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CN101619282B - Preparation method of mulberry dry red wine - Google Patents

Preparation method of mulberry dry red wine Download PDF

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CN101619282B
CN101619282B CN2009101017579A CN200910101757A CN101619282B CN 101619282 B CN101619282 B CN 101619282B CN 2009101017579 A CN2009101017579 A CN 2009101017579A CN 200910101757 A CN200910101757 A CN 200910101757A CN 101619282 B CN101619282 B CN 101619282B
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mulberry
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CN101619282A (en
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陈祖满
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Zhejiang Pharmaceutical College
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Ningbo Tiangong Fazenda Fruit Juice & Fruit Wine Co ltd
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Abstract

The invention discloses a preparation method of mulberry dry red wine, which comprises the following steps: selecting and cleaning fresh mulberries, crushing mulberries, juicing, sterilizing, adjusting components, fermenting, pouring, ageing, clarifying, filtering, blending, cold treating, filtering, returning to the temperature and filtering by a membrane. The mulberry dry red wine prepared by the invention belongs to high-grade consumer goods, the added value of the product is high, so that the higher commercial value of the mulberry can be fully reflected, and the juice is squeezed by adopting a vacuum air bag in the juice squeezing step, so that the phenomenon that the heat generated in the subsequent fermentation process is difficult to dissipate due to the existence of mulberry fruit peel and the wine is acidified is effectively avoided; moreover, the maximum juice yield of the mulberry is further ensured, raw materials are fully utilized, the manufacturing cost is reduced, and the quality of the final mulberry dry red wine is improved.

Description

桑果干红酒的制备方法The preparation method of mulberry dry red wine

技术领域 technical field

本发明涉及桑果汁加工技术领域,具体涉及一种桑果干红酒的制备方法。The invention relates to the technical field of mulberry fruit juice processing, in particular to a preparation method of mulberry fruit dry red wine.

背景技术 Background technique

桑果,又称桑葚,其营养非常丰富,含有葡萄糖、维生素和各种氨基酸,对人体健康非常有利。目前,由于桑果的季节性很强,多以实用新鲜桑果为主,为了延长桑果的食用期限,现在市场上出现了不少的桑果酒饮品,受到消费者的喜爱。Mulberry, also known as mulberry, is very nutritious and contains glucose, vitamins and various amino acids, which are very beneficial to human health. At present, due to the strong seasonality of mulberry fruit, most of them are practical and fresh mulberry fruit. In order to prolong the edible period of mulberry fruit, many mulberry fruit wine drinks have appeared on the market now, which are loved by consumers.

但是,现有市场上的桑果酒,配方相对复杂,如食品科学,1997,Vol 18,No5中,董玉新发表的《桑果酒的研制》,介绍了在桑果汁中加入枣花蜂蜜、砂糖、柠檬酸等综合调配而成,属于配制酒,桑果原汁含量低,缺少桑果产品的天然风味和营养,多定价为中、低端消费品,因此,产品附加值低,不能充分体现桑果的商业价值。But, the mulberry fruit wine on the existing market, formula is relatively complicated, as food science, 1997, Vol 18, among No5, " the development of mulberry fruit wine " that Dong Yuxin publishes, has introduced in mulberry fruit juice and adds jujube flower honey, granulated sugar, lemon It belongs to the blended wine. The content of mulberry juice is low, which lacks the natural flavor and nutrition of mulberry products. Most of them are priced as medium and low-end consumer goods. Therefore, the added value of the product is low and cannot fully reflect the mulberry fruit. commercial value.

