CN101993502B - Method for extracting inulin syrup from yacon - Google Patents
Method for extracting inulin syrup from yacon Download PDFInfo
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- CN101993502B CN101993502B CN201010587300A CN201010587300A CN101993502B CN 101993502 B CN101993502 B CN 101993502B CN 201010587300 A CN201010587300 A CN 201010587300A CN 201010587300 A CN201010587300 A CN 201010587300A CN 101993502 B CN101993502 B CN 101993502B
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- yacon
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- 238000000034 method Methods 0.000 title claims abstract description 17
- 244000134540 Polymnia sonchifolia Species 0.000 title abstract description 13
- 235000003406 Polymnia sonchifolia Nutrition 0.000 title abstract description 13
- 229920001202 Inulin Polymers 0.000 title abstract 4
- JYJIGFIDKWBXDU-MNNPPOADSA-N inulin Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)OC[C@]1(OC[C@]2(OC[C@]3(OC[C@]4(OC[C@]5(OC[C@]6(OC[C@]7(OC[C@]8(OC[C@]9(OC[C@]%10(OC[C@]%11(OC[C@]%12(OC[C@]%13(OC[C@]%14(OC[C@]%15(OC[C@]%16(OC[C@]%17(OC[C@]%18(OC[C@]%19(OC[C@]%20(OC[C@]%21(OC[C@]%22(OC[C@]%23(OC[C@]%24(OC[C@]%25(OC[C@]%26(OC[C@]%27(OC[C@]%28(OC[C@]%29(OC[C@]%30(OC[C@]%31(OC[C@]%32(OC[C@]%33(OC[C@]%34(OC[C@]%35(OC[C@]%36(O[C@@H]%37[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O%37)O)[C@H]([C@H](O)[C@@H](CO)O%36)O)[C@H]([C@H](O)[C@@H](CO)O%35)O)[C@H]([C@H](O)[C@@H](CO)O%34)O)[C@H]([C@H](O)[C@@H](CO)O%33)O)[C@H]([C@H](O)[C@@H](CO)O%32)O)[C@H]([C@H](O)[C@@H](CO)O%31)O)[C@H]([C@H](O)[C@@H](CO)O%30)O)[C@H]([C@H](O)[C@@H](CO)O%29)O)[C@H]([C@H](O)[C@@H](CO)O%28)O)[C@H]([C@H](O)[C@@H](CO)O%27)O)[C@H]([C@H](O)[C@@H](CO)O%26)O)[C@H]([C@H](O)[C@@H](CO)O%25)O)[C@H]([C@H](O)[C@@H](CO)O%24)O)[C@H]([C@H](O)[C@@H](CO)O%23)O)[C@H]([C@H](O)[C@@H](CO)O%22)O)[C@H]([C@H](O)[C@@H](CO)O%21)O)[C@H]([C@H](O)[C@@H](CO)O%20)O)[C@H]([C@H](O)[C@@H](CO)O%19)O)[C@H]([C@H](O)[C@@H](CO)O%18)O)[C@H]([C@H](O)[C@@H](CO)O%17)O)[C@H]([C@H](O)[C@@H](CO)O%16)O)[C@H]([C@H](O)[C@@H](CO)O%15)O)[C@H]([C@H](O)[C@@H](CO)O%14)O)[C@H]([C@H](O)[C@@H](CO)O%13)O)[C@H]([C@H](O)[C@@H](CO)O%12)O)[C@H]([C@H](O)[C@@H](CO)O%11)O)[C@H]([C@H](O)[C@@H](CO)O%10)O)[C@H]([C@H](O)[C@@H](CO)O9)O)[C@H]([C@H](O)[C@@H](CO)O8)O)[C@H]([C@H](O)[C@@H](CO)O7)O)[C@H]([C@H](O)[C@@H](CO)O6)O)[C@H]([C@H](O)[C@@H](CO)O5)O)[C@H]([C@H](O)[C@@H](CO)O4)O)[C@H]([C@H](O)[C@@H](CO)O3)O)[C@H]([C@H](O)[C@@H](CO)O2)O)[C@@H](O)[C@H](O)[C@@H](CO)O1 JYJIGFIDKWBXDU-MNNPPOADSA-N 0.000 title abstract 4
- 229940029339 inulin Drugs 0.000 title abstract 4
- 239000006188 syrup Substances 0.000 title abstract 4
- 235000020357 syrup Nutrition 0.000 title abstract 4
- 235000011389 fruit/vegetable juice Nutrition 0.000 claims abstract description 22
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 16
- 238000001914 filtration Methods 0.000 claims abstract description 13
- 108010059820 Polygalacturonase Proteins 0.000 claims abstract description 6
- 238000010438 heat treatment Methods 0.000 claims abstract 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 10
- 239000007788 liquid Substances 0.000 claims description 10
- 235000007516 Chrysanthemum Nutrition 0.000 claims description 5
- 108090000790 Enzymes Proteins 0.000 claims description 5
- 102000004190 Enzymes Human genes 0.000 claims description 5
- 238000001816 cooling Methods 0.000 claims description 5
- 239000011259 mixed solution Substances 0.000 claims description 5
- 239000002002 slurry Substances 0.000 claims description 5
- 239000006228 supernatant Substances 0.000 claims description 5
- 244000189548 Chrysanthemum x morifolium Species 0.000 claims 1
- 235000013305 food Nutrition 0.000 abstract description 5
- 235000013376 functional food Nutrition 0.000 abstract description 2
- 108010093305 exopolygalacturonase Proteins 0.000 abstract 1
- 241000723353 Chrysanthemum Species 0.000 description 4
- 241000196324 Embryophyta Species 0.000 description 4
- 150000001413 amino acids Chemical class 0.000 description 3
- 230000001681 protective effect Effects 0.000 description 3
