CN101954107B - Solid aromatic sleep aid and preparation method thereof - Google Patents

Abstract

The invention discloses a solid aromatic sleep aid and a preparation method thereof. The solid aromatic sleep aid contains 0.75-1.50% sleep aid essence, 0.50-1.50% solid air freshening gel, 8.00-10.00% high-efficiency solubilizer, 0.40-0.60% preservative, and distilled water as the balance. The preparation method comprises four steps of blending the sleep-aid essence, solubilizing the sleep-aid essence, preparing a gel colloid, and combining the sleep-aid essence and the gel. The solid aromatic sleep aid product of the present invention uses sleep aid essential oils such as ylang ylang oil as main raw materials, and is a pure natural, non-toxic, harmless and safe product. And because the solid aromatic sleep aid contains rose oil and other ingredients, it emits a fresh and soft fragrance of flowers and herbs, which can not only purify the air, but also eliminate fatigue. It is especially suitable for people who have long-term poor sleep quality and can continuously release 5 ~10 days of pleasant aroma, no pollution to the environment.

Description

A kind of solid aromatic sleep aid and preparation method thereof

technical field

The invention belongs to the field of chemical technology, and in particular relates to a compounding technology of a solid aromatic sleep-aiding essence and a preparation method of a solid aromatic sleep-aiding agent.

Background technique

Good sleep is the guarantee of people's health. With the development of society, people's awareness of health and self-protection is also increasing, and various products that help people improve sleep quality have emerged one after another.

At present, there are many sleep aid products on the domestic market, which are mainly prepared into medicines (sleeping pills, tranquilizing pills, etc.), health care products, etc. Most of the ingredients in these sleep aid products contain synthetic organic chemical ingredients (such as zolpidem tartrate, alprazolam, etc.), and people can achieve the sleep aid effect by ingesting them in their bodies. But it can have side effects in humans.

The solid aromatic sleep aid of the present invention is compounded from several essential oils, which can achieve better sleep aid effect. Among them, the effective sleep aid ingredients include ylang ylang oil, eucalyptus essential oil, lavender oil, etc. People can better achieve the effect of soothing, relaxing, calming and sleeping through the smell. This product is a pure natural, non-toxic, harmless and safe product. At present, there is no similar product in China.

Contents of the invention

One of the purposes of the present invention is to provide a solid fragrance sleep aid in order to solve the above problems.

The second object of the present invention is to provide a preparation method of a solid aromatic sleep aid.

The third object of the present invention is to provide a sleep aid essence used in the preparation method of a solid aromatic sleep aid.

Technical scheme of the present invention

A solid aromatic sleep aid, the mass percentage of each component contained in it is as follows:

Sleep aid essence 0.75～1.50%

Solid air freshener 0.50～1.50%

Efficient solubilizer 8.00～10.00%

Preservatives 0.40～0.60%

The balance is distilled water;

The high-efficiency solubilizers are mainly non-ionic and zwitterionic surfactants, mainly organic compounds with alcohol and ether structures: polyoxypropylene fatty alcohol ether, polyoxyethylene fatty alcohol ether (12-13 alkanol poly oxyethylene alcohol ether) etc.; preferably 12-13 alkanol polyoxyethylene alcohol ether;

Wherein the solid air freshening glue is polyvinyl alcohol, hydroxypropyl methylcellulose or modified cellulose and other macromolecular materials; preferably modified cellulose;

The preservative is a mixture of DMDMH (dimethyloldimethylhydantoin) and IPBC (butyl 3-iodo-2-propynylcarbamate); it is preferably G.P.L in the Chinese daily chemical industry product;

The sleep aid essence described therein includes ylang ylang oil, eucalyptus essential oil, jasmine essential oil, Roman chamomile essential oil, coriander seed oil, nard pine essential oil, lavender oil, rose flower oil, clove oil, patchouli oil, sage oil , juniper oil, antioxidants and other components;

And the mass percentage of each component described in the sleep aid essence is shown in Table 1:

