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CN101822620A - Dandruff-removing and hair-washing composition with quick acting - Google Patents

Dandruff-removing and hair-washing composition with quick acting Download PDF

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Publication number
CN101822620A
CN101822620A CN200910213662A CN200910213662A CN101822620A CN 101822620 A CN101822620 A CN 101822620A CN 200910213662 A CN200910213662 A CN 200910213662A CN 200910213662 A CN200910213662 A CN 200910213662A CN 101822620 A CN101822620 A CN 101822620A
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China
Prior art keywords
salicylate
dandruff
salicylic acid
hexamidine
quick acting
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CN200910213662A
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Chinese (zh)
Inventor
张毅
张太军
范新雨
聂胜
杨盼盼
李涛
谢付凤
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Guangdong Mingchen Co Ltd
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Guangdong Mingchen Co Ltd
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Priority to CN200910213662A priority Critical patent/CN101822620A/en
Publication of CN101822620A publication Critical patent/CN101822620A/en
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Abstract

The invention discloses a dandruff-removing and hair-washing composition with quick acting. Calculated by weight percent, a formula of the dandruff-removing and hair-washing composition comprises the following components: 5.0 to 50.0 percent of surfactant, 0.1 to 5.0 percent of antidandruff agent, 0.01 to 6.0 percent of salicylic acid or derivative thereof and the balance of water-containing carrier, wherein the antidandruff agent is a mixture of dichlorophenyl imidazole dioxolane and a hexamidine derivative. The invention utilizes the dichlorophenyl imidazole dioxolane to combine with the hexamidine derivative so as to form a complementary antimicrobial spectrum; and the salicylic acid or the derivative thereof attached to the scalp can slowly release the trace salicylic acid under the inherent subacid condition of the scalp, and the trace salicylic acid can generate a mild keratose stripping effect, thereby promoting the quick falling of keratinized scalp cells and creating a condition for the more sufficient contact of the antidandruff agent and microorganisms in the corneum so as to suppress and kill microorganisms (a malassezia yeast) which exists on the scalp and causes dandruffs effectively and finally achieve the aim of controlling the dandruffs.

Description

A kind of anti-dandruff shampoo composition of quick acting
Technical field
The present invention relates to household chemicals field, particularly a kind of anti-dandruff shampoo composition.
Background technology
Comprise detersive surfactant and conditioner, particularly the various shampoo composites of polysiloxanes conditioner are known in the art and are to have bought.Have been found that many in these shampoo composites can provide the excellent cleaning hair and the effect of conditioning hair.For example wherein comprise the shampoo of surfactant and polysiloxanes conditioner etc., in the time of on being applied to hair, can bringing outstanding cleaning, conditioning and send out the sense benefit.
Dandruff control shampoo also is known in the art, and can buy.Usually anti-dandruff active substance and detersive surfactant have been introduced in the dandruff control shampoo.Wherein, the dandruff removing agent of common type is as the divalent metal salt of sulfur, selenium sulfide, pyrithione, climbazole, piroctone olamine salt, also be as known in the art.The anti-dandruff efficacy of prior art is controlled anti-dandruff dose of deposition on hair and scalp of granule by the condensed phase that uses a kind of anion surfactant and cation-modified polymer formation.But it is very unfortunate, use the most effective condensed phase on hair and scalp, to deposit the anti-dandruff active substance, feeling in the time of can be to opsonic action particularly cleaning hair has a negative impact, and the most effective condensed phase is wrapped up in the particle deposition in generation and do not indicated best bioavailability.
Yet life stress and fast-changing rhythm of life are affecting our health and living habit, and more crowd begins to be subjected to the puzzlement of dandruff.On the other hand, air and environmental pollution further worsen, and dying has a perm also becomes more frequent, and scalp is subjected to more stimulation naturally, the normal keratinization physiological period of scalp, scalp sebaceous gland function begin disorder, and this also provides perfect environmental condition for bacteria live and breeding.The too fast keratinization of microorganism, scalp, vigorous sebum three mutually promote, and dandruff begins malignant development.The scalp care hair shampoo of prior art preparation is handled the dandruff problem of general symptom, needs a long time just can tell on usually.The puzzlement of dandruff has had influence on the image and the confidence of people's social activity, the modern that rhythm of life is accelerated all the more is more and more lower to the tolerance of dandruff, increasing consumer wishes that for the commercially available prod of prior art preparation a kind of dandruff control shampoo of energy quick acting is arranged.
