oil 1-4 part;
Fructus Citri Limoniae quintessence oil 1-4 part;
Herba Menthae quintessence oil 1-3 part;
Herba Cymbopogonis Citrari quintessence oil 0.5-2.5 part.
Two of purpose of the present invention is to provide a kind of air freshener, and it also has the effect of sterilization, refreshment, anti-carsickness, anophelifuge concurrently in fresh air, removing abnormal flavour.
For achieving the above object, technical scheme of the present invention is:
The air freshener that contains described essential oil composition, calculate composed of the following components by weight:
Rhizoma Zingiberis corallini quintessence oil 1-4 part;
Fructus Citri Limoniae quintessence oil 1-4 part;
Herba Menthae quintessence oil 1-3 part;
Herba Cymbopogonis Citrari quintessence oil 0.5-2.5 part;
Polyoxyethylenesorbitan sorbitan monooleate 0.5-2 part;
Water 20-30 part;
Volume fraction is 95% ethanol 60-70 part;
Further, described air freshener, calculate composed of the following components by weight:
4 parts of Rhizoma Zingiberis corallini quintessence oil;
Fructus Citri Limoniae quintessence oil 1-4 part;
Herba Menthae quintessence oil 1-3 part;
Herba Cymbopogonis Citrari quintessence oil 0.5-2.5 part;
Polyoxyethylenesorbitan sorbitan monooleate 0.5-2 part;
Water 20-30 part;
Volume fraction is 95% ethanol 60-70 part.
Further, described air freshener, calculate composed of the following components by weight:
Rhizoma Zingiberis corallini quintessence oil 1-4 part;
Fructus Citri Limoniae quintessence oil 1-4 part;
3 parts of Herba Menthae quintessence oils;
Herba Cymbopogonis Citrari quintessence oil 0.5-2.5 part;
Polyoxyethylenesorbitan sorbitan monooleate 0.5-2 part;
Water 20-30 part;
Volume fraction is 95% ethanol 60-70 part.
Further, described air freshener, calculate composed of the following components by weight:
Rhizoma Zingiberis corallini quintessence oil 1-4 part;
Fructus Citri Limoniae quintessence oil 1-4 part;
Herba Menthae quintessence oil 1-3 part;
2.5 parts of Herba Cymbopogonis Citrari quintessence oils;
Polyoxyethylenesorbitan sorbitan monooleate 0.5-2 part;
Water 20-30 part;
Volume fraction is 95% ethanol 60-70 part.
Three of purpose of the present invention is to provide a kind of preparation method of air freshener, and this method is simple to operate, is applicable to large-scale production.
For achieving the above object, technical scheme of the present invention is:
The preparation method of described air freshener specifically may further comprise the steps:
A. by described formula ratio Rhizoma Zingiberis corallini quintessence oil, Fructus Citri Limoniae quintessence oil, Herba Menthae quintessence oil, Herba Cymbopogonis Citrari quintessence oil, polyoxyethylenesorbitan sorbitan monooleate are mixed and stir, get mixture;
B. the mixture with step a gained adds in the ethanol of formula ratio, stirs;
C. required water is added under stirring condition in the mixture of step b gained slowly, mix homogeneously gets air freshener.
Further, described air freshener is filtered with 〉=200 purpose filter screens or filter cloth, send into the can packing machine quantitative filling, get finished product.
Beneficial effect of the present invention is: contain multiple efficient natural plants essential oil in the described air freshener that contains Rhizoma Zingiberis corallini quintessence oil, this essential oil composition can use separately, also can be prepared into air freshener.Wherein, Rhizoma Zingiberis corallini quintessence oil is a kind of natural plants antibacterial, and very strong sterilization and bacteriostasis are arranged; Fructus Citri Limoniae quintessence oil has pure and fresh fragrant and sweet, fresh fragrance, can inspire enthusiasm, and pure and fresh brains is focused one's attention on, and improves study and work efficient, has anti-carsick function concurrently; The peppermint essence salted cake fried in sesame oil Qi Cheongju people that feels nice and cool can excited brain, and blood circulation promoting improves spirit, prevents carsickness, and has bactericidal action concurrently; The Herba Cymbopogonis Citrari quintessence oil distributes strong citris aromas, and abnormal smells from the patient is pure and fresh pleasant, can improve emotion, can express and separate depressed mood, has the function of deodorizing sterilizing, anophelifuge concurrently.The air freshener that the present invention relates to, natural plant composition is prepared by scientific and reasonable coordination, possess fresh air, sterilization, refreshment, removing abnormal flavour, prevent functions such as carsickness, can improve air quality comprehensively, reach the purpose that purifies air, promotes health; This freshener bactericidal effect is obvious, and the killing rate to escherichia coli and gold-coloured staphylococci is 95.0% after testing; The natural essential oil that contains can be inspired enthusiasm, pure and fresh brains, raising study and work efficient; The quintessence oil bioactive molecule that contains can with the abnormal flavour molecular reaction, decompose to eliminate abnormal flavour.The present invention contains the refrigerant fragrance of air freshener abnormal smells from the patient of Rhizoma Zingiberis corallini quintessence oil, and effect is remarkable, and natural green is harmless, is fit in room, office, toilet, the car, occasion such as hotel uses.This preparation method technology is simple, and equipment investment is few, and production process is easy to control, and the spray bottle packing is adopted in large-scale production easily, and is easy to use.
