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CN101159228B - Processing gas supplying mechanism, supplying method and gas processing unit - Google Patents

Processing gas supplying mechanism, supplying method and gas processing unit Download PDF

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CN101159228B
CN101159228B CN200710154446XA CN200710154446A CN101159228B CN 101159228 B CN101159228 B CN 101159228B CN 200710154446X A CN200710154446X A CN 200710154446XA CN 200710154446 A CN200710154446 A CN 200710154446A CN 101159228 B CN101159228 B CN 101159228B
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processing gas
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tank
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佐藤亮
齐藤均
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Tokyo Electron Ltd
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    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01JELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J9/00Apparatus or processes specially adapted for the manufacture, installation, removal, maintenance of electric discharge tubes, discharge lamps, or parts thereof; Recovery of material from discharge tubes or lamps
    • H01J9/38Exhausting, degassing, filling, or cleaning vessels
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C16/00Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
    • C23C16/44Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating
    • C23C16/455Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating characterised by the method used for introducing gases into reaction chamber or for modifying gas flows in reaction chamber
    • C23C16/45563Gas nozzles
    • C23C16/45565Shower nozzles
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01JELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J11/00Gas-filled discharge tubes with alternating current induction of the discharge, e.g. alternating current plasma display panels [AC-PDP]; Gas-filled discharge tubes without any main electrode inside the vessel; Gas-filled discharge tubes with at least one main electrode outside the vessel
    • H01J11/20Constructional details
    • H01J11/34Vessels, containers or parts thereof, e.g. substrates
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01JELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J11/00Gas-filled discharge tubes with alternating current induction of the discharge, e.g. alternating current plasma display panels [AC-PDP]; Gas-filled discharge tubes without any main electrode inside the vessel; Gas-filled discharge tubes with at least one main electrode outside the vessel
    • H01J11/20Constructional details
    • H01J11/50Filling, e.g. selection of gas mixture
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01JELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J11/00Gas-filled discharge tubes with alternating current induction of the discharge, e.g. alternating current plasma display panels [AC-PDP]; Gas-filled discharge tubes without any main electrode inside the vessel; Gas-filled discharge tubes with at least one main electrode outside the vessel
    • H01J11/20Constructional details
    • H01J11/54Means for exhausting the gas
    • H10P50/242

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Abstract

本发明涉及处理气体供给机构、供给方法及气体处理装置,该处理气体供给机构能够在短时间内供给使处理容器内变成设定压力的量的处理气体。处理气体供给机构(3)包括:用于向作为收容基板(G)的处理容器的腔室(2)内供给作为处理气体的氦气的He气体供给源(30);用于暂时贮存来自He气体供给源(30)的氦气的处理气体罐(33);和将来自He气体供给源(30)的氦气供给处理气体罐(33)并将处理气体罐(33)内的氦气供给腔室(2)内的处理气体流通部件(35),氦气经由处理气体流通部件(35)被从He气体供给源(30)暂时贮存在处理气体罐(33)中,并从处理气体罐(33)供给到腔室(2)内。

Figure 200710154446

The present invention relates to a processing gas supply mechanism, a supply method, and a gas processing apparatus capable of supplying a processing gas in an amount to bring the inside of a processing container to a set pressure in a short time. The processing gas supply mechanism (3) includes: a He gas supply source (30) for supplying helium gas as a processing gas into the chamber (2) serving as a processing container for accommodating the substrate (G); the processing gas tank (33) of the helium of the gas supply source (30); The processing gas circulation part (35) in the chamber (2), through which the helium gas is temporarily stored in the processing gas tank (33) from the He gas supply source (30), and from the processing gas tank (33) is fed into the chamber (2).

Figure 200710154446

Description

处理气体供给机构、供给方法及气体处理装置Processing gas supply mechanism, supply method, and gas processing device

技术领域technical field

本发明涉及处理气体供给机构及处理气体供给方法、以及具备这种处理气体供给机构的气体处理装置,其按照对收容在处理容器内的平板显示器(FPD)用的玻璃基板等被处理体实施规定的处理的方式向处理容器内供给处理气体。The present invention relates to a processing gas supply mechanism, a processing gas supply method, and a gas processing apparatus provided with such a processing gas supply mechanism, in accordance with the regulations for a processing object such as a glass substrate for a flat panel display (FPD) accommodated in a processing container. The processing method supplies the processing gas into the processing container.

背景技术Background technique

在FPD的制造工艺过程中,为了对作为被处理体的FPD用的玻璃基板实施蚀刻处理或成膜处理等规定的处理而使用着等离子体蚀刻装置或等离子体CVD成膜装置等的等离子体处理装置。在等离子体处理装置中,一般情况下,玻璃基板是在被载置在处理容器内的载置台上的状态下,通过在向处理容器内供给处理气体的同时产生高频电场而生成的处理气体的等离子体而进行处理的。In the FPD manufacturing process, plasma processing such as plasma etching equipment or plasma CVD film formation equipment is used to perform predetermined treatments such as etching treatment and film formation treatment on the glass substrate for FPD as the object to be processed. device. In a plasma processing apparatus, in general, a glass substrate is a processing gas generated by generating a high-frequency electric field while supplying a processing gas into the processing chamber while being placed on a stage in the processing chamber. treated with plasma.

向处理容器内供给处理气体通常是经由一端与处理气体供给源连接、另一端与处理容器连接着的配管等流路,并且在通过质量流量控制器等流量调整机构调整流量的同时所进行的(例如参照专利文献1)。The processing gas is usually supplied into the processing container through a flow channel such as a pipe connected to a processing gas supply source at one end and to the processing container at the other end, while adjusting the flow rate by a flow rate adjustment mechanism such as a mass flow controller ( For example, refer to Patent Document 1).

但是,近来,FPD朝着大型化的方向发展,甚至也出现了一边超过2m的巨大玻璃基板,处理容器也随之变大,因此,如果使用所述现有技术的处理气体供给方式,则从开始供给处理气体至处理容器内的压力达到设定压力则需要很长的时间,于是就会出现总处理能力下降的问题。However, recently, FPDs have been increasing in size, and even huge glass substrates exceeding 2 m on one side have appeared, and the processing chamber has also become larger. Therefore, if the processing gas supply method of the prior art is used, from It takes a long time to start supplying the processing gas until the pressure in the processing container reaches the set pressure, and thus there is a problem that the total processing capacity is lowered.

【专利文献1】日本特开2002-313898号公报[Patent Document 1] Japanese Unexamined Patent Publication No. 2002-313898

发明内容Contents of the invention

本发明就是鉴于上述情况而产生的,其目的在于提供能够在短时间内供给使得处理容器内变成设定压力的处理气体的处理气体供给机构以及处理气体供给方法、具备这样的处理气体供给机构的气体处理装置、以及存储着用于实施这种处理气体供给方法的控制程序的计算机可读取的存储介质。The present invention was made in view of the above circumstances, and an object of the present invention is to provide a processing gas supply mechanism and a processing gas supply method capable of supplying a processing gas at a set pressure in a processing container in a short time, and a processing gas supply mechanism having such a processing gas supply mechanism. A gas processing device, and a computer-readable storage medium storing a control program for implementing the processing gas supply method.

为了解决上述课题,在本发明的第一观点中提供一种处理气体供给机构,其特征在于,该处理气体供给机构按照对收容在处理容器内的被处理体实施规定处理的方式向上述处理容器内供给处理气体,并且该处理气体供给机构包括:用于向上述处理容器内供给处理气体的处理气体供给源;用于暂时贮存来自上述处理气体供给源的处理气体的处理气体罐;和将来自上述处理气体供给源的处理气体供给上述处理气体罐,并将上述处理气体罐内的处理气体供给上述处理容器内的处理气体流通部件,并且,处理气体从上述处理气体供给源被暂时贮存在上述处理气体罐中,并从上述处理气体罐向上述处理容器内供给。In order to solve the above-mentioned problems, the first aspect of the present invention provides a processing gas supply mechanism, characterized in that the processing gas supply mechanism supplies the processing gas to the processing container so as to perform a predetermined process on the object to be processed accommodated in the processing container. The processing gas is supplied inside, and the processing gas supply mechanism includes: a processing gas supply source for supplying processing gas into the above-mentioned processing container; a processing gas tank for temporarily storing the processing gas from the above-mentioned processing gas supply source; The processing gas from the processing gas supply source is supplied to the processing gas tank, and the processing gas in the processing gas tank is supplied to the processing gas circulation part in the processing container, and the processing gas is temporarily stored in the processing gas supply source from the processing gas supply source. The processing gas tank is supplied from the processing gas tank to the processing container.

