CN102199500A - Formula of Chinese soapberry fruit handmade soap and method for preparing Chinese soapberry fruit handmade soap - Google Patents
Formula of Chinese soapberry fruit handmade soap and method for preparing Chinese soapberry fruit handmade soap Download PDFInfo
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- CN102199500A CN102199500A CN2011101019232A CN201110101923A CN102199500A CN 102199500 A CN102199500 A CN 102199500A CN 2011101019232 A CN2011101019232 A CN 2011101019232A CN 201110101923 A CN201110101923 A CN 201110101923A CN 102199500 A CN102199500 A CN 102199500A
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- 239000000344 soap Substances 0.000 title claims abstract description 46
- 241000580955 Sapindus mukorossi Species 0.000 title claims abstract description 42
- 238000000034 method Methods 0.000 title claims abstract description 12
- 235000013399 edible fruits Nutrition 0.000 title abstract description 8
- -1 acyloxy isethionates Chemical class 0.000 claims abstract description 17
- 235000021355 Stearic acid Nutrition 0.000 claims abstract description 9
- POULHZVOKOAJMA-UHFFFAOYSA-N dodecanoic acid Chemical compound CCCCCCCCCCCC(O)=O POULHZVOKOAJMA-UHFFFAOYSA-N 0.000 claims abstract description 9
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 claims abstract description 9
- 238000003809 water extraction Methods 0.000 claims abstract description 9
- OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 claims abstract description 8
- 238000003756 stirring Methods 0.000 claims abstract description 7
- 239000002253 acid Substances 0.000 claims description 9
- OUCUOMVLTQBZCY-BYPYZUCNSA-N (2s)-1-azaniumylpyrrolidine-2-carboxylate Chemical compound NN1CCC[C@H]1C(O)=O OUCUOMVLTQBZCY-BYPYZUCNSA-N 0.000 claims description 8
- 241000628997 Flos Species 0.000 claims description 8
- 235000009508 confectionery Nutrition 0.000 claims description 8
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 claims description 8
- 229940033355 lauric acid Drugs 0.000 claims description 7
- 239000008117 stearic acid Substances 0.000 claims description 7
- 239000000203 mixture Substances 0.000 claims description 6
- 239000000284 extract Substances 0.000 claims description 5
- 238000004519 manufacturing process Methods 0.000 claims description 4
- 238000009963 fulling Methods 0.000 claims description 3
- 238000002360 preparation method Methods 0.000 claims description 3
- 230000008569 process Effects 0.000 claims description 3
- 239000008234 soft water Substances 0.000 claims description 3
- 238000005303 weighing Methods 0.000 claims description 3
- 230000000694 effects Effects 0.000 abstract description 6
- 239000001397 quillaja saponaria molina bark Substances 0.000 abstract description 4
- 229930182490 saponin Natural products 0.000 abstract description 4
- 150000007949 saponins Chemical class 0.000 abstract description 4
- 238000004140 cleaning Methods 0.000 abstract description 3
- 239000000126 substance Substances 0.000 abstract description 3
- 241000607142 Salmonella Species 0.000 abstract description 2
- 241000191967 Staphylococcus aureus Species 0.000 abstract description 2
- 230000032683 aging Effects 0.000 abstract description 2
- 230000006378 damage Effects 0.000 abstract description 2
- 239000006260 foam Substances 0.000 abstract description 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 abstract 2
- 229910052708 sodium Inorganic materials 0.000 abstract 2
- 239000011734 sodium Substances 0.000 abstract 2
- TUNFSRHWOTWDNC-UHFFFAOYSA-N tetradecanoic acid Chemical compound CCCCCCCCCCCCCC(O)=O TUNFSRHWOTWDNC-UHFFFAOYSA-N 0.000 abstract 2
- 241000588724 Escherichia coli Species 0.000 abstract 1
- ONIBWKKTOPOVIA-UHFFFAOYSA-N Proline Natural products OC(=O)C1CCCN1 ONIBWKKTOPOVIA-UHFFFAOYSA-N 0.000 abstract 1
- 241000220317 Rosa Species 0.000 abstract 1