The specific embodiment
Embodiment 1 room air freshener
1 prescription
Essential oil composition: 4 parts of Rhizoma Zingiberis corallini quintessence oil, 1 part of Fructus Citri Limoniae quintessence oil, 1 part of Herba Menthae quintessence oil, 2 parts of Herba Cymbopogonis Citrari quintessence oils.
Auxiliary agent: 1 part of polyoxyethylenesorbitan sorbitan monooleate, 20 parts in water, volume fraction is 70 parts of 95% ethanol.
2 preparation methoies are as follows:
A. in described ratio Rhizoma Zingiberis corallini quintessence oil, Fructus Citri Limoniae quintessence oil, Herba Menthae quintessence oil, Herba Cymbopogonis Citrari quintessence oil, polyoxyethylenesorbitan sorbitan monooleate are mixed and stir, get mixture.
B. the mixture with step a gained adds in the described ethanol, stirs.
C. required water is added in the mixture of step b gained slowly mix homogeneously under stirring condition.
D. the gained mixed liquor is filtered with 〉=200 purpose filter screens or filter cloth, send into can packing machine then, quantitative filling, the fog-spray nozzle of screwing on is finished product.
3, result of use test:
1) taste removal effect (ammonia clearance)
Laboratory Module: volume 0.1m
--3, 20 ± 1 ℃ of temperature, humidity 50 ± 5%RH, surface wind speed 0.3m/s, sample detection consumption 0.1ml, ammonia clearance are in 3h, and initial concentration is 2.1mg/m--3, naturally decay 14%.Ammonia content is measured by the method for national standard " ammonia assay method in the public place air " GB/T 18204.25 regulations.The ammonia clearance reaches 82%.
2) bactericidal effect
Test organisms 24h slant culture is washed with PBS, and (concentration of requirement is: drip on the contrast print with 100 μ L, reclaiming the bacterium number is 1 * 10 to make bacteria suspension
4～9 * 10
4Cfu/sheet).Get that (each 4 of 2.0cm * 3.0cm) and contrast prints (with the sample homogeneous material, equal size, but do not contain anti-biotic material, and through sterilization treatment) are divided into 4 groups and place in 4 sterilization plates by coupons.Get above-mentioned bacteria suspension, dripped 100 μ L at each by coupons and contrast print respectively, evenly be coated with filter cloth, pick up counting, effect 2,5,10,20 min, respectively print is thrown the people with aseptic tweezer and contained the corresponding nertralizer of 5 m1 in vitro, fully mixing is done suitably dilution, gets wherein 2-3 dilution factor then, draw 0.5ml respectively, place two plates, pour into cool nutrient agar 15m1 to 40-45 ℃, rotate plate, make it full and uniform, it is dull and stereotyped that agar solidifies the back upset, and 35 ℃ of scholars cultivate 48h for 2 ℃, do the viable bacteria colony counting.Killing rate to escherichia coli and gold-coloured staphylococci is 95.0%.
Embodiment 2 Vehicular air freshener
1 prescription
Essential oil composition: 1 part of Rhizoma Zingiberis corallini quintessence oil, 4 parts of Fructus Citri Limoniae quintessence oil, 3 parts of Herba Menthae quintessence oils, 0.5 part of Herba Cymbopogonis Citrari quintessence oil.
Auxiliary agent: 0.5 part of polyoxyethylenesorbitan sorbitan monooleate, 30 parts in water, volume fraction is 60 parts of 95% ethanol.