Table 1 The mass percentage of each component in the sleep aid essence used

serial number Raw material name Mass percentage (%) 1 Ylang Ylang Oil 25.00～35.00 2 Eucalyptus essential oil 8.00～15.00 3 Jasmine essential oil 1.00～5.00 4 Roman Chamomile Essential Oil 0.50～5.00 5 Coriander Seed Oil 1.00～7.00 6 Nardin essential oil 1.00～7.00 7 lavender oil 25.00～35.00 8 rose oil 0.50～5.00 9 clove oil 1.00～5.00 10 patchouli oil 1.00～5.00 11 Sage Oil 3.00～10.00 12 juniper oil 3.00～10.00 13 Antioxidants 1.00～2.00 solvent Dipropylene glycol margin

The antioxidant described therein is BHT (2.6-di-tert-butyl-p-cresol).

The mass percentages of the components described in the sleep aid essence are preferably shown in Table 2:

Table 2 The mass percentage of each component in the sleep aid essence used

serial number Raw material name Mass percentage (%) 1 Ylang Ylang Oil 25.00～32.00 2 Eucalyptus essential oil 8.00～10.00 3 Jasmine essential oil 3.00～4.00 4 Roman Chamomile Essential Oil 1.00 5 Coriander Seed Oil 2.00 6 Nardin essential oil 4.00～5.00 7 lavender oil 32.00～35.00 8 rose oil 1.00 9 clove oil 2.00～3.00 10 patchouli oil 1.00～4.00 11 Sage Oil 4.00～6.00 12 juniper oil 4.00～6.00 13 Antioxidants 1.00 solvent Dipropylene glycol margin

The antioxidant described therein is BHT (2.6-di-tert-butyl-p-cresol).

A preparation method of a solid aromatic sleep aid, comprising the following preparation steps:

(1) Deployment of sleep aid essence

Put each component in the sleep aid essence into the antiseptic container (1) in sequence according to the serial number, and stir until it reaches uniformity after 15 minutes;

(2) Solubilization of sleep aid essence

Solubilize the prepared sleep aid essence in step (1):

First, add a high-efficiency solubilizer accounting for 8.00-10.00% of the total mass of the solid aromatic sleep aid product (hereinafter referred to as: the total product) into the antiseptic container (2), heat it to 55-60°C, and after 15 minutes, until it is clear and transparent ;

Then add the sleep aid essence prepared in step (1) which accounts for 0.75-1.50% of the total product, stir with a stirrer for 5-10 minutes, stir evenly, and let it cool naturally at room temperature, that is, increase Dissolving sleep aid essence;

(3) Preparation of gel colloid

Add distilled water accounting for 86.40-90.50% of the total product to the anti-corrosion container (3). In order to prevent the change of the total weight caused by the evaporation of distilled water during the heating process, add more distilled water accounting for 10.00-15.00% of the total product during the process. Distilled water, heated, while stirring, gradually sprinkled solid air freshening glue accounting for 0.50-1.50% of the total product, and heated and stirred to 85-90°C. After 20-30 minutes, the powder was dissolved, and the heating was stopped. Stir and cool until the temperature is around 60°C to obtain the gel colloid;

(4) Combination of sleep aid essence and gel

Add 0.40% to 0.60% of the preservative to the gel colloid obtained in step (3) and continue to stir, and when it is naturally cooled to 40-50°C, slowly pour step (2) into the gel colloid After the obtained solubilizing and sleep-aiding essence is continuously stirred for several minutes, when the temperature is naturally cooled back to 30-40°C, the stirring is stopped, that is, it is combined into a solid aromatic sleep-aiding agent;

Pour it into an anti-corrosion forming mold, let it cool naturally to normal temperature, and obtain the solid fragrance sleep aid product of the present invention.

The important feature of the invention lies in the blending technology of the sleep-aiding essence in the solid aromatic sleep-aiding agent.

Beneficial effects of the present invention

The present invention uses ylang-ylang oil, eucalyptus essential oil and lavender oil as the main raw materials of sleep aid essence components, and the obtained solid aromatic sleep aid product is a pure natural, non-toxic, harmless and safe product. And because the solid aromatic sleep aid also contains ingredients such as rose oil, Roman chamomile essential oil, and jasmine absolute, the solid aromatic sleep aid of the present invention emits a fresh and soft fragrance of flowers and herbs, which can not only purify the air, but also has the effect of expelling Fatigue, anti-depression, and calming emotions, it brings fresh and fragrant fragrance to the air, and at the same time relieves work pressure, bringing joy, relaxation and stability to the mood.