Summary of the invention
For addressing the above problem, the invention provides a kind of anti-dandruff shampoo composition of quick acting, it possesses the ability of controlling scalp microorganism (chlosma yeast) breeding at short notice, thereby realizes satisfying fast the purpose of consumer away from dandruff worry.
The object of the present invention is achieved like this: a kind of anti-dandruff shampoo composition of quick acting, it is characterized in that counting by weight percentage, and its prescription comprises following component:
A) 5.0～50.0% surfactant;
B) 0.1～5.0% dandruff removing agent, this anti-dandruff dose is the mixture of Dichlorobenzene base imidazoles dioxolanes and hexamidine derivant;
C) 0.01～6.0% salicylic acid or derivatives thereof;
D) aqueous carrier surplus.
The present invention has overcome prior art and has only considered to deposit anti-dandruff active matter to scalp, and no matter the shortcoming whether anti-dandruff active matter that deposition gets on plays a role, outstanding advantage of the present invention is: utilize and suppress the biosynthetic Dichlorobenzene base imidazoles of fungus ergosterol dioxolanes in conjunction with the hexamidine derivant, the two forms complementary antimicrobial spectrum; Under the inherent slightly acidic condition of scalp, can slowly release the salicylic acid of trace attached to the salicylic acid or derivatives thereof on the scalp, the salicylic acid of trace can produce gentle cutin and peel off effect, thereby promote the keratinization scalp cells to quicken to come off, for condition has been created in anti-dandruff dose of microorganism (chlosma yeast) that touches more fully in the horny layer, and then effectively suppress and kill the microorganism that causes dandruff (chlosma yeast) that is present on the scalp, finally reach the purpose of control dandruff.
The specific embodiment
The present invention is a kind of anti-dandruff shampoo composition of quick acting, counts by weight percentage, and its prescription comprises following component: 5.0～50.0% surfactant; 0.1～5.0% dandruff removing agent, wherein said anti-dandruff dose is the compositions of Dichlorobenzene base imidazoles dioxolanes and hexamidine derivant, and both weight ratios are 104: 1 to 1: 10; 0.01～6.0% salicylic acid or derivatives thereof; The aqueous carrier surplus.
Surfactant
Of the present invention 5.0～50.0% surface active agent composition is selected from least a in anion surfactant, amphoteric surfactant, the non-ionic surface active agent or their combination.
The suitable anion surfactant that is used for the present composition comprises known hair-care or other personal care cleansing of can be used for.The anion surfactant component concentrations should be enough to the cleaning and the foaming effect that provide required in the compositions, and concentration is 5% to about 50% usually by weight, preferred about 8% to about 30%, and more preferably from about 10% to about 25%, even more preferably from about 12% to about 18%.
Be applicable to that preferred anionic surfactants surfactant of the present invention is alkyl and alkyl ether sulfate.These materials have general formula R OSO separately 3M and RO (C 2H 4O) XSO 3M, wherein R is about 8 alkyl or alkenyls to about 18 carbon atoms, x is that value is 1 to 10 integer, and M is cation, as ammonium, alkanolamine, as triethanolamine, the monovalence metal is as sodium ion and potassium ion.
In alkyl and alkyl ether sulfate, R has preferred about 8 to about 18 carbon atoms, and more preferably from about 10 to about 16 carbon atoms, even more preferably from about 12 to about 14 carbon atoms.This alkyl ether sulfate typically can and have the about 8 condensation product preparations to the monohydric alcohol of about 24 carbon atoms by oxirane.Monohydric alcohol and about 0 is to about 10, and preferred about 2 to about 5, and the mixture of the more preferably from about reacting ethylene oxide of 3 mol ratios, and gained molecular species has about 3 moles of ethylene oxide of for example average every mol of alcohol by sulphation and neutralization.
Other suitable anionic detersive surfactant is to meet formula [RSO 3M] the water soluble salt of organic sulfur acid reaction product, wherein R has about 8 to about 24 carbon atoms, preferred about 10 straight chain or side chain, radical of saturated aliphatic alkyl to about 18 carbon atoms; And M is a cation mentioned above.