2 preparation methoies are as follows:
A. in described ratio Rhizoma Zingiberis corallini quintessence oil, Fructus Citri Limoniae quintessence oil, Herba Menthae quintessence oil, Herba Cymbopogonis Citrari quintessence oil, polyoxyethylenesorbitan sorbitan monooleate are mixed and stir, get mixture.
B. the mixture with step a gained adds in the described ethanol, stirs.
C. required deionized water is added in the mixture of step b gained slowly mix homogeneously under stirring condition.
D. the gained mixed liquor is filtered with 〉=200 purpose filter screens or filter cloth, send into can packing machine then, quantitative filling, the fog-spray nozzle of screwing on is finished product.
3, resisting fatigue and anti-carsick measure of merit:
The test group is made up of 16 volunteers (25-30 years old, wherein the men and women is each 8).Experimental group is totally 8 people (5 have carsick history), and 4 people are 1 group, are divided into 2 groups; Spray 8ml embodiment 2 Vehicular air freshener in the car of experimental group, silence drives to travel 300 kilometers on highway.Matched group is totally 8 people (5 have carsick history), and 4 people are 1 group, are divided into 2 groups, do not spray in car under the situation of air freshener, and same silence drives to travel 300 kilometers.Then, each group is investigated individual's the mental status, degree of fatigue and carsick degree.
Test result is as follows:
Embodiment 3 domestic air freshener
Essential oil composition: 3 parts of Rhizoma Zingiberis corallini quintessence oil, 3 parts of Fructus Citri Limoniae quintessence oil, 2 parts of Herba Menthae quintessence oils, 2.5 parts of Herba Cymbopogonis Citrari quintessence oils.
Auxiliary agent: 2 parts of polyoxyethylenesorbitan sorbitan monooleate, 25 parts in water, volume fraction is 65 parts of 95% ethanol.
2 preparation methoies are as follows:
A. in described ratio Rhizoma Zingiberis corallini quintessence oil, Fructus Citri Limoniae quintessence oil, Herba Menthae quintessence oil, Herba Cymbopogonis Citrari quintessence oil, polyoxyethylenesorbitan sorbitan monooleate are mixed and stir, get mixture.
B. the mixture with step a gained adds in the described ethanol, stirs.
C. required water is added in the mixture of step b gained slowly mix homogeneously under stirring condition.
D. the gained mixed liquor is filtered with 〉=200 purposes filter screen/filter cloth, send into can packing machine then, quantitative filling, the fog-spray nozzle of screwing on is finished product.
The test of 3 effect exterminating mosquitos
Test in the cabinet at two glass that are placed with culex pipiens pallens fully, press 0.5ml/m with the aerosol rifle
3The spray medicine moves to receptacle behind the observation 30min and raises calculating K T
50Reach the 24h mortality rate, and compare with commercially available jasmine fragrance air freshener.The result is as follows:
Reference substance (universal air freshener) prescription, composed of the following components by weight percentage: jasmin essence 3.6%, metering system dodecyl gallate 3.6%, dehydrated alcohol 10.0%, diethylene glycol monomethyl ether 24.2%, nonyl phenol 0.2%, hydrocarbon propellant 58.4%, wherein the hydrocarbon propellant is that 20% propane and volume ratio are that 80% iso-butane is formed by volume ratio.
The subjective appreciation of embodiment 4 air fresheners
The subjective appreciation of air freshener carries out in the sensory test chamber.Form scoring group by 10 people (22-30 years old, each 5 of men and women possess the rudimentary knowledge of sensory evaluation), under room temperature, mark, get its meansigma methods.By a certain amount of organoleptic test chamber that is sprayed on, the person of participating in evaluation and electing stops 10min in the organoleptic test chamber, mark then with air freshener.Standards of grading: fresh air effect (40 minutes); The comfortable effect of fragrance (30 minutes); Improve spiritual effect (30 minutes).The scoring situation is as follows:
Reference substance (universal air freshener) prescription, composed of the following components by weight percentage: jasmin essence 3.6%, metering system dodecyl gallate 3.6%, dehydrated alcohol 10.0%, diethylene glycol monomethyl ether 24.2%, nonyl phenol 0.2%, hydrocarbon propellant 58.4%, wherein the hydrocarbon propellant is that 20% propane and volume ratio are that 80% iso-butane is formed by volume ratio.
Explanation is at last, above embodiment is only unrestricted in order to technical scheme of the present invention to be described, although by invention has been described with reference to the preferred embodiments of the present invention, but those of ordinary skill in the art is to be understood that, can make various changes to it in the form and details, and not depart from the spirit and scope of the present invention that appended claims limits.