Compared with other types of products on the market, the solid aromatic sleep aid of the present invention is safe, has no side effects on the human body, is easy to carry, and is not easily affected by temperature, humidity, etc., and is especially suitable for people who have long-term poor sleep quality. Under normal circumstances, it can continuously release a pleasant fragrance for 5-10 days without any harm to people, and the smell is fragrant and natural, and it has no pollution to the environment.

Detailed ways

Below by embodiment, the present invention is further described, but does not limit the present invention.

Now use the Cosmacd NⅡ-9 product produced by Shanghai Dike Fine Chemical Co., Ltd. as a high-efficiency solubilizer in solid aromatic sleep aids;

Now use the product model LA01 produced by Shanghai Weimei Biotechnology Development Co., Ltd. as the solid air freshener in the solid aromatic sleep aid;

The product of model G.P.L produced by Shanghai Dike Fine Chemical Co., Ltd. is now used as a preservative in solid aromatic sleep aids;

The product BHT (2.6-di-tert-butyl-p-cresol) produced by Shanghai Sinopharm is now used as an antioxidant for solid aromatic sleep aids.

Example 1

A solid aromatic sleep aid, the mass percentage of each component contained in it is as follows:

Sleep Aid Fragrance A 0.75%

Solid air freshener 0.50%

Efficient solubilizer 8.00%

Preservatives 0.40%

The balance is distilled water 90.35%

The above-mentioned preparation method of a solid aromatic sleep aid comprises the following preparation steps:

(1) Deployment of sleep aid essence A

The mass percentages of each raw material in the sleep aid essence A example are shown in Table 3:

Table 3 The mass percentage content of each component in the sleep aid fragrance A case

serial number Raw material name Mass percentage (%) A 1 Ylang Ylang Oil 32.00 2 Eucalyptus essential oil 8.00 3 Jasmine essential oil 3.00 4 Roman Chamomile Essential Oil 1.00 5 Coriander Essential Oil 2.00 6 Nardin essential oil 4.00 7 lavender oil 32.00 8 rose oil 1.00 9 clove oil 3.00 10 patchouli oil 1.00 11 Sage Oil 6.00 12 juniper oil 6.00 13 Antioxidants 1.00 solvent Dipropylene glycol 0.00

According to the mass percentage of each component in Table 3, add each component into the anti-corrosion container (1) according to the serial number in Table 3, and stir until it reaches uniformity after 15 minutes;

(2) Solubilization of sleep aid essence A

Solubilize the sleep aid essence A prepared in step (1): First, add a high-efficiency solubilizer accounting for 8.00% of the total product in the antiseptic container (2), heat it to 55°C-60°C, and after 15 minutes, until it is clear and transparent; then add the sleep-promoting fragrance A prepared in step (1) which accounts for 0.75% of the total product, stir with a stirrer for 10 minutes, stir evenly, and let it cool naturally at room temperature to obtain Solubilizing sleep aid essence A;

(3) Preparation of gel colloid

Add distilled water accounting for 90.35% of the total product to the anti-corrosion container (3). In order to prevent the change of the total weight caused by the evaporation of distilled water during the heating process, you can add more distilled water accounting for 15.00% of the total product during the process. Heat, while stirring, gradually sprinkle 0.50% solid air freshening glue in the total product, and heat and stir to 85-90°C. After 30 minutes, after the powder is dissolved, stop heating, stir and cool to a temperature of 60 At about ℃, the gel colloid is obtained;

(4) The combination of sleep aid essence A and gel

Add preservatives accounting for 0.40% of the total product to the gel colloid obtained in step (3) and continue to stir. When it is naturally cooled to 40-50°C, slowly pour the preservative obtained in step (2) into the gel colloid. Dissolve sleep aid essence A, continue to stir, and stop stirring when the temperature naturally cools back to 30-40°C, that is, it will be combined into a solid aromatic sleep aid. Pour it into an anti-corrosion forming mold, let it cool naturally to normal temperature, and obtain the solid fragrance sleep aid product of the present invention.