而且,在现有桑果酒的制备过程中,有的将粉碎后的桑果直接进行发酵,如申请号为200810044833.2的专利申请文件《一种生产桑椹果酒的方法及产品》,就是将桑果粉碎后直接发酵,但在产业化过程中处理不好,容易出现桑果酒酸败现象,导致酒的变质败坏;粉碎后的桑果中含有大量的桑果皮,桑果皮中存在大量的原始杂菌会引起后续发酵工序中产生的热量散发困难,杂菌得以迅速生长,使酒酸败,则整批桑果就要丢弃,造成原料的大量浪费,并增加制作成本,同时污染整个生产环境,影响后续生产。且现有的桑果酒在澄清处理工序中处理不当,工艺不成熟,会导致澄清效果不理想,有时在保质期内也会出现浑浊和沉淀等现象,严重影响桑果酒的销售。And in the preparation process of existing mulberry fruit wine, what have will directly ferment the mulberry fruit after the pulverization, as the patent application document " a kind of method and product of producing mulberry fruit wine " that application number is 200810044833.2, exactly mulberry fruit is pulverized Afterwards, it is directly fermented, but if it is not properly handled in the industrialization process, the phenomenon of rancidity of mulberry wine is prone to occur, resulting in deterioration of the wine; the crushed mulberry contains a large amount of mulberry peel, and there is a large amount of original miscellaneous bacteria in the mulberry peel that will cause The heat generated in the subsequent fermentation process is difficult to dissipate, and the bacteria can grow rapidly, making the wine rancid, and the whole batch of mulberries will be discarded, resulting in a large waste of raw materials, increasing production costs, polluting the entire production environment, and affecting subsequent production. And the existing mulberry wine is improperly handled in the clarification process, and the technology is immature, which can cause the clarification effect to be unsatisfactory, and phenomena such as turbidity and precipitation also occur during the shelf life sometimes, which has a strong impact on the sales of mulberry wine.

发明内容 Contents of the invention

本发明要解决的技术问题,是针对现有技术的上述不足,提供一种产品附加值高,能充分体现桑果更高商业价值,且能充分利用原材料、制作成本低的桑果干红酒的制备方法。The technical problem to be solved by the present invention is to provide a product with high added value, which can fully reflect the higher commercial value of mulberry fruit, and can make full use of raw materials and low production cost. method of preparation.

为了解决上述技术问题,本发明的技术方案为:一种桑果干红酒的制备方法,其制备工艺流程如下:In order to solve the above-mentioned technical problems, the technical scheme of the present invention is: a kind of preparation method of mulberry fruit dry red wine, and its preparation technological process is as follows:

(1)新鲜桑果的挑选和清洗;(1) selection and cleaning of fresh mulberries;

(2)破碎:将挑选、清洗后的桑果进行破碎,破碎至整果的1/8~1/4;(2) Crushing: crush the selected and cleaned mulberries to 1/8 to 1/4 of the whole fruit;

(3)榨汁:对破碎后的桑果进行榨汁,得到桑果汁;(3) Juicing: squeeze the crushed mulberry fruit to obtain mulberry juice;

(4)杀菌:温度110~121℃,时间3~6秒;(4) Sterilization: temperature 110-121°C, time 3-6 seconds;

(5)成份调整:向杀菌后的桑果汁中添加白砂糖,加入重量百分比以桑果汁计为7%~12%的白砂糖,以使得桑果汁的总糖含量为200~230g/L,添加亚硫酸至SO2含量:60~80ppm;(5) Ingredient adjustment: add white granulated sugar in the mulberry fruit juice after sterilization, add the white granulated sugar of 7%~12% by weight percentage with mulberry fruit juice, so that the total sugar content of mulberry fruit juice is 200~230g/L, add Sulfurous acid to SO2 content: 60-80ppm;

(6)发酵:成份调整完后,加入酵母,酵母与桑果汁重量比为1~1.5∶10000,控制温度在10~25℃,发酵时间5~10天;(6) Fermentation: After adjusting the ingredients, add yeast, the weight ratio of yeast to mulberry juice is 1-1.5:10000, control the temperature at 10-25°C, and ferment for 5-10 days;

(7)倒灌:发酵结束后,将沉淀在酒罐底部的果泥与杂物分离得到原酒;(7) Back pouring: after the fermentation is finished, the fruit puree and sundries deposited at the bottom of the wine tank are separated to obtain raw wine;

(9)陈酿:将原酒转入陈酿罐中,在10~20℃温度条件下,存放半年以上;(9) Aging: transfer the original wine into the aging tank, and store it for more than half a year at a temperature of 10-20°C;

(10)澄清:向陈酿结束后的原酒中加入澄清剂搅拌均匀,然后静置5~10天进行澄清;(10) clarification: add clarifier to the original wine after aging and stir evenly, then let stand for 5 to 10 days to clarify;

(11)过滤:将澄清后的原酒,用硅澡土过滤机过滤;(11) Filtration: filter the clarified raw wine with a silicon bath soil filter;