另外,在本发明的第二观点中提供一种气体处理装置,其特征在于,包括:收容被处理体的处理容器;向上述处理容器内供给处理气体的处理气体供给机构;以及对上述处理容器内进行排气的排气单元,并且,在将被处理体收容在上述处理容器内的状态下,利用上述排气单元进行排气,同时利用上述处理气体供给机构供给处理气体,对被处理体实施规定处理,上述处理气体供给机构包括:用于向上述处理容器内供给处理气体的处理气体供给源;用于暂时贮存来自上述处理气体供给源的处理气体的处理气体罐;和将来自上述处理气体供给源的处理气体供给上述处理气体罐,并将上述处理气体罐内的处理气体供给上述处理容器内的处理气体流通部件,且,处理气体从上述处理气体供给源被暂时贮存在上述处理气体罐中,并从上述处理气体罐向上述处理容器内供给。In addition, in a second aspect of the present invention, there is provided a gas processing apparatus, characterized by comprising: a processing container for accommodating an object to be processed; a processing gas supply mechanism for supplying processing gas into the processing container; Exhaust unit for exhausting inside, and in the state where the object to be processed is accommodated in the above-mentioned processing container, the exhaust unit is used to exhaust gas, and at the same time, the processing gas is supplied by the above-mentioned processing gas supply mechanism, and the object to be processed is To perform a predetermined process, the processing gas supply mechanism includes: a processing gas supply source for supplying processing gas into the processing container; a processing gas tank for temporarily storing the processing gas from the processing gas supply source; The processing gas from the gas supply source is supplied to the processing gas tank, and the processing gas in the processing gas tank is supplied to the processing gas circulation part in the processing container, and the processing gas is temporarily stored in the processing gas supply source from the processing gas supply source. tank, and is supplied from the processing gas tank to the processing container.

在本发明的第二观点中,有一种优选实施方式,上述处理气体流通部件包括:与上述处理气体供给源以及上述处理容器连接着的第一处理气体流路;以及从上述第一处理气体流路分支并与上述处理气体罐连接着的第二处理气体流路,上述处理气体供给机构也从上述处理气体供给源向上述处理容器内供给处理气体。In a second aspect of the present invention, in a preferred embodiment, the processing gas circulation means includes: a first processing gas flow path connected to the processing gas supply source and the processing container; The second processing gas flow path is branched and connected to the processing gas tank, and the processing gas supply mechanism also supplies processing gas from the processing gas supply source into the processing container.

在这种情况下,有另一种优选实施方式,设置有多个上述处理气体罐,并且,与上述处理气体罐的数量对应而设置有多个上述第二处理气体流路,上述各第二处理气体流路分别具有用于将处理气体送入上述处理气体罐的送入流路;以及用于将处理气体从上述处理气体罐送出的送出流路。在这种情况下,还优选,包括控制上述处理气体供给机构的控制部,上述控制部进行如下控制:使处理气体从上述多个处理气体罐的一部分通过上述送出流路向上述处理容器内供给,同时使处理气体从上述处理气体供给源通过上述送入流路贮存在上述多个处理气体罐的剩余的一部分或全部中。In this case, there is another preferred embodiment. A plurality of the above-mentioned processing gas tanks are provided, and a plurality of the above-mentioned second processing gas flow paths are provided corresponding to the number of the above-mentioned processing gas tanks. The processing gas flow paths respectively have an inlet flow path for sending a processing gas into the processing gas tank; and a delivery flow path for sending a processing gas out of the processing gas tank. In this case, it is also preferable to include a control unit for controlling the processing gas supply mechanism, the control unit controlling to supply the processing gas from a part of the plurality of processing gas tanks into the processing container through the delivery channel, Simultaneously, the processing gas is stored in some or all of the remaining plurality of processing gas tanks from the processing gas supply source through the feeding flow path.

或者说,在这种情况下,还有另一种优选实施方式,上述第二处理气体流路分别具有用于将处理气体送入上述处理气体罐的送入流路;以及用于将处理气体从上述处理气体罐送出的送出流路,并设置有多个上述处理气体供给源以供给不同的多种处理气体,并且,上述第一处理气体流路具有与上述处理气体供给源的数量相对应地分支成多个并与上述各处理气体供给源连接着的供给源连接流路,上述第二处理气体流路的上述送入流路是从上述第一处理气体流路的上述各供给源连接流路分支的。再者,在这种情况下,还可优选,包括控制上述处理气体供给机构的控制部,上述控制部进行如下控制:在使由规定种类及比例组成的处理气体从上述处理气体罐通过上述送出流路向上述处理容器内供给之后,使由上述规定种类及比例组成的处理气体从上述多个处理气体供给源的一部分或全部通过上述第一处理气体流路向上述处理容器内供给,与此同时,使由与上述规定种类及比率不同的种类以及/或者比例组成的处理气体,从上述多个处理气体供给源的一部分或者全部通过上述送入流路贮存在上述处理气体罐中。In other words, in this case, there is another preferred embodiment, the above-mentioned second processing gas flow path respectively has an inlet flow path for sending the processing gas into the above-mentioned processing gas tank; The sending flow path sent out from the processing gas tank is provided with a plurality of processing gas supply sources to supply different types of processing gases, and the first processing gas flow path has a number corresponding to the number of processing gas supply sources. Branched into a plurality of supply source connection flow paths connected to the respective processing gas supply sources, the feeding flow path of the second processing gas flow path is connected from the respective supply sources of the first processing gas flow path stream branch. Furthermore, in this case, it is also preferable to include a control unit for controlling the processing gas supply mechanism, and the control unit performs the following control: when the processing gas composed of a predetermined type and ratio is passed from the processing gas tank through the After the flow path is supplied into the processing container, the processing gas composed of the predetermined type and ratio is supplied from part or all of the plurality of processing gas supply sources into the processing container through the first processing gas flow path, and at the same time, A processing gas having a type and/or ratio different from the predetermined type and ratio is stored in the processing gas tank from some or all of the plurality of processing gas supply sources through the feeding flow path.

另外,在这种情况下,有一种优选实施方式,设置有多个上述处理气体罐,并且,与上述处理气体罐的数量对应而设置有多个上述第二处理气体流路,上述各第二处理气体流路分别具有用于将处理气体送入上述处理气体罐的送入流路;以及用于将处理气体从上述处理气体罐送出的送出流路,设置有多个上述处理气体供给源以供给不同的多种处理气体,并且,上述第一处理气体流路具有与上述处理气体供给源的数量相对应地分支成多个并与上述各处理气体供给源连接着的供给源连接流路,上述各第二处理气体流路的上述送入流路是从上述第一处理气体流路的上述各供给源连接流路分支的。再者,在这种情况下,还优选,包括控制上述处理气体供给机构的控制部,上述控制部进行如下控制:使由规定种类及比例组成的处理气体从上述多个处理气体罐的一部分通过上述送出流路向上述处理容器内供给,并且使由上述规定种类及比例组成的处理气体从上述多个处理气体供给源的一部分或全部通过上述第一处理气体流路向上述处理容器内供给,与此同时,使由与上述规定种类及比率不同的种类以及/或者比例组成的处理气体,从上述多个处理气体供给源的一部分或者全部通过上述送入流路贮存在上述多个处理气体罐剩余的一部分或者全部中。In addition, in this case, in a preferred embodiment, a plurality of the processing gas tanks are provided, and a plurality of the second processing gas passages are provided corresponding to the number of the processing gas tanks, and each of the second processing gas channels The processing gas flow path respectively has an input flow path for sending the processing gas into the above-mentioned processing gas tank; different types of processing gases are supplied, and the first processing gas flow path has a supply source connection flow path branched into a plurality corresponding to the number of the processing gas supply sources and connected to each of the processing gas supply sources, The supply flow paths of the second processing gas flow paths are branched from the respective supply source connection flow paths of the first processing gas flow paths. Furthermore, in this case, it is also preferable to include a control unit for controlling the processing gas supply mechanism, and the control unit controls to pass the processing gas composed of a predetermined type and ratio through a part of the plurality of processing gas tanks. The delivery flow path supplies the processing gas into the processing container, and the processing gas composed of the predetermined type and ratio is supplied from part or all of the plurality of processing gas supply sources into the processing container through the first processing gas flow path. At the same time, the processing gas composed of a type and/or ratio different from the above-mentioned predetermined type and ratio is stored in the remaining of the plurality of processing gas tanks from a part or all of the plurality of processing gas supply sources through the above-mentioned feeding flow path. part or all of it.

