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CN101251460A - Method for the measurement of moisture and oil content in recovered refrigerants - Google Patents

Method for the measurement of moisture and oil content in recovered refrigerants Download PDF

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Publication number
CN101251460A
CN101251460A CNA2008100525127A CN200810052512A CN101251460A CN 101251460 A CN101251460 A CN 101251460A CN A2008100525127 A CNA2008100525127 A CN A2008100525127A CN 200810052512 A CN200810052512 A CN 200810052512A CN 101251460 A CN101251460 A CN 101251460A
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weight
refrigerant
drying
moisture
filter
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Pending
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CNA2008100525127A
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Chinese (zh)
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刘斌
臧润清
董小勇
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Tianjin University of Commerce
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Tianjin University of Commerce
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Priority to CNA2008100525127A priority Critical patent/CN101251460A/en
Publication of CN101251460A publication Critical patent/CN101251460A/en
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Abstract

The present invention discloses a measurement method for the content of water and oil in recycled refrigerant, aiming to provide a measurement method which can effectively judge the content of water and oil in recycled refrigerant and is beneficial to solve the problems in actual operation. The present invention comprises the following steps that: the weight of a drying filter is measured and recorded as G1; the drying filter is filled with recycled refrigerant and then has the weight measured and recorded as G2; the refrigerant is kept liquid and is fully absorbed by the drying filter, then the refrigerant liquid in the filter is exhausted, and the drying filter is measured and recorded as G3; the emptied filter is put into a drying box, and after the filter is fully dried, the filter is measured and recorded as G4; G2 minus G1 is the weight of the refrigerant poured into the drying filer; G3 minus G1 is the weight of water and oil in the recycled refrigerant; G3 minus G4 is the weight of the water in the recycled refrigerant; G4 minus G1 is the weight of the oil in the recycled refrigerant. The method of the present invention is simple, economical and reliable.

Description

回收的制冷剂中水分和油含量的测量方法 Method for the measurement of moisture and oil content in recovered refrigerants

技术领域 technical field

本发明涉及到一种测量方法,更具体地说是涉及到一种计算回收制冷中水分和含油量的测量方法。The present invention relates to a measurement method, more specifically to a measurement method for calculating the moisture and oil content in recovery refrigeration.

背景技术 Background technique

为环保和其它方面要求,回收各种制冷系统中的制冷剂是必要的。在制冷系统的运行中,由于密封和润滑等原因,回收的制冷剂中必然含有水分和润滑油。如果要对所回收的制冷剂进行回收再利用,或是利用回收的制冷剂来判断制冷系统的运行,就必须对回收的制冷剂中的水分和油含水量进行测定。但是如何确定回收的制冷剂中的水分和含油量还没有一个简单经济可行的方法。For environmental protection and other requirements, it is necessary to recover refrigerants in various refrigeration systems. During the operation of the refrigeration system, due to reasons such as sealing and lubrication, the recovered refrigerant must contain moisture and lubricating oil. If the recovered refrigerant is to be recovered and reused, or the recovered refrigerant is used to judge the operation of the refrigeration system, the water and oil water content in the recovered refrigerant must be measured. However, there is no simple, economical and feasible method for determining the moisture and oil content in the recovered refrigerant.

发明内容 Contents of the invention

本发明是为了克服现有技术中的不足之处,提供一种可以有效地判断回收的制冷剂中的水分和含油量,有利于解决现实操作中的问题的回收的制冷剂中水分和油含量的测量方法。The purpose of the present invention is to overcome the deficiencies in the prior art and provide a water and oil content in the recovered refrigerant that can effectively judge the moisture and oil content in the recovered refrigerant, which is beneficial to solve the problems in actual operation. measurement method.

本发明通过下述技术方案实现:The present invention realizes through following technical scheme:

一种回收的制冷剂中水分和油含量的测量方法,其特征在于,包括下述步骤:A method for measuring moisture and oil content in the recovered refrigerant, characterized in that it comprises the following steps:

(1)称量干燥过滤器的重量并记录为G1;(1) Weigh the weight of the dry filter and record it as G1;

(2)在干燥过滤器中充满回收的制冷剂,称重并记录为G2;(2) Fill the dry filter with recovered refrigerant, weigh it and record it as G2;

(3)使制冷剂保持液态,经干燥过滤器充分吸收后,排空过滤器中的制冷剂液体,称重并记录为G3;(3) Keep the refrigerant in a liquid state. After being fully absorbed by the dry filter, empty the refrigerant liquid in the filter, weigh it and record it as G3;

(4)把排空后的过滤器放入干燥箱内,待过滤器充分干燥后,称重并记录为G4;(4) Put the emptied filter into the drying box, after the filter is fully dried, weigh and record it as G4;