Other anionic detersive surfactant that is suitable for is a succinate, embodiment comprises N-disodium octadecyl sulfosuccinate, lauryl disodium sulfosuccinate, lauryl 2-Sulfosuccinic acid diammonium, N-(1,2-dicarboxyl ethyl)-N-octadecyl 2-Sulfosuccinic acid four sodium, the diamyl ester of sodium sulfosuccinate, the dihexyl ester of sulfo group coloured glaze succinum sodium and the dioctyl ester of 2-Sulfosuccinic acid sodium salt.
The preferred anionic surfactants detersive surfactant that is used for the present composition is selected from ammonium lauryl sulfate; lauryl polyethenoxy ether sodium sulfate; the lauryl sulfate triethylamine; laureth sulphuric acid triethylamine; triethanolamine lauryl sulfate; laureth sulphuric acid triethanolamine; lauryl sulfate monoethanolamine; laureth sulphuric acid monoethanolamine; lauryl sulfate diethanolamine; laureth sulphuric acid diethanolamine; Glyceryl Monolaurate sodium sulfate; sodium lauryl sulfate; sodium laureth sulfate; lauryl potassium sulfate; the laureth potassium sulfate; sodium lauryl sarcosinate; sodium lauroyl sarcosine; the sarcosine lauryl; the cocoyl sarcosine; cocoyl ammonium sulfate; lauroyl ammonium sulfate; cocoyl sodium sulfate; lauroyl sodium sulfate; the cocoyl potassium sulfate; lauryl potassium sulfate; triethanolamine lauryl sulfate; cocoyl sulphuric acid monoethanolamine; the lauryl sulfate monoethanolamine; the tridecyl benzene sulfonic acid sodium salt; dodecylbenzene sodium sulfonate; cocoyl sodium isethionate, or their combination.
Be suitable for amphoteric surfactant of the present invention and comprise known those of hair-care or other personal care cleansing of being used for.It is about 0.5% to about 20%, preferred about 1% to about 5% that above-mentioned amphoteric surfactant accounts for composition weight.Suitable amphoteric surfactants is described to those surfactants of the derivant of aliphatic secondary amine and tertiary amine, wherein aliphatic group can be a straight or branched, and one of them aliphatic substituent group comprises about 8 to about 18 carbon atoms, and an aliphatic substituent group comprises anionic group, as carboxyl, sulfonate radical, sulfate radical, phosphate radical.Be used for amphoteric surfactant of the present invention and comprise N-cocamidopropyl ethyl-N hydroxyethyl acetate, N-cocamidopropyl ethyl-N hydroxyethyl diacetin, N-lauroyl amido ethyl-N hydroxyethyl acetate, N-lauroyl amido ethyl-N hydroxyethyl diacetin, and their mixture.Zwitterionic compound such as betanin are preferred.
Being suitable for surfactant of the present invention also comprises and accounts for composition weight 0.2% to 5.0%, preferred 0.5% to 2.5% non-ionic surface active agent, this non-ionic surface active agent is meant the surfactant with prolongation and stable foam, mainly be selected from fatty acid alkanol amides, preferred coconut oil single ethanol amide.
Dandruff removing agent
Be applicable to that it is 0.01%-5.0% that dandruff removing agent of the present invention accounts for shampoo composite weight, is preferably 0.02%-3.0%, more preferably at 0.03%-1.01%.
Be applicable to that anti-dandruff dose of the present invention is the mixture of Dichlorobenzene base imidazoles dioxolanes and hexamidine derivant, both weight ratios are 104: 1 to 1: 10, preferably at 85: 1 to 1: 8, more preferably at 65: 1 to 1: 6.The hexamidine derivant is selected from hexamidine two (hydroxyethylsulfonic acid .) salt, hexamidine two PARABEN salt, hexamidine PARABEN salt etc.Preferred anti-dandruff dose preferred anti-dandruff dose is the two compositions of Dichlorobenzene base imidazoles dioxolanes and hexamidine two (hydroxyethylsulfonic acid .) salt.
Salicylic acid or derivatives thereof (ester or salt)
It is about 0.01% to 6.0% to be applicable to that salicylic acid or derivatives thereof of the present invention (ester or salt) accounts for composition weight, is preferably 0.05% to 2.8%.