(12)勾兑:将不同批次的原酒按产量比例进行整体勾兑,使酒品质风味一致,同时补充亚硫酸使得SO2含量至60~100ppm;(12) Blending: Blend different batches of original wine according to the production ratio to make the quality and flavor of the wine consistent, and at the same time add sulfurous acid to make the SO2 content reach 60-100ppm;

(13)冷处理:将勾兑好的原酒在-2~2℃条件下,存放7~10天;(13) Cold treatment: store the blended raw wine for 7 to 10 days at -2 to 2°C;

(14)过滤:将冷处理结束后的酒,用纸板进行过滤;(14) Filtration: filter the wine after cold treatment with cardboard;

(15)回温:将过滤后的酒,回复到常温;(15) Return to temperature: return the filtered wine to normal temperature;

(16)膜过滤:采用微孔膜过滤器对回温后的酒进行过滤。(16) Membrane filtration: use a microporous membrane filter to filter the wine after returning to temperature.

本发明上述的榨汁,采用意大利西柏梅公司生产VS150真空气囊压榨机榨汁。The above-mentioned juice extraction of the present invention adopts the VS150 vacuum air bag press machine produced by Italy Xibaimei Company to extract juice.

上述步骤(10)中所述的澄清剂为占桑果原酒总量的重量百分比为:0.1~0.6%的皂土和0.1~1.0%的壳聚糖。The clarifying agent described in the above step (10) is 0.1-0.6% of bentonite and 0.1-1.0% of chitosan in the weight percent of the total amount of mulberry fruit wine.

上述步骤(14)中的用纸板进行过滤为采用板框纸板过滤机进行过滤。Filtrating with cardboard in the above step (14) is filtering with a plate-and-frame cardboard filter.

本发明的桑果干红酒的制备方法,它还包括膜过滤后的灌装、封口。The preparation method of the mulberry dry red wine of the present invention also includes filling and sealing after membrane filtration.

本发明的优点:1.本发明制备的桑果干红酒,桑果汁含量高,属于高品位消费品,产品附加值高,从而能充分体现桑果更高的商业价值。Advantages of the present invention: 1. The mulberry fruit dry red wine prepared by the present invention has high mulberry juice content, belongs to high-grade consumer goods, and has high added value of the product, thereby fully reflecting the higher commercial value of mulberry fruit.

2.本发明在桑果干红酒的制备方法中,采用意大利西柏梅公司生产VS150真空气囊压榨机榨汁,从而有效地避免了桑果压榨过程中引起的果汁氧化,以及桑果果皮的存在而引起的后续发酵过程中产生的热量散发困难,使酒酸化的现象;而且,更进一步地保证了桑果的最大出汁率,(桑果出汁率达70~80%,比现有技术的出汁率高约5~10%)并减少了桑果汁固有的苦味和涩味,因此,充分利用了原材料、降低了制作成本,提高了最终桑果干红酒的品质。2. In the preparation method of mulberry dry red wine, the present invention adopts the VS150 vacuum air bag press machine produced by Italy Xibaimei Company to squeeze the juice, thereby effectively avoiding the fruit juice oxidation caused in the mulberry squeezing process and the existence of mulberry peel And the heat that produces in the follow-up fermentation process that causes is distributed difficulty, makes the phenomenon of wine acidification; And, further guaranteed the maximum juice yield of mulberry fruit, (the juice yield of mulberry fruit reaches 70~80%, is higher than the juice of prior art The rate is about 5~10% higher) and has reduced the inherent bitterness and astringency of mulberry fruit juice, therefore, has fully utilized raw material, has reduced production cost, has improved the quality of final mulberry fruit dry red wine.

3.本发明的桑果干红酒的制备方法中,澄清工序采用加入占原酒总量的0.1%~0.6%的皂土和0.1%~1.0%的壳聚糖进行澄清,与传统的用单一皂土进行澄清的工序相比,澄清后所得产品更透明有光泽(澄清后的原酒的透光率达70%以上),且无浑浊和沉淀现象,产品的品质更加稳定。3. in the preparation method of mulberry fruit dry red wine of the present invention, clarification process adopts adding and accounts for the bentonite of 0.1%~0.6% of former wine total amount and the chitosan of 0.1%~1.0% to carry out clarification, and traditional single Compared with the process of clarifying with bentonite, the product obtained after clarification is more transparent and shiny (the light transmittance of the original wine after clarification reaches more than 70%), and there is no turbidity and precipitation phenomenon, and the quality of the product is more stable.