- 108010077895 Sarcosine Proteins 0.000 abstract 1
- MRUAUOIMASANKQ-UHFFFAOYSA-N cocamidopropyl betaine Chemical compound CCCCCCCCCCCC(=O)NCCC[N+](C)(C)CC([O-])=O MRUAUOIMASANKQ-UHFFFAOYSA-N 0.000 abstract 1
- 229940073507 cocamidopropyl betaine Drugs 0.000 abstract 1
- 230000002401 inhibitory effect Effects 0.000 abstract 1
- 230000007794 irritation Effects 0.000 abstract 1
- FSYKKLYZXJSNPZ-UHFFFAOYSA-N sarcosine Chemical compound C[NH2+]CC([O-])=O FSYKKLYZXJSNPZ-UHFFFAOYSA-N 0.000 abstract 1
- 239000000341 volatile oil Substances 0.000 abstract 1
- 229930183111 sapindoside Natural products 0.000 description 7
- 239000003921 oil Substances 0.000 description 5
- 235000019198 oils Nutrition 0.000 description 5
- 238000011161 development Methods 0.000 description 4
- 230000018109 developmental process Effects 0.000 description 4
- 238000004659 sterilization and disinfection Methods 0.000 description 3
- DKVBOUDTNWVDEP-NJCHZNEYSA-N teicoplanin aglycone Chemical compound N([C@H](C(N[C@@H](C1=CC(O)=CC(O)=C1C=1C(O)=CC=C2C=1)C(O)=O)=O)[C@H](O)C1=CC=C(C(=C1)Cl)OC=1C=C3C=C(C=1O)OC1=CC=C(C=C1Cl)C[C@H](C(=O)N1)NC([C@H](N)C=4C=C(O5)C(O)=CC=4)=O)C(=O)[C@@H]2NC(=O)[C@@H]3NC(=O)[C@@H]1C1=CC5=CC(O)=C1 DKVBOUDTNWVDEP-NJCHZNEYSA-N 0.000 description 3
- 238000005406 washing Methods 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- 208000002474 Tinea Diseases 0.000 description 2
- 241000893966 Trichophyton verrucosum Species 0.000 description 2
- 230000009471 action Effects 0.000 description 2
- 239000000470 constituent Substances 0.000 description 2
- 239000000839 emulsion Substances 0.000 description 2
- 238000000605 extraction Methods 0.000 description 2
- 239000003205 fragrance Substances 0.000 description 2
- 230000001954 sterilising effect Effects 0.000 description 2
- 241000233866 Fungi Species 0.000 description 1
- 235000009814 Luffa aegyptiaca Nutrition 0.000 description 1
- 244000302544 Luffa aegyptiaca Species 0.000 description 1
- 239000004909 Moisturizer Substances 0.000 description 1
- 235000009001 Quillaja saponaria Nutrition 0.000 description 1
- 241000694414 Sapindus saponaria Species 0.000 description 1
- 102000003425 Tyrosinase Human genes 0.000 description 1
- 108060008724 Tyrosinase Proteins 0.000 description 1
- 208000027418 Wounds and injury Diseases 0.000 description 1
- 206010048222 Xerosis Diseases 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 239000013543 active substance Substances 0.000 description 1
- 230000001139 anti-pruritic effect Effects 0.000 description 1
- 239000003908 antipruritic agent Substances 0.000 description 1
- 230000000975 bioactive effect Effects 0.000 description 1
- 238000005282 brightening Methods 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 238000005187 foaming Methods 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 239000003112 inhibitor Substances 0.000 description 1
- 208000014674 injury Diseases 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 235000013336 milk Nutrition 0.000 description 1
- 239000008267 milk Substances 0.000 description 1
- 210000004080 milk Anatomy 0.000 description 1
- 230000001333 moisturizer Effects 0.000 description 1
- 230000003020 moisturizing effect Effects 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 238000012827 research and development Methods 0.000 description 1
- 230000000452 restraining effect Effects 0.000 description 1
- 238000007127 saponification reaction Methods 0.000 description 1
- 239000002453 shampoo Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 230000003068 static effect Effects 0.000 description 1
- 230000000638 stimulation Effects 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
- 230000008719 thickening Effects 0.000 description 1
- 235000015112 vegetable and seed oil Nutrition 0.000 description 1
- 239000008158 vegetable oil Substances 0.000 description 1