Be applicable to that salicylic acid or derivatives thereof of the present invention (ester or salt) comprises at least a in the following material: amyl salicylate, nonanedioyl two (ethyl salicylate), benzyl salicylate, betanin Salicylate, butyl capryl alcohol salicylate, calcium salicylate, C 12-15The alcohol salicylate, the decoyl salicylic acid, the chitosan Salicylate, the dipropylene glycol salicylate, ethylhexyl salicylate, the ethylene glycol salicylate, 1,6-hexanediol two salicylates, hexyl lauryl alcohol salicylate, 1-Hexyl salicylate, salicylic acid isodecyl ester, benzylamino isopropyl alcohol salicylate, magnesium salicylate, salicylic acid MEA salt, the menthol salicylate, methyl salicylate, the myristyl alcohol salicylate, phenyl salicytate, potassium salicylate, salicylic acid, the silandiol salicylate, sodium salicylate, salicylic acid TEA salt, thiosalicylic acid, the tridecyl alcohol salicylate, zinc salicylate, thiosalicylic acid zinc, salicylic acid titanium etc.Be preferably tridecyl alcohol salicylate, zinc salicylate, C 12-15The alcohol salicylate.
Aqueous carrier
The form of the liquid that the present composition (under environmental condition) is dumpable typically.Therefore, said composition will typically comprise aqueous carrier, and its content is about 50% to about 95%, preferred about 60% to about 85%.Aqueous carrier can comprise water or can miscible water and the mixture of organic solvent, but comprises that also all kinds of homogeneous are dispersed or dissolved in polymer in the compositions, non-ionic surface active agent, emulsified silicone oil, amido silicon oil, cation opsonizing agent or the like additive.
Help additive of the present invention and also comprise hydrolyzed protein and derivant thereof, mainly contain hydrolyzed silk protein, hydrolyzed wheat protein, hydrolyzed gluten, hydrolyzed soybean protein, hydrolytic collagen, hydrolysis of keratin, elastin hydrolysis, hydrolysis milk proem etc., the molecular weight of described hydrolyzed protein is between 3000D to 5000D, and preferred molecular weight is between 3500D to 4500D; The hydrolyzed protein derivant comprises: Laurel hydroxypropyl hydrolyzed protein alkyl dimethyl ammonium chloride, cocoyl hydroxypropyl hydrolyzed protein alkyl dimethyl ammonium chloride, hydroxypropyl hydrolyzed protein trimethyl ammonium chloride etc.
Be applicable to that polydimethylsiloxane of the present invention is the mixture of nonvolatile silicone rubber resina and polydimethylsiloxane, it comprise viscosity in the time of 25 ℃ more than or equal to 800000mm 2.s -1With less than 10000mm 2.s -1The polysiloxane mixtures of material.Its detailed description comprises US 4152416 that authorized people such as Spitzer on May 1st, 1979 and the Chemistry and Technology of silicones that Noll, Walter are shown, New York:Academic Press 1968. describes General Electric (now renaming Momentive Performance Material company as) Silicone Rubber Product Data Sheets ES30, SE33, SE54 and the SE76 in addition of silicone rubber in addition.The molal weight of typical case's silicone rubber is more than 150000, general between between in 150000 to 900000, instantiation comprises polydimethylsiloxane, poly-(dimethyl siloxane, ethylene methacrylic radical siloxane) copolymer and their mixture.It also is included in the preparation siloxanes process by trifunctional or four functional silane are sneaked into the crosslinked polymer siloxane that obtains in simple function or the two functional silane.Each silicon atom has about 1.1 oxygen atoms at least, preferably between 1.2-1.0.Preferred embodiment comprises the XF49-B8324 of Momentive Performance Material company.
Help amino silicones of the present invention and account for compositions 0.01-3%, preferably at 0.03-2%, more preferably it possesses following general formula at 0.05-1%.:
Figure G2009102136626D00051
Wherein: n is the integer of 0-1000, and m is the integer of 1-500, and m and n sum are the integers of 1-1000, and R1 and R2 are hydrogen, C 1-C 4Alkyl or alkane hydroxyl.Satisfy in the amino silicones of above-mentioned general formula and contain 0.1% weight or volatile solvent still less or hexamethyl siloxanes, be less than 0.5% weight prestox siloxanes and be less than 1.0% weight decamethyl siloxanes, and the molal weight of described amino silicones is between 2000-600000. the commercially available amino silicones that can be used for inventing includes but not limited to available from Dow Corning company, Dow Corning 8566 Amino Fluids; Available from SM 2115 of MomentivePerformance Material company etc.
