CN101768514B - Alhagi sparsifolia extract and preparation method and application thereof - Google Patents
Alhagi sparsifolia extract and preparation method and application thereof Download PDFInfo
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- CN101768514B CN101768514B CN2008102315424A CN200810231542A CN101768514B CN 101768514 B CN101768514 B CN 101768514B CN 2008102315424 A CN2008102315424 A CN 2008102315424A CN 200810231542 A CN200810231542 A CN 200810231542A CN 101768514 B CN101768514 B CN 101768514B
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- 239000000284 extract Substances 0.000 title claims abstract description 57
- 238000002360 preparation method Methods 0.000 title claims abstract description 15
- 238000000605 extraction Methods 0.000 title claims abstract description 11
- 241001626384 Alhagi sparsifolia Species 0.000 title abstract description 36
- 241000208125 Nicotiana Species 0.000 claims abstract description 18
- 235000002637 Nicotiana tabacum Nutrition 0.000 claims abstract description 18
- 239000012535 impurity Substances 0.000 claims abstract description 14
- 239000002994 raw material Substances 0.000 claims abstract description 13
- 230000032683 aging Effects 0.000 claims abstract description 7
- 241000214035 Alhagi maurorum Species 0.000 claims description 35
- 235000008011 Alhagi graecorum Nutrition 0.000 claims description 34
- 235000017398 Alhagi maurorum Nutrition 0.000 claims description 34
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 31
- 239000007788 liquid Substances 0.000 claims description 17
- 239000000047 product Substances 0.000 claims description 15
- 235000013599 spices Nutrition 0.000 claims description 14
- 239000006228 supernatant Substances 0.000 claims description 13
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical group CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 12
- 239000003795 chemical substances by application Substances 0.000 claims description 10
- 238000000034 method Methods 0.000 claims description 7
- 229930002875 chlorophyll Natural products 0.000 claims description 6
- 235000019804 chlorophyll Nutrition 0.000 claims description 6
- ATNHDLDRLWWWCB-AENOIHSZSA-M chlorophyll a Chemical compound C1([C@@H](C(=O)OC)C(=O)C2=C3C)=C2N2C3=CC(C(CC)=C3C)=[N+]4C3=CC3=C(C=C)C(C)=C5N3[Mg-2]42[N+]2=C1[C@@H](CCC(=O)OC\C=C(/C)CCC[C@H](C)CCC[C@H](C)CCCC(C)C)[C@H](C)C2=C5 ATNHDLDRLWWWCB-AENOIHSZSA-M 0.000 claims description 6
- 239000012141 concentrate Substances 0.000 claims description 5
- 238000000926 separation method Methods 0.000 claims description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 2
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims 6
- 239000007864 aqueous solution Substances 0.000 claims 3
- 238000010992 reflux Methods 0.000 claims 2
- 239000000243 solution Substances 0.000 claims 2
- 238000001556 precipitation Methods 0.000 claims 1
- 235000019504 cigarettes Nutrition 0.000 abstract description 6
- 230000000694 effects Effects 0.000 abstract description 5
- 239000000654 additive Substances 0.000 abstract description 4
- 230000000996 additive effect Effects 0.000 abstract description 4
- 239000003205 fragrance Substances 0.000 abstract description 4
- 239000000779 smoke Substances 0.000 abstract description 4
- 235000019505 tobacco product Nutrition 0.000 abstract description 4
- 238000004519 manufacturing process Methods 0.000 abstract description 3
- 201000007100 Pharyngitis Diseases 0.000 abstract description 2
- 230000000391 smoking effect Effects 0.000 abstract description 2
- 230000001376 precipitating effect Effects 0.000 abstract 1
- 241000196324 Embryophyta Species 0.000 description 6
- 238000001914 filtration Methods 0.000 description 4
- 238000004062 sedimentation Methods 0.000 description 4
- 238000002156 mixing Methods 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 2
- 240000008866 Ziziphus nummularia Species 0.000 description 2
- 235000013399 edible fruits Nutrition 0.000 description 2
- 238000000855 fermentation Methods 0.000 description 2
- 230000004151 fermentation Effects 0.000 description 2
- 239000003546 flue gas Substances 0.000 description 2
- HNZUNIKWNYHEJJ-UHFFFAOYSA-N geranyl acetone Natural products CC(C)=CCCC(C)=CCCC(C)=O HNZUNIKWNYHEJJ-UHFFFAOYSA-N 0.000 description 2
