CN102293216A - Bactericidal preservative for chemical fiber oil agent and preparation method thereof - Google Patents
Bactericidal preservative for chemical fiber oil agent and preparation method thereof Download PDFInfo
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- CN102293216A CN102293216A CN2011101835616A CN201110183561A CN102293216A CN 102293216 A CN102293216 A CN 102293216A CN 2011101835616 A CN2011101835616 A CN 2011101835616A CN 201110183561 A CN201110183561 A CN 201110183561A CN 102293216 A CN102293216 A CN 102293216A
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Abstract
The invention discloses a bactericidal preservative for a chemical fiber oil agent and a preparation method thereof. The bactericidal preservative for the chemical fiber oil agent comprises bactericidal and preservative active components of a thiocyano compound, an organic bromine compound, and an isothiazolone compound, an assistant, an emulsifier, a surfactant, and the balance propylene glycol. A preparation (the bactericidal preservative) concretely comprises, by weight, 0.5-5.0% of the thiocyano compound, 0-15% of the organic bromine compound, 0.5-5.0% of the isothiazolone compound, 1.0-3.5% of the emulsifier, 0-10% of the assistant, 0-15% of the surfactant, and the balance propylene glycol. The preparation is prepared by respectively mixing the thiocyano compound with the organic bromine compound and the isothiazolone compound under normal pressure and normal temperature conditions, adding rest raw materials, mixing, and stirring. The preparation which organically combines bactericidal drugs with preservative drugs has the advantages of high efficiency, low toxicity, good compatibleness with various chemical fiber oil agents, low production cost, convenient usage, safety and reliability, and easy implementation.
Description
Technical field
The present invention relates to the preservative production field, be specifically related to a kind of preparation medium sterilization antiseptic and preparation method thereof.
Background technology
Preparation medium is mainly formed by surfactant compound, and be used to prevent static, improve fibre cohesion, improve feel and serviceability etc., be one of indispensable auxiliary agent in fiber production and the process.
The preparation medium sterilization antiseptic is a kind of preparation medium to be carried out the preparation of sterilization and anticorrosion, is applicable to various preparation mediums, all is widely used in finish systems such as POY, FDY, UDY.It generally forms by multiple efficient antiseptic is composite, can kill various bacteria, fungi, saccharomycete, at present, the sterilization antiseptic that is used for preparation medium mostly is nontransparent shape preparation greatly, and general domestic sulfur-bearing cyano compound is creamy, its fatal weakness is that inconvenient preparation medium corrosion-resistant production is used, cause with various preparation medium compatibilities badly, persistence is poor, and life cycle is short, the production cost height, economic results in society are poor.
Summary of the invention
In view of this, first purpose of the present invention is to provide a kind of preparation medium sterilization antiseptic with characteristics such as pollution-free, high-efficiency low-toxicity, production cost are low.
Second purpose of the present invention is to provide the preparation method of above-mentioned preparation medium sterilization antiseptic, make that above-mentioned preparation medium sterilization antiseptic has that fungicidal spectrum is wider, persistence is better, good with various preparation medium compatibilities, produce and use in high-efficiency low-toxicity, production cost is low, pesticide resistance is little, life cycle is long.
For achieving the above object, technical scheme of the present invention is as follows:
A kind of preparation medium sterilization antiseptic is made up of the propane diols of sterilization and anticorrosion active ingredients such as sulfur-bearing cyano compound, organobromine compound, isothiazolone compounds and auxiliary agent, emulsifier, surfactant and aequum.The parts by weight percentage of said preparation is:
Preferably, the parts by weight percentage of said preparation is:
Preferably, described thiocyanogen compound is the clear or dithiocyano-methane of benzene thiophene bacterium.
Preferably, described organobromine compound is dibromo nitroethyl alcohol, bronopol or dibromo cyano group propionamide.
Preferably, described isothiazolone is benzene a pair of horses going side by side isothiazolinone, octyl group isothiazolinone, Ka Song or dichloro octyl group isothiazolinone.
A kind of preparation method of preparation medium sterilization antiseptic, described thiocyanogen compound and described organobromine compound, isothiazolone compounds are prepared earlier respectively, and then the adding surplus stock adopts special mixing stirring means to prepare.
Preferably, described thiocyanogen compound and described organobromine compound, isothiazolone compounds are prepared earlier respectively, add surplus stock again and mix to stir to be formulated as under normal pressure, normal temperature and prepare.
Can find out that from above-mentioned technical scheme a kind of preparation medium sterilization antiseptic disclosed in this invention has characteristics such as pollution-free, the high and low poison of drug effect, production cost be low.
