CN101670017B - Medicine combination for tonifying blood - Google Patents
Medicine combination for tonifying blood Download PDFInfo
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- CN101670017B CN101670017B CN2009103060126A CN200910306012A CN101670017B CN 101670017 B CN101670017 B CN 101670017B CN 2009103060126 A CN2009103060126 A CN 2009103060126A CN 200910306012 A CN200910306012 A CN 200910306012A CN 101670017 B CN101670017 B CN 101670017B
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Abstract
The invention discloses a medicine combination for tonifying blood and a preparation method thereof, which belongs to the technical field of medicines. The medicine combination comprises the following components: 11.5 to 15.5 g of iron porphyrin extract, 0.05 to 0.09 g of zinc sulfate, 0.7 to 1.3 g of jujube, 0.8 to 1.4 g of Chinese wolfberry, 0.7 to 1.3 g of hawthorn and 1.1 to 1.5 g of sugar. The medicine combination can effectively treat iron-deficiency anemia, and simultaneously has the functions of reinforcing middle, replenishing Qi, tonifying blood, promoting digestion and the like.
Description
Technical field
The invention belongs to medical technical field.
Background technology
Iron deficiency anemia is a Deficiency disease common among the crowd, and the haemachrome ferrous porphyrin is the most effective source of iron that supplies of iron deficiency anemia that domestic and international nutritionist is generally acknowledged.Containing a large amount of haemachrome in the animal blood powder, is the effectively nutrient substance of treatment iron deficiency anemia that world nutrition educational circles generally acknowledges, U.S. FDA approved in 1973 becomes to produce and use.Simultaneously, modern science studies have shown that rapid exsiccant tea tree ' s old leaf, silkworm excrement etc. contain a large amount of chlorophylls, extract chlorophyll with them, and ferrous iron is gone in complexation, forms iron pheophytin, and anemia is had significant curative effect.
Hemachrome extract and iron chlorophyll extract combined is prepared into the pharmaceutical composition that is used to enrich blood, and rarely has report in patent and document.
Summary of the invention
The objective of the invention is to address the above problem and a kind of pharmaceutical composition of enriching blood and preparation method thereof is provided.This pharmaceutical composition can effectively be treated iron deficiency anemia, has invigorating middle warmer, QI invigorating simultaneously, rises blood and function such as help digestion.
The technical solution adopted in the present invention is:
A kind of pharmaceutical composition that is used to enrich blood, the component of described pharmaceutical composition is: ferrous porphyrin extract 11.5～15.5g, zinc sulfate 0.05～0.09g, Fructus Jujubae 0.7～1.3g, Fructus Lycii 0.8～1.4g, Fructus Crataegi 0.7～1.3g and sugar 1.1～1.5g.
Preferably, the component of described pharmaceutical composition is: ferrous porphyrin extract 12.8～14.1g, zinc sulfate 0.06～0.08g, Fructus Jujubae 0.8～1.1g, Fructus Lycii 0.9～1.2g, Fructus Crataegi 0.8～1.2g and sugar 1.2～1.4g.
Preferably, the component of described pharmaceutical composition is: ferrous porphyrin extract 13.2～13.9g, zinc sulfate 0.07～0.078g, Fructus Jujubae 0.9～1.0g, Fructus Lycii 1.0～1.1g, Fructus Crataegi 0.9～1.1g and sugar 1.23～1.3g.
