CN101857977A - Tea fiber capable of releasing anion and preparation method thereof - Google Patents
Tea fiber capable of releasing anion and preparation method thereof Download PDFInfo
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- CN101857977A CN101857977A CN200910131844A CN200910131844A CN101857977A CN 101857977 A CN101857977 A CN 101857977A CN 200910131844 A CN200910131844 A CN 200910131844A CN 200910131844 A CN200910131844 A CN 200910131844A CN 101857977 A CN101857977 A CN 101857977A
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- 238000000034 method Methods 0.000 claims abstract description 16
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- 238000005516 engineering process Methods 0.000 claims abstract description 13
- 239000004594 Masterbatch (MB) Substances 0.000 claims abstract description 12
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- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- MYMOFIZGZYHOMD-UHFFFAOYSA-N Dioxygen Chemical compound O=O MYMOFIZGZYHOMD-UHFFFAOYSA-N 0.000 description 1
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- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 1
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- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
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- PNDPGZBMCMUPRI-UHFFFAOYSA-N iodine Chemical compound II PNDPGZBMCMUPRI-UHFFFAOYSA-N 0.000 description 1
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- WPBNNNQJVZRUHP-UHFFFAOYSA-L manganese(2+);methyl n-[[2-(methoxycarbonylcarbamothioylamino)phenyl]carbamothioyl]carbamate;n-[2-(sulfidocarbothioylamino)ethyl]carbamodithioate Chemical compound [Mn+2].[S-]C(=S)NCCNC([S-])=S.COC(=O)NC(=S)NC1=CC=CC=C1NC(=S)NC(=O)OC WPBNNNQJVZRUHP-UHFFFAOYSA-L 0.000 description 1
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Landscapes
- Chemical Or Physical Treatment Of Fibers (AREA)
Abstract
The preparation of a tea fiber capable of releasing anion comprises: 1. natural tea protofiber: tea protofiber is a natural tea fiber prepared from natural tea tree by combining physical and chemical methods; 2. chemical dissolution method tea pulp fiber: the tea pulp fiber is prepared into tea pulp dregs by multi-section bleaching and refining with the hydrolysis-alkaline method, cellulose content is improved by catalytic treatment, and tea fiber is processed and prepared by a chemical fibre factory on the basis of satisfying fiber production requirements; 3. tea carbon fiber: 1) micro nanoscale tea carbon powder is chosen, is added into spinning solution by a special technology and is weaved into fiber products by a similar common wet method, a wet method or a dry-wet method spinning technology; and 2) tea carbon is subjected to surface treatment to prepare master batch and is molten and spun; and 4. tea fiber tissue is tidied and coated. The tea fiber is natural and environmentally-friendly and is suitable for producing close fitting and protective fabrics; the function of tea fiber is permanent and is not affected by washing times; and the tea fiber can be widely applied to fields of textile, clothes, health promotion and health care.
Description
Technical field:
The invention belongs to fields such as material, chemical, weaving, clothes, dyeing and finishing, health, environmental protection, what relate to is a kind of tencel with specific function and preparation method thereof.
Background technology:
Tea tree belongs to the Theaceae Camellia, is the perennial evergreen xylophyta.China is the country of planting tea, tea making in the world the earliest, drinking tea, the history in existing several thousand of the cultivation of tea tree.Lu Yu is shown in the Tang Dynasty " tea warp " is the science monograph of the first in the world portion about tea, and he is called No. 1 in the world tealeaves expert by people.Contain the organic chemistry composition in the tea tree and reach kind more than 450, inorganic mineral element reaches kind more than 40.Organic chemistry composition and inorganic mineral element in the tea tree contain many nutritional labelings and effective component.The organic chemistry composition mainly contains: Tea Polyphenols class, vegetable soda, protein, amino acid, vitamin, pectin element, organic acid, lipopolysaccharides, carbohydrate, enzyme, pigment etc.Inorganic mineral element mainly contains: potassium, calcium, magnesium, cobalt, iron, manganese, aluminium, sodium, zinc, copper, nitrogen, phosphorus, fluorine, iodine, selenium etc.Metallic element in the tea tree has pyroelectricity and piezoelectricity, under the situation that temperature and pressure changes (even small variation), can cause the electrical potential difference between the anion crystal, and this static is up to 1 * 10
6V, thus make air generation ionization, and the electron attachment of being hit is in water that closes on and oxygen molecule and make it be converted into air negative oxgyen ion.The height of negative ion concentration is relevant closely with the health of human body, and sealing dwelling house in city is 40～50/cm usually
3, be the main cause of bringing out human physiological disorder such as headache, insomnia, neurasthenia, burnout etc.Street greening district negative ion concentration is the edge that brings out physiological barrier, and tea fiber transmitting anion concentration is 1000～5000/cm
3, be equivalent to imitate outer field, can strengthen body immunity and antimicrbial power.