The solid aromatic sleep aid obtained above has obvious ylang-ylang floral fragrance, but the floral fragrance is heavy, unnatural, too single, not round, thick, opaque, and has a transparent gel-like appearance. After a period of time, the aroma gradually weakens, loses the aroma, and the colloid volatilizes quickly. It can continuously release the aroma for 4-6 days, and the effect of helping sleep is less obvious.

Example 2

A solid aromatic sleep aid, the mass percentage of each component contained in it is as follows:

Sleep Aid Fragrance B 1.50%

Solid air freshener 1.50%

Efficient solubilizer 10.00%

Preservatives 0.60%

The balance is distilled water.

The above-mentioned preparation method of a solid aromatic sleep aid comprises the following preparation steps:

(1) Deployment of sleep aid essence B

See Table 4 for the mass percentages of each raw material in sleep aid essence B example:

The mass percentage content of each component in table 4 used sleep aid fragrance B example

serial number Raw material name Mass percentage (%) B 1 Ylang Ylang Oil 30.00 2 Eucalyptus essential oil 10.00 3 Jasmine essential oil 4.00 4 Roman Chamomile Essential Oil 1.00 5 Coriander Essential Oil 2.00 6 Nardin essential oil 4.00 7 lavender oil 35.00 8 rose oil 1.00 9 clove oil 2.00 10 patchouli oil 2.00 11 Sage Oil 4.00 12 juniper oil 4.00 13 Antioxidants 1.00 solvent Dipropylene glycol 0.00

According to the mass percentage of each component in Table 4, add each component into the anti-corrosion container (1) according to the serial number in Table 4, and stir until it reaches uniformity after 15 minutes;

(2) Solubilization of sleep aid essence B

Solubilize the sleep aid essence B prepared in step (1): First, add a high-efficiency solubilizer accounting for 10.00% of the total product into the antiseptic container (2), heat to 55-60°C, and after 15 minutes, until It is clear and transparent; then add the sleep aid essence B that has been prepared in step (1) which accounts for 1.50% of the total product, stir with a stirrer for 10 minutes, stir evenly, and let it cool naturally at room temperature, that is, increase Dissolve sleep aid essence B;

(3) Preparation of gel colloid

Add distilled water accounting for 86.40% of the total product to the anticorrosion container (3). In order to prevent the change of the total weight caused by the evaporation of distilled water during the heating process, you can add more distilled water accounting for 15.00% of the total product during the process. Heat, while stirring, gradually sprinkle 1.50% solid air freshening glue in the total product, and heat and stir to 85-90°C. After 30 minutes, after the powder is dissolved, stop heating, stir and cool it until the temperature is 60°C or so, the gel colloid is obtained;

(4) Combination of sleep aid essence B and gel

Add preservatives accounting for 0.60% of the total product to the gel colloid obtained in step (3) and continue to stir, and when it is naturally cooled to 40-50°C, slowly pour the preservative obtained in step (2) into the gel colloid. Dissolve sleep aid essence B, continue to stir, and stop stirring when the temperature naturally cools back to 30-40°C, that is, it will be combined into a solid aromatic sleep aid;

Pour it into an anti-corrosion forming mold, let it cool naturally to normal temperature, and obtain the solid fragrance sleep aid product of the present invention.

The solid aromatic sleep aid obtained above has an obvious complex fragrance with faint floral fragrance, slightly cool and delicate fragrance. The aroma is penetrating, harmonious, mellow, round, transparent in appearance, and has a certain gelatinous state. With the passage of time, the aroma can slowly volatilize and still maintain a good aroma. The base fragrance still has a compound floral fragrance with woody aroma, and the appearance of the colloid can gradually become smaller with time, but its gel The state does not change. It can continuously release a pleasant aroma for 7-10 days, and can effectively achieve the effect of helping sleep.