The concrete steps of this preparation of pharmaceutical compositions method are:
(1) preparation of ferrous porphyrin extract:
At first, get the animal blood powder, add water and carry out homogenate, boiled 8～15 minutes, cooling back is that 0.1～1% NaOH modulation pH value is 7～9 with mass percent, the hydrolyzed protein enzymatic solution of adding 2000～5000 units, mix homogeneously, hydrolysis under 30～50 ℃ of temperature adds ethanol to precipitation and does not show red, filter, with solution concentration to relative density is 1.05～1.20, adds ethanol once more and removes deproteinize, filters, it is 1.05～1.30 that filtrate is concentrated into relative density, obtains hemachrome extract;
Then, will contain chlorophyllous biomaterial and dry, use the ethanol lixiviate, extract chlorophyll, at 60～95 ℃ of concentrated recovered alcohols, regulating pH value with hydrochloric acid is 3～7, adds ferrous sulfate in 10: 1～10: 5 according to chlorophyll amount and iron ion amount, under boiled condition, generate iron pheophytin, precipitation is separated out, and excessive ferrous sulfate runs off with supernatant, and flushing is precipitated to the iron-free reactant salt repeatedly, carry out drying, obtain iron chlorophyll extract;
Be mixing in 1: 9～4: 6 with above-mentioned hemachrome extract and iron chlorophyll extract according to mass ratio at last, form the ferrous porphyrin extract;
(2) preparation of medicine juice extractum:
After Fructus Lycii, Fructus Jujubae and Fructus Crataegi mixing, decoct with water 1～4 hour, filter, medicinal residues decoct with water 0.5～2 hour again, and the waste extracting juice merges medicine juice, and being concentrated into relative density is 1.05～1.20, obtains medicine juice extractum
(3) preparation of pharmaceutical compositions:
Ferrous porphyrin extract and medicine juice extractum are mixed, add zinc sulfate and sugar, at room temperature dry, promptly obtain this pharmaceutical composition.
The present invention has the following advantages:
Production technology of the present invention is simple, production cost is low; This drug regimen mainly is made up of hemachrome extract and iron pheophytin thing, can effectively treat iron deficiency anemia, has invigorating middle warmer, QI invigorating simultaneously, rises blood and function such as help digestion.
Figure of description
Fig. 1 is the process chart of preparation method of the present invention.
The specific embodiment
Embodiment 1
The pharmaceutical composition that is used to enrich blood, the component of this pharmaceutical composition is: ferrous porphyrin extract 11.5g, zinc sulfate 0.09g, Fructus Jujubae 1.1g, Fructus Lycii 1.0g, Fructus Crataegi 0.9g and sugared 1.1g.
With reference to Fig. 1, the preparation method of this drug regimen is: the preparation of (1) ferrous porphyrin extract: at first, get the animal blood powder, add water and carry out homogenate, boiled 8 minutes, cooling back with mass percent be 1% NaOH to modulate pH value be 8, add the hydrolyzed protein enzymatic solution of 5000 units, mix homogeneously, hydrolysis under 30 ℃ of temperature, adding ethanol to precipitation and do not show red, filter, is 1.10 with solution concentration to relative density, add ethanol once more and remove deproteinize, filter, it is 1.05 that filtrate is concentrated into relative density, obtains hemachrome extract; Then, will contain chlorophyllous biomaterial and dry, use the ethanol lixiviate, extract chlorophyll, at 80 ℃ of concentrated recovered alcohols, regulating pH value with hydrochloric acid is 7, adds ferrous sulfate at 10: 5 according to chlorophyll amount and iron ion amount, under boiled condition, generate iron pheophytin, precipitation is separated out, and excessive ferrous sulfate runs off with supernatant, and flushing is precipitated to the iron-free reactant salt repeatedly, carry out drying, obtain iron chlorophyll extract; Be mixing in 1: 9 with above-mentioned hemachrome extract and iron chlorophyll extract according to mass ratio at last, form the ferrous porphyrin extract; (2) preparation of medicine juice extractum: after Fructus Lycii, Fructus Jujubae and Fructus Crataegi mixing, decoct with water 1 hour, filter, medicinal residues decoct with water 2 hours again, and the waste extracting juice merges medicine juice, and being concentrated into relative density is 1.20, obtains medicine juice extractum; (3) preparation of pharmaceutical compositions: ferrous porphyrin extract and medicine juice extractum are mixed, add zinc sulfate and sugar, at room temperature dry, promptly obtain this pharmaceutical composition.