Tea fiber is divided into four classes: the first kind: the natural tea fibrillation.The tea fibrillation is that the method that adopts physics, chemistry to combine is processed natural tea tree the natural tea fiber that makes.Do not add any chemical reagent in the process, the whole process of producing is a kind of pure natural environment protection fiber truly to human body nonhazardous, non-environmental-pollution.Produce process: tea material → tea making sheet, tea section → steaming sifting tea, tea section → crushing decomposition → biological enzyme degumming → carded fiber → textile fiber.Second class: chemical dissolution method tea pulp fibres: the tea pulp fibres is a raw material with natural high-quality tea tree, employing hydrolysis-alkaline process and multistage bleaching are refining and make the tea pulp, pass through catalytic treatment again, improve content of cellulose, on the basis of satisfying the fiber production requirement, be processed into tea fiber by the chemical fibre factory.The 3rd class: tea charcoal fiber: 1. be to select micro/nano level tea powdered carbon for use, add in the spinning solution, again the fiber product of weaving out through approximate conventional wet method, dry method or dry-wet spinning technology through special process; 2. be the tea charcoal to be carried out surface treatment prepare masterbatch, the melting spinning.The arrangement of the 4th class applies the tea fiber fabric.
Tea fiber has that raw material sources is abundant, environmental protection, negative ion health, the mothproof deodorizing of natural antibacterial, humidity absorption and release and the incomparable natural characteristic of other fiber such as good permeability, uvioresistant, effect such as have antipruritic simultaneously, stimulate circulation, more can help immune system opposing communicable disease, instigate white blood cell and form guard wire, meeting head on the organism of invasion, and can shorten the time of falling ill.Because it has nature and environmental protection characteristic, be applicable to and produce next to the shin and protection type textiles that the fabric made from tea fiber can directly adsorb chemical gas such as bed body smell, tobacco tar flavor and formaldehyde.The function of tea fiber has permanent, not influenced by washing times, makes it be widely used in weaving, clothes, health, healthcare field.The present invention has improved the comprehensive utilization ratio of tea tree greatly, and obtains a kind of health care fiber of novel release anion.
Summary of the invention:
Invention prescription: natural tea tree 0-100 parts by mass; Micro/nano level tea powdered carbon 0-10 parts by mass; Resin 0-90 parts by mass; Auxiliary agent 0-20 parts by mass; Colouring agent 0-6 parts by mass; Adhesive 0-20 parts by mass; Solvent 0-100 parts by mass; Softener 0-5 parts by mass.
Technology: 1, natural tea fibrillation: tea material → tea making sheet, tea section → steaming sifting tea tea section → crushing decomposition → biological enzyme degumming → carded fiber → textile fiber.2, chemical dissolution method tea pulp fibres: the tea pulp fibres is a raw material with natural high-quality tea tree, employing hydrolysis-alkaline process and multistage bleaching are refining and make the tea pulp, pass through catalytic treatment again, improve content of cellulose, on the basis of satisfying the fiber production requirement, be processed into tea fiber by the chemical fibre factory.3, tea charcoal fiber: micro/nano level tea powdered carbon, resin, auxiliary agent, colouring agent and natural minerals nano material are added in the double screw extruder, and blend is extruded, cooling, and pelletizing makes tea charcoal master batch.To add in the double screw extruder with resin slicer after the tea charcoal master batch drying, extrude the spray silk under the temperature that configures, coiling can make the tea fiber that discharges anion.4, arrangement applies the tea fiber fabric: micro/nano level tea carbon powder is distributed in water-soluble, the thermoplastic resin, and the resin after will making up again is applied on the base cloths such as woven fabric, knitted fabric.