4.本发明采用先对桑果进行破碎,然后再压榨取汁,破碎工序对桑果首先进行了细化,更有利于后续压榨过程的桑果出汁。4. The present invention first crushes the mulberries, and then squeezes them to extract juice. The crushing process first refines the mulberries, which is more conducive to the subsequent squeezing process of the mulberry juices.

5.本发明采用将桑果汁先进行超高温瞬时(UHT)杀菌,再发酵,既保持了桑果的营养和天然风味,又有效避免了桑果酒的酸败现象。5. The present invention adopts that the mulberry fruit juice is first subjected to ultra-high temperature instantaneous (UHT) sterilization, and then fermented, which not only maintains the nutrition and natural flavor of the mulberry fruit, but also effectively avoids the rancidity of the mulberry fruit wine.

6.本产品在加工过程中不添加防腐剂、香精和色素,为天然健康食品。满足出口和人们对天然食品的需求。6. This product does not add preservatives, flavors and pigments during processing, and is a natural and healthy food. To meet the export and people's demand for natural food.

具体实施方式 Detailed ways

下面通过具体实施方式,对本发明做进一步详细描述,但本发明不仅仅局限于以下实施例。The present invention will be described in further detail below through specific embodiments, but the present invention is not limited to the following examples.

实施例1Example 1

桑果干红酒的制备:Preparation of mulberry dry red wine:

(1)新鲜桑果的挑选和清洗;首先挑选出九成熟,新鲜无异味的桑果,然后用清水清洗桑果,除去桑果上的泥沙、石子和表面微生物等,再挑出其中的树枝、杂物及霉烂果;(1) Selection and cleaning of fresh mulberries; first select nine-ripe, fresh and odorless mulberries, then wash the mulberries with clear water to remove silt, stones and surface microorganisms on the mulberries, and then pick out the mulberries. Branches, sundries and rotten fruit;

(2)破碎:然后对步骤(1)所得的桑果进行破碎,采用靖江前卫食品机械厂生产的TSZ-056型号的破碎机对整个桑果进行破碎,破碎至整果的1/8~1/4,目的是对整个桑果进行细化,以利于出汁;(2) Crushing: Then the mulberry fruit obtained in step (1) is broken, and the whole mulberry fruit is broken by using the crusher of the TSZ-056 model produced by Jingjiang Qianwei Food Machinery Factory until 1/8-1 of the whole fruit is crushed. /4, the purpose is to refine the whole mulberry fruit to facilitate juice production;

(3)榨汁:对步骤(2)所得的破碎后的桑果采用意大利西柏梅公司生产VS150真空气囊压榨机榨汁,最后得到桑果出汁率为80%的果汁;(3) Juicing: the mulberry fruit after the fragmentation of step (2) gained adopts the production of VS150 vacuum air bag squeezer to squeeze the juice from Italy Xibaimei Company, finally obtain the fruit juice with 80% mulberry fruit juice yield;

(4)杀菌:使用张家港新美星包装机械有限公司生产的UHT4000全自动瞬时杀菌机,在110~115℃,5~6秒条件下对步骤(3)所得的果汁进行杀菌,以杀灭料液中的杂菌;(4) Sterilization: Use the UHT4000 automatic instant sterilizer produced by Zhangjiagang Newamstar Packaging Machinery Co., Ltd. to sterilize the juice obtained in step (3) at 110-115°C for 5-6 seconds to kill the feed liquid bacteria in

(5)成份调整:向杀菌后的桑果汁中添加白砂糖,加入重量百分比以桑果汁计为8%的白砂糖,添加亚硫酸使得SO2含量至:65ppm(采用GB/T15038-2006中的SO2检测方法进行检测);SO2加入目的主要是抑制杂菌生长,但不抑制酵母生长;(5) Ingredient adjustment: add white granulated sugar in the mulberry fruit juice after sterilization, add the white granulated sugar that the weight percentage is 8% with mulberry fruit juice, add sulfurous acid and make SO Content to: 65ppm (adopting in GB/T15038-2006 SO 2 detection method for detection); the purpose of adding SO 2 is mainly to inhibit the growth of miscellaneous bacteria, but not to inhibit the growth of yeast;