Embodiment 2
The pharmaceutical composition that is used to enrich blood, the component of this pharmaceutical composition is: ferrous porphyrin extract 12.8g, zinc sulfate 0.078g, Fructus Jujubae 0.7g, Fructus Lycii 1.4g, Fructus Crataegi 0.8g and sugared 1.4g.
With reference to Fig. 1, the preparation method of this drug regimen is: the preparation of (1) ferrous porphyrin extract: at first, get the animal blood powder, add water and carry out homogenate, boiled 15 minutes, cooling back with mass percent be 0.1% NaOH to modulate pH value be 7, add the hydrolyzed protein enzymatic solution of 2000 units, mix homogeneously, hydrolysis under 50 ℃ of temperature, adding ethanol to precipitation and do not show red, filter, is 1.05 with solution concentration to relative density, add ethanol once more and remove deproteinize, filter, it is 1.30 that filtrate is concentrated into relative density, obtains hemachrome extract; Then, will contain chlorophyllous biomaterial and dry, use the ethanol lixiviate, extract chlorophyll, at 60 ℃ of concentrated recovered alcohols, regulating pH value with hydrochloric acid is 3, adds ferrous sulfate at 10: 1 according to chlorophyll amount and iron ion amount, under boiled condition, generate iron pheophytin, precipitation is separated out, and excessive ferrous sulfate runs off with supernatant, and flushing is precipitated to the iron-free reactant salt repeatedly, carry out drying, obtain iron chlorophyll extract; Be mixing in 4: 6 with above-mentioned hemachrome extract and iron chlorophyll extract according to mass ratio at last, form the ferrous porphyrin extract; (2) preparation of medicine juice extractum: after Fructus Lycii, Fructus Jujubae and Fructus Crataegi mixing, decoct with water 4 hours, filter, medicinal residues decoct with water 0.5 hour again, and the waste extracting juice merges medicine juice, and being concentrated into relative density is 1.05, obtains medicine juice extractum; (3) preparation of pharmaceutical compositions: ferrous porphyrin extract and medicine juice extractum are mixed, add zinc sulfate and sugar, at room temperature dry, promptly obtain this pharmaceutical composition.
Embodiment 3
The pharmaceutical composition that is used to enrich blood, the component of this pharmaceutical composition is: ferrous porphyrin extract 13.2g, zinc sulfate 0.05g, Fructus Jujubae 0.8g, Fructus Lycii 0.9g, Fructus Crataegi 1.1g and sugared 1.23g.
With reference to Fig. 1, the preparation method of this drug regimen is: the preparation of (1) ferrous porphyrin extract: at first, get the animal blood powder, add water and carry out homogenate, boiled 12 minutes, cooling back with mass percent be 0.5% NaOH to modulate pH value be 9, add the hydrolyzed protein enzymatic solution of 3500 units, mix homogeneously, hydrolysis under 40 ℃ of temperature, adding ethanol to precipitation and do not show red, filter, is 1.20 with solution concentration to relative density, add ethanol once more and remove deproteinize, filter, it is 1.20 that filtrate is concentrated into relative density, obtains hemachrome extract; Then, will contain chlorophyllous biomaterial and dry, use the ethanol lixiviate, extract chlorophyll, at 95 ℃ of concentrated recovered alcohols, regulating pH value with hydrochloric acid is 5, adds ferrous sulfate at 10: 2 according to chlorophyll amount and iron ion amount, under boiled condition, generate iron pheophytin, precipitation is separated out, and excessive ferrous sulfate runs off with supernatant, and flushing is precipitated to the iron-free reactant salt repeatedly, carry out drying, obtain iron chlorophyll extract; Be mixing in 1: 8 with above-mentioned hemachrome extract and iron chlorophyll extract according to mass ratio at last, form the ferrous porphyrin extract; (2) preparation of medicine juice extractum: after Fructus Lycii, Fructus Jujubae and Fructus Crataegi mixing, decoct with water 2.5 hours, filter, medicinal residues decoct with water 1 hour again, and the waste extracting juice merges medicine juice, and being concentrated into relative density is 1.18, obtains medicine juice extractum; (3) preparation of pharmaceutical compositions: ferrous porphyrin extract and medicine juice extractum are mixed, add zinc sulfate and sugar, at room temperature dry, promptly obtain this pharmaceutical composition.