Helping additive of the present invention also comprises: Polyquaternium-10 or Guar Quats or Polyquaternium-7 and their compositions, and the Polyquaternium-10 addition is at 0.01-0.6% when needing; Guar Quats addition is at 0.01-0.5% when needing; The Polyquaternium-7 addition is at 0.01-0.44% and other all kinds of suitable high molecular weight water soluble polymers when needing.Antiseptic: Kazon, p-Hydroxybenzoate, diazolidinyl urea, imidazolidinyl urea, DMDM Hydantoin etc.; Acidity regulator: citric acid, Etidronic Acid, sodium hydroxide etc.; Pigment: FD﹠amp; C or D﹠amp; Dyestuff among the C; Essence; Intercalating agent: Etidronic Acid, EDTA-2Na etc.; Pearling agent; Inorganic salt: sodium chloride, ammonium chloride, zinc chloride etc.; Antioxidant; Freshener; Deionized water etc.
Embodiment
Following embodiment and reference examples further describe and the interior embodiment of for example clear scope of the invention.These embodiment that given only are illustrative; unintelligible is limitation of the present invention; because under the situation that does not deviate from the present invention's spirit and protection domain, can carry out many changes; and all by weight percentage; unless explanation is hereinafter arranged in addition, is suitable for composition in addition and is trade name or INCI name.
The prescription of example A-K sees Table 1, and wherein F, G, J, K are non-limiting example of the present invention, and A-E and H-I are reference examples.
Table 1.
Figure G2009102136626D00061
The test of test-anti-dandruff effect hair caring chamber
The test of hair caring chamber is to utilize the well-known on the market product Y salable of China to compare for the sample among benchmark product and the embodiment. the experimenter is provided the 0-10 branch by double blinding two products on probation to every index, representative in 10 fens is own the most satisfied to this performance, representative in 0 fen is dissatisfied. and experimenter (totally 44 people, 1 group of per 4 people) is the long hair women of dandruff worry.The specialty teacher adopts identical program and time that product is done the half a head test, and the water with identical and capacity rinses out then.The experimenter that participation is estimated fixedly half a head uses the Y sample, and another side uses the sample among the embodiment, uses continuously 14 days, follows the tracks of after stopping using 5 days again.By 18 professional teachers every experimenter's dandruff situation is carried out tracking evaluation marking (10 are divided into dandruff seldom, and 0 is divided into the dandruff especially severe) before using every day, average is as the dandruff score value on the same day.The result gathers as table 2.
Table 2.
Figure G2009102136626D00071
The continuous table of going up:
Figure G2009102136626D00072
From table 2 data as can be seen this patent indication hair-washing composition and market hit product or tradition utilize the anti-dandruff shampoo composition of pyrithione slaine to compare to have obviously rapid-action, act on characteristics completely.Salicylic acid or derivatives thereof (ester or salt) has makes anti-dandruff effect more thorough, and this comes from its slight hydrolysis sustained release performance.The free salicylic acid of trace has promoted that the scalp horn cell quickens to come off, and provides more opportunity for the Dichlorobenzene base imidazoles dioxolanes in the hair-washing composition after the dilution and hexamidine derivant directly act on the antibacterial that causes dandruff.

Claims (8)

1. the anti-dandruff shampoo composition of a quick acting is characterized in that counting by weight percentage, and its prescription comprises following component:
A) 5.0～50.0% surfactant;
B) 0.1～5.0% dandruff removing agent, this anti-dandruff dose is the mixture of Dichlorobenzene base imidazoles dioxolanes and hexamidine derivant;
C) 0.01～6.0% salicylic acid or derivatives thereof;
D) aqueous carrier surplus.
2. the anti-dandruff shampoo composition of quick acting according to claim 1 is characterized in that: described surface active agent composition is selected from least a in anion surfactant, amphoteric surfactant, the non-ionic surface active agent or their combination.
3. the anti-dandruff shampoo composition of quick acting according to claim 1, it is characterized in that: described anion surfactant is selected from: water soluble salt, the succinate of alkyl or alkyl ether sulfate, organic sulfur acid reaction product.
4. the anti-dandruff shampoo composition of quick acting according to claim 1, it is characterized in that: described amphoteric surfactant is the derivant of aliphatic secondary amine or tertiary amine.
5. the anti-dandruff shampoo composition of quick acting according to claim 1, it is characterized in that: described non-ionic surface active agent is selected from fatty acid alkanol amides.
6. the anti-dandruff shampoo composition of quick acting according to claim 1 is characterized in that: in described anti-dandruff dose, Dichlorobenzene base imidazoles dioxolanes and hexamidine derivant weight ratio be 104: 1 to 1: 10.