(6)发酵:在成份调整完后,按照酵母与桑果汁重量比为1.5∶10000加入酵母,控制温度在20℃,发酵时间6天,测定其中总糖含量小于4.0g/L,视为发酵结束;(6) Fermentation: After adjusting the ingredients, add yeast according to the weight ratio of yeast and mulberry juice of 1.5:10000, control the temperature at 20°C, and ferment for 6 days. The total sugar content in it is determined to be less than 4.0g/L, which is regarded as fermentation Finish;

(7)倒灌:发酵结束后,将沉淀在酒罐底部的果泥与杂物分离除去得到原酒;(7) back pouring: after the fermentation is finished, the fruit puree and sundries deposited at the bottom of the wine tank are separated and removed to obtain raw wine;

(9)陈酿:将原酒转入陈酿罐中,在15℃温度条件下,存放半年以上;(9) Aging: transfer the original wine into the aging tank, and store it for more than half a year at a temperature of 15°C;

(10)澄清:向陈酿结束后的原酒中加入进行澄清剂搅拌均匀,加入占桑果原酒总量的0.6%的皂土和0.1%的壳聚糖,搅拌均匀,然后静止6天进行澄清;(10) clarification: in the original wine after aging, add and carry out clarifying agent and stir, add and account for 0.6% bentonite and 0.1% chitosan of mulberry original wine total amount, stir, stand still for 6 days to clarify then;

(11)过滤:将澄清后的原酒,采用扬州润明轻工机械厂生产的TSJ-016硅藻土机过滤,去除其中的浮物和杂物,使产品透明有光泽,无沉淀(经检测透光率达75%);(11) Filtration: The clarified original wine is filtered by a TSJ-016 diatomite machine produced by Yangzhou Runming Light Industry Machinery Factory to remove floating objects and sundries, so that the product is transparent and shiny without precipitation (after testing Light transmittance up to 75%);

(12)勾兑:将不同批次的原酒进行按产量进行整体勾兑,所述的将不同批次的原酒进行按产量进行整体勾兑可理解为:如以5天内生产的原酒为例:第一天生产50000kg,第二天生产40000kg,第三天生产50000kg,第四天生产20000kg,第五天生产60000kg,则五天的生产总量为220000kg,以勾兑100000kg酒为例,则取第一天的原酒量为(50000/220000)×100000kg、取第二天的原酒(40000/220000)×100000kg、取第三天的原酒(50000/220000)×100000kg、取第四天的原酒(20000/220000)×100000kg、取第五天的原酒(60000/220000)×100000kg,然后混合均匀,即勾兑完成,同时补充SO2含量至80ppm;(12) Blending: the overall blending of different batches of original wine according to the production volume can be understood as: taking the original wine produced within 5 days as an example: the first day Produce 50,000kg on the second day, 40,000kg on the second day, 50,000kg on the third day, 20,000kg on the fourth day, and 60,000kg on the fifth day, so the total production in the five days is 220,000kg. Taking the blending of 100,000kg wine as an example, the first day’s The amount of original wine is (50000/220000)×100000kg, take the original wine of the second day (40000/220000)×100000kg, take the original wine of the third day (50000/220000)×100000kg, take the original wine of the fourth day (20000/220000) × 100000kg, get the former wine (60000/220000) × 100000kg of the fifth day, then mix evenly, that is, the blending is completed, and supplement SO content to 80ppm;

(13)冷处理:将勾兑好的原酒在-2~2℃条件下,储存8天,增加酒的稳定性;(13) Cold treatment: store the blended raw wine at -2-2°C for 8 days to increase the stability of the wine;

(14)过滤:将冷处理结束后的酒,用板框纸板过滤机进行过滤,以去除酒中的杂物,(14) Filtration: filter the wine after the cold treatment with a plate-and-frame cardboard filter to remove impurities in the wine,

(15)回温:将过滤后的酒,回复到常温,以备灌装用;(15) Return to temperature: return the filtered wine to normal temperature for filling;

(16)膜过滤:利用温州沙城食品机械三厂生产的TSJ-012微孔膜过滤器对回温后的酒进行过滤,以除去其中的微生物;(16) Membrane filtration: use the TSJ-012 microporous membrane filter produced by Wenzhou Shacheng Food Machinery No. 3 Factory to filter the warmed wine to remove microorganisms therein;

(17)灌装、封口:将过滤好的酒灌入瓶中,并及时封口。(17) Filling and sealing: pour the filtered wine into the bottle and seal it in time.