The specific embodiment:
Embodiment 1: natural tea tree 100 parts by mass.By following technology: tea material → tea making sheet, tea section → steaming sifting tea, tea section → crushing decomposition → biological enzyme degumming → carded fiber → textile fiber make and discharge 1000/cm of anion
3Above natural tea fibrillation.
Embodiment 2: natural tea tree 20 parts by mass; Resin 20 parts by mass; Auxiliary agent 3 parts by mass; Colouring agent 2 parts by mass; Adhesive 3 parts by mass; Solvent 50 parts by mass; Softener 2 parts by mass.By following technology: the tea material → blank of getting the raw materials ready → screen → wash material → water or steam prehydrolysis → sulphate cook → desanding, concentrate oxidation → alkali refining → bleaching → acid treatment → desanding → concentrate → manufacture paper with pulp → flood → squeeze → pulverize → experienced → sulfonation → grinding → dissolving → filtration → spinning → drawing-off → cut-out → post processing → drying → packing, make 1000/cm of release anion
3Above tea pulp fibres.
Embodiment 3: micro/nano level tea powdered carbon 10 parts by mass; Resin 80 parts by mass; Auxiliary agent 3 parts by mass; Colouring agent 2 parts by mass; Adhesive 3 parts by mass; Softener 2 parts by mass.Preparation technology: micro/nano level tea powdered carbon, resin, auxiliary agent, colouring agent and adhesive are added in the double screw extruder, and blend is extruded, cooling, and pelletizing makes tea charcoal master batch.Dried tea charcoal master batch, colouring agent, softener and resin slicer are added in the double screw extruder, extrude the spray silk under the temperature that configures, coiling can make and discharge 1000/cm of anion
3Above tea charcoal fiber.
Embodiment 4: micro/nano level tea powdered carbon 5 parts by mass; Resin 80 parts by mass; Auxiliary agent 5 parts by mass; Colouring agent 3 parts by mass; Adhesive 5 parts by mass; Softener 2 parts by mass.Preparation technology: micro/nano level tea powdered carbon, resin, auxiliary agent, colouring agent and adhesive are added in the double screw extruder, and blend is extruded, cooling, and pelletizing makes tea charcoal master batch.Dried tea charcoal master batch, colouring agent, softener and resin slicer are added in the double screw extruder, extrude the spray silk under the temperature that configures, coiling can make and discharge 1000/cm of anion
3Above tea charcoal fiber.
Embodiment 5: resin 85 parts by mass; Auxiliary agent 5 parts by mass; Colouring agent 3 parts by mass; Adhesive 5 parts by mass; Softener 2 parts by mass.Preparation technology: resin, auxiliary agent, colouring agent and adhesive are added in the double screw extruder, and blend is extruded, cooling, and pelletizing makes master batch.Dried master batch, colouring agent, softener and resin slicer are added in the double screw extruder, extrude the spray silk under the temperature that configures, coiling can make and discharge the following fiber of 500/cm3 of anion.
Embodiment 6: micro/nano level tea powdered carbon 5 parts by mass; Resin 85 parts by mass; Auxiliary agent 3 parts by mass; Colouring agent 3 parts by mass; Adhesive 2 parts by mass; Softener 2 parts by mass; Water is an amount of.Preparation technology: micro/nano level tea powdered carbon is distributed in water-soluble, the thermoplastic resin, adds auxiliary agent, colouring agent, adhesive, softener simultaneously, make the combination resin emulsion.The resin emulsion for preparing is coated on the base cloths such as woven fabric, knitted fabric, drying and shaping in the baking oven can make 1000/cm of release anion
3Above tea fiber.
Embodiment 7: resin 90 parts by mass; Auxiliary agent 3 parts by mass; Colouring agent 3 parts by mass; Adhesive 2 parts by mass; Softener 2 parts by mass; Water is an amount of.Preparation technology: auxiliary agent, colouring agent, adhesive, softener are distributed in water-soluble, the thermoplastic resin, make the combination resin emulsion.The resin emulsion for preparing is coated on the base cloths such as woven fabric, knitted fabric, drying and shaping in the baking oven can make 500/cm of release anion
3Following tea fiber.