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- 235000005911 diet Nutrition 0.000 description 2
- 230000000378 dietary effect Effects 0.000 description 2
- 229910052500 inorganic mineral Inorganic materials 0.000 description 2
- 239000011707 mineral Substances 0.000 description 2
- 235000010755 mineral Nutrition 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 241000554155 Andes Species 0.000 description 1
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- 235000008495 Chrysanthemum leucanthemum Nutrition 0.000 description 1
- 244000192528 Chrysanthemum parthenium Species 0.000 description 1
- 235000000604 Chrysanthemum parthenium Nutrition 0.000 description 1
- 206010012735 Diarrhoea Diseases 0.000 description 1
- RFSUNEUAIZKAJO-ARQDHWQXSA-N Fructose Chemical compound OC[C@H]1O[C@](O)(CO)[C@@H](O)[C@@H]1O RFSUNEUAIZKAJO-ARQDHWQXSA-N 0.000 description 1
- 208000031226 Hyperlipidaemia Diseases 0.000 description 1
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- 240000005334 Syzygium guineense Species 0.000 description 1
- 235000006651 Syzygium guineense Nutrition 0.000 description 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
- 206010000496 acne Diseases 0.000 description 1
- 235000013361 beverage Nutrition 0.000 description 1
- 239000008280 blood Substances 0.000 description 1
- 210000004369 blood Anatomy 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 230000003750 conditioning effect Effects 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- 230000029087 digestion Effects 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 235000008384 feverfew Nutrition 0.000 description 1
- 239000005417 food ingredient Substances 0.000 description 1
- 235000015203 fruit juice Nutrition 0.000 description 1
- 210000001035 gastrointestinal tract Anatomy 0.000 description 1
- 235000021474 generally recognized As safe (food) Nutrition 0.000 description 1
- 235000021473 generally recognized as safe (food ingredients) Nutrition 0.000 description 1
- 125000002791 glucosyl group Chemical group C1([C@H](O)[C@@H](O)[C@H](O)[C@H](O1)CO)* 0.000 description 1
- 230000003053 immunization Effects 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 210000000936 intestine Anatomy 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 239000011777 magnesium Substances 0.000 description 1
- 229910052749 magnesium Inorganic materials 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000006116 polymerization reaction Methods 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 239000011573 trace mineral Substances 0.000 description 1
- 235000013619 trace mineral Nutrition 0.000 description 1
- 235000013343 vitamin Nutrition 0.000 description 1
- 239000011782 vitamin Substances 0.000 description 1
- 229940088594 vitamin Drugs 0.000 description 1
- 229930003231 vitamin Natural products 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
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- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
The invention relates to a method for extracting inulin syrup from yacon. The method comprises the following steps of: crushing, juicing and filtering the screened, washed and drained yacon tuberous roots to obtain yacon juice; placing the yacon juice into a container and decocting the yacon juice for 5 to 15 minutes; adding pectinase in an amount which is 0.01 to 0.05 percent based on the net weight of the yacon juice obtained by filtering; gradually heating for 1 to 3 hours; and recovering alcohol which the juice comprises until the juice is in a thermal concentrated state so as to obtain the inulin syrup. The method for extracting the inulin syrup from the yacon has the advantages that: the yacon extract can be widely applied to health-care foods and functional foods; the yacon is planted in mountain regions with altitude of about more than 1,000 meters and the normal marketing time is the middle ten days of December, so the yacon is unfavorable for storage. The method of the invention becomes an important way to increase farmer incomes and contributes to an important pillar industry for increasing planting economy.