再者,在这些情况下,也可以是上述第一处理气体流路分别具有:在使来自上述处理气体供给源的处理气体贮存在上述处理气体罐中的时候而使其流通的贮存用流路;以及在将来自上述处理气体供给源的处理气体供给上述处理容器内的时候而使其流通的供给用流路。Furthermore, in these cases, each of the first processing gas flow paths may include a storage flow path through which the processing gas from the processing gas supply source is stored in the processing gas tank. ; and a flow path for supplying the processing gas from the processing gas supply source to be circulated when the processing gas is supplied into the processing container.

另外,在以上本发明的第二观点中,还有一种优选实施方式,上述排气单元具有多个与上述处理容器连接着的排气流路;以及通过上述排气流路对上述处理容器内进行排气的排气装置,在这种情况下,在上述处理气体流通部件与上述多个排气流路中的一部分上连接着旁通流路,构成为上述处理气体流通部件内的处理气体通过上述旁通流路能够被上述排气单元排出,连接着上述旁通流路的上述排气流路在比其与上述旁通流路的连接部还靠上游的上游侧自如开闭。In addition, in the above second viewpoint of the present invention, there is still a preferred embodiment, the above-mentioned exhaust unit has a plurality of exhaust flow paths connected to the above-mentioned processing container; An exhaust device for exhausting, in this case, a bypass flow path is connected to the above-mentioned processing gas flow part and a part of the plurality of exhaust flow paths, and the processing gas in the above-mentioned processing gas flow part The bypass flow path can be discharged by the exhaust unit, and the exhaust flow path connected to the bypass flow path can be freely opened and closed on an upstream side of a connection portion with the bypass flow path.

另外,在以上本发明的第二观点中,还优选,在上述处理容器内,还具备等离子体生成机构,其生成由上述处理气体供给机构所供给的处理气体的等离子体,上述规定的处理是使用着处理气体的等离子体的等离子体处理。In addition, in the above second aspect of the present invention, it is also preferable that a plasma generating mechanism for generating plasma of the processing gas supplied by the processing gas supplying mechanism is further provided in the processing container, and the above-mentioned predetermined processing is Plasma treatment using a plasma of a process gas.

另外,在本发明的第三观点中提供一种处理气体供给方法,其特征在于,其按照对收容在处理容器内的被处理体实施规定处理的方式向上述处理容器内供给处理气体,要准备:用于向上述处理容器内供给处理气体的处理气体供给源;用于暂时贮存来自上述处理气体供给源的处理气体的处理气体罐;和将来自上述处理气体供给源的处理气体供给上述处理气体罐,并将上述处理气体罐内的处理气体供给上述处理容器内的处理气体流通部件,将处理气体从上述处理气体供给源暂时贮存在上述处理气体罐中,并从上述处理气体罐向上述处理容器内供给。In addition, in a third aspect of the present invention, there is provided a processing gas supply method, characterized in that the processing gas is supplied into the processing container in such a manner that a predetermined process is performed on an object accommodated in the processing container. : a processing gas supply source for supplying processing gas into the above-mentioned processing container; a processing gas tank for temporarily storing the processing gas from the above-mentioned processing gas supply source; and supplying the processing gas from the above-mentioned processing gas supply source to the above-mentioned processing gas tank, and supply the processing gas in the processing gas tank to the processing gas circulation part in the processing container, temporarily store the processing gas in the processing gas tank from the processing gas supply source, and send the processing gas from the processing gas tank to the processing Supplied in container.

在本发明的第三观点中,有一种优选实施方式,预先由与上述处理气体供给源以及上述处理容器连接着的第一处理气体流路;以及从上述第一处理气体流路分支并与上述处理气体罐连接着的第二处理气体流路构成上述处理气体流通部件,也从上述处理气体供给源向上述处理容器内供给处理气体。In a third viewpoint of the present invention, in a preferred embodiment, a first processing gas flow path connected to the processing gas supply source and the processing container; and branched from the first processing gas flow path and connected to the The second processing gas channel to which the processing gas tank is connected constitutes the processing gas circulation means, and also supplies processing gas from the processing gas supply source into the processing container.

在这种情况下,还有另一种优选实施方式,设置多个上述处理气体罐,并且与上述处理气体罐的数量相对应而设置多个上述第二处理气体流路,分别具有用于将处理气体送入上述处理气体罐中的送入流路;以及用于将处理气体从上述处理气体罐送出的送出流路,构成上述各个第二处理气体流路,从上述多个处理气体罐的一部分通过上述送出流路向上述处理容器内供给处理气体,同时,从上述处理气体供给源通过上述送入流路在上述多个处理气体罐的剩余的一部分或全部中贮存处理气体。In this case, there is another preferred embodiment, a plurality of the above-mentioned processing gas tanks are provided, and corresponding to the number of the above-mentioned processing gas tanks, a plurality of the above-mentioned second processing gas flow paths are provided, each having a The feeding flow path for sending the processing gas into the above-mentioned processing gas tank; and the sending flow path for sending the processing gas out of the above-mentioned processing gas tank, constituting each of the above-mentioned second processing gas flow paths, from the plurality of processing gas tanks A part of the processing gas is supplied into the processing container through the delivery flow path, and processing gas is stored in the remaining part or all of the plurality of processing gas tanks from the processing gas supply source through the delivery flow path.

或者,在这种情况下,还有另一种优选实施方式,分别具有用于将处理气体送入上述处理气体罐中的送入流路;以及用于将处理气体从上述处理气体罐送出的送出流路,构成上述第二处理气体流路,设置多个上述处理气体供给源以供给不同的多种处理气体,并且,将上述第一处理气体流路构成为具有与上述处理气体供给源的数量相对应地分支成多个并与上述各处理气体供给源连接着的供给源连接流路,将上述第二处理气体流路的上述送入流路从上述第一处理气体流路的上述各供给源连接流路分支,从上述处理气体罐通过上述送出流路向上述处理容器内供给由规定种类以及比例组成的处理气体后,从上述多个处理气体供给源的一部分或全部通过上述第一处理气体流路向上述处理容器内供给由上述规定种类以及比例组成的处理气体,与此同时,从上述多个处理气体供给源的一部分或全部通过上述送入流路在上述处理气体罐中贮存由与上述规定种类以及比例不同的种类以及/或者比例组成的处理气体。Or, in this case, there is another preferred embodiment, which respectively has a feeding flow path for sending the processing gas into the above-mentioned processing gas tank; and a flow path for sending the processing gas out of the above-mentioned processing gas tank. The sending flow path constitutes the second processing gas flow path, and a plurality of the processing gas supply sources are provided to supply different types of processing gases, and the first processing gas flow path is configured to have a connection with the processing gas supply source. Correspondingly branched into a plurality of supply source connecting flow paths connected to the respective processing gas supply sources, connecting the feeding flow path of the second processing gas flow path from the respective supply flow paths of the first processing gas flow path The supply source is connected to a channel branch, and after the process gas of a predetermined type and proportion is supplied from the process gas tank to the process container through the delivery channel, part or all of the plurality of process gas supply sources is passed through the first process. The gas flow path supplies the processing gas composed of the above-mentioned predetermined types and proportions into the above-mentioned processing container, and at the same time, a part or all of the plurality of processing gas supply sources is stored in the above-mentioned processing gas tank through the above-mentioned feeding flow path. Processing gases of different types and/or ratios from the above-mentioned predetermined types and ratios.