Example 3

A solid aromatic sleep aid, the mass percentage of each component contained in it is as follows:

Sleep Aid Fragrance C 1.13%

Solid air freshener 1.00%

Efficient solubilizer 9.00%

Preservatives 0.50%

The balance is distilled water.

The above-mentioned preparation method of a solid aromatic sleep aid comprises the following preparation steps:

(1) Deployment of sleep aid essence C

The mass percentages of each raw material in the sleep aid essence C example are shown in Table 5:

Table 5 The mass percentage of each component in the sleep aid essence C used

serial number Raw material name Mass percentage (%) C 1 Ylang Ylang Oil 25.00 2 Eucalyptus essential oil 10.00 3 Jasmine essential oil 4.00 4 Roman Chamomile Essential Oil 1.00 5 Coriander Essential Oil 2.00 6 Nardin essential oil 5.00 7 lavender oil 35.00 8 rose oil 1.00 9 clove oil 2.00 10 patchouli oil 4.00 11 Sage Oil 6.00 12 juniper oil 4.00 13 Antioxidants 1.00 solvent Dipropylene glycol 0.00

According to the mass percentage of each component in Table 5, add each component into the anti-corrosion container (1) according to the serial number in Table 5, and stir until it reaches uniformity after 15 minutes;

(2) Solubilization of sleep aid essence C

Solubilize the sleep aid essence C prepared in step (1): First, add a high-efficiency solubilizer accounting for 9.00% of the total product into the antiseptic container (2), heat to 55-60°C, and after 15 minutes, until It is clear and transparent; then add 1.13% of the total product to it, the sleep aid essence C that has been prepared in step (1), stir with a stirrer for 10 minutes, stir evenly, and let it cool naturally at room temperature to obtain solubilization Sleep aid essence C;

(3) Preparation of gel colloid

Add distilled water accounting for 88.37% of the total product to the anti-corrosion container (3). In order to prevent the change of the total weight caused by the evaporation of distilled water during the heating process, you can add more distilled water accounting for 15.00% of the total product during the process. Heat, while stirring, gradually sprinkle 1.00% solid air-cleaning glue in the total product, and heat and stir to 85-90°C. After 30 minutes, after the powder is dissolved, stop heating, stir and cool it to a temperature of 60 At about ℃, the gel colloid is obtained;

(4) Combination of sleep aid essence C and gel

Add preservatives accounting for 0.50% of the total product to the gel colloid obtained in step (3) and continue to stir, and when it is naturally cooled to 40-50°C, slowly pour the preservative obtained in step (2) into the gel colloid. Dissolve sleep aid essence C, continue to stir, and stop stirring when the temperature naturally cools back to 30-40°C, that is, it will be combined into a solid aromatic sleep aid;

Pour it into an anti-corrosion forming mold, let it cool naturally to normal temperature, and obtain the solid fragrance sleep aid product of the present invention.

The solid aromatic sleep aid obtained above has obvious floral aroma, but the aroma is blue and monotonous, with obvious floral and woody aroma of lavender, and the aroma is not round and mellow. Although the appearance is transparent gel, the gel The effect is not good. After a period of time, not only the aroma is weakened, but also the single floral aroma is lost, and the colloid volatilizes quickly. It can continuously release the aroma for 5-7 days, and the effect of helping sleep is less obvious.

The above content is only a basic description of the concept of the present invention, and any equivalent transformation made according to the technical solution of the present invention shall fall within the scope of protection of the present invention.

Claims (12)

1. a solid aromatic sleep aid is characterized in that, by percentage to the quality, its composition is:

Sleeping essence 0.75～1.50%

Solid air freshening glue 0.50～1.50%

Efficient solubilizing agents 8.00～10.00%

Antiseptic 0.40～0.60%

Surplus is distilled water;

Efficient solubilizing agents wherein is polyoxypropylene fatty alcohol ether, polyoxyethylene aliphatic alcohol ether;

Solid air freshening glue wherein is polyvinyl alcohol, hydroxypropyl emthylcellulose or modified cellulose;

Antiseptic wherein is the mixture of dihydroxymethyl dimethyl hydantoin and 3-iodo-2-propynyl butyl carbamate;