Embodiment 4
The pharmaceutical composition that is used to enrich blood, the component of this pharmaceutical composition is: ferrous porphyrin extract 15.5g, zinc sulfate 0.06g, Fructus Jujubae 1.0g, Fructus Lycii 1.1g, Fructus Crataegi 0.7g and sugared 1.5g.
With reference to Fig. 1, the preparation method of this drug regimen is: the preparation of (1) ferrous porphyrin extract: at first, get the animal blood powder, add water and carry out homogenate, boiled 8 minutes, cooling back with mass percent be 0.5% NaOH to modulate pH value be 7, add the hydrolyzed protein enzymatic solution of 2000 units, mix homogeneously, hydrolysis under 50 ℃ of temperature, adding ethanol to precipitation and do not show red, filter, is 1.15 with solution concentration to relative density, add ethanol once more and remove deproteinize, filter, it is 1.20 that filtrate is concentrated into relative density, obtains hemachrome extract; Then, will contain chlorophyllous biomaterial and dry, use the ethanol lixiviate, extract chlorophyll, at 60 ℃ of concentrated recovered alcohols, regulating pH value with hydrochloric acid is 7, adds ferrous sulfate at 10: 3 according to chlorophyll amount and iron ion amount, under boiled condition, generate iron pheophytin, precipitation is separated out, and excessive ferrous sulfate runs off with supernatant, and flushing is precipitated to the iron-free reactant salt repeatedly, carry out drying, obtain iron chlorophyll extract; Be mixing in 1: 9 with above-mentioned hemachrome extract and iron chlorophyll extract according to mass ratio at last, form the ferrous porphyrin extract; (2) preparation of medicine juice extractum: after Fructus Lycii, Fructus Jujubae and Fructus Crataegi mixing, decoct with water 4 hours, filter, medicinal residues decoct with water 2 hours again, and the waste extracting juice merges medicine juice, and being concentrated into relative density is 1.20, obtains medicine juice extractum; (3) preparation of pharmaceutical compositions: ferrous porphyrin extract and medicine juice extractum are mixed, add zinc sulfate and sugar, at room temperature dry, promptly obtain this pharmaceutical composition.
Embodiment 5
The pharmaceutical composition that is used to enrich blood, the component of this pharmaceutical composition is: ferrous porphyrin extract 14.1g, zinc sulfate 0.07g, Fructus Jujubae 1.3g, Fructus Lycii 0.8g, Fructus Crataegi 1.3g and sugared 1.2g.
With reference to Fig. 1, the preparation method of this drug regimen is: the preparation of (1) ferrous porphyrin extract: at first, get the animal blood powder, add water and carry out homogenate, boiled 15 minutes, cooling back with mass percent be 0.5% NaOH to modulate pH value be 9, add the hydrolyzed protein enzymatic solution of 5000 units, mix homogeneously, hydrolysis under 50 ℃ of temperature, adding ethanol to precipitation and do not show red, filter, is 1.15 with solution concentration to relative density, add ethanol once more and remove deproteinize, filter, it is 1.30 that filtrate is concentrated into relative density, obtains hemachrome extract; Then, will contain chlorophyllous biomaterial and dry, use the ethanol lixiviate, extract chlorophyll, at 95 ℃ of concentrated recovered alcohols, regulating pH value with hydrochloric acid is 7, adds ferrous sulfate at 10: 5 according to chlorophyll amount and iron ion amount, under boiled condition, generate iron pheophytin, precipitation is separated out, and excessive ferrous sulfate runs off with supernatant, and flushing is precipitated to the iron-free reactant salt repeatedly, carry out drying, obtain iron chlorophyll extract; Be mixing in 4: 6 with above-mentioned hemachrome extract and iron chlorophyll extract according to mass ratio at last, form the ferrous porphyrin extract; (2) preparation of medicine juice extractum: after Fructus Lycii, Fructus Jujubae and Fructus Crataegi mixing, decoct with water 2.5 hours, filter, medicinal residues decoct with water 22 hours again, and the waste extracting juice merges medicine juice, and being concentrated into relative density is 1.05, obtains medicine juice extractum; (3) preparation of pharmaceutical compositions: ferrous porphyrin extract and medicine juice extractum are mixed, add zinc sulfate and sugar, at room temperature dry, promptly obtain this pharmaceutical composition.