The preparation method of above-mentioned preparation medium sterilization antiseptic provided by the invention, by under normal pressure, normal temperature, thiocyanogen compound and organobromine compound, isothiazolone compounds being prepared earlier respectively, and then the adding surplus stock adopts special mixing stirring means to prepare, make that above-mentioned preparation medium sterilization antiseptic has that fungicidal spectrum is wider, persistence is better, good with various preparation medium compatibilities, produce and use in pollution-free, the high and low poison of drug effect, characteristics such as production cost is low, pesticide resistance is little, life cycle is long, economic results in society are remarkable.
Embodiment
Below the technical scheme in the embodiment of the invention is clearly and completely described, obviously, described embodiment only is the present invention's part embodiment, rather than whole embodiment.Based on the embodiment among the present invention, those of ordinary skills are not making the every other embodiment that is obtained under the creative work prerequisite, all belong to the scope of protection of the present invention.
The invention discloses a kind of preparation medium sterilization antiseptic, with reach pollution-free, high-efficiency low-toxicity, production cost is low, pesticide resistance is little, life cycle is long, the significant purpose of economic results in society.
Embodiment 1.
A kind of preparation medium sterilization antiseptic is made up of the propane diols of sterilization and anticorrosion active ingredients such as sulfur-bearing cyano compound, organobromine compound, isothiazolone compounds and auxiliary agent, emulsifier, surfactant and aequum.The parts by weight percentage of said preparation is:
The preferred parts by weight percentage of said preparation is:
Wherein, described thiocyanogen compound is the clear or dithiocyano-methane of benzene thiophene bacterium; Described organobromine compound is dibromo nitroethyl alcohol, bronopol or dibromo cyano group propionamide; Described isothiazolone is benzene a pair of horses going side by side isothiazolinone, octyl group isothiazolinone, Ka Song or dichloro octyl group isothiazolinone.
The preparation method of above-mentioned preparation medium sterilization antiseptic is: by under normal pressure, normal temperature thiocyanogen compound and organobromine compound, isothiazolone compounds being prepared earlier respectively, and then the propane diols that adds a certain amount of emulsifier, auxiliary agent, surfactant and surplus adopts special mixing stirring means to prepare, thus make above-mentioned preparation medium sterilization antiseptic have that fungicidal spectrum is wider, persistence better, good with various preparation medium compatibilities.Produce and use in easy to implement, characteristics such as production cost is low, pesticide resistance is little, life cycle is long, economic results in society are remarkable, and pollution-free, high-efficiency low-toxicity, this preparation is 566mg/kg to the acute oral toxicity LD50 of male white rat, belong to low toxicity preparation medium preservative, easy to use, safe and reliable.
More than be description,, make this area professional and technical personnel can realize or use the present invention by above-mentioned explanation to the disclosed embodiments to a kind of preparation medium sterilization antiseptic of the present invention and preparation method thereof embodiment.Multiple modification to these embodiment will be conspicuous concerning those skilled in the art, and defined herein General Principle can realize under the situation that does not break away from the spirit or scope of the present invention in other embodiments.Therefore, the present invention will can not be restricted to these embodiment shown in this article, but will meet and principle disclosed herein and features of novelty the wideest corresponding to scope.
Claims (7)
1. a preparation medium sterilization antiseptic is characterized in that, is made up of the propane diols of sterilization and anticorrosion active ingredients such as sulfur-bearing cyano compound, organobromine compound, isothiazolone compounds and auxiliary agent, emulsifier, surfactant and aequum.The parts by weight percentage of said preparation is:
2. a kind of preparation medium sterilization antiseptic according to claim 1 is characterized in that, the parts by weight percentage of said preparation is:
3. a kind of preparation medium sterilization antiseptic according to claim 1 and 2 is characterized in that, described thiocyanogen compound is the clear or dithiocyano-methane of benzene thiophene bacterium.
4. a kind of preparation medium sterilization antiseptic according to claim 1 and 2 is characterized in that, described organobromine compound is dibromo nitroethyl alcohol, bronopol or dibromo cyano group propionamide.
5. a kind of efficient preparation medium sterilization antiseptic according to claim 1 and 2 is characterized in that, described isothiazolone is benzene a pair of horses going side by side isothiazolinone, octyl group isothiazolinone, Ka Song or dichloro octyl group isothiazolinone.
6. the preparation method of a kind of preparation medium sterilization antiseptic according to claim 1 and 2, it is characterized in that, described thiocyanogen compound and described organobromine compound, isothiazolone compounds are prepared earlier respectively, add surplus stock mixing stirring again and prepare.