7. the anti-dandruff shampoo composition of quick acting according to claim 1, it is characterized in that: described hexamidine derivant is selected from hexamidine two (hydroxyethylsulfonic acid .) salt, hexamidine two PARABEN salt or hexamidine PARABEN salt.
8. the anti-dandruff shampoo composition of quick acting according to claim 1 is characterized in that: described salicylic acid or derivatives thereof comprises at least a in the following material: amyl salicylate, nonanedioyl two (ethyl salicylate), benzyl salicylate, betanin Salicylate, butyl capryl alcohol salicylate, calcium salicylate, C 12-15The alcohol salicylate, the decoyl salicylic acid, the chitosan Salicylate, the dipropylene glycol salicylate, ethylhexyl salicylate, the ethylene glycol salicylate, 1,6-hexanediol two salicylates, hexyl lauryl alcohol salicylate, 1-Hexyl salicylate, salicylic acid isodecyl ester, benzylamino isopropyl alcohol salicylate, magnesium salicylate, salicylic acid MEA salt, the menthol salicylate, methyl salicylate, the myristyl alcohol salicylate, phenyl salicytate, potassium salicylate, salicylic acid, the silandiol salicylate, sodium salicylate, salicylic acid TEA salt, thiosalicylic acid, the tridecyl alcohol salicylate, zinc salicylate, thiosalicylic acid zinc, salicylic acid titanium etc.Be preferably tridecyl alcohol salicylate, zinc salicylate, C 12-15The alcohol salicylate.
CN200910213662A 2009-12-11 2009-12-11 Dandruff-removing and hair-washing composition with quick acting Pending CN101822620A (en)

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Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103799936A (en) * 2012-11-01 2014-05-21 松下电器产业株式会社 Dishwasher
CN110585046A (en) * 2019-10-12 2019-12-20 曹志军 Dandruff removing, dandruff stopping, alopecia preventing and hair increasing component and product
CN112057381A (en) * 2020-09-19 2020-12-11 石狮市瑞鹰纺织科技有限公司 Sleep-aiding shampoo and preparation method thereof
CN112312891A (en) * 2018-05-30 2021-02-02 艾维德姆研究所股份公司 Mild composition for topical treatment of viral and fungal skin and nail disorders
CN113057916A (en) * 2021-03-03 2021-07-02 胡旭英 Hair-care and anti-dandruff shampoo and preparation method thereof
CN117898968A (en) * 2024-03-19 2024-04-19 江苏亨瑞生物医药科技有限公司 Collagen shampoo with sun-screening, anti-dandruff and repairing functions and preparation method thereof
CN118873421A (en) * 2024-07-04 2024-11-01 王叔和(武汉)生物科技工程有限公司 A long-lasting stable selenium disulfide micropowder and its preparation method and application

Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103799936A (en) * 2012-11-01 2014-05-21 松下电器产业株式会社 Dishwasher
CN112312891A (en) * 2018-05-30 2021-02-02 艾维德姆研究所股份公司 Mild composition for topical treatment of viral and fungal skin and nail disorders
CN110585046A (en) * 2019-10-12 2019-12-20 曹志军 Dandruff removing, dandruff stopping, alopecia preventing and hair increasing component and product
CN112057381A (en) * 2020-09-19 2020-12-11 石狮市瑞鹰纺织科技有限公司 Sleep-aiding shampoo and preparation method thereof
CN113057916A (en) * 2021-03-03 2021-07-02 胡旭英 Hair-care and anti-dandruff shampoo and preparation method thereof
CN113057916B (en) * 2021-03-03 2022-12-27 胡旭英 Hair-care and anti-dandruff shampoo and preparation method thereof
CN117898968A (en) * 2024-03-19 2024-04-19 江苏亨瑞生物医药科技有限公司 Collagen shampoo with sun-screening, anti-dandruff and repairing functions and preparation method thereof
CN117898968B (en) * 2024-03-19 2024-06-07 江苏亨瑞生物医药科技有限公司 Collagen shampoo with sun-screening, anti-dandruff and repairing functions and preparation method thereof
CN118873421A (en) * 2024-07-04 2024-11-01 王叔和(武汉)生物科技工程有限公司 A long-lasting stable selenium disulfide micropowder and its preparation method and application

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Application publication date: 20100908