Embodiment 6
The pharmaceutical composition that is used to enrich blood, the component of this pharmaceutical composition is: ferrous porphyrin extract 13.9g, zinc sulfate 0.08g, Fructus Jujubae 0.9g, Fructus Lycii 1.2g, Fructus Crataegi 1.2g and sugared 1.3g.
With reference to Fig. 1, the preparation method of this drug regimen is: the preparation of (1) ferrous porphyrin extract: at first, get the animal blood powder, add water and carry out homogenate, boiled 15 minutes, cooling back with mass percent be 0.5% NaOH to modulate pH value be 7, add the hydrolyzed protein enzymatic solution of 2000 units, mix homogeneously, hydrolysis under 30 ℃ of temperature, adding ethanol to precipitation and do not show red, filter, is 1.15 with solution concentration to relative density, add ethanol once more and remove deproteinize, filter, it is 1.20 that filtrate is concentrated into relative density, obtains hemachrome extract; Then, will contain chlorophyllous biomaterial and dry, use the ethanol lixiviate, extract chlorophyll, at 95 ℃ of concentrated recovered alcohols, regulating pH value with hydrochloric acid is 7, adds ferrous sulfate at 10: 5 according to chlorophyll amount and iron ion amount, under boiled condition, generate iron pheophytin, precipitation is separated out, and excessive ferrous sulfate runs off with supernatant, and flushing is precipitated to the iron-free reactant salt repeatedly, carry out drying, obtain iron chlorophyll extract; Be mixing in 1: 9 with above-mentioned hemachrome extract and iron chlorophyll extract according to mass ratio at last, form the ferrous porphyrin extract; (2) preparation of medicine juice extractum: after Fructus Lycii, Fructus Jujubae and Fructus Crataegi mixing, decoct with water 2 hours, filter, medicinal residues decoct with water 1.5 hours again, and the waste extracting juice merges medicine juice, and being concentrated into relative density is 1.05, obtains medicine juice extractum; (3) preparation of pharmaceutical compositions: ferrous porphyrin extract and medicine juice extractum are mixed, add zinc sulfate and sugar, at room temperature dry, promptly obtain this pharmaceutical composition.
Embodiment 7
Pharmaceutical composition in the foregoing description can be made graininess, capsule shape or tablet shape.The pharmaceutical composition that is used to enrich blood that adopts above-mentioned any embodiment to make can effectively be treated iron deficiency anemia after taking for a long time, strengthens body immunity.
It should be noted last that, above embodiment is only unrestricted in order to technical scheme of the present invention to be described, although the present invention is had been described in detail with reference to preferred embodiment, those of ordinary skill in the art is to be understood that, can make amendment or be equal to replacement technical scheme of the present invention, and not breaking away from the spirit and scope of technical solution of the present invention, it all should be encompassed in the middle of the claim scope of the present invention.