(5)用步骤2中的重量G2减去步骤1中的重量G1为干燥过滤器中所充灌的制冷剂量;用步骤3中的重量G3减去步骤1中的重量G1为回收的制冷剂中水分和油的重量;用步骤3中的重量G3减去步骤4中的重量G4为回收的制冷剂中水分的重量;用步骤4中的重量G4减去步骤1中的重量G1为回收的制冷剂中油的重量。(5) Use the weight G2 in step 2 to subtract the weight G1 in step 1 to be the amount of refrigerant charged in the dry filter; use the weight G3 in step 3 to subtract the weight G1 in step 1 to be the recovered refrigerant The weight of water and oil in the medium; subtract the weight G4 in step 4 from the weight G3 in step 3 to get the weight of water in the recovered refrigerant; subtract the weight G1 in step 1 from the weight G4 in step 4 to get the recovered The weight of oil in the refrigerant.

其中所述步骤3中的环境温度,一般高于制冷剂的凝固温度,低于水的结冰温度。步骤4中干燥箱的温度,一般高于常温,低于油激烈挥发的温度。The ambient temperature in step 3 is generally higher than the freezing temperature of the refrigerant and lower than the freezing temperature of water. The temperature of the drying oven in step 4 is generally higher than normal temperature and lower than the temperature at which the oil is violently volatilized.

本发明具有下述技术效果:The present invention has following technical effect:

使用本发明的测量方法可以有效地判断回收的制冷剂中的水分和含油量,有利于对回收的制冷剂进行回收再利用,并通过回收的制冷剂中所含有的水分和油来判断制冷系统的运行状况,有利于解决现实操作中的问题。而且,方法简单、经济、可靠。Using the measurement method of the present invention can effectively judge the moisture and oil content in the recovered refrigerant, which is beneficial to the recovery and reuse of the recovered refrigerant, and the refrigeration system can be judged by the moisture and oil contained in the recovered refrigerant The operation status is conducive to solving the problems in actual operation. Moreover, the method is simple, economical and reliable.

附图说明 Description of drawings

图1为本发明回收的制冷剂中水分和油含量的测量方法的流程图。Fig. 1 is a flow chart of the method for measuring the moisture and oil content in the recovered refrigerant of the present invention.

具体实施方式 Detailed ways

以下结合附图,并以R22回收制冷剂为具体实施例对本发明详细说明。Hereinafter, the present invention will be described in detail with reference to the accompanying drawings and taking R22 recovered refrigerant as a specific embodiment.

图1为本发明回收的制冷剂中水分和油含量的测量方法的流程图,本发明回收的制冷剂中水分和油含量的测量方法包括下述步骤:Fig. 1 is the flow chart of the measuring method of moisture and oil content in the refrigerant that the present invention reclaims, and the measuring method of moisture and oil content in the refrigerant that the present invention reclaims comprises the following steps:

(1)首先选择一种与所待测量的回收制冷剂所对应使用的小型干燥过滤器,本实施例选择了R22z专用小型干燥过滤器,并在过滤器两端装有单向阀,用高精度天秤称出这时干燥过滤器的重量记录为G1。(1) First, select a small dry filter corresponding to the recovered refrigerant to be measured. In this embodiment, a small dry filter dedicated to R22z is selected, and a check valve is installed at both ends of the filter. The precision balance weighs the weight of the dry filter at this time and records it as G1.

(2)打开两端的单向阀,从干燥过滤器一端充灌回收的制冷剂,直到从另一端的单向阀流出液体的制冷剂,这时关上过滤器两端的单向阀,用高精度天秤称重并记录为G2。(2) Open the one-way valves at both ends, fill the recovered refrigerant from one end of the dry filter until the liquid refrigerant flows out from the one-way valve at the other end, then close the one-way valves at both ends of the filter, and use high-precision The scale is weighed and recorded as G2.

(3)把充满回收制冷剂的过滤器放入到-10℃环境中,在48小时后拿出过滤器,使干燥过滤器充分吸收回收的制冷剂后,打开单向阀,排空过滤器中的制冷剂液体,用高精度天秤称重并记录为G3。(3) Put the filter full of recovered refrigerant into the -10°C environment, take out the filter after 48 hours, make the dry filter fully absorb the recovered refrigerant, open the one-way valve, and empty the filter The refrigerant liquid in the liquid is weighed with a high-precision balance and recorded as G3.

(4)把打开两端单向阀的过滤器放入到干燥箱中,温度为35℃,在30分钟后拿出过滤器,用高精度天秤称重并记录为G4。(4) Put the filter with the one-way valves at both ends into a drying oven at a temperature of 35° C. Take out the filter after 30 minutes, weigh it with a high-precision balance and record it as G4.

