CN101445773B - Method for preparing fancy soap - Google Patents
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- CN101445773B CN101445773B CN 200810220380 CN200810220380A CN101445773B CN 101445773 B CN101445773 B CN 101445773B CN 200810220380 CN200810220380 CN 200810220380 CN 200810220380 A CN200810220380 A CN 200810220380A CN 101445773 B CN101445773 B CN 101445773B
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Abstract
The invention provides a method for preparing a fancy soap, comprising the steps as follows: (1) genuine soap, powdery polymer, lubricant additive, water, preservative, whitening agent and essence are prepared according to the proportion; (2) the water, the preservative and the whitening agent are uniformly mixed, thus gaining water solution; (3) the genuine soap and the water solution are added in a mixing pot and uniformly mixed; (4) the powdery polymer is added in the mixing pot and mixed uniformly; (5) the lubricant additive and the essence are uniformly mixed, added in the mixing pot and uniformly mixed, thus gaining the mixed material; (6) the mixed material is ground and extruded; (7) the mixed material gained in the step (6) is extruded to form bar-shaped articles by a single-screw extruder; (8) the bar-shaped articles are printed and cut into blocks. The method uses the powdery polymer to replace part of genuine soap so as to prepare the fancy soap, therefore, degreasing degree and stimulation of the fancy soap are reduced, the functions of the fancy soap such as foaming degree and decontamination, and the like are kept, the preparation cost of the fancy soap is reduced, and the fancy soap is environment friendly.
Description
Technical field
The present invention relates to a kind of manufacture method of perfumed soap, specifically, relate to a kind of manufacture method that is suitable for clean and the perfumed soap of taking a shower.
Background technology
At present common perfumed soap is all to make take the soap base that obtained after the sodium hydroxide saponification by plam oil, Oleum Cocois or animal grease as starting material, its degreasing dynamics is strong, alkalescence is strong, pungency to skin is very large, therefore usually be only suitable for for shower, and be not suitable for washing one's face, clean when removing ornaments and formal dress skin of face.
In addition, the soap base taste after the animal grease saponification is larger, and easily variable color, therefore generally adopts the plant soap base when producing.Continuous maturation along with biodiesel technology, plam oil, Oleum Cocois also become the main raw material(s) source of biofuel, these factors cause world market plam oil, coconut wet goods raw-material in short supply, and price significantly rises, so that the manufacturing cost of perfumed soap constantly rises.
Summary of the invention
Technical problem to be solved by this invention is to provide a kind of manufacture method of perfumed soap, the perfumed soap low cost of manufacture that this method is made, and both be suitable for taking a shower, be suitable for again clean.
The technical scheme that adopts is as follows:
A kind of manufacture method of perfumed soap is characterized in that comprising the steps:
(1) be equipped with following raw material by following weight ratio: soap base 20-70 part, powdery polymer 20-70 part, lubricating auxiliary agent 0-25 part, water 0-20 part, sanitas 0-1 part, whitening agent 0-5 part, essence 0-2 part;
(2) water and sanitas, whitening agent are mixed, obtain the aqueous solution;
(3) soap base is added agitator kettle, then the aqueous solution that step (2) is obtained adds agitator kettle, and be stirred to and mix;
(4) powdery polymer is added agitator kettle, and be stirred to and mix;
(5) lubricating auxiliary agent and essence are mixed, then add agitator kettle, and be stirred to and mix, obtain mixture;
(6) mixture that step (5) is obtained is milled, is pushed, and the various raw materials in mixture are further mixed;
(7) mixture that step (6) is obtained pushes by single screw extrusion machine, extrudes bar;
(8) print (can adopt the printer that is connected with cooling fluid to print) on the bar that step (7) is extruded, and carry out stripping and slicing, can obtain perfumed soap.
In preferred steps (1), the weight ratio of lubricating auxiliary agent is 5-15 part.
In preferred steps (7), the temperature of single screw extrusion machine die head is between 30 ℃ to 70 ℃.
The purpose of printing in step (8) is to make the perfumed soap surface have required word and/or pattern.
In preferred version, in order to make perfumed soap have shower, clean function in addition, for example, make perfumed soap have physical beauty hold or invigorate blood circulation, the functions such as whitening, tender skin, (as quartz sand powder, polypropylene powder, polyethylene powder, chrysanthemum sheet, walnut powder, ginseng powder or ginseng tablet, wherein the fineness of quartz sand powder, polypropylene powder and polyethylene powder is generally the 80-500 order preferably also to be equipped with functional additive in above-mentioned steps (1); These functional additives can use separately, also can compound use) 0.1-10 part; Increase step (3-2) between step (3) and step (4), functional additive is added agitator kettle, and be stirred to and mix.The above-mentioned functions additive does not change the original attribute of perfumed soap.