另外,在这种情况下,还有另一种优选实施方式,设置多个上述处理气体罐,并且与上述处理气体罐的数量相对应而设置多个上述第二处理气体流路,分别具有用于将处理气体送入上述处理气体罐中的送入流路;以及用于将处理气体从上述处理气体罐送出的送出流路,构成上述各第二处理气体流路,设置多个上述处理气体供给源以供给不同的多种处理气体,并且,将上述第一处理气体流路构成为具有与上述处理气体供给源的数量相对应地分支成多个并与上述各处理气体供给源连接着的供给源连接流路,将上述第二处理气体流路的上述送入流路从上述第一处理气体流路的上述各供给源连接流路分支,从上述多个处理气体罐的一部分通过上述送出流路向上述处理容器内供给由规定种类以及比例组成的处理气体,并且从上述多个处理气体供给源的一部分或全部通过上述第一处理气体流路向上述处理容器内供给由上述规定种类以及比例组成的处理气体,与此同时,从上述多个处理气体供给源的一部分或全部通过上述送入流路在上述多个处理气体罐的剩余的一部分或者全部中贮存由与上述规定种类以及比例不同的种类以及/或者比例组成的处理气体。In addition, in this case, there is another preferred embodiment. A plurality of the above-mentioned processing gas tanks are provided, and a plurality of the above-mentioned second processing gas flow paths are provided corresponding to the number of the above-mentioned processing gas tanks, each having a Each of the above-mentioned second processing gas flow paths is composed of a flow path for sending a processing gas into the processing gas tank; and a sending flow path for sending the processing gas out of the processing gas tank, and a plurality of the processing gas flow paths are provided. The supply source is used to supply different kinds of processing gases, and the above-mentioned first processing gas flow path is configured to have a plurality of branches corresponding to the number of the above-mentioned processing gas supply sources and connected to each of the above-mentioned processing gas supply sources. A supply source connection flow path is branched from the supply source connection flow path of the second processing gas flow path to each of the supply source connection flow paths of the first processing gas flow path, and passes through the delivery flow path from a part of the plurality of processing gas tanks. The flow path supplies a processing gas composed of a predetermined type and ratio into the processing container, and supplies a portion or all of the plurality of processing gas supply sources into the processing container through the first processing gas flow path. At the same time, part or all of the above-mentioned multiple processing gas supply sources are stored in the remaining part or all of the above-mentioned multiple processing gas tanks through the above-mentioned feeding flow channel. The type and/or proportion composition of the process gas.

再者,在本发明的第四观点中,提供一种计算机可读取的存储介质,其特征在于,其存储着在计算机上运行的控制程序,上述控制程序在执行时按照实施上述处理气体供给方法的方式使计算机控制处理装置。Moreover, in the fourth aspect of the present invention, there is provided a computer-readable storage medium, which is characterized in that it stores a control program running on a computer, and the control program is executed according to the process gas supply process described above. The method is in the form of a computer controlling the processing means.

根据本发明,由于使处理气体经由处理气体流通部件从处理气体供给源暂时贮存在处理气体罐中,并从处理气体罐供给处理容器内,因此能够在短时间内供给使处理容器内变成设定压力的量的处理气体。因此,能够缩短被处理体的处理时间。According to the present invention, since the processing gas is temporarily stored in the processing gas tank from the processing gas supply source through the processing gas flow member, and then supplied into the processing container from the processing gas tank, it is possible to supply the processing gas in a short time so that the inside of the processing container becomes a device. The amount of process gas at a constant pressure. Therefore, the processing time of the object to be processed can be shortened.

附图说明Description of drawings

图1是本发明所涉及的气体处理装置的一实施方式的等离子体蚀刻装置的大致截面图。FIG. 1 is a schematic cross-sectional view of a plasma etching apparatus according to an embodiment of a gas processing apparatus according to the present invention.

图2是测定处理气体的填充时间、以及处理气体供给时的稳定时间所使用的等离子体蚀刻装置的大致截面图。2 is a schematic cross-sectional view of a plasma etching apparatus used to measure the filling time of the processing gas and the stabilization time when the processing gas is supplied.

图3是表示处理气体的填充时间、以及处理气体供给时的稳定时间的测定结果的图。3 is a graph showing the measurement results of the filling time of the processing gas and the stabilization time when the processing gas is supplied.

图4是本发明所涉及的气体处理装置的其它实施方式的等离子体蚀刻装置的大致截面图。4 is a schematic cross-sectional view of a plasma etching device according to another embodiment of the gas processing device according to the present invention.

图5是在等离子体蚀刻装置中所设置的处理气体供给机构的供给源连接流路的变形例子。5 is a modified example of a supply source connection flow path of a process gas supply mechanism provided in a plasma etching apparatus.

符号说明Symbol Description

1、1`:等离子体蚀刻装置(气体处理装置)1, 1`: Plasma etching device (gas processing device)

2:腔室(处理容器)2: Chamber (processing container)

3、3`:处理气体供给机构3, 3`: Processing gas supply mechanism

4:排气单元4: exhaust unit

5:等离子体生成机构5: Plasma generation mechanism

41:排气管(排气流路)41: exhaust pipe (exhaust flow path)

42:排气装置42: exhaust device

30:He气体供给源(处理气体供给源)30: He gas supply source (processing gas supply source)

31:HCl气体供给源(处理气体供给源)31: HCl gas supply source (processing gas supply source)

32:SF6气体供给源(处理气体供给源)32: SF 6 gas supply source (processing gas supply source)

33、34:处理气体罐(tank)33, 34: Processing gas tank (tank)

35:处理气体流通部件35: Handling Gas Flow Components

36:第一处理气体流路36: First process gas flow path

36a、36b、36c:供给源连接流路36a, 36b, 36c: supply source connection flow path

36j、36k、36l:贮存用流路36j, 36k, 36l: flow paths for storage

36m、36n、36o:供给用流路36m, 36n, 36o: Flow path for supply

37、37`、38、38`:第二处理气体流路37, 37`, 38, 38`: the second process gas flow path

37a、37a`、38a、38a`:送入流路37a, 37a`, 38a, 38a`: sending flow path

37b、38b:送出流路37b, 38b: delivery flow path

39、39`:旁通流路39, 39`: bypass flow path

90:工艺控制器90: Process controller

91:用户接口91: User interface

92:存储部92: Storage Department

93:单元控制器(控制部)93: Unit controller (control department)

G:玻璃基板(被处理体)G: glass substrate (object to be processed)

具体实施方式Detailed ways

下面,参照附图,对本发明的实施方式进行说明。Hereinafter, embodiments of the present invention will be described with reference to the drawings.

图1是作为本发明所涉及的处理装置的一实施方式的等离子体蚀刻装置的大致截面图。FIG. 1 is a schematic cross-sectional view of a plasma etching apparatus as one embodiment of a processing apparatus according to the present invention.

该等离子体蚀刻装置1构成为对作为被处理体的FPD用的玻璃基板(以下简称“基板”)G进行蚀刻处理的电容耦合型平行平板等离子体蚀刻装置。作为FPD可以列举出:液晶显示器(LCD)、电致发光(Electro Luminescence;EL)显示器、等离子体显示面板(PDP)等。等离子体蚀刻装置1包括:作为收容基板G的处理容器的腔室2、向腔室2内供给处理气体的处理气体供给机构3、对腔室2内进行排气的排气单元4、以及生成被处理气体供给机构3供给到腔室2内的处理气体的等离子体的等离子体生成机构5。This plasma etching apparatus 1 is configured as a capacitively coupled parallel plate plasma etching apparatus for etching a glass substrate for FPD (hereinafter referred to simply as “substrate”) G as an object to be processed. Examples of the FPD include a liquid crystal display (LCD), an electroluminescence (EL) display, a plasma display panel (PDP), and the like. The plasma etching apparatus 1 includes: a chamber 2 as a processing container for accommodating a substrate G, a processing gas supply mechanism 3 for supplying a processing gas into the chamber 2, an exhaust unit 4 for exhausting the chamber 2, and a generator. The processing gas supply mechanism 3 supplies the plasma generation mechanism 5 of the processing gas plasma in the chamber 2 .