Claims (7)
1. discharge tea fiber of anion and preparation method thereof, it is characterized in that: it is made by following raw material: natural tea tree 0-100 parts by mass; Micro/nano level tea powdered carbon 0-10 parts by mass; Resin 0-90 parts by mass; Auxiliary agent 0-20 parts by mass; Colouring agent 0-6 parts by mass; Adhesive 0-20 parts by mass; Solvent 0-100 parts by mass; Softener 0-5 parts by mass.
1. natural tea fibrillation: tea material → tea making sheet, tea section → steaming sifting tea tea section → crushing decomposition → biological enzyme degumming → carded fiber → textile fiber.
2. chemical dissolution method tea pulp fibres: the tea pulp fibres is a raw material with natural high-quality tea tree, employing hydrolysis-alkaline process and multistage bleaching are refining and make the tea pulp, pass through catalytic treatment again, improve content of cellulose, on the basis of satisfying the fiber production requirement, be processed into tea fiber by the chemical fibre factory.
3. tea charcoal fiber: micro/nano level tea powdered carbon, resin, auxiliary agent, colouring agent and natural minerals nano material are added in the double screw extruder, and blend is extruded, cooling, and pelletizing makes tea charcoal master batch.To add in the double screw extruder with resin slicer after the tea charcoal master batch drying, extrude the spray silk under the temperature that configures, coiling can make the tea fiber that discharges anion.
4. arrangement applies the tea fiber fabric: micro/nano level tea carbon powder is distributed in water-soluble, the thermoplastic resin, and the resin after will making up again is applied on the base cloths such as woven fabric, knitted fabric.
2. comprise all tea trees that can be used for preparing green tea, yellow tea, white tea, black tea, black tea, oolong tea according to claims 1 described natural tea tree.
3. select natural tea tree for use according to claims 1 described micro/nano level tea powdered carbon, utilize the high temperature carbonization technology to be fired into the tea charcoal, make by ultra-fine grinding again, meet national standard, can be even with mixed with resin.
4. comprise polyethylene (PE), polypropylene (PP), polystyrene (PS), polyethylene terephthalate (PET), polyamide (PA), the acrylonitrile-butadiene-styrene copolymer (ABS) that can be used for melt spinning according to claims 1 described resin; The polyacrylonitrile (PAN), polyvinyl chloride (PVC), polyvinyl alcohol (PVA), the viscose that can be used for dry method and wet spinning.
5. comprise according to claims 1 described auxiliary agent: surfactant, adhesive, coupling agent, promoter and other textile auxiliaries.
4, be dyestuff and the pigment of preparing by national standard according to claims 1 described colouring agent.
6. all meet national standard according to claims 1 described adhesive, solvent, softener.
7. the tea fiber of the release anion that goes out according to claims 1 described prepared discharges anion number at 1000/cm
3More than, reached and kept healthy basic need.