Wherein said sleeping essence comprises Cananga odorata oil, eucalyptus quintessence oil, jasmin quintessence oil, Anthemis nobilis quintessence oil, coriander seed oil, Radix Et Rhizoma Nardostachyos quintessence oil, Oleum lavandula angustifolia, rose oil, Oleum Caryophylli, Herba Pogostemonis oil, sage oil, cade oil, antioxidant and dipropylene glycol;

And the mass percent of each component described in the sleeping essence is:

1. Cananga odorata oil: 25.00～35.00%; 2. eucalyptus quintessence oil: 8.00～15.00%; 3. jasmin quintessence oil: 1.00～5.00%; 4. Anthemis nobilis quintessence oil: 0.50～5.00%; 5. coriander seed oil: 1.00～7.00 %; 6. Radix Et Rhizoma Nardostachyos quintessence oil: 1.00～7.00%; 7. Oleum lavandula angustifolia: 25.00～35.00%; 8. rose oil: 0.50～5.00%; 9. Oleum Caryophylli: 1.00～5.00%; 10. Herba Pogostemonis oil: 1.00～5.00%;

Sage oil: 3.00～10.00%;

Cade oil: 3.00～10.00%;

Antioxidant: 1.00～2.00%;

Dipropylene glycol:

Surplus; Wherein said antioxidant is the 2.6-ditertbutylparacresol.

2. a kind of solid aromatic sleep aid as claimed in claim 1 is characterized in that:

Efficient solubilizing agents wherein is polyoxyethylene aliphatic alcohol ether;

Solid air freshening glue wherein is modified cellulose.

3. a kind of solid aromatic sleep aid as claimed in claim 1 or 2 is characterized in that, by percentage to the quality, its composition is: sleeping essence 0.75～1.50%

Solid air freshening glue 0.50～1.50%

Efficient solubilizing agents 8.00～10.00%

Antiseptic 0.40～0.60%

Surplus is distilled water;

Wherein said sleeping essence by percentage to the quality, its composition is:

Cananga odorata oil: 25.00～32.00%; Eucalyptus quintessence oil: 8.00～10.00%; Jasmin quintessence oil: 3.00～4.00%; Anthemis nobilis quintessence oil: 1.00%; Coriander seed oil: 2.00%; Radix Et Rhizoma Nardostachyos quintessence oil: 4.00～5.00%; Oleum lavandula angustifolia: 32.00～35.00%; Rose oil: 1.00%; Oleum Caryophylli: 2.00～3.00%; Herba Pogostemonis oil: 1.00～4.00%; Sage oil: 4.00～6.00%; Cade oil: 4.00～6.00%; Antioxidant: 1.00%; Dipropylene glycol: surplus; Wherein said antioxidant is the 2.6-ditertbutylparacresol.

4. a kind of solid aromatic sleep aid as claimed in claim 1 or 2 is characterized in that, by percentage to the quality, its composition is: sleeping essence 0.75%

Solid air freshening glue 0.50%

Efficient solubilizing agents 8.00%

Antiseptic 0.40%

Surplus is distilled water;

Wherein said sleeping essence by percentage to the quality, its composition is:

Cananga odorata oil: 32.00%; Eucalyptus quintessence oil: 8.00%; Jasmin quintessence oil: 3.00%; Anthemis nobilis quintessence oil: 1.00%; Coriander quintessence oil: 2.00%; Radix Et Rhizoma Nardostachyos quintessence oil: 4.00%; Oleum lavandula angustifolia: 32.00%; Rose oil: 1.00%; Oleum Caryophylli: 3.00%; Herba Pogostemonis oil: 1.00%; Sage oil: 6.00%; Cade oil: 6.00%; Antioxidant: 1.00%; Dipropylene glycol: 0.00%; Wherein said antioxidant is the 2.6-ditertbutylparacresol.