- HNZUNIKWNYHEJJ-FMIVXFBMSA-N geranyl acetone Chemical compound CC(C)=CCC\C(C)=C\CCC(C)=O HNZUNIKWNYHEJJ-FMIVXFBMSA-N 0.000 description 2
- HJOVHMDZYOCNQW-UHFFFAOYSA-N isophorone Chemical compound CC1=CC(=O)CC(C)(C)C1 HJOVHMDZYOCNQW-UHFFFAOYSA-N 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 229920000642 polymer Polymers 0.000 description 2
- 239000001674 (E)-1-(2,6,6-trimethyl-1-cyclohexenyl)but-2-en-1-one Substances 0.000 description 1
- BGTBFNDXYDYBEY-UHFFFAOYSA-N 1-(2,6,6-trimethylcyclohexen-1-yl)but-2-en-1-one Chemical compound CC=CC(=O)C1=C(C)CCCC1(C)C BGTBFNDXYDYBEY-UHFFFAOYSA-N 0.000 description 1
- 239000001278 2-(5-ethenyl-5-methyloxolan-2-yl)propan-2-ol Substances 0.000 description 1
- 241000214034 Alhagi Species 0.000 description 1
- 235000007516 Chrysanthemum Nutrition 0.000 description 1
- 244000189548 Chrysanthemum x morifolium Species 0.000 description 1
- 235000019750 Crude protein Nutrition 0.000 description 1
- BRHDDEIRQPDPMG-UHFFFAOYSA-N Linalyl oxide Chemical compound CC(C)(O)C1CCC(C)(C=C)O1 BRHDDEIRQPDPMG-UHFFFAOYSA-N 0.000 description 1
- 206010028980 Neoplasm Diseases 0.000 description 1
- 235000014676 Phragmites communis Nutrition 0.000 description 1
- 241000219000 Populus Species 0.000 description 1
- 241000124033 Salix Species 0.000 description 1
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 1
- WPYMKLBDIGXBTP-UHFFFAOYSA-N benzoic acid Chemical compound OC(=O)C1=CC=CC=C1 WPYMKLBDIGXBTP-UHFFFAOYSA-N 0.000 description 1
- POIARNZEYGURDG-UHFFFAOYSA-N beta-damascenone Natural products CC=CC(=O)C1=C(C)C=CCC1(C)C POIARNZEYGURDG-UHFFFAOYSA-N 0.000 description 1
- 201000011510 cancer Diseases 0.000 description 1
- 235000019784 crude fat Nutrition 0.000 description 1
- 230000008021 deposition Effects 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 238000002481 ethanol extraction Methods 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 241000411851 herbal medicine Species 0.000 description 1
- 235000021579 juice concentrates Nutrition 0.000 description 1
- 238000002386 leaching Methods 0.000 description 1
- 210000004185 liver Anatomy 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 238000000643 oven drying Methods 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 239000002304 perfume Substances 0.000 description 1
- 230000008092 positive effect Effects 0.000 description 1
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- 150000003839 salts Chemical class 0.000 description 1
- 239000004576 sand Substances 0.000 description 1
- 239000011780 sodium chloride Substances 0.000 description 1
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- 210000004881 tumor cell Anatomy 0.000 description 1
- 235000021122 unsaturated fatty acids Nutrition 0.000 description 1
- 150000004670 unsaturated fatty acids Chemical class 0.000 description 1
- 235000015112 vegetable and seed oil Nutrition 0.000 description 1
- 239000000341 volatile oil Substances 0.000 description 1
- 238000005303 weighing Methods 0.000 description 1
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- Manufacture Of Tobacco Products (AREA)
- Seasonings (AREA)
Abstract
The invention relates to a alhagi sparsifolia extract, a preparation method and application thereof, wherein the extract is prepared by the following steps: taking alhagi sparsifolia as a raw material for extraction, concentrating the extracted extracting solution, precipitating, removing impurities, concentrating in vacuum, and aging to obtain the alhagi sparsifolia extract. The alhagi sparsifolia extract is added to tobacco, so that the natural fragrance of the tobacco can be improved, the smoking quality of cigarettes and the aroma quality of tobacco can be improved, smoke can be softened, and throat can be comfortable; has the function of treating pharyngitis. The alhagi sparsifolia extract is mainly used as an additive of a tobacco product in two aspects of feeding and flavoring in the cigarette manufacturing process. The results of multiple tests and practical applications carried out on several types of tobacco show that: the alhagi sparsifolia extract is suitable for being used as an additive of various tobacco products, and has obvious effects of improving the fragrance quality of tobacco, softening smoke and comforting throat.