腔室2由例如表面被耐蚀铝处理(阳极氧化处理)过的铝构成,并与基板G的形状对应而形成四角筒形状。在腔室2内的底壁上设置有作为载置基板G的载置台的基座20。基座20与基板G的形状对应而形成四角板状或柱状,它具有由金属等导电性材料构成的基底20a;由覆盖基底20a的周边的绝缘材料构成的绝缘部件20b;和按照覆盖基底20a及绝缘部件20b的底部的方式而设置并且由对它们进行支承的绝缘材料构成的绝缘部件20c。在基底20a中内置有用于吸附被载置着的基板G的静电吸附机构、以及由用于对被载置着的基板G的温度进行调节的制冷剂流路等冷却单元等组成的温度调节机构(图中均未表示)。The chamber 2 is made of, for example, aluminum whose surface is alumite-treated (anodized), and has a rectangular cylindrical shape corresponding to the shape of the substrate G. As shown in FIG. A susceptor 20 as a mounting table on which the substrate G is mounted is provided on the bottom wall in the chamber 2 . The base 20 is formed into a quadrangular plate shape or a column shape corresponding to the shape of the substrate G, and has a base 20a made of a conductive material such as metal; an insulating member 20b made of an insulating material covering the periphery of the base 20a; The insulating member 20c is provided in such a manner as to form the bottom of the insulating member 20b and is made of an insulating material supporting them. The base 20a incorporates an electrostatic adsorption mechanism for adsorbing the mounted substrate G, and a temperature adjustment mechanism including a cooling unit such as a refrigerant flow path for adjusting the temperature of the mounted substrate G. (Not shown in the figure).

在腔室2的侧壁上形成有用于搬入搬出基板G的搬入搬出口21,并且设置有开闭该搬入搬出口21的闸阀22。当搬入搬出口21开放时,利用图中未示的搬送机构向腔室2的内外搬入搬出基板G。A loading/unloading port 21 for loading and unloading the substrate G is formed on a side wall of the chamber 2 , and a gate valve 22 for opening and closing the loading/unloading port 21 is provided. When the loading and unloading port 21 is opened, the substrate G is loaded and unloaded into and out of the chamber 2 by a transport mechanism (not shown).

在腔室2的底壁以及基座20上,例如在基座20的周边部位置隔开间隔地形成有多个贯通它们的通插孔23。在各通插孔23中,按照能够相对于基座20的基板载置面突出没入的方式插入有从下方支承基板G并使其升降的升降销24。在各个升降销24的下部形成有法兰部25,在各个法兰部25上连接有按照围绕升降销24的方式而设置着的能够伸缩的波形管26的一个端部(下端部),该波形管26的另一个端部(上端部)与腔室2的底壁连接。这样,波形管26随着升降销24的升降而伸缩,并且对通插孔23与升降销24的间隙进行密封。On the bottom wall of the chamber 2 and the base 20 , for example, a plurality of insertion holes 23 passing through them are formed at intervals at positions around the base 20 . Lift pins 24 for supporting and lifting the substrate G from below are inserted into each through hole 23 so as to protrude and sink relative to the substrate mounting surface of the susceptor 20 . A flange portion 25 is formed on the lower portion of each lift pin 24, and one end portion (lower end portion) of a telescopic corrugated tube 26 arranged so as to surround the lift pin 24 is connected to each flange portion 25. The other end (upper end) of the corrugated tube 26 is connected to the bottom wall of the chamber 2 . In this way, the corrugated tube 26 expands and contracts as the lift pin 24 moves up and down, and seals the gap between the insertion hole 23 and the lift pin 24 .

在腔室2的上部或者上壁,按照与基座20相向的方式设置有向腔室2内吐出被后述的处理气体供给机构3所供给的处理气体,并且具有作为上部电极的功能的喷头27。喷头27被接地,形成有使处理气体在内部扩散的气体扩散空间28,并在下表面或者与基座20的相对面上形成有用于吐出在气体扩散空间28中被扩散后的处理气体的多个吐出孔29。On the upper part or the upper wall of the chamber 2, a shower head that discharges the processing gas supplied by the processing gas supply mechanism 3 described later into the chamber 2 and functions as an upper electrode is provided so as to face the susceptor 20. 27. The shower head 27 is grounded, and a gas diffusion space 28 for diffusing the processing gas inside is formed, and a plurality of nozzles for spouting the processing gas diffused in the gas diffusion space 28 are formed on the lower surface or the surface opposite to the susceptor 20 . Spit hole 29 .

排气单元4包括:作为与腔室2的例如底壁连接着的排气流路的排气管41;与该排气管41连接并且通过排气管41对腔室2内进行排气的排气装置42;以及被设置在排气管41的比其与排气装置42的连接部还靠向上游的上游侧,用于调整腔室2内的压力的压力调整阀43。排气装置42构成为具有涡轮分子泵等真空泵,由此,能够将腔室2内抽真空至规定的减压气氛。在腔室2的圆周方向上隔开间隔地设置有多个排气管41,与各排气管41对应地设置有多个排气装置42以及压力调整阀43。The exhaust unit 4 includes: an exhaust pipe 41 as an exhaust flow path connected to, for example, the bottom wall of the chamber 2; an exhaust device 42 ; and a pressure regulating valve 43 for adjusting the pressure in the chamber 2 , which is provided on the upstream side of the exhaust pipe 41 rather than the connection portion with the exhaust device 42 . The exhaust device 42 is configured to include a vacuum pump such as a turbomolecular pump, whereby the inside of the chamber 2 can be evacuated to a predetermined reduced pressure atmosphere. A plurality of exhaust pipes 41 are provided at intervals in the circumferential direction of the chamber 2 , and a plurality of exhaust devices 42 and pressure adjustment valves 43 are provided corresponding to the respective exhaust pipes 41 .

等离子体生成机构5包括与基座20的基底20a连接着的,用于供给高频电力的供电线51;以及与该供电线51连接着的匹配器52以及高频电源53。从高频电源53向基座20供给例如13.56MHz的高频电力,这样,基座20就具有作为下部电极的功能,并与喷头27共同构成一对平行平板电极。基座20以及喷头27构成等离子体生成机构5的一部分。The plasma generating mechanism 5 includes a power supply line 51 connected to the base 20 a of the susceptor 20 for supplying high-frequency power; and a matching unit 52 and a high-frequency power supply 53 connected to the power supply line 51 . High-frequency power of, for example, 13.56 MHz is supplied to the susceptor 20 from the high-frequency power supply 53 , so that the susceptor 20 functions as a lower electrode and forms a pair of parallel plate electrodes together with the shower head 27 . Susceptor 20 and shower head 27 constitute a part of plasma generation mechanism 5 .

处理气体供给机构3包括:用于向腔室2内供给处理气体、例如He气体、HCl气体以及SF6气体的处理气体供给源、例如He气体供给源30、HCl气体供给源31以及SF6气体供给源32;用于暂时贮存或填充来自He气体供给源30、HCl气体供给源31以及SF6气体供给源32的处理气体的多个例如2个处理气体罐33、34;以及处理气体流通部件35,该处理气体流通部件包括将来自He气体供给源30、HCl气体供给源31以及SF6气体供给源32的处理气体向处理气体罐33、34以及腔室2内供给,并将被贮存在处理气体罐33、34中的处理气体供给腔室2内的配管等。处理气体流通部件35包括:连接着He气体供给源30、HCl气体供给源31以及SF6气体供给源32和腔室2的第一处理气体流路36;和按照与2个处理气体罐33、34相对应的方式分别从第一处理气体流路36分支并与处理气体罐33、34连接着的第二处理气体流路37、38。The processing gas supply mechanism 3 includes: a processing gas supply source for supplying processing gas, such as He gas, HCl gas, and SF gas into the chamber 2, such as a He gas supply source 30 , an HCl gas supply source 31, and SF gas. Supply source 32; A plurality of, for example, two processing gas tanks 33, 34 for temporarily storing or filling processing gases from He gas supply source 30, HCl gas supply source 31, and SF 6 gas supply source 32; and processing gas circulation means 35, the processing gas circulation part includes supplying the processing gas from the He gas supply source 30, the HCl gas supply source 31 and the SF 6 gas supply source 32 to the processing gas tanks 33, 34 and the chamber 2, and will be stored in The processing gas contained in the processing gas tanks 33 and 34 is supplied to piping and the like in the chamber 2 . The processing gas circulation part 35 includes: the first processing gas flow channel 36 connected with the He gas supply source 30, the HCl gas supply source 31 and the SF 6 gas supply source 32 and the chamber 2; 34 are respectively branched from the first processing gas flow path 36 and connected to the second processing gas flow paths 37 , 38 connected to the processing gas tanks 33 , 34 .