5. a kind of solid aromatic sleep aid as claimed in claim 1 or 2 is characterized in that, by percentage to the quality, its composition is: sleeping essence 1.50%

Solid air freshening glue 1.50%

Efficient solubilizing agents 10.00%

Antiseptic 0.60%

Surplus is distilled water;

Wherein said sleeping essence by percentage to the quality, its composition is:

Cananga odorata oil: 30.00%; Eucalyptus quintessence oil: 10.00%; Jasmin quintessence oil: 4.00%; Anthemis nobilis quintessence oil: 1.00%; Coriander quintessence oil: 2.00%; Radix Et Rhizoma Nardostachyos quintessence oil: 4.00%; Oleum lavandula angustifolia: 35.00%; Rose oil: 1.00%; Oleum Caryophylli: 2.00%; Herba Pogostemonis oil: 2.00%; Sage oil: 4.00%; Cade oil: 4.00%; Antioxidant: 1.00%; Dipropylene glycol: 0.00%; Wherein said antioxidant is the 2.6-ditertbutylparacresol.

6. a kind of solid aromatic sleep aid as claimed in claim 1 or 2 is characterized in that, by percentage to the quality, its composition is: sleeping essence 1.13%

Solid air freshening glue 1.00%

Efficient solubilizing agents 9.00%

Antiseptic 0.50%

Surplus is distilled water;

Wherein said sleeping essence by percentage to the quality, its composition is:

Cananga odorata oil: 25.00%; Eucalyptus quintessence oil: 10.00%; Jasmin quintessence oil: 4.00%; Anthemis nobilis quintessence oil: 1.00%; Coriander quintessence oil: 2.00%; Radix Et Rhizoma Nardostachyos quintessence oil: 5.00%; Oleum lavandula angustifolia: 35.00%; Rose oil: 1.00%; Oleum Caryophylli: 2.00%; Herba Pogostemonis oil: 4.00%; Sage oil: 6.00%; Cade oil: 4.00%; Antioxidant: 1.00%; Dipropylene glycol: 0.00%;

Wherein said antioxidant is the 2.6-ditertbutylparacresol.

7. the preparation method of solid aromatic sleep aid as claimed in claim 1 or 2 is characterized in that, the preparation process of the method is:

(1), the allotment of sleeping essence

Each component in the sleeping essence is added in the anticorrosion container I successively by sequence number, be stirred to 15 minutes and namely reach later on even;

(2), the solubilising of sleeping essence

The sleeping essence that step (1) is deployed carries out solubilising:

Add in the anticorrosion container II at first that to account for solid aromatic sleep aid product gross mass be 8.00～10.00% efficient solubilizing agents, be heated to 55～60 ℃, after 15 minutes, to clear;

Then to account for solid aromatic sleep aid product gross mass be deployed sleeping essence of 0.75～1.50% step (1) to wherein adding, and after stirring 5～10 minutes with agitator, stirs, and at room temperature allows its natural cooling, namely gets solubilising sleeping essence;

(3), the preparation of gel colloid

Add that to account for solid aromatic sleep aid product gross mass be 86.40～90.50% distilled water in the anticorrosion container III, for preventing that distilled water evaporates the variation that causes gross weight in the heating process, can add into accounting for solid aromatic sleep aid product gross mass in this process is 10.00～15.00% distilled water, heat, progressively being sprinkled into while stirring and accounting for solid aromatic sleep aid product gross mass is 0.50～1.50% solid air freshening glue, and heated and stirred to 85～90 ℃, after 20～30 minutes, after making powder dissolution, stopped heating, its stirring is cooled to temperature about 60 ℃, namely gets the gel colloid;

(4), sleeping essence and gel and close

Add that to account for solid aromatic sleep aid product gross mass be to continue to stir after 0.40～0.60% the antiseptic in the gel colloid of step (3) gained, when naturally cooling to 40～50 ℃, slowly pour the solubilising sleeping essence of step (2) gained in the gel colloid into, after continuing stirred for several minute, when treating that the temperature natural cooling is got back to 30～40 ℃, stop to stir, namely and be combined into solid aromatic sleep aid;

It is poured in the anticorrosion mould, allow it naturally cool to room temperature, namely get the solid aromatic sleep aid product.