Description
Technical field
The present invention relates to the syrupy method of a kind of extraction chrysanthemum, relate in particular to a kind of syrupy method of chrysanthemum of from foreign root, extracting.
Background technology
Ocean root (yacon) belongs to feverfew, and the former Andes of originating from South America is a kind of traditional rhizome food of local Indian, and the locals is " yacon " meaning of " refreshing fruit " (Ya Gong) promptly.Foreign root success is introduced a fine variety in Japan Saitama County in 1985, gets into China through number of ways in recent years, at present in Yunnan, ground introducing culture successes such as Fujian, Hainan, Guizhou, Hunan, Hubei, Shandong, Jiangxi, Henan, Hebei.Contain 90% fruit juice in the root of ocean, pulp is tasted mouthfeel but the spitting image of the water pears, and juice is many and glittering and translucent, fragrant and sweet crisp and refreshing.Research proof is rich in Nutriflora P in the foreign root, and its content is 60～70% of dry-matter, is the highest plant of Nutriflora P content in the plant of finding at present, and Nutriflora P has: 1. digestion promoting, recuperating gastrointestinal tract; 2. be the growth-promoting agent of useful flora in the intestines, produce bifidus factor; 3. conditioning blood is removed hyperlipidemia, controls SUV and mellitus effectively; 4. defaecation, control diarrhea; 5. fiery detoxicating, control pimples, dark sore are fallen; 6. raising immunizing power.Also containing simultaneously 20 multiple amino acids, VITAMINs of trace element such as higher potassium, calcium, zinc, iron, magnesium and needed by human etc. in the foreign root, is the brand-new functional ingredient of current protective foods, beverage.Synanthrin is a kind of natural Polylevulosan that can from plant, extract, and does not have artificial compound method so far, and synanthrin is a kind of biological polyoses.Connect generation by D-fructofuranose molecule with β-(2,1) glycosidic link, each synanthrin molecule end connects a glucosyl residue with a-(1,2) glycosidic link, and the polymerization degree is generally 2～60, and mean polymerisation degree is 10 (1).Synanthrin is the functional food ingredient that has just risen in the world, and U.S. FDA in 2003 has confirmed that synanthrin is GRAS (an internationally recognized safe material), actively recommends to be used for foodstuff production.
Summary of the invention
The object of the present invention is to provide a kind of syrupy method of chrysanthemum of from foreign root, extracting; This extract is rich in 20 multiple amino acids and multivitamin, the mineral substance of Nutriflora P and needed by human body; Variation along with dietary structure; The raising of health desire, foreign root extract can be widely used in protective foods and functional foodstuff.
The present invention realizes that like this method steps is: will screen, clean the foreign root piece root that drains through broken, squeeze the juice, cross and filter foreign root juice, put into container decoction 5-15 minute; Add and the percent 0.01-0.05 polygalacturonase that filters the foreign root juice nt wt net weight that obtains,, went out enzyme 4-8 minute after enzymolysis is complete at 45-60 ℃ of following enzymolysis 45-95min; Place after 12 hours after the cooling and extract supernatant liquid filtering, add activated carbon this mixed solution is heated 80-115 ℃ of decolouring, filters, be concentrated into partly thick after the filtration; The normal temperature edible ethanol of use 95% down soaked 40-55 minute; The charging capacity part by weight of ocean root liquid concentrator and alcohol is 1:8, is heated to 55 ℃-78 ℃ then, and progressively be 1-3 hour heat-up time; Reclaim institute's spirituosity to heat and concentrated shape, promptly obtained the synanthrin slurry.