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| CN102677227A (en) * | 2012-06-13 | 2012-09-19 | 福建省晋江市华宇织造有限公司 | Composite tea carbon polyster fiber of continuous high-strength core sheath |
| CN103060945A (en) * | 2012-12-27 | 2013-04-24 | 江苏南纬悦达纺织研究院有限公司 | Manufacturing method for polymer fiber containing tea material component |
| CN103526395A (en) * | 2013-09-29 | 2014-01-22 | 吴江市凌通纺织整理有限公司 | Multifunctional washing-free fabric |
| CN103556363A (en) * | 2013-11-07 | 2014-02-05 | 江苏华杰丝绸进出口有限公司 | Composite silk fabric containing mulberry silk, pearl fiber and tea fiber |
| CN103643344A (en) * | 2013-11-30 | 2014-03-19 | 常熟涤纶有限公司 | Production process of tea-carbon polyester monofilament |
| CN104146550A (en) * | 2014-06-23 | 2014-11-19 | 惠州市欧野科技有限公司 | Imitated ramie infant pillow |
| CN104339762A (en) * | 2014-11-04 | 2015-02-11 | 苏州利森服饰贸易有限公司 | Multifunctional double-layer composite shell fabric for men's clothing |
| CN104746172A (en) * | 2015-04-09 | 2015-07-01 | 苏州金辉纤维新材料有限公司 | Preparation method of coffee carbon polyester fiber with high-efficient adsorption and hygroscopic properties |
| CN104746173A (en) * | 2015-04-09 | 2015-07-01 | 苏州金辉纤维新材料有限公司 | Preparation method of hemp stalk carbon polyester fiber with high-efficient adsorption and hygroscopic properties |
| CN104746171A (en) * | 2015-04-09 | 2015-07-01 | 苏州金辉纤维新材料有限公司 | Preparation method of hemp carbon polyester fiber with high-efficient adsorption and hygroscopic properties |
| CN104975374A (en) * | 2015-07-31 | 2015-10-14 | 爱谱诗（苏州）服装有限公司 | Preparation process of blended yarn weaved fabric containing tea fiber |
| CN107794586A (en) * | 2017-11-09 | 2018-03-13 | 浙江花小匠网络科技有限公司 | A kind of process for being used to produce the tea fiber of silk stocking |
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| CN102677227A (en) * | 2012-06-13 | 2012-09-19 | 福建省晋江市华宇织造有限公司 | Composite tea carbon polyster fiber of continuous high-strength core sheath |
| CN102677227B (en) * | 2012-06-13 | 2014-04-09 | 福建省晋江市华宇织造有限公司 | Composite tea carbon polyster fiber of continuous high-strength core sheath |
| CN103060945A (en) * | 2012-12-27 | 2013-04-24 | 江苏南纬悦达纺织研究院有限公司 | Manufacturing method for polymer fiber containing tea material component |
| CN103060945B (en) * | 2012-12-27 | 2014-08-27 | 江苏南纬悦达纺织研究院有限公司 | Manufacturing method for polymer fiber containing tea material component |
| CN103526395A (en) * | 2013-09-29 | 2014-01-22 | 吴江市凌通纺织整理有限公司 | Multifunctional washing-free fabric |
| CN103556363A (en) * | 2013-11-07 | 2014-02-05 | 江苏华杰丝绸进出口有限公司 | Composite silk fabric containing mulberry silk, pearl fiber and tea fiber |
| CN103643344A (en) * | 2013-11-30 | 2014-03-19 | 常熟涤纶有限公司 | Production process of tea-carbon polyester monofilament |
| CN104146550A (en) * | 2014-06-23 | 2014-11-19 | 惠州市欧野科技有限公司 | Imitated ramie infant pillow |
| CN104339762A (en) * | 2014-11-04 | 2015-02-11 | 苏州利森服饰贸易有限公司 | Multifunctional double-layer composite shell fabric for men's clothing |
| CN104339762B (en) * | 2014-11-04 | 2016-05-11 | 苏州万图明电子软件有限公司 | A kind of men's clothing multifunction double-layer composite material |
| CN104746172A (en) * | 2015-04-09 | 2015-07-01 | 苏州金辉纤维新材料有限公司 | Preparation method of coffee carbon polyester fiber with high-efficient adsorption and hygroscopic properties |
| CN104746173A (en) * | 2015-04-09 | 2015-07-01 | 苏州金辉纤维新材料有限公司 | Preparation method of hemp stalk carbon polyester fiber with high-efficient adsorption and hygroscopic properties |
| CN104746171A (en) * | 2015-04-09 | 2015-07-01 | 苏州金辉纤维新材料有限公司 | Preparation method of hemp carbon polyester fiber with high-efficient adsorption and hygroscopic properties |
| CN104975374A (en) * | 2015-07-31 | 2015-10-14 | 爱谱诗（苏州）服装有限公司 | Preparation process of blended yarn weaved fabric containing tea fiber |
| CN107794586A (en) * | 2017-11-09 | 2018-03-13 | 浙江花小匠网络科技有限公司 | A kind of process for being used to produce the tea fiber of silk stocking |
| CN112482021A (en) * | 2020-12-03 | 2021-03-12 | 郑州诺肯新材料科技有限公司 | Preparation method of tea shell carbon fiber |
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Application publication date: 20101013 |