- 239000000080 wetting agent Substances 0.000 description 1
Landscapes
- Detergent Compositions (AREA)
Abstract
The invention discloses a formula of a Chinese soapberry fruit handmade soap and a method for preparing the Chinese soapberry fruit handmade soap. The method comprises the following steps of: mixing sodium fatty acyloxy isethionates, soap grains, cocamidopropyl betaine, sodium fatty acyloxy isethionates and Chinese soapberry fruit water extraction concentrated solution, stirring, dissolving, adding octadecanoic acid, tetradecanoic acid and dodecanoic acid, dissolving, adding methyl glycine proline and rose essential oil, stirring uniformly, completely dissolving, and solidifying. The Chinese soapberry fruit handmade soap has the advantages that: the Chinese soapberry fruit water extraction solution is a main source of saponin in the ecological soap, and has a cleaning effect; the soap has the effects of killing and inhibiting staphylococcus aureus, salmonella and Escherichia coli; and the soap is nonirritant to skin, has exquisite foam, effectively relieves the irritation and harm of chemical substances to the skin, and reduces the aging degree of the skin.
Description
Technical field
The present invention relates to the prescription and the making method of the manual soap of a kind of Seed of Chinese Soapberry.
Background technology
Seed of Chinese Soapberry has another name called the soap tree, and main product is in Southeast Asian countries, and all there is cultivation in the Yangtze valley of China, southern each province and Hainan Island.Sapindoside is present in the arillus of natural phant Seed of Chinese Soapberry, and content has 4% approximately.Sapindoside can reduce the surface tension of water, has good whipability, strong detergency, and sterilization, antipruritic, fragrance characteristics such as pure are arranged.In brightening emulsion, can be used as the active effective constituent of restraint of tyrosinase, also can be used in natural shampoo and the various cleaning and protecting skin makeup (as cleansing milk, brighten emulsion) effective constituent as natural active matter.In addition, sapindoside and aglycon thereof also have germ resistance, and skin is had disinfection, especially fungi such as acrothesium floccosum (Epidemophyton flocco-sum) etc. are had special efficacy, and external application can be treated the ringworm of the foot and ringworm.
Because of various reasons, the above-mentioned effect of sapindoside and aglycon thereof all also is in the qualitative examination stage, and relevant elaboration sapindoside extraction process and development and use have a small amount of bibliographical information [1] [2] [3] [4].Meanwhile, annual but have a large amount of Seed of Chinese Soapberry fruits by the roadside that the people abandons, and lets alone to run its course, and causes the great wasting of resources.21 century is Biological Century by expert's prophesy, and the development of bio-science and application thereof more and more are subject to people's attention, and believe the research and development with special bioactive sapindoside and aglycon thereof, also will get more and more people's extensive concerning.
At present, China only rests on the extraction aspect of sapindoside in the application of Seed of Chinese Soapberry pulp, perhaps have only in the development of small part washing composition, does not find the research that saponin(e is used in soap in the Seed of Chinese Soapberry pulp.Along with China's constant development of economy, people's income improves constantly, and security, the health of food and daily necessities are more and more paid attention to.So chemical cleaner will be gradually away from our life, the ecological soap of Seed of Chinese Soapberry also will be subjected to liking of people.