Claims (2)
1. contain the air freshener of essential oil composition, it is characterized in that, calculate composed of the following components by weight:
Rhizoma Zingiberis corallini quintessence oil 1-4 part;
Fructus Citri Limoniae quintessence oil 1-4 part;
Herba Menthae quintessence oil 1-3 part;
Herba Cymbopogonis Citrari quintessence oil 0.5-2.5 part;
Polyoxyethylenesorbitan sorbitan monooleate 0.5-2 part;
Water 20-30 part;
Volume fraction is 95% ethanol 60-70 part.
2. air freshener according to claim 1 is characterized in that, calculates composed of the following components by weight:
4 parts of Rhizoma Zingiberis corallini quintessence oil;
Fructus Citri Limoniae quintessence oil 1-4 part;
Herba Menthae quintessence oil 1-3 part;
Herba Cymbopogonis Citrari quintessence oil 0.5-2.5 part;
Polyoxyethylenesorbitan sorbitan monooleate 0.5-2 part;
Water 20-30 part;
Volume fraction is 95% ethanol 60-70 part.
3, air freshener according to claim 1 is characterized in that, calculates composed of the following components by weight:
Rhizoma Zingiberis corallini quintessence oil 1-4 part;
Fructus Citri Limoniae quintessence oil 1-4 part;
3 parts of Herba Menthae quintessence oils;
Herba Cymbopogonis Citrari quintessence oil 0.5-2.5 part;
Polyoxyethylenesorbitan sorbitan monooleate 0.5-2 part;
Water 20-30 part;
Volume fraction is 95% ethanol 60-70 part.
4, air freshener according to claim 1 is characterized in that, calculates composed of the following components by weight:
Rhizoma Zingiberis corallini quintessence oil 1-4 part;
Fructus Citri Limoniae quintessence oil 1-4 part;
Herba Menthae quintessence oil 1-3 part;
2.5 parts of Herba Cymbopogonis Citrari quintessence oils;
Polyoxyethylenesorbitan sorbitan monooleate 0.5-2 part;
Water 20-30 part;
Volume fraction is 95% ethanol 60-70 part.
5, the preparation method of each described air freshener among the claim 1-4 is characterized in that, specifically may further comprise the steps:
A. by described formula ratio Rhizoma Zingiberis corallini quintessence oil, Fructus Citri Limoniae quintessence oil, Herba Menthae quintessence oil, Herba Cymbopogonis Citrari quintessence oil, polyoxyethylenesorbitan sorbitan monooleate are mixed and stir, get mixture;
B. the mixture with step a gained adds in the ethanol of formula ratio, stirs;
C. required aqueous medium is added under stirring condition in the mixture of step b gained slowly, mix homogeneously gets air freshener.
6, the preparation method of air freshener according to claim 5 is characterized in that, described air freshener is filtered with 〉=200 purpose filter screens or filter cloth, sends into the can packing machine quantitative filling, gets the finished product of air freshener.
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| KR101377652B1 (en) * | 2012-04-24 | 2014-03-26 | 주식회사 워터레스랩 | Composition for proventing backflow of stink |
| CN104178339B (en) * | 2014-08-11 | 2016-08-17 | 安徽丰乐香料有限责任公司 | Solubility natural plant essential oils and preparation method thereof |
| CN105519597A (en) * | 2016-01-11 | 2016-04-27 | 安佑生物科技集团股份有限公司 | Animal barn air disinfectant containing plant essential oil, and application method thereof |
| CN106729872A (en) * | 2016-12-10 | 2017-05-31 | 钦州学院 | A kind of air freshener and preparation method thereof |
| CN107083282B (en) * | 2017-06-12 | 2020-12-15 | 杨佳宁 | Refreshing essential oil and preparation method and application thereof |
| CN108294972A (en) * | 2018-03-21 | 2018-07-20 | 深圳市集强仁通科技有限公司 | A kind of pure natural taste removal essential oil and preparation method thereof |
| CN113512467A (en) * | 2021-05-11 | 2021-10-19 | 上海应用技术大学 | Citrus-ginger fragrance air freshener and preparation method thereof |
| CN114569695A (en) * | 2022-03-28 | 2022-06-03 | 上海应用技术大学 | Aromatic essential oil with functions of removing peculiar smell and preventing carsickness and application thereof |
| CN115569225A (en) * | 2022-10-14 | 2023-01-06 | 安徽信息工程学院 | an air freshener |
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