Above-mentioned soap base can adopt a kind of in plant soap base and animal soap base or both mixtures.The plant soap base can be obtained after the sodium hydroxide saponification by plam oil or Oleum Cocois, and the animal soap base can be obtained after the sodium hydroxide saponification by animal grease.
Above-mentioned powdery polymer can be powdery natural high molecular substance or the semi-synthetic polymer substance of powdery, the perhaps mixture of powdery natural high molecular substance and the semi-synthetic polymer substance of powdery.Wherein natural high molecular substance usually take plant as raw material, gets by physical process or the extraction of physicochemical method; This class material mainly contains flours (as whole meal flour, potato flour, sweet potato flour, corn flour etc.) and starch based (as wheat starch, potato starch, sweet potato starch, W-Gum etc.).Semi-synthetic polymer substance is to be got through modification by crude substance, be mainly modified-cellulose family macromolecule material and modified starch series polymeric material, wherein modified-cellulose family macromolecule material comprises carboxymethyl cellulose, methylcellulose gum, Walocel MT 20.000PV, ethyl cellulose, Natvosol, hydroxypropylcellulose, Vltra tears and methylol Natvosol, and the modified starch series polymeric material comprises carboxymethyl starch, hydroxyethylamyle, cyanoethyl starch, starch acetates, starch phosphates, cationic starch and polymerization starch.Powdery polymer of the present invention can be a kind of in above-mentioned various polymer substance or multiple mixture wherein.
After adopting powdery polymer to replace the part soap base to form to mix soap base, mix soap base viscosity larger, tending to run in actual production can not the normal extrusion shaping, demoulding difficulty, print speed more slowly, the problem that even can not print.The effect of above-mentioned lubricating auxiliary agent is to reduce the viscosity of mixing soap base, increases the plasticity and the force of cohesion that mix soap base, makes and mixes normally shaping, the demoulding and printing of soap base.Above-mentioned lubricating auxiliary agent can be a kind of in polyalcohols material (as ethylene glycol, propylene glycol, glycerol, sorbyl alcohol, wych-elm alcohol, tetramethylolmethane, hexadecanol, stearyl alcohol, two Lauryl Alcohols, polyoxyethylene glycol, polypropylene glycol, polyglycerol and polysorbate), glucose material (material that namely has the glucose structure), urea, polyacrylamide or multiple kind mixture wherein.
The effect of above-mentioned water is that sanitas, whitening agent, soap base, powdery polymer can be mixed uniformly, and it is reached be fit to mill, the purpose of shaping, printing.Most preferably water is deionized water.
The effect of foregoing preservatives is to prevent perfumed soap moldy metamorphism in use and storage process.Foregoing preservatives can be a kind of in isothiazolinone (being Kathon CG), Sodium Benzoate, glycolylurea (being DMDMH), diazonium alkyl imidazole urea (namely extremely beautiful), Tegosept M and propylben or multiple mixture wherein.
The effect of above-mentioned whitening agent is to make perfumed soap more attractive in appearance in appearance.Above-mentioned whitening agent can be white dyes (as: 2,5-pair-(the 5-tertiary butyl-2-benzoxazolyl) thiophene, 4, two (the 2-dimethoxy-styryl-) biphenyl of 4-, Isosorbide-5-Nitrae-two (5-methyl-2-benzoxazolyl) naphthalene etc.), a kind of in titanium dioxide, talcum powder, calcium carbonate, Calcium hydrogen carbonate, sodium carbonate, sodium bicarbonate, zinc oxide and calcium oxide or multiple mixture wherein.
The effect of above-mentioned essence is taste and the smell of covering other raw material (as soap base, powdery polymer) itself, makes perfumed soap have better taste and smell.Above-mentioned essence can be fruit class essence, animal class essence, fragrance of a flower class essence, the fragrant class essence of powder and other class essence.
The present invention adopts powdery polymer to replace the part soap base, for the manufacture of perfumed soap, powdery polymer is as the integral part of perfumed soap, reduce on the one hand degreasing dynamics and the pungency of perfumed soap, make its performance gentle, be suitable for washing one's face, in the situation such as makeup removing clean (namely cleaning skin of face), the functions such as the foaming dynamics of perfumed soap, detersive power are not lost again simultaneously, still be suitable for taking a shower, and the shower function do not weaken, gentleer; On the other hand, the powdery polymer source is abundant, with low cost, and can degrade, and so greatly reduces the manufacturing cost of perfumed soap, and very friendly to environment.