Description
Technical field
The present invention relates to a kind of Alhagi sparsifolia extract, the process for extracting that also relates to a kind of this Alhagi sparsifolia extract simultaneously with and as the application of spices aspect, relate in particular to its application as the tobacco aromatics using aspect.
Background technology
Camel thorn is the general designation that the pulse family camel thorn belongs to (Alhagi) several plant, and main product is in Xinjiang, and camel thorn is a per nnial herb, stem branch green or greyish-green, and complete stool has the needle-like thorn, opens the red-purple papilionaceous flower.Camel thorn is very important feeding, medicinal and nectariferous plant.Camel thorn plants can be the single dominant kind and forms group, also can with middle life or drought in give birth to salt tolerant drought-enduring plant such as reed, draft such as Zhang Mao, colored bavin, black fruit lyceum, fetters willow, diversiform-leaved poplar, shrub, half arbor and arbor constitute group.Traditionally among the people, to mix life and all be referred to as camel thorn group with camel thorn with the common group that forms of other plant of camel thorn equal advantage, such group has the view of camel thorn.Camel thorn group mainly is grown in the saline meadow environment of lowland, Plain, is one of representative group of non-regional intrazonal vegetation, and camel thorn is to have to utilize herbage, herbal medicine that is worth and the economic plants of checking winds and fixing drifting sand.Contain crude protein 9.37%, crude fat 2.20%, robust fibre 16.74%, no nitrogen leaching 57.49%, ash content 8.9%, Ca 1.12%, P 0.072% in the camel thorn; The seed oil content of camel thorn is high; The content of edible, especially unsaturated fatty acids is high especially; Among the peoplely also camel thorn is used to treat rheumatism and cancer.Its pharmaceutical research proves: give mouse camel thorn ethanol extraction repeatedly, the effect that suppresses the growth of transplantability tumor cell of liver is arranged.
Summary of the invention
The object of the present invention is to provide a kind of can be as the Alhagi sparsifolia extract of natural plant pefume.
Simultaneously, the present invention also aims to provide a kind of preparation method of this Alhagi sparsifolia extract.
Further, the present invention also aims to provide a kind of Alhagi sparsifolia extract in the application aspect spices.
To achieve these goals; Technical scheme of the present invention has adopted a kind of Alhagi sparsifolia extract, and this extract is got by following method preparation: be raw material with the camel thorn, extract; Extracting solution after extracting is concentrated, precipitates removal of impurities, vacuum concentration, ageing, make Alhagi sparsifolia extract.
Described Alhagi sparsifolia extract is specifically by the preparation of following method and get: being raw material with the camel thorn, is extraction agent with the aqueous ethanolic solution, and solid-liquid ratio is 1: (6-9), and 80 ℃-85 ℃ temperature refluxed 7-9 hour; It is 6 ° of F-8 ° of F that extracting solution is evaporated to degree Beaume after filtering, and liquid concentrator dissolves with the ethanol of 2-4 times of volume ratio, and temperature is controlled at 15-25 ℃; Sedimentation is spent the night, and inclines to supernatant, discards lower floor's chlorophyll and impurity; Vacuum concentration supernatant to degree Beaume is 8 ° of F-10 ° of F then, adds Ucar 35 or USP Kosher, and the finished product that concentrates out is after ageing; Shunting bottom clear liquid discards top impurity and promptly gets Alhagi sparsifolia extract.
The addition of said Ucar 35 or USP Kosher for through extraction separation last the 15%-20% of the product weight of degree Beaume when being 8 ° of F-10 ° of F.The purpose of adding Ucar 35 or USP Kosher mainly is to play water retention, to improve product steady dissolution property, flowability and to play the rot-resistant effect.
Simultaneously, technical scheme of the present invention has also adopted a kind of preparation method of Alhagi sparsifolia extract, may further comprise the steps: with the camel thorn is raw material, is extraction agent with the aqueous ethanolic solution, and solid-liquid ratio is 1: (6-9), and 80 ℃-85 ℃ temperature refluxed 7-9 hour; It is 6 ° of F-8 ° of F that extracting solution is evaporated to degree Beaume after filtering, and liquid concentrator dissolves with the ethanol of 2-4 times of volume ratio, and temperature is controlled at 15-25 ℃; Sedimentation is spent the night, and inclines to supernatant, discards lower floor's chlorophyll and impurity; Vacuum concentration supernatant to degree Beaume is 8 ° of F-10 ° of F then, adds Ucar 35 or USP Kosher, and the finished product that concentrates out is after ageing; Shunting bottom clear liquid promptly gets Alhagi sparsifolia extract.