Technique effect of the present invention is: compare with existing most of synanthrin on the market, the present invention selects green feverfew-foreign root, and this extract is rich in 20 multiple amino acids and multivitamin, the mineral substance of Nutriflora P and needed by human body; Variation along with dietary structure; The raising of health desire, foreign root extract can be widely used in protective foods and functional foodstuff, because foreign root is planted in about more than the 1000 meters high mountain areas of height above sea level; Normal Time To Market is mid-December, unfavorable storage.The present invention becomes an important channel of increasing peasant income and plants a mainstay industry of economic growth.
Embodiment
Embodiment 1
The present invention realizes that like this method steps is: will screen, clean the foreign root piece root that drains through broken, squeeze the juice, cross and filter foreign root juice, put into container decoction 5 minutes; Add and 0.01 percent polygalacturonase that filters the foreign root juice nt wt net weight that obtains,, went out enzyme 4-8 minute after enzymolysis is complete at 45 ℃ of following enzymolysis 45min; Place after 12 hours after the cooling and extract supernatant liquid filtering, add activated carbon this mixed solution is heated 80 ℃ of decolourings, filters, be concentrated into partly thick after the filtration; The normal temperature edible ethanol of use 95% down soaked 40 minutes; The charging capacity part by weight of ocean root liquid concentrator and alcohol is 1:8, is heated to 55 ℃ then, and progressively be 1 hour heat-up time; Reclaim institute's spirituosity to heat and concentrated shape, promptly obtained the synanthrin slurry.
Embodiment 2
The present invention realizes that like this method steps is: will screen, clean the foreign root piece root that drains through broken, squeeze the juice, cross and filter foreign root juice, put into container decoction 15 minutes; Add and 0.05 percent polygalacturonase that filters the foreign root juice nt wt net weight that obtains, at 60 ℃ of following enzymolysis 95min, go out after fully enzyme 8 minutes of enzymolysis; Place after 12 hours after the cooling and extract supernatant liquid filtering, add activated carbon this mixed solution is heated 115 ℃ of decolourings, filters, be concentrated into partly thick after the filtration; The normal temperature edible ethanol of use 95% down soaked 55 minutes; The charging capacity part by weight of ocean root liquid concentrator and alcohol is 1:8, is heated to 78 ℃ then, and progressively be 3 hours heat-up time; Reclaim institute's spirituosity to heat and concentrated shape, promptly obtained the synanthrin slurry.
Embodiment 3
The present invention realizes that like this method steps is: will screen, clean the foreign root piece root that drains through broken, squeeze the juice, cross and filter foreign root juice, put into container decoction 10 minutes; Add and 0.03 percent polygalacturonase that filters the foreign root juice nt wt net weight that obtains, at 50 ℃ of following enzymolysis 70min, go out after fully enzyme 6 minutes of enzymolysis; Place after 12 hours after the cooling and extract supernatant liquid filtering, add activated carbon this mixed solution is heated 100 ℃ of decolourings, filters, be concentrated into partly thick after the filtration; The normal temperature edible ethanol of use 95% down soaked 50 minutes; The charging capacity part by weight of ocean root liquid concentrator and alcohol is 1:8, is heated to 60 ℃ then, and progressively be 2 hours heat-up time; Reclaim institute's spirituosity to heat and concentrated shape, promptly obtained the synanthrin slurry.