Description of drawings
Accompanying drawing is the process flow sheet that the preferred embodiment of the present invention 1 is made perfumed soap.
Embodiment
Embodiment 1
With reference to accompanying drawing, the manufacture method of this perfumed soap comprises the steps: successively
(1) be equipped with in proportion the raw materials such as soap base, powdery polymer, lubricating auxiliary agent, water, sanitas, whitening agent, essence, functional additive; In the present embodiment, by weight, get 60 parts of soap bases (being all the plant soap base), 40 parts of powdery polymers (being all hydroxypropylcellulose), 10 parts of lubricating auxiliary agent (being all sorbyl alcohol), 5 parts, water (being all deionized water), 0.5 part of sanitas (being all isothiazolinone (being Kathon CG)), 0.15 part, whitening agent (being all titanium dioxide), 1.5 parts, essence, 6 parts of functional additives (being all walnut powder);
(2) water and sanitas, whitening agent are mixed, obtain the aqueous solution;
(3) soap base is added agitator kettle, then the aqueous solution that step (2) is obtained adds agitator kettle, and be stirred to and mix;
(4) functional additive is added agitator kettle, and be stirred to and mix;
(5) powdery polymer is added agitator kettle, and be stirred to and mix;
(6) lubricating auxiliary agent and essence are mixed, then add agitator kettle, and be stirred to and mix, obtain mixture;
(7) mixture that step (6) is obtained is milled, is pushed, and the various raw materials in mixture are further mixed;
(8) mixture that step (7) is obtained pushes (temperature of single screw extrusion machine die head can be arranged between 30 ℃ to 70 ℃) by single screw extrusion machine, extrudes bar;
(9) print (can adopt the printer that is connected with cooling fluid to print) on the bar that step (8) is extruded, and carry out stripping and slicing, can obtain perfumed soap.Through printing, have required word and/or pattern on the perfumed soap surface.
In the perfumed soap of making, contain 60 parts of soap bases (being all the plant soap base), 40 parts of powdery polymers (being all hydroxypropylcellulose), 10 parts of lubricating auxiliary agent (being all sorbyl alcohol), 5 parts, water (being all deionized water), 0.5 part of sanitas (being all isothiazolinone (being Kathon CG)), 0.15 part, whitening agent (being all titanium dioxide), 1.5 parts, essence, 6 parts of functional additives (being all walnut powder).
Embodiment 2
The manufacture method of this perfumed soap comprises the steps: successively
(1) be equipped with in proportion the raw materials such as soap base, powdery polymer, lubricating auxiliary agent, water, sanitas, whitening agent, essence, functional additive; in the present embodiment, by weight, (wherein the plant soap base is 30 parts to get 40 parts of soap bases, 10 parts of animal soap bases), (wherein hydroxyethylamyle is 40 parts for 60 parts of powdery polymers, 20 parts of methylcellulose gum), (wherein ethylene glycol is 11 parts for 15 parts of lubricating auxiliary agent, 4 parts, urea), 3 parts, water (being all deionized water), (wherein Sodium Benzoate is 0.5 part for 0.6 part of sanitas, 0.1 part of diazonium alkyl imidazole urea (namely extremely beautiful)), (wherein zinc oxide is 1.35 parts for 4.58 parts, whitening agent, 3.23 parts of titanium dioxides), 1 part, essence, 5 parts of functional additives (being all the chrysanthemum sheet),
Step (2)-(9) are identical with embodiment 1.
in the perfumed soap of making, (wherein the plant soap base is 30 parts to contain 40 parts of soap bases, 10 parts of animal soap bases), (wherein hydroxyethylamyle is 40 parts for 60 parts of powdery polymers, 20 parts of methylcellulose gum), (wherein ethylene glycol is 11 parts for 15 parts of lubricating auxiliary agent, 4 parts, urea), 3 parts, water (being all deionized water), (wherein Sodium Benzoate is 0.5 part for 0.6 part of sanitas, 0.1 part of diazonium alkyl imidazole urea (namely extremely beautiful)), (wherein zinc oxide is 1.35 parts for 4.58 parts, whitening agent, 3.23 parts of titanium dioxides), 1 part, essence, 5 parts of functional additives (being all the chrysanthemum sheet).