Described aqueous ethanolic solution is that 95% ethanol and water are (6-8) with volume ratio by concentration: mixed (3-5) gets.
The addition of said Ucar 35 or USP Kosher for through extraction separation last the 15%-20% of the product weight of degree Beaume when being 8 ° of F-10 ° of F.
Say that further technical scheme of the present invention has also adopted a kind of Alhagi sparsifolia extract in the application aspect spices.
Specifically adopted the application of a kind of Alhagi sparsifolia extract aspect the preparation tobacco aromatics using.
The present invention is raw material with the camel thorn, makes Alhagi sparsifolia extract through extraction, concentrating under reduced pressure, deposition removal of impurities, vacuum concentration, after aged.Alhagi sparsifolia extract of the present invention is added on the tobacco, can improves the tobacco natural fragrance, improve the smoking property of cigarette quality and improve tobacco aroma matter, can also soft flue gas, comfortable throat; Effect with treatment pharyngitis.Alhagi sparsifolia extract is mainly used in the cigarette manufacturing processed reinforced with two aspects of perfuming as additive of tobacco product: the one, Alhagi sparsifolia extract and other material are made into feed liquid; The 2nd, Alhagi sparsifolia extract and other spices are deployed into perfuming liquid (essence) use.When Alhagi sparsifolia extract is applied in the spices, account for the 5-85% of spices gross weight, it can be used as the blending material, also can be used as independent a kind of spices and carries out perfuming.
The test of many times and the result of practical application of in the several types tobacco, carrying out show: the suitable additive of making all kinds tobacco product of Alhagi sparsifolia extract, and to improving tobacco aroma matter, soft flue gas, comfortable throat has than positive effect.
Effect on tobacco: the solution that Alhagi sparsifolia extract is diluted to 10% (weight ratio) with 70% edible ethanol; Get each 50g of flue-cured tobacco sample leaf group (according to 0.5% tobacco weight ratio), take by weighing the spirituous solution for preparing, evenly be sprayed at Ye Zuzhong with atomizer for medicine, control samples adopts 70% alcohol of same amount.The sample of handling well is airtight puts about 4h, the oven drying at low temperature tobacco, and cigarette is made by handwork; Smoke panel test through judging panel (more than each 6 people), smoke panel test and adopt single scoring, estimate from fragrance matter, perfume quantity, concentration, exquisiteness, the aspects such as gas, stimulation, pleasant impression of mixing of cigarette respectively.
Its odor type is blue or green odor type
Embodiment
Embodiment 1
The Alhagi sparsifolia extract of present embodiment is by the preparation of following method and get: being raw material with the camel thorn, was extraction agent with the aqueous ethanolic solution, and solid-liquid ratio is 1: 8,80 ℃ temperature refluxed 8 hours; Then extracting solution being evaporated to degree Beaume after filtering is 7 ° of F, and liquid concentrator dissolves with the ethanol of 3 times of volume ratios, and wherein concentration of ethanol is 95%; Temperature is controlled at 20 ℃, and sedimentation is spent the night, and inclines to supernatant; Discard lower floor's chlorophyll and impurity, vacuum concentration supernatant to degree Beaume is 9 ° of F then, adds Ucar 35; The finished product that concentrates out is after ageing, and shunting bottom clear liquid discards top impurity and promptly gets Alhagi sparsifolia extract.
Embodiment 2
The Alhagi sparsifolia extract of present embodiment is by the preparation of following method and get: being raw material with the camel thorn, was extraction agent with the aqueous ethanolic solution, and solid-liquid ratio is 1: 9,85 ℃ temperature refluxed 7 hours; It is 8 ° of F that extracting solution is evaporated to degree Beaume after filtering, and it is that 95% ethanol dissolves that liquid concentrator uses 4 times of volume by volume concentrations, and temperature is controlled at 25 ℃; Sedimentation is spent the night, and inclines to supernatant, discards lower floor's chlorophyll and impurity; Vacuum concentration supernatant to degree Beaume is 10 ° of F then, adds USP Kosher, and the finished product that concentrates out is after ageing; Shunting bottom clear liquid discards top impurity and promptly gets Alhagi sparsifolia extract.