第一处理气体流路36在一侧或者说上游侧部具有按照与3个处理气体供给源(He气体供给源30、HCl气体供给源31以及SF6气体供给源32)相对应的方式而分支成3个并与各个处理气体供给源连接着的供给源连接流路36a、36b、36c,另一端部或下游侧端部按照与气体扩散空间28连通的方式与喷头27的上面连接。在第一处理气体流路36中,在供给源连接流路36a、36b、36c中分别设置有用于调整处理气体的流量的质量流量控制器36d、36e、36f以及阀36g、36h、36i,在比其与第二处理气体流路37、38的分支部还靠向另一侧的例如一个端部以及另一个端部上也分别设置有阀36s、36t。The first processing gas flow path 36 is branched in a manner corresponding to three processing gas supply sources (He gas supply source 30, HCl gas supply source 31, and SF 6 gas supply source 32) on one side or the upstream side. Three supply source connection channels 36 a , 36 b , and 36 c are connected to respective processing gas supply sources, and the other or downstream end is connected to the upper surface of shower head 27 so as to communicate with gas diffusion space 28 . In the first processing gas flow path 36, mass flow controllers 36d, 36e, 36f and valves 36g, 36h, 36i for adjusting the flow rate of the processing gas are respectively provided in the supply source connection flow paths 36a, 36b, 36c. Valves 36 s , 36 t are also provided on, for example, one end and the other end on the other side than the branching portion of the second process gas flow path 37 , 38 .

第二处理气体流路37、38分别从比第一处理气体流路36的供给源连接流路36a、36b、36c还靠向下游的下游侧分支,并按照与气体扩散空间28连通的方式与喷头27的上面连接,在中间部连接着处理气体罐33、34。这样,第二处理气体流路37、38分别具有:用于将处理气体送入处理气体罐33、34中的送入流路37a、38a;以及用于从处理气体罐33、34送出处理气体的送出流路37b、38b。在送入流路37a、38a以及送出流路37b、38b中分别设置有阀37c、38c以及阀37d、38d,在处理气体罐33、34上分别设置有用于测定内部压力的压力计33a、34a。The second processing gas flow paths 37 and 38 branch from the supply source connection flow paths 36 a , 36 b , and 36 c of the first processing gas flow path 36 respectively on the downstream side, and communicate with the gas diffusion space 28 . The upper surface of the shower head 27 is connected, and the processing gas tanks 33 and 34 are connected in the middle part. In this way, the second processing gas flow paths 37, 38 respectively have: feeding flow paths 37a, 38a for feeding processing gas into the processing gas tanks 33, 34; The delivery channels 37b, 38b. Valves 37c, 38c and valves 37d, 38d are respectively provided in the sending flow paths 37a, 38a and the sending flow paths 37b, 38b, and pressure gauges 33a, 34a for measuring the internal pressure are respectively installed on the processing gas tanks 33, 34. .

在处理气体流通部件35、例如第一处理气体流路36和多个排气管41中的一部分例如1根中连接着配管等旁通流路39,处理气体流通部件35内的处理气体就能够通过旁通流路39被排气单元4排出。旁通流路39构成为,被连接在排气管41的压力调整阀43和排气装置42之间,通过关闭该压力调整阀43,则能够防止从旁通流路39被排出的处理气体通过排气管41而流入腔室2内。A bypass channel 39 such as a pipe is connected to the processing gas flow part 35, for example, a part of the first processing gas flow path 36 and a plurality of exhaust pipes 41, so that the processing gas in the processing gas flow part 35 can be It is exhausted by the exhaust unit 4 through the bypass flow path 39 . The bypass flow path 39 is configured to be connected between the pressure regulating valve 43 of the exhaust pipe 41 and the exhaust device 42. By closing the pressure regulating valve 43, the process gas discharged from the bypass flow path 39 can be prevented from It flows into the chamber 2 through the exhaust pipe 41 .

等离子体蚀刻装置1的各个构成部分被具有微处理器(计算机)的工艺控制器90所控制。在该工艺控制器90上,连接着用户接口91,该用户接口由工艺过程管理者为管理等离子体蚀刻装置1而进行命令输入操作等的键盘以及可视化地显示等离子体蚀刻装置1的运转情况的显示器等构成;以及存储部92,该存储部存储着对用于在工艺控制器90的控制下而实现在等离子体蚀刻装置1中所实施的处理的控制程序和处理条件数据等进行记录的方案。根据需要,按照来自用户接口91的指示等从存储部92中调取任意的方案并使其在工艺控制器90中运行,这样,就能在工艺控制器90的控制下实施在等离子体蚀刻装置1中的处理。所述方案可以被存储在例如CD-ROM、硬盘、闪存等计算机能够读取的存储介质中,或者从其它的装置例如通过专线随时进行传送,以加以利用。Each component of the plasma etching apparatus 1 is controlled by a process controller 90 having a microprocessor (computer). A user interface 91 is connected to the process controller 90. The user interface consists of a keyboard for the process manager to perform command input operations for managing the plasma etching apparatus 1, and a keyboard for visually displaying the operation status of the plasma etching apparatus 1. a display and the like; and a storage unit 92 that stores a plan for recording control programs and processing condition data for realizing the processing performed in the plasma etching apparatus 1 under the control of the process controller 90 . According to the instruction from the user interface 91, etc., according to the instructions from the user interface 91, any scheme is called from the storage unit 92 and made to run in the process controller 90, so that it can be implemented in the plasma etching device under the control of the process controller 90. 1 processing. The recipe can be stored in a computer-readable storage medium such as CD-ROM, hard disk, or flash memory, or can be transmitted from other devices at any time, such as via a dedicated line, for use.

更具体地来讲,处理气体供给机构3的各阀36g、36h、36i、36s、36t、37c、37d、38c、38d、39a构成为被与工艺控制器90连接着的单元控制器93(控制部)所控制。根据需要,按照来自用户接口91的指示等,工艺控制器90从存储部92中调取任意的方案并使其由单元控制器93所控制。More specifically, the valves 36g, 36h, 36i, 36s, 36t, 37c, 37d, 38c, 38d, and 39a of the process gas supply mechanism 3 are configured to be controlled by the unit controller 93 connected to the process controller 90. Ministry) controlled. According to an instruction from the user interface 91 or the like, the process controller 90 retrieves an arbitrary recipe from the storage unit 92 and controls it by the unit controller 93 as needed.

在采用上述方式构成的等离子体蚀刻装置1中,通过排气单元4将腔室2内保持为规定的真空度,在维持着这种状态的情况下,首先,在通过闸阀22使搬入搬出口21被打开着的状态下,由图中未示的搬送机构从被打开着的搬入搬出口21搬入基板G,之后使各升降销24上升,利用各升降销24从搬送机构接收基板G并支承基板。搬送机构从搬入搬出口21退出至腔室2外之后,利用闸阀22关闭搬入搬出口21,并且使各升降销24下降并使其没入基座20的基板载置面,使基板G载置在基座20上。In the plasma etching apparatus 1 configured as described above, the inside of the chamber 2 is maintained at a predetermined vacuum degree by the exhaust unit 4, and when this state is maintained, first, the loading and unloading port is opened by the gate valve 22. 21 is opened, the substrate G is carried in from the opened loading and unloading port 21 by a conveying mechanism not shown, and then each lift pin 24 is raised, and the substrate G is received and supported by each lift pin 24 from the conveying mechanism. substrate. After the conveying mechanism exits from the loading and unloading port 21 to the outside of the chamber 2, the loading and unloading port 21 is closed by the gate valve 22, and the lift pins 24 are lowered to sink into the substrate mounting surface of the susceptor 20, so that the substrate G is placed on the substrate. on the base 20.