Embodiment 3
The manufacture method of this perfumed soap comprises the steps: successively
(1) be equipped with in proportion the raw materials such as soap base, powdery polymer, lubricating auxiliary agent, water, sanitas, whitening agent, essence; in the present embodiment, by weight, get 50 parts of soap bases (being all the plant soap base), (wherein whole meal flour is 50 parts for 55 parts of powdery polymers, 5 parts of carboxymethyl celluloses), (wherein polysorbate is 3 parts for 6 parts of lubricating auxiliary agent, 3 parts, urea), 10 parts, water (being all deionized water), (wherein isothiazolinone (being Kathon CG) is 0.2 part for 0.3 part of sanitas, 0.1 part of Buddhist nun uncle tortoise beetle ester), (wherein white dyes 2 for 2.6 parts, whitening agent, 0.1 part, 5-pair-(the 5-tertiary butyl-2-benzoxazolyl) thiophene, 0.5 part of titanium dioxide, 2.0 parts of talcum powder), 0.5 part, essence,
Owing to not containing functional additive, therefore compare with embodiment 1, omit step (4), namely from step (3) directly to step (5); Step (2), (3), (5)-(9) are identical with embodiment 1.
in the perfumed soap of making, contain 50 parts of soap bases (being all the plant soap base), (wherein whole meal flour is 50 parts for 55 parts of powdery polymers, 5 parts of carboxymethyl celluloses), (wherein polysorbate is 3 parts for 6 parts of lubricating auxiliary agent, 3 parts, urea), 10 parts, water (being all deionized water), (wherein isothiazolinone (being Kathon CG) is 0.2 part for 0.3 part of sanitas, 0.1 part of Buddhist nun uncle tortoise beetle ester), (wherein white dyes 2 for 2.6 parts, whitening agent, 0.1 part, 5-pair-(the 5-tertiary butyl-2-benzoxazolyl) thiophene, 0.5 part of titanium dioxide, 2.0 parts of talcum powder), 0.5 part, essence.
Embodiment 4
The manufacture method of this perfumed soap comprises the steps: successively
(1) be equipped with in proportion the raw materials such as soap base, powdery polymer, lubricating auxiliary agent, water, sanitas, whitening agent, essence, functional additive; In the present embodiment, by weight, get 20 parts of soap bases (being all the animal soap base), 70 parts of powdery polymers (wherein 5 parts of corn flours, 65 parts of Natvosols), 25 parts of lubricating auxiliary agent (wherein 10 parts of sorbyl alcohols, 10 parts of polyacrylamides, 5 parts of ethylene glycol), 15 parts, water, 1 part of sanitas (wherein 0.2 part of glycolylurea, 0.8 part of Sodium Benzoate), 3.5 parts, whitening agent (wherein 1 part, zinc oxide, 0.5 part of Calcium hydrogen carbonate, 2.0 parts of talcum powder), 2 parts of functional additives (being all that fineness is 200 purpose polypropylene powders);
Step (6) adds agitator kettle with lubricating auxiliary agent, and is stirred to and mixes, and obtains mixture; Step (2)-(5), (7)-(9) are identical with embodiment 1.
In the perfumed soap of making, contain 20 parts of soap bases (being all the animal soap base), 70 parts of powdery polymers (wherein 5 parts of corn flours, 65 parts of Natvosols), 25 parts of lubricating auxiliary agent (wherein 10 parts of sorbyl alcohols, 10 parts of polyacrylamides, 5 parts of ethylene glycol), 15 parts, water, 1 part of sanitas (wherein 0.2 part of glycolylurea, 0.8 part of Sodium Benzoate), 3.5 parts, whitening agent (wherein 1 part, zinc oxide, 0.5 part of Calcium hydrogen carbonate, 2.0 parts of talcum powder), 2 parts of functional additives (being all that fineness is 200 purpose polypropylene powders).
Embodiment 5
The manufacture method of this perfumed soap comprises the steps: successively
(1) be equipped with in proportion the raw materials such as soap base, powdery polymer, lubricating auxiliary agent, water, sanitas, whitening agent, essence, functional additive; in the present embodiment, by weight, (wherein the plant soap base is 30 parts to get 68 parts of soap bases, 38 parts of animal soap bases), (wherein sweet potato starch is 10 parts for 25 parts of powdery polymers, 15 parts of starch acetateses), (wherein polypropylene glycol is 1 part for 2 parts of lubricating auxiliary agent, 1 part of glucose material), 1 part, water, 0.1 part of sanitas (being all propylben), 1 part, whitening agent (wherein 1,0.3 part of 4-two (5-methyl-2-benzoxazolyl) naphthalene, 0.7 part, sodium carbonate), 2 parts, essence, (wherein quartz sand powder is 5.5 parts for 9.5 parts of functional additives, 4 parts of ginseng powders),
Step (2)-(9) are identical with embodiment 1.