7. the preparation method of a kind of preparation medium sterilization antiseptic according to claim 6, it is characterized in that, described thiocyanogen compound and described organobromine compound, isothiazolone compounds are prepared earlier respectively, add surplus stock again and mix to stir to be formulated as under normal pressure, normal temperature and prepare.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2011101835616A CN102293216A (en) | 2011-07-01 | 2011-07-01 | Bactericidal preservative for chemical fiber oil agent and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2011101835616A CN102293216A (en) | 2011-07-01 | 2011-07-01 | Bactericidal preservative for chemical fiber oil agent and preparation method thereof |
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| CN102293216A true CN102293216A (en) | 2011-12-28 |
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| CN2011101835616A Pending CN102293216A (en) | 2011-07-01 | 2011-07-01 | Bactericidal preservative for chemical fiber oil agent and preparation method thereof |
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Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103598196A (en) * | 2013-10-25 | 2014-02-26 | 中国海洋石油总公司 | Biological slime stripping agent for water treatment, and preparation method thereof |
| CN103768956A (en) * | 2014-01-23 | 2014-05-07 | 南通苏通分离工程科技有限公司 | Reverse osmosis membrane bactericide and preparation method thereof |
| CN104594030A (en) * | 2015-01-26 | 2015-05-06 | 江苏文凤化纤集团有限公司 | Preparation method for spinning composite finishing agent |
| CN104606188A (en) * | 2015-02-06 | 2015-05-13 | 武汉中博水产生物技术有限公司 | Bactericidal composition and application thereof in preparation of medicines for treating aquaculture diseases |
| CN105123719A (en) * | 2015-08-08 | 2015-12-09 | 江苏神涛环保科技有限公司 | Chemical fiber oil sterilization preservative and compounding method thereof |
| CN107047603A (en) * | 2016-08-01 | 2017-08-18 | 中国石油天然气股份有限公司 | Bactericide and preparation method and application thereof |
| CN108041076A (en) * | 2017-12-29 | 2018-05-18 | 常州达奥新材料科技有限公司 | A kind of preparation method of sterilization antiseptic |
| CN108184891A (en) * | 2018-02-28 | 2018-06-22 | 陕西理工大学 | A kind of sterilization agent emulsion and preparation method thereof |
| CN112450217A (en) * | 2020-12-18 | 2021-03-09 | 湖南幻影三陆零科技有限公司 | Disinfectant and disinfectant composition containing same |
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| JP2001261509A (en) * | 2000-03-17 | 2001-09-26 | Kurita Water Ind Ltd | Industrial antibacterial composition and industrial antibacterial method |
| JP2003171209A (en) * | 2001-09-26 | 2003-06-17 | K I Chemical Industry Co Ltd | Industrial microbicidal antiseptic agent and microbicidal antiseptic method |
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| JP2003171209A (en) * | 2001-09-26 | 2003-06-17 | K I Chemical Industry Co Ltd | Industrial microbicidal antiseptic agent and microbicidal antiseptic method |
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Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103598196A (en) * | 2013-10-25 | 2014-02-26 | 中国海洋石油总公司 | Biological slime stripping agent for water treatment, and preparation method thereof |
| CN103768956A (en) * | 2014-01-23 | 2014-05-07 | 南通苏通分离工程科技有限公司 | Reverse osmosis membrane bactericide and preparation method thereof |
| CN104594030A (en) * | 2015-01-26 | 2015-05-06 | 江苏文凤化纤集团有限公司 | Preparation method for spinning composite finishing agent |
| CN104606188A (en) * | 2015-02-06 | 2015-05-13 | 武汉中博水产生物技术有限公司 | Bactericidal composition and application thereof in preparation of medicines for treating aquaculture diseases |
| CN105123719A (en) * | 2015-08-08 | 2015-12-09 | 江苏神涛环保科技有限公司 | Chemical fiber oil sterilization preservative and compounding method thereof |
| CN107047603A (en) * | 2016-08-01 | 2017-08-18 | 中国石油天然气股份有限公司 | Bactericide and preparation method and application thereof |
| CN107047603B (en) * | 2016-08-01 | 2019-09-06 | 中国石油天然气股份有限公司 | Bactericide and preparation method and application thereof |
| CN108041076A (en) * | 2017-12-29 | 2018-05-18 | 常州达奥新材料科技有限公司 | A kind of preparation method of sterilization antiseptic |
| CN108184891A (en) * | 2018-02-28 | 2018-06-22 | 陕西理工大学 | A kind of sterilization agent emulsion and preparation method thereof |
| CN112450217A (en) * | 2020-12-18 | 2021-03-09 | 湖南幻影三陆零科技有限公司 | Disinfectant and disinfectant composition containing same |
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Application publication date: 20111228 |