Application implementation example 1
Alhagi sparsifolia extract of the present invention is applied to prepare on the spices, and the concrete component of spices is: 0.10 part of soft spices, 10.00 parts of Ucar 35,10.00 parts of careless imperial pearl fermented products, 35.00 parts of ethanol are moistened in 0.01 part of Sucus Mali pumilae, 0.45 part of geranyl acetone, 0.05 part of extra large red pieces juice concentrate, 0.15 part of extract of fermentation aromatic acid fruit, 0.80 part of linalool oxide, 0.20 part of the huge medicinal extract of chrysanthemum, 3.50 parts of Alhagi sparsifolia extracts, smart 2.00 parts of jujube, 3.50 parts of polymer brown things, 0.40 part of oak extract, low 8.00 parts of the volatile oil that boil of tobacco fermentation, elegant Tianjin 0.20 part of spices of profit, Tianjin; During preparation, the above-mentioned raw materials of each parts by weight is mixed, and thin up to 100.00 weight part gets product.
Application implementation example 2
The spices of present embodiment is got by the feedstock production of following parts by weight: 0.015 part of dorinone, 0.30 part of oxidation isophorone, 0.05 part of β-damascone, 5.00 parts of Alhagi sparsifolia extracts, 0.20 part of geranyl acetone, smart 5.00 parts of jujube, 2.00 parts of polymer brown things, 3.00 parts of Fructus Crataegi extracts, 10.00 parts of Ucar 35,40.00 parts of ethanol; During preparation, with the raw material uniform mixing of above-mentioned each parts by weight, and thin up to 100.00 weight part, get product.
It should be noted last that: above embodiment is only in order to explanation; And unrestricted technical scheme of the present invention; Although with reference to the foregoing description the present invention is specified, those of ordinary skill in the art should be appreciated that like the replacement that is equal to each raw material; And replace any modification or the part that do not break away from the spirit and scope of the present invention, and it all should be encompassed in the middle of the claim scope of the present invention.
Claims (7)
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| CN2008102315424A CN101768514B (en) | 2008-12-29 | 2008-12-29 | Alhagi sparsifolia extract and preparation method and application thereof |
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| CN101768514B true CN101768514B (en) | 2012-11-28 |
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Families Citing this family (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102058157A (en) * | 2011-01-19 | 2011-05-18 | 云南烟草科学研究院 | Application of oak chip extracting solution in Chinese-style cigarette |
| CN102178125B (en) * | 2011-05-06 | 2013-08-07 | 塔里木大学 | Mixed silage of Alhagi sparsifolia Shap. in initial bloom stage and Medicago Sativa in initial bloom stage and preparation method thereof |
| CN102204627B (en) * | 2011-05-06 | 2013-07-24 | 塔里木大学 | Mixed silage prepared from alhagi sparsifolia in branching stage and alfalfa and preparation method thereof |
| CN102178124B (en) * | 2011-05-06 | 2013-07-24 | 塔里木大学 | Fructicative-period alhagi sparsifolia and alfalfa mixed silage and preparation method thereof |
| CN102204626B (en) * | 2011-05-06 | 2013-07-24 | 塔里木大学 | Mixed silage of alhagi sparsifolia at full-bloom stage and alfalfa and preparation method thereof |
| CN102515942B (en) * | 2011-11-30 | 2013-10-23 | 新疆汇通旱地龙腐植酸有限责任公司 | Antitranspirant, and preparation and application thereof |
| CN102687903A (en) * | 2012-06-04 | 2012-09-26 | 云南烟草科学研究院 | Pomelo leaf extract and application thereof |
| CN103006754B (en) * | 2012-12-28 | 2014-11-26 | 新疆维吾尔自治区中药民族药研究所 | Manaplant alhagi extract and preparation method thereof |
| CN107653066A (en) * | 2017-09-28 | 2018-02-02 | 河南省新郑金叶香料有限公司 | A kind of cigarette radix glycyrrhizae aroma component and its extracting method and application |
| CN110179041A (en) * | 2019-05-09 | 2019-08-30 | 湖南川渝食品有限公司 | A kind of solid-state chafing dish bottom flavorings containing Alhagi sparsifolia extract |
| CN114502185B (en) * | 2019-10-03 | 2024-05-03 | 奥古尔·米尔扎尤索夫娜·穆萨哈诺娃 | Use of alhagi plant extracts (variants) |
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| CN101259159A (en) * | 2008-04-17 | 2008-09-10 | 中国科学院新疆理化技术研究所 | A kind of preparation method and application of camel thorn total flavonoids |
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