in the perfumed soap of making, (wherein the plant soap base is 30 parts to contain 68 parts of soap bases, 38 parts of animal soap bases), (wherein sweet potato starch is 10 parts for 25 parts of powdery polymers, 15 parts of starch acetateses), (wherein polypropylene glycol is 1 part for 2 parts of lubricating auxiliary agent, 1 part of glucose material), 1 part, water, 0.1 part of sanitas (being all propylben), 1 part, whitening agent (wherein 1,0.3 part of 4-two (5-methyl-2-benzoxazolyl) naphthalene, 0.7 part, sodium carbonate), 2 parts, essence, (wherein quartz sand powder is 5.5 parts for 9.5 parts of functional additives, 4 parts of ginseng powders).
Claims (2)
1. the manufacture method of a perfumed soap, is characterized in that comprising the steps: successively
(1) be equipped with following raw material by following weight ratio: 60 parts of soap bases, 40 parts of powdery polymers, 10 parts of lubricating auxiliary agent, 5 parts, water, 0.5 part of sanitas, 0.15 part, whitening agent, 1.5 parts, essence, 6 parts of functional additives; Described soap base is the plant soap base, and described powdery polymer is hydroxypropylcellulose, and described lubricating auxiliary agent is sorbyl alcohol, and described water is deionized water, and described sanitas is isothiazolinone, and described whitening agent is titanium dioxide, and described functional additive is walnut powder;
(2) water and sanitas, whitening agent are mixed, obtain the aqueous solution;
(3) soap base is added agitator kettle, then the aqueous solution that step (2) is obtained adds agitator kettle, and be stirred to and mix;
(4) functional additive is added agitator kettle, and be stirred to and mix;
(5) powdery polymer is added agitator kettle, and be stirred to and mix;
(6) lubricating auxiliary agent and essence are mixed, then add agitator kettle, and be stirred to and mix, obtain mixture;
(7) mixture that step (6) is obtained is milled, is pushed, and the various raw materials in mixture are further mixed;
(8) mixture that step (7) is obtained pushes by single screw extrusion machine, extrudes bar;
(9) print on the bar that step (8) is extruded, and carry out stripping and slicing, can obtain perfumed soap.
2. the manufacture method of perfumed soap according to claim 1 is characterized in that: in described step (8), the temperature of single screw extrusion machine die head is between 30 ℃ to 70 ℃.
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| Application Number | Priority Date | Filing Date | Title |
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| CN 200810220380 CN101445773B (en) | 2008-12-20 | 2008-12-20 | Method for preparing fancy soap |
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| CN 200810220380 CN101445773B (en) | 2008-12-20 | 2008-12-20 | Method for preparing fancy soap |
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| CN101445773A CN101445773A (en) | 2009-06-03 |
| CN101445773B true CN101445773B (en) | 2013-05-29 |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104928082A (en) * | 2015-06-18 | 2015-09-23 | 罗晓安 | Preparing method for composite type gentle and moistening soap base |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2019179597A1 (en) * | 2018-03-19 | 2019-09-26 | Symrise Ag | Water-soluble release forms for an active substance |
| CN114774219B (en) * | 2022-04-30 | 2023-10-20 | 南通汉迪自动化设备有限公司 | Strip discharging machine for manufacturing perfumed soap and perfumed soap preparation method |
| CN117431129B (en) * | 2023-12-18 | 2024-02-20 | 广东麦你玩创新科技有限公司 | Safe and environment-friendly multifunctional soap mud and preparation method thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1636048A (en) * | 2002-02-21 | 2005-07-06 | 雷克特本克斯尔有限公司 | Hard surface cleaning compositions |
| WO2008070015A1 (en) * | 2006-12-01 | 2008-06-12 | The Procter & Gamble Company | Cleansing bar compositions comprising a high level of water |
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- 2008-12-20 CN CN 200810220380 patent/CN101445773B/en active Active
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1636048A (en) * | 2002-02-21 | 2005-07-06 | 雷克特本克斯尔有限公司 | Hard surface cleaning compositions |
| WO2008070015A1 (en) * | 2006-12-01 | 2008-06-12 | The Procter & Gamble Company | Cleansing bar compositions comprising a high level of water |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104928082A (en) * | 2015-06-18 | 2015-09-23 | 罗晓安 | Preparing method for composite type gentle and moistening soap base |
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