Claims (3)
1. pharmaceutical composition that is used to enrich blood, it is characterized in that the component of making described pharmaceutical composition is: ferrous porphyrin extract 11.5～15.5g, zinc sulfate 0.05～0.09g, Fructus Jujubae 0.7～1.3g, Fructus Lycii 0.8～1.4g, Fructus Crataegi 0.7～1.3g and sugar 1.1～1.5g; The preparation method of said composition is:
(1) preparation of ferrous porphyrin extract:
At first, get the animal blood powder, add water and carry out homogenate, boiled 8～15 minutes, cooling back is that 0.1～1% NaOH modulation pH value is 7～9 with mass percent, the hydrolyzed protein enzymatic solution of adding 2000～5000 units, and mix homogeneously is 30～50
oHydrolysis under the C temperature adds ethanol to precipitation and does not show red, filters, and be 1.05～1.20 with solution concentration to relative density, add ethanol once more and remove deproteinize, to filter, it is 1.05～1.30 that filtrate is concentrated into relative density, obtains hemachrome extract;
Then, will contain chlorophyllous biomaterial and dry, use the ethanol lixiviate, extract chlorophyll, 60～95
oC concentrates recovered alcohol, regulating pH value with hydrochloric acid is 3～7, add ferrous sulfate according to chlorophyll amount and iron ion amount 10:1～10:5, under boiled condition, generate iron pheophytin, precipitation is separated out, and excessive ferrous sulfate runs off with supernatant, and flushing is precipitated to the iron-free reactant salt repeatedly, carry out drying, obtain iron chlorophyll extract;
Be that 1:9～4:6 mixes with above-mentioned hemachrome extract and iron chlorophyll extract according to mass ratio at last, form the ferrous porphyrin extract;
(2) preparation of medicine juice extractum:
After Fructus Lycii, Fructus Jujubae and Fructus Crataegi mixing, decoct with water 1～4 hour, filter, medicinal residues decoct with water 0.5～2 hour again, and the waste extracting juice merges medicine juice, and being concentrated into relative density is 1.05～1.20, obtains medicine juice extractum;
(3) preparation of pharmaceutical compositions:
Ferrous porphyrin extract and medicine juice extractum are mixed, add zinc sulfate and sugar, at room temperature dry, promptly obtain this pharmaceutical composition.
2. the pharmaceutical composition that is used to enrich blood according to claim 1, it is characterized in that the component of making described pharmaceutical composition is: ferrous porphyrin extract 12.8～14.1g, zinc sulfate 0.06～0.08g, Fructus Jujubae 0.8～1.1g, Fructus Lycii 0.9～1.2g, Fructus Crataegi 0.8～1.2g and sugar 1.2～1.4g.
3. the pharmaceutical composition that is used to enrich blood according to claim 1, it is characterized in that the component of making described pharmaceutical composition is: ferrous porphyrin extract 13.2～13.9g, zinc sulfate 0.07～0.078g, Fructus Jujubae 0.9～1.0g, Fructus Lycii 1.0～1.1g, Fructus Crataegi 0.9～1.1g and sugar 1.23～1.3g.
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| CN2009103060126A CN101670017B (en) | 2009-08-25 | 2009-08-25 | Medicine combination for tonifying blood |
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| CN2009103060126A CN101670017B (en) | 2009-08-25 | 2009-08-25 | Medicine combination for tonifying blood |
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| CN101670017B true CN101670017B (en) | 2011-05-18 |
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| CN103638529A (en) * | 2013-12-16 | 2014-03-19 | 红桃开集团股份有限公司 | Preparation method of medicament for enriching blood |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1112006A (en) * | 1994-09-10 | 1995-11-22 | 谭世平 | Tonic instant medicine granules for treatment of anaemia, asthenia and deterioration of functions of organs, and its preparing method |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1112006A (en) * | 1994-09-10 | 1995-11-22 | 谭世平 | Tonic instant medicine granules for treatment of anaemia, asthenia and deterioration of functions of organs, and its preparing method |
Non-Patent Citations (1)
| Title |
|---|
| 湘夷.女性补血 永驻新颜.《中国健康月刊》.2004,(第2期),92-96. * |
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