Summary of the invention
The object of the present invention is to provide the prescription and the making method of the manual soap of a kind of Seed of Chinese Soapberry, this soap green, environmental protection.
Technical scheme of the present invention is: the prescription and the making method of the manual soap of a kind of Seed of Chinese Soapberry, the composition by weight of this soap: 35-40 part Seed of Chinese Soapberry water extraction concentrated solution, 18-20 part fat acyloxy ethylsulfonic acid sodium, 4-5 part neat soap, 3-4 part AMONYL 380LC, 1-2 part fat acyloxy ethylsulfonic acid sodium, 1-2 part stearic acid, 2-3 part TETRADECONIC ACID, 2-3 part laurostearic acid, the sweet amino proline of 1-2 part methyl, 0.3-0.5 part Flos Rosae Rugosae quintessence oil.
The manufacture craft of this soap: (1) Seed of Chinese Soapberry tucking: Seed of Chinese Soapberry is adopted the back select not to be had the Seed of Chinese Soapberry that goes mouldy and go seed to stay pericarp, and----drying----takes by weighing the soft water that dried pericarp 5kg thousand adds 10kg and----extracts 3 hours----in the temperature about 90 ℃ and filter screen 60-100 order, repeat a process again and----the Seed of Chinese Soapberry extracting solution merging----that obtains for twice is concentrated into 10kg in Vacuumdrier.(2) preparation of soap: fat acyloxy ethylsulfonic acid sodium 18-20 part, neat soap 4-5 part, AMONYL 380LC 3-4 part, fat acyloxy ethylsulfonic acid sodium 1-2 part is mixed, and----adding Seed of Chinese Soapberry water extraction concentrated solution 35-40 part fully stirs and----dissolves----under 60 ℃ the situation and add stearic acid 1-2 part again, TETRADECONIC ACID 2-3 part, the sweet amino proline 1-2 of methyl part is added in laurostearic acid 2-3 part dissolving----, Flos Rosae Rugosae quintessence oil 0.1-0.2 part----was stirred after 20-35 minute, the spy stirs, after the dissolving fully, pour in the mould of 100-120 gram volume of soap and solidified 2-3 hour--------packing----finished product of finishing curing after 24 hours immediately into.
The invention has the advantages that: the Seed of Chinese Soapberry water extract: the main source of the saponin(e in the ecological soap, play cleaning action.Streptococcus aureus, Salmonellas and colibacillus are had extremely and restraining effect., foaming exquisiteness very gentle to skin effectively alleviate the stimulation injury of chemical substance to skin, reduce the degree of aging of skin.
Fat acyloxy ethylsulfonic acid sodium: be a kind of neutral surface active agent, detersive power is moderate, and is non-stimulated to the skin gentleness.
CAB-35: be a kind of good softening amendment, also can be used as washing composition, wetting agent, thickening material, static inhibitor and sterilant etc.
Neat soap: be the washing solid matter of a vegetable oil after saponification.
Stearic acid, TETRADECONIC ACID and laurostearic acid: be a kind of slightly acidic tensio-active agent, play the effect of regulating soap pH in addition.
Natural moisturizing factor: be the sweet amino proline of methyl that from sea-tangle, extracts.Moisture factor is that a kind of absorption is fast, and active high new moisturizer is in personal care product's application, can improve the moisture holding capacity of skin and hair rapidly, the vigor of activated cell, have keep skin moisten, smooth, prevent the effect of xerosis cutis and obfuscation.Major function has: preserve moisture, gentle skin, crease-resistant, brighten, clearly.
Flos Rosae Rugosae quintessence oil: the reodorant of soap also has effects such as replenishing water and preserving moisture, sterilization, tender skin.