8. used sleeping essence in a kind of solid aromatic sleep aid as claimed in claim 1 or 2 is characterized in that, by percentage to the quality, its composition is:

Cananga odorata oil: 25.00～35.00%; Eucalyptus quintessence oil: 8.00～15.00%; Jasmin quintessence oil: 1.00～5.00%; Anthemis nobilis quintessence oil: 0.50～5.00%; Coriander quintessence oil: 1.00～7.00%; Radix Et Rhizoma Nardostachyos quintessence oil: 1.00～7.00%; Oleum lavandula angustifolia: 25.00～35.00%; Rose oil: 0.50～5.00%; Oleum Caryophylli: 1.00～5.00%; Herba Pogostemonis oil: 1.00～5.00%; Sage oil: 3.00～10.00%; Cade oil: 3.00～10.00%; Antioxidant: 1.00～2.00%; Dipropylene glycol: surplus;

Wherein said antioxidant is the 2.6-ditertbutylparacresol.

9. sleeping essence as claimed in claim 8 is characterized in that, by percentage to the quality, its composition is:

Cananga odorata oil: 25.00～32.00%; Eucalyptus quintessence oil: 8.00～10.00%; Jasmin quintessence oil: 3.00～4.00%; Anthemis nobilis quintessence oil: 1.00%; Coriander seed oil: 2.00%; Radix Et Rhizoma Nardostachyos quintessence oil: 4.00～5.00%; Oleum lavandula angustifolia: 32.00～35.00%; Rose oil: 1.00%; Oleum Caryophylli: 2.00～3.00%; Herba Pogostemonis oil: 1.00～4.00%; Sage oil: 4.00～6.00%; Cade oil: 4.00～6.00%; Antioxidant: 1.00%; Dipropylene glycol: surplus; Wherein said antioxidant is the 2.6-ditertbutylparacresol.

10. sleeping essence as claimed in claim 8 is characterized in that, by percentage to the quality, its composition is:

Cananga odorata oil: 32.00%; Eucalyptus quintessence oil: 8.00%; Jasmin quintessence oil: 3.00%; Anthemis nobilis quintessence oil: 1.00%; Coriander quintessence oil: 2.00%; Radix Et Rhizoma Nardostachyos quintessence oil: 4.00%; Oleum lavandula angustifolia: 32.00%; Rose oil: 1.00%; Oleum Caryophylli: 3.00%; Herba Pogostemonis oil: 1.00%; Sage oil: 6.00%; Cade oil: 6.00%; Antioxidant: 1.00%; Dipropylene glycol: 0.00%; Wherein said antioxidant is the 2.6-ditertbutylparacresol.

11. sleeping essence as claimed in claim 8 is characterized in that, by percentage to the quality, its composition is:

Cananga odorata oil: 30.00%; Eucalyptus quintessence oil: 10.00%; Jasmin quintessence oil: 4.00%; Anthemis nobilis quintessence oil: 1.00%; Coriander quintessence oil: 2.00%; Radix Et Rhizoma Nardostachyos quintessence oil: 4.00%; Oleum lavandula angustifolia: 35.00%; Rose oil: 1.00%; Oleum Caryophylli: 2.00%; Herba Pogostemonis oil: 2.00%; Sage oil: 4.00%; Cade oil: 4.00%; Antioxidant: 1.00%; Dipropylene glycol: 0.00%; Wherein said antioxidant is the 2.6-ditertbutylparacresol.

12. sleeping essence as claimed in claim 8 is characterized in that, by percentage to the quality, its composition is:

Cananga odorata oil: 25.00%; Eucalyptus quintessence oil: 10.00%; Jasmin quintessence oil: 4.00%; Anthemis nobilis quintessence oil: 1.00%; Coriander quintessence oil: 2.00%; Radix Et Rhizoma Nardostachyos quintessence oil: 5.00%; Oleum lavandula angustifolia: 35.00%; Rose oil: 1.00%; Oleum Caryophylli: 2.00%; Herba Pogostemonis oil: 4.00%; Sage oil: 6.00%; Cade oil: 4.00%; Antioxidant: 1.00%; Dipropylene glycol: 0.00%; Wherein said antioxidant is the 2.6-ditertbutylparacresol.