Claims (1)
1. one kind is extracted the syrupy method of chrysanthemum from foreign root, it is characterized in that method steps is: will screen, clean the foreign root piece root that drains through broken, squeeze the juice, mistake filters foreign root juice, puts into container decoction 5-15 minute; Add and the percent 0.01-0.05 polygalacturonase that filters the foreign root juice nt wt net weight that obtains; At 45-60 ℃ of following enzymolysis 45-95min, to go out enzyme 4-8 minute after enzymolysis is complete, the cooling back is placed after 12 hours and is extracted supernatant liquid filtering; Add activated carbon with 80-115 ℃ of decolouring of this mixed solution heating, filtration; Be concentrated into half thickly after the filtration, normal temperature uses 95% edible ethanol to soak down 40-55 minute, and the charging capacity part by weight of foreign root liquid concentrator and alcohol is 1:8; Be heated to 55 ℃-78 ℃ then; Progressively be 1-3 hour heat-up time, reclaimed institute's spirituosity to heat and concentrated shape, promptly obtains the synanthrin slurry.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201010587300A CN101993502B (en) | 2010-12-14 | 2010-12-14 | Method for extracting inulin syrup from yacon |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201010587300A CN101993502B (en) | 2010-12-14 | 2010-12-14 | Method for extracting inulin syrup from yacon |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101993502A CN101993502A (en) | 2011-03-30 |
| CN101993502B true CN101993502B (en) | 2012-09-05 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201010587300A Expired - Fee Related CN101993502B (en) | 2010-12-14 | 2010-12-14 | Method for extracting inulin syrup from yacon |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN101993502B (en) |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1706957A (en) * | 2005-04-08 | 2005-12-14 | 江苏天士力帝益药业有限公司 | Process of extracting synanthrin from girasole |
| CN1831014A (en) * | 2006-01-19 | 2006-09-13 | 昆明瑞鹏生态农业科技有限公司 | Process for preparing inslin and oligofructose using xuelianguo fruits as raw material |
| CN101402984A (en) * | 2008-11-12 | 2009-04-08 | 南京泛成生物化工有限公司 | Method for extracting inulin with assistance of biological enzyme |
| CN101731509A (en) * | 2008-11-20 | 2010-06-16 | 郝琳琳 | Method for extracting inulin from Canada potato |
| RU2396283C1 (en) * | 2009-04-06 | 2010-08-10 | Олег Иванович Квасенков | Method for preparing inulin-containing solution |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0930317A1 (en) * | 1998-01-21 | 1999-07-21 | Tiense Suikerraffinaderij N.V. (Raffinerie Tirlemontoise S.A.) | Process for the manufacture of chicory inulin, hydrolysates and derivatives of inulin, and improved chicory inulin products, hydrolysates and derivatives |
-
2010
- 2010-12-14 CN CN201010587300A patent/CN101993502B/en not_active Expired - Fee Related
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1706957A (en) * | 2005-04-08 | 2005-12-14 | 江苏天士力帝益药业有限公司 | Process of extracting synanthrin from girasole |
| CN1831014A (en) * | 2006-01-19 | 2006-09-13 | 昆明瑞鹏生态农业科技有限公司 | Process for preparing inslin and oligofructose using xuelianguo fruits as raw material |
| CN101402984A (en) * | 2008-11-12 | 2009-04-08 | 南京泛成生物化工有限公司 | Method for extracting inulin with assistance of biological enzyme |
| CN101731509A (en) * | 2008-11-20 | 2010-06-16 | 郝琳琳 | Method for extracting inulin from Canada potato |
| RU2396283C1 (en) * | 2009-04-06 | 2010-08-10 | Олег Иванович Квасенков | Method for preparing inulin-containing solution |
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| Publication number | Publication date |
|---|---|
| CN101993502A (en) | 2011-03-30 |
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Inventor after: Zeng Yonghui Inventor after: Zeng Meishu Inventor after: Wang Houhong Inventor before: Zeng Meishu Inventor before: Wang Houhong |
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Effective date of registration: 20170106 Address after: 343700 Ji'an city of Jiangxi Province Taihe County Industrial Park Patentee after: JIANGXI BEIDELI BIOLOGICAL ENGINEERING CO.,LTD. Address before: Pingshan Town Longgang District of Shenzhen City, Guangdong province 518000 Lixin Road No. 38 Patentee before: Zeng Meishu |
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| CF01 | Termination of patent right due to non-payment of annual fee | ||
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Granted publication date: 20120905 |