利用上述方法称得的重量进行计算:步骤3中的重量G3减去步骤4中的重量G4的为制冷剂中含有水分的重量,步骤4中的重量G4减去步骤1中的重量G1为制冷剂中含有油的重量,步骤2中的重量G2减去步骤1中的重量G1为充灌的回收制冷剂的重量,步骤3中的重量G3减去步骤1中的重量G1为回收制冷剂中含有的水分和油的总量。Use the weight obtained by the above method to calculate: the weight G3 in step 3 minus the weight G4 in step 4 is the weight of moisture contained in the refrigerant, and the weight G4 in step 4 minus the weight G1 in step 1 is the refrigerant The weight of the oil contained in the refrigerant, the weight G2 in step 2 minus the weight G1 in step 1 is the weight of the recovered refrigerant charged, the weight G3 in step 3 minus the weight G1 in step 1 is the weight of the recovered refrigerant The total amount of water and oil contained.

Claims (3)

1, the measuring method of moisture and oil content in a kind of cold-producing medium of recovery is characterized in that, comprises the steps:
(1) weight of weighing device for drying and filtering and be recorded as G1;
(2) in device for drying and filtering, be full of the cold-producing medium of recovery, weigh and be recorded as G2;
(3) make cold-producing medium keep liquid, after the drying filtrator fully absorbed, the refrigerant liquid in the emptying filtrator was weighed and is recorded as G3;
(4) filtrator after the emptying is put into drying box, after the abundant drying of device to be filtered, weigh and be recorded as G4;
(5) the weight G1 that deducts in the step 1 with the weight G2 in the step 2 is the refrigerant amount that is charged in the device for drying and filtering; The weight G1 that deducts in the step 1 with the weight G in the step 33 is moisture and an oily weight in the cold-producing medium that reclaims; The weight G4 that deducts in the step 4 with the weight G3 in the step 3 is the weight of moisture in the cold-producing medium that reclaims; The weight G1 that deducts in the step 1 with the weight G4 in the step 4 is the weight of oil in the cold-producing medium that reclaims.
According to the measuring method of moisture and oil content in the cold-producing medium of right 1 described recovery, it is characterized in that 2, the environment temperature in the described step 3 is higher than the temperature of solidification of cold-producing medium, be lower than the freezing temperature of water.
According to the measuring method of moisture and oil content in the cold-producing medium of right 1 described recovery, it is characterized in that 3, the temperature of drying box is higher than normal temperature in the described step 4, be lower than the evaporating temperature of oil.
CNA2008100525127A 2008-03-25 2008-03-25 Method for the measurement of moisture and oil content in recovered refrigerants Pending CN101251460A (en)

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Application Number Priority Date Filing Date Title
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Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101726447B (en) * 2009-12-29 2011-09-21 常州广为仪器科技有限公司 Method and device for measuring moisture absorptivity of aggregates
CN102937556A (en) * 2011-08-16 2013-02-20 贵州兴化化工股份有限公司 Method for measuring content of suspension sulfur in desulphurization solution
CN104089844A (en) * 2014-07-16 2014-10-08 安徽鑫科新材料股份有限公司 Method for measuring content of oil in scrap copper
CN104634015A (en) * 2013-11-14 2015-05-20 珠海格力电器股份有限公司 Extraction device and extraction method for compressor lubricating oil
CN106288556A (en) * 2016-08-09 2017-01-04 珠海格力电器股份有限公司 Oil content acquisition device and method and air conditioning system
CN107290242A (en) * 2016-04-01 2017-10-24 上海梅山钢铁股份有限公司 The detection method of oil content in a kind of waste oil containing metallurgical slag
CN112944758A (en) * 2015-08-03 2021-06-11 大金工业株式会社 Determination method and determination device

Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101726447B (en) * 2009-12-29 2011-09-21 常州广为仪器科技有限公司 Method and device for measuring moisture absorptivity of aggregates
CN102937556A (en) * 2011-08-16 2013-02-20 贵州兴化化工股份有限公司 Method for measuring content of suspension sulfur in desulphurization solution
CN104634015A (en) * 2013-11-14 2015-05-20 珠海格力电器股份有限公司 Extraction device and extraction method for compressor lubricating oil
CN104634015B (en) * 2013-11-14 2017-08-01 珠海格力电器股份有限公司 Extraction device and extraction method for compressor lubricating oil
CN104089844A (en) * 2014-07-16 2014-10-08 安徽鑫科新材料股份有限公司 Method for measuring content of oil in scrap copper
CN112944758A (en) * 2015-08-03 2021-06-11 大金工业株式会社 Determination method and determination device
CN107290242A (en) * 2016-04-01 2017-10-24 上海梅山钢铁股份有限公司 The detection method of oil content in a kind of waste oil containing metallurgical slag
CN106288556A (en) * 2016-08-09 2017-01-04 珠海格力电器股份有限公司 Oil content acquisition device and method and air conditioning system
CN106288556B (en) * 2016-08-09 2017-11-24 珠海格力电器股份有限公司 Oil content acquisition device and method and air conditioning system

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Open date: 20080827