接着,通过处理气体供给机构3向腔室2内供给处理气体。此处的处理气体的供给是通过打开阀37d,放出从He气体供给源30、HCl气体供给源31以及SF6气体供给源32被预先填充在处理气体罐33中的He气体、HCl气体以及SF6气体而进行的。Next, a processing gas is supplied into the chamber 2 by the processing gas supply mechanism 3 . The supply of the processing gas here is by opening the valve 37d, releasing the He gas, the HCl gas and the SF gas which are previously filled in the processing gas tank 33 from the He gas supply source 30, the HCl gas supply source 31 and the SF gas supply source 32. 6 gas is carried out.

由于腔室2内被排气单元4排气,因此,如果仅供给被填充在处理气体罐33中的处理气体,则经过一段时间之后,腔室2内的压力就会降低。因此,供给被填充在处理气体罐33中的处理气体时或紧接着的供给之后,打开阀36s、36t、36g、36h、36i,通过质量流量控制器36d、36e、36f来调整来自He气体供给源30、HCl气体供给源31以及SF6气体供给源32的He气体、HCl气体以及SF6气体的流量,并供给到腔室2内,同时,利用压力控制阀43将腔室2内保持在设定压力、例如23.3Pa(0.175Torr)。这样,就能迅速地保持在腔室2内的设定压力。另外,处理气体流通部件35包括连接着He气体供给源30、HCl气体供给源31以及SF6气体供给源32和腔室2的第一处理气体流路36;以及从第一处理气体流路36分支并分别与处理气体罐33、34连接着的第二处理气体流路37、38,所以,没有使来自He气体供给源30、HCl气体供给源31以及SF6气体供给源32的氦气、氯化氢气体以及SF6气体经由第一处理气体流路36而通过作为较大空间的处理气体罐33、34,能够在短时间内供给到腔室2内,这样,就能实现腔室2内的压力保持的进一步迅速化。Since the inside of the chamber 2 is evacuated by the exhaust unit 4 , if only the processing gas filled in the processing gas tank 33 is supplied, the pressure inside the chamber 2 will decrease after a certain period of time. Therefore, when supplying the processing gas filled in the processing gas tank 33 or immediately after the supply, the valves 36s, 36t, 36g, 36h, 36i are opened, and the gas supply from He is adjusted by the mass flow controllers 36d, 36e, 36f. source 30, HCl gas supply source 31 and SF 6 gas supply source 32 He gas, HCl gas and the flow rate of SF 6 gas, and supply in the chamber 2, meanwhile, utilize the pressure control valve 43 to keep the chamber 2 at Set the pressure, for example 23.3Pa (0.175Torr). In this way, the set pressure in the chamber 2 can be quickly maintained. In addition, the processing gas circulation part 35 includes a first processing gas flow path 36 connecting the He gas supply source 30, the HCl gas supply source 31, the SF 6 gas supply source 32 and the chamber 2; Branched and connected to the second processing gas flow paths 37, 38 of the processing gas tanks 33, 34, respectively, so the helium gas, the helium gas from the He gas supply source 30, the HCl gas supply source 31, and the SF 6 gas supply source 32 are not used. Hydrogen chloride gas and SF 6 gas can be supplied in the chamber 2 in a short time by the processing gas tanks 33, 34 as relatively large spaces through the first processing gas flow path 36, like this, just can realize in the chamber 2. Further rapidity of pressure maintenance.

在此状态下,向被内置在基座20中的静电吸附机构施加直流电压从而使基板G吸附在基座20上,同时,利用被内置在基座20中的调温机构来调节基板G的温度。从高频电源53经由匹配器52向基座20施加高频电力,在作为下部电极的基座20与作为上部电极的喷头27之间生成高频电场,并使腔室2内的处理气体等离子体化。利用该处理气体的等离子体对基板G实施蚀刻处理。In this state, a DC voltage is applied to the electrostatic adsorption mechanism built in the susceptor 20 so that the substrate G is adsorbed on the susceptor 20, and at the same time, the temperature of the substrate G is adjusted by the temperature adjustment mechanism built in the susceptor 20. temperature. High-frequency power is applied to the susceptor 20 from the high-frequency power supply 53 through the matching device 52, and a high-frequency electric field is generated between the susceptor 20 as the lower electrode and the shower head 27 as the upper electrode, and the processing gas in the chamber 2 is plasma Integrate. The substrate G is etched using the plasma of the processing gas.

对基板G实施蚀刻处理之后,停止施加来自高频电源53的高频电力。接着,关闭阀36g、36h、36i并停止供给来自He气体供给源30、HCl气体供给源31以及SF6气体供给源32的氦气、氯化氢气体以及SF6气体,同时,利用排气单元4排出腔室2内以及第一处理气体流路36或处理气体流通部件35内的处理气体。解除静电吸附机构对基板G的吸附,之后,在向腔室2内供给处理气体,并将腔室2内保持在设定压力、例如26.7Pa(0.2Torr)的状态下,向基座20施加高频电力并使处理气体等离子体化,对基板G实施除电处理。此处的处理气体的供给是通过以下方式进行的,打开阀38d,放出从He气体供给源30预先填充在处理气体罐34中的氦气,并且,打开阀36s、36t、36g,按照将腔室2内保持在设定压力的方式,利用质量流量控制器36d来调整来自He气体供给源30的氦气的流量并将其送出。这样,不仅能使腔室2内的压力瞬间保持在设定压力或接近设定压力,还能够迅速地进行基板G的除电处理。After performing the etching process on the substrate G, the application of high-frequency power from the high-frequency power supply 53 is stopped. Next, close the valves 36g, 36h, 36i and stop supplying helium gas, hydrogen chloride gas, and SF gas from the He gas supply source 30, the HCl gas supply source 31, and the SF gas supply source 32 , and at the same time, use the exhaust unit 4 to discharge The processing gas in the chamber 2 and in the first processing gas channel 36 or the processing gas flow member 35 . Release the adsorption of the electrostatic adsorption mechanism to the substrate G, and then supply the processing gas into the chamber 2 and keep the chamber 2 at a set pressure, for example, 26.7Pa (0.2Torr), and then apply the gas to the susceptor 20. High-frequency power is used to turn the processing gas into plasma, and a static elimination process is performed on the substrate G. The supply of the processing gas here is carried out by opening the valve 38d to discharge the helium gas previously filled in the processing gas tank 34 from the He gas supply source 30, and opening the valves 36s, 36t, and 36g according to the chamber The flow rate of the helium gas from the He gas supply source 30 is adjusted and sent out by the mass flow controller 36d so that the inside of the chamber 2 is kept at the set pressure. In this way, not only can the pressure in the chamber 2 be kept at the set pressure or close to the set pressure instantaneously, but also the static elimination treatment of the substrate G can be performed quickly.

一旦进行过基板G的除电处理,则通过排气单元4排出腔室2内以及第一处理气体流路36或处理气体流通部件35内的处理气体。接着,使用闸阀22开放搬入搬出口21,并且使升降销24上升,使基板G从基座20向上方离开。之后,在图中未示的搬送机构从搬入搬出口21进入腔室2内之后,使升降销24下降,将基板G转移到搬送机构上。之后,基板G被搬送机构从搬入搬出口21搬出至腔室2外。Once the destaticization process of the substrate G is performed, the process gas in the chamber 2 and the first process gas channel 36 or the process gas flow member 35 is exhausted through the exhaust unit 4 . Next, the loading/unloading port 21 is opened using the gate valve 22 , and the lift pin 24 is raised to separate the substrate G upward from the susceptor 20 . After that, after the transport mechanism (not shown) enters the chamber 2 through the loading and unloading port 21, the lift pins 24 are lowered to transfer the substrate G to the transport mechanism. Thereafter, the substrate G is carried out from the loading/unloading port 21 to the outside of the chamber 2 by the transfer mechanism.