The raw material of the manual soap of Seed of Chinese Soapberry makes full use of natural saponin(e in the Seed of Chinese Soapberry mainly from nature, and is gentle non-stimulated, particularly outstanding to the maintenance action of skin, and both can be used as and washed one's face, makeup removing, can be used as again takes a shower uses.The foam of this soap is fine and smooth abundant, can thoroughly remove the greasy dirt of pore depths.Make skin moisten gloss, high resilience.
The moulding of the manual soap of Seed of Chinese Soapberry is colourful especially, lovely heart type, flower type are arranged, true to nature animal-shaped and human-like or the like, can also do the clearly demarcated natural sponge gourd grain of wire vent network is embedded in the transparent soap, collection culture, art, quality and fashion are dissolved in the glamour of the uniqueness of one, in our life, spread silently, with the color of the romantic charm as the crystal, fresh flower and fragrance, unlimited intention collection with all over the body, glittering and translucent, bright and colourful, graceful free from vulgarity.
Summary of the invention
Key in technical field herein and describe paragraph.
Embodiment
Example 1:
The prescription and the making method of the manual soap of a kind of Seed of Chinese Soapberry, the composition by weight of this soap: 35kg Seed of Chinese Soapberry water extraction concentrated solution, 18kg fat acyloxy ethylsulfonic acid sodium, 4kg neat soap, 3kg AMONYL 380LC, 1 gram fat acyloxy ethylsulfonic acid sodium, 1kg stearic acid, 2kg TETRADECONIC ACID, 2kg laurostearic acid, the sweet amino proline of 1kg methyl, 0. kg restrain Flos Rosae Rugosae quintessence oil.The manufacture craft of this soap: (1) Seed of Chinese Soapberry tucking: Seed of Chinese Soapberry is adopted the back select not to be had the Seed of Chinese Soapberry that goes mouldy and go seed to stay pericarp, and----drying----takes by weighing the soft water that dried pericarp 5kg adds 10kg and----extracts 3 hours----in the temperature about 90 ℃ and filter screen 60-100 order, repeat a process again and----the Seed of Chinese Soapberry extracting solution merging----that obtains for twice is concentrated into 10kg in Vacuumdrier.(2) preparation of soap: 18kg fat acyloxy ethylsulfonic acid sodium, the 4kg neat soap, 3 kg AMONYL 380LC, 1 kg fat acyloxy ethylsulfonic acid sodium mixes, and----adding Seed of Chinese Soapberry water extraction concentrated solution 35kg fully stirs and----dissolves----under 60 ℃ the situation and add the 1kg stearic acid again, the 2kg TETRADECONIC ACID, the sweet amino proline of 1kg methyl is added in 2kg laurostearic acid dissolving----, 0.3kg Flos Rosae Rugosae quintessence oil----stirred after 20-35 minute, the spy stirs, after the dissolving fully, pour in the mould of 100 grams-120 gram volumes of soap and solidified 2-3 hour--------packing----finished product of finishing curing after 24 hours immediately into.
Example 2:
Choose the composition by weight of soap: 40 kg Seed of Chinese Soapberry water extraction concentrated solution, 20 kg fat acyloxy ethylsulfonic acid sodium, 5 kg neat soaps, 4 kg AMONYL 380LC, 2 kg fat acyloxy ethylsulfonic acid sodium, 2 kg stearic acids, 3 kg TETRADECONIC ACID, 3 kg laurostearic acids, the sweet amino proline of 2 kg methyl, 0.1 kg Flos Rosae Rugosae quintessence oil.Manufacture craft is with example one.[0002] keys in technical field herein and describe paragraph.