实施例2Example 2

步骤(4)中采用在116~121℃,3~4秒的超高温瞬时处理杀菌;步骤(5)中成份调整,向杀菌后的桑果汁中添加白砂糖,加入重量百分比以桑果汁计为12%的白砂糖,添加亚硫酸使得SO2含量至:80ppm;步骤(10)中澄清:向陈酿结束后的原酒中加入进行澄清剂搅拌均匀,加入占桑果原酒总量的0.2%的皂土和0.8%的壳聚糖进行澄清;其他制备步骤同实施例1。Adopt in step (4) at 116~121 DEG C, 3~4 seconds ultra-high temperature instantaneous treatment sterilization; In step (5), component is adjusted, and white granulated sugar is added in the mulberry fruit juice after the sterilization, and adding weight percentage is counted as mulberry fruit juice 12% white granulated sugar, add sulfurous acid to make SO content to: 80ppm; clarification in the step (10): add clarification agent in the original wine after aging and stir evenly, add the soap that accounts for 0.2% of mulberry fruit original wine total amount Soil and 0.8% chitosan are clarified; other preparation steps are with embodiment 1.

Claims (4)

1. preparation method of mulberry dry red wine, it is characterized in that: its preparation technology's flow process is following:
(1) fresh sorosis selecting and cleaning;
(2) fragmentation: the sorosis after will selecting, cleaning carries out fragmentation, is crushed to 1/8~1/4 of whole fruit;
(3) squeeze the juice: the sorosis to after the fragmentation is squeezed the juice, and obtains Fructus Mori juice;
(4) sterilization: 110~121 ℃ of temperature, 3~6 seconds time;
(5) composition adjustment: add white sugar in the Fructus Mori juice after sterilization, add weight percent and count 7%~12% white sugar with Fructus Mori juice, the Fructus Mori juice total sugar content is reached: 220~230g/L adds sulfurous acid to SO 2Content: 60~80ppm;
(6) fermentation: after composition adjust, the adding yeast, yeast and Fructus Mori juice weight ratio are 1~1.5: 10000, controlled temperature is at 10~25 ℃, fermentation time 5~10 days;
(7) pour in down a chimney: after the fermentation ends, the puree that is deposited in the wine pot bottom separated obtaining former wine with foreign material;
(9) ageing: former wine is changed in the ageing jar, under 10~20 ℃ of temperature condition, deposit more than half a year;
(10) clarification: add finings in the former wine after ageing finishes and stir, leave standstill then and clarified in 5~10 days;
(11) filter: the former wine after will clarifying, filter with silicon bath soil filter;
(12) blend: the former wine of different batches is carried out integral body in the output ratio blend, make the wine quality and flavor consistent, replenish sulfurous acid simultaneously and make SO 2Content to 60~100ppm;
(13) deepfreeze: the former wine that will blend was deposited 7~10 days under-2~2 ℃ of conditions;
(14) filter: the wine after deepfreeze is finished, filter with cardboard;
(15) rise again: the wine after will filtering is returned to normal temperature;
(16) membrane filtration: adopt microporous membrane filters that the wine after rising again is filtered;
Finings in the said step (10) is bentonite and chitosan, and the weight percent that they account for former wine total amount is: bentonite 0.1%~0.6%, chitosan 0.1%~1.0%.
2. preparation method of mulberry dry red wine according to claim 1 is characterized in that: the squeezing the juice to adopting the vacuum Atmosphere Presser to squeeze the juice of said step (3).
3. preparation method of mulberry dry red wine according to claim 1 is characterized in that: being filtered into cardboard in the said step (14) adopts sheet frame cardboard filter machine to filter.
4. preparation method of mulberry dry red wine according to claim 1 is characterized in that: it also comprises can behind the membrane filtration, seals.
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