Claims (1)
1. the prescription and the making method of the manual soap of a Seed of Chinese Soapberry is characterized in that: the composition by weight of this soap:
Seed of Chinese Soapberry water extraction concentrated solution 35-40 part, fat acyloxy ethylsulfonic acid sodium 18-20 part, neat soap 4-5 part, AMONYL 380LC 3-4 part, fat acyloxy ethylsulfonic acid sodium 1-2 part, stearic acid 1-2 part, TETRADECONIC ACID 2-3 part, laurostearic acid 2-3 part, the sweet amino proline 1-2 of methyl part, Flos Rosae Rugosae quintessence oil 0.1-0.2 part;
The manufacture craft of this soap:
(1) Seed of Chinese Soapberry tucking: Seed of Chinese Soapberry is adopted the back select not to be had the Seed of Chinese Soapberry that goes mouldy and go seed to stay pericarp, and----drying----takes by weighing the soft water that dried pericarp 5kg adds 10kg and----extracts 3 hours----in the temperature about 90 ℃ and filter screen 60-100 order, repeat a process again and----the Seed of Chinese Soapberry extracting solution merging----that obtains for twice is concentrated into 10kg in Vacuumdrier;
(2) preparation of soap: fat acyloxy ethylsulfonic acid sodium 18-20 part, neat soap 4-5 part, AMONYL 380LC 3-4 part, fat acyloxy ethylsulfonic acid sodium 1-2 part is mixed----and is added Seed of Chinese Soapberry water extraction concentrated solution 35-40 part, fully stir and----dissolve----under 60 ℃ the situation and add stearic acid 1-2 part again, TETRADECONIC ACID 2-3 part, laurostearic acid 2-3 part, dissolving----are added the sweet amino proline 1-2 of methyl part, Flos Rosae Rugosae quintessence oil 0.1-0.2 part----was stirred 25-35 minute and----is poured in the mould of 100-120 gram volume of soap and solidified--------packing----finished product of completely solidified after 24 hours 2-3 hours.
Priority Applications (2)
Application Number | Priority Date | Filing Date | Title |
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CN2011101019232A CN102199500A (en) | 2011-04-22 | 2011-04-22 | Formula of Chinese soapberry fruit handmade soap and method for preparing Chinese soapberry fruit handmade soap |
CN2012100129579A CN102533479A (en) | 2011-04-22 | 2012-01-17 | Formulation and manufacturing method of Sapindus handmade soap |
Applications Claiming Priority (1)
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CN2011101019232A CN102199500A (en) | 2011-04-22 | 2011-04-22 | Formula of Chinese soapberry fruit handmade soap and method for preparing Chinese soapberry fruit handmade soap |
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CN102199500A true CN102199500A (en) | 2011-09-28 |
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CN2011101019232A Pending CN102199500A (en) | 2011-04-22 | 2011-04-22 | Formula of Chinese soapberry fruit handmade soap and method for preparing Chinese soapberry fruit handmade soap |
CN2012100129579A Pending CN102533479A (en) | 2011-04-22 | 2012-01-17 | Formulation and manufacturing method of Sapindus handmade soap |
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CN2012100129579A Pending CN102533479A (en) | 2011-04-22 | 2012-01-17 | Formulation and manufacturing method of Sapindus handmade soap |
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CN103122287A (en) * | 2013-03-26 | 2013-05-29 | 西南大学 | Soapberry total-nutrient handmade soap and preparation method thereof |
CN104788526A (en) * | 2015-03-23 | 2015-07-22 | 福建省轻工业研究所 | Soapberry saponin solution containing clear and stable compounds and preparation method thereof |
CN105199882A (en) * | 2015-09-29 | 2015-12-30 | 广西防城港市明良长富石化科技有限公司 | Natural handmade soap |
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WO2006007741A1 (en) * | 2004-07-16 | 2006-01-26 | Thoeny Rolf | Liquid detergent based on saponin |
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2011
- 2011-04-22 CN CN2011101019232A patent/CN102199500A/en active Pending
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2012
- 2012-01-17 CN CN2012100129579A patent/CN102533479A/en active Pending
Cited By (17)
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CN103122287A (en) * | 2013-03-26 | 2013-05-29 | 西南大学 | Soapberry total-nutrient handmade soap and preparation method thereof |
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