向处理气体罐33、34再次填充处理气体是在基板G的搬入搬出时进行的。首先,打开阀37c,向处理气体罐33中填充处理气体。此时,为了防止处理气体流入处理气体罐34以及腔室2内,预先关闭阀37d、38c、36s。向处理气体罐33填充处理气体完成之后,关闭阀37c,为了排出残留在第一处理气体流路36以及送入流路37a、38a中的处理气体而打开阀39a。此时,为了使处理气体不流入腔室2内,预先关闭连接着旁通流路39的排气管41的压力调整阀43。排出处理气体完成之后,与向处理气体罐33填充同样,向处理气体罐34填充处理气体,填充结束后,同样进行残留在第一处理气体流路36以及送入流路37a、38a中的处理气体的排出。再者,也可以先进行向处理气体罐34的处理气体的填充。Refilling of the processing gas tanks 33 and 34 with the processing gas is performed when the substrate G is loaded and unloaded. First, the valve 37c is opened to fill the processing gas tank 33 with processing gas. At this time, in order to prevent the processing gas from flowing into the processing gas tank 34 and the chamber 2, the valves 37d, 38c, and 36s are closed in advance. After filling the processing gas tank 33 with processing gas, the valve 37c is closed, and the valve 39a is opened to discharge the processing gas remaining in the first processing gas channel 36 and the supply channels 37a and 38a. At this time, the pressure regulating valve 43 of the exhaust pipe 41 connected to the bypass channel 39 is closed in advance so that the processing gas does not flow into the chamber 2 . After the processing gas is exhausted, the processing gas tank 34 is filled with the processing gas in the same way as the processing gas tank 33 is filled, and after the filling is completed, the processing remaining in the first processing gas flow path 36 and the feeding flow paths 37a and 38a is similarly performed. Exhaust of gas. In addition, filling of the processing gas to the processing gas tank 34 may be performed first.

在本实施方式中,由于通过处理气体流通部件35,在处理气体罐33、34中暂时填充来自处理气体供给源、例如He气体供给源30、HCl气体供给源31以及SF6气体供给源32的处理气体、例如氦气、氯化氢气体以及SF6气体,将被填充在处理气体罐33、34中的处理气体供给腔室2内并进行包括基板G的等离子体蚀刻的处理,因此,即使腔室2的容量较大,也能在短时间内供给使该腔室2内变成设定压力的处理气体,这样就能实现处理时间的缩短。In the present embodiment, the processing gas tanks 33 and 34 are temporarily filled with processing gas from a processing gas supply source, such as a He gas supply source 30, an HCl gas supply source 31, and an SF gas supply source 32, through the processing gas circulation member 35. Processing gases, such as helium gas, hydrogen chloride gas, and SF 6 gas, will be filled in the processing gas tanks 33, 34 to supply the chamber 2 and perform processing including plasma etching of the substrate G, so even if the chamber 2 has a large capacity, and it is also possible to supply the processing gas that makes the inside of the chamber 2 into a set pressure in a short time, so that the processing time can be shortened.

另外,在本实施方式中,填充等离子体蚀刻处理时所供给的处理气体而使用处理气体罐33,填充等离子体蚀刻处理后所供给的处理气体而使用处理气体罐34,它们也可以替换使用。另外,在本实施方式中,使第二处理气体流路37、38分别从第一处理气体流路36分支而设置,但是,也可以在使它们的一个端部汇合的状态下从第一处理气体流路36分支而设置。或者,也可以使第二处理气体流路37、38不与喷头27的上面连接,而是与腔室2的其它部分例如侧壁连接,于是不通过喷头27而将处理气体供给腔室2内。再者,在本实施方式中,使第二处理气体流路37、38的送出流路37b、38b分别与腔室2连接,但是,它们也可以与第一处理气体流路36连接。在本实施方式中,为了连续进行使用着不同的处理气体的两种处理而使用了两个处理气体罐33、34,但是,在处理仅为一种的情况下,可以仅使用一个处理气体罐,在连续进行三种以上的处理等的情况下,也可以使用三个以上的处理气体罐。In addition, in this embodiment, the processing gas tank 33 is used for filling the processing gas supplied during the plasma etching process, and the processing gas tank 34 is used for filling the processing gas supplied after the plasma etching process, and these can be used instead. In addition, in the present embodiment, the second processing gas flow paths 37 and 38 are branched from the first processing gas flow path 36 respectively, but they may be connected from the first processing gas flow path in a state where one ends thereof are merged. The gas flow path 36 is branched and provided. Alternatively, the second processing gas flow paths 37 and 38 may not be connected to the top of the shower head 27, but to other parts of the chamber 2 such as side walls, so that the processing gas is supplied to the chamber 2 without passing through the shower head 27. . In addition, in this embodiment, the delivery flow paths 37 b and 38 b of the second processing gas flow paths 37 and 38 are respectively connected to the chamber 2 , but they may also be connected to the first processing gas flow path 36 . In this embodiment, two processing gas tanks 33 and 34 are used to continuously perform two types of processing using different processing gases, but only one processing gas tank may be used when only one type of processing is performed. , In the case where three or more processes are performed continuously, three or more process gas tanks may be used.

下面,使用等离子体蚀刻装置1,分别测定了以规定的压力在处理气体罐33中填充处理气体的时间(以下记作填充时间)、以及将填充在处理气体罐33中的处理气体及来自处理气体供给源30、31、32的处理气体供给腔室2内,至腔室2内的压力稳定在设定压力左右的时间(以下记作稳定时间)。如图2所示,此处的等离子体蚀刻装置1使用了将处理气体供给机构3的第二处理气体流路37、38变形为简化结构之后的例子。此处的第二处理气体流路37、38分别是一个端部从第一处理气体流路36分支、另一个端部与处理气体罐33、34连接,并在中间部设置有阀37z、38z。因此,此处的第二处理气体流路37、38分别兼具用于将来自处理气体供给源30、31、32的处理气体导入处理气体罐33、34中的流路;以及用于将处理气体罐33、34内的处理气体导入腔室2内的流路。Next, using the plasma etching apparatus 1, the time for filling the processing gas tank 33 at a predetermined pressure (hereinafter referred to as filling time), and the amount of time for the processing gas to be filled in the processing gas tank 33 and the time from the process were measured. The processing gas from the gas supply sources 30 , 31 , and 32 is supplied into the chamber 2 until the pressure in the chamber 2 stabilizes at about the set pressure (hereinafter referred to as stabilization time). As shown in FIG. 2 , the plasma etching apparatus 1 here uses an example in which the second processing gas passages 37 and 38 of the processing gas supply mechanism 3 are modified into a simplified structure. Here, the second processing gas flow paths 37 and 38 are respectively branched from the first processing gas flow path 36 at one end and connected to the processing gas tanks 33 and 34 at the other ends, and valves 37z and 38z are provided in the middle. . Therefore, the second processing gas flow paths 37, 38 here also serve as flow paths for introducing the processing gas from the processing gas supply sources 30, 31, 32 into the processing gas tanks 33, 34; The processing gas in the gas tanks 33 and 34 is introduced into the flow path in the chamber 2 .

设定作为处理气体的氦气、氯化氢气体以及SF6气体的流量比为2∶1∶1,总流量为5slm,腔室2的容量l0为23101,处理气体罐33的容量l1为3l,腔室2内的设定压力P0为23.3Pa(0.175Torr),分别对下述情况进行测定,被填充在处理气体罐33中的处理气体的压力P1为26.7kPa(200Torr)的情况(实施例1);53.3kPa(400Torr)的情况(实施例2);以及80.0kPa(600Torr)的情况(实施例3)。另外,作为比较例,测定了未使用处理气体罐33而仅将来自处理气体供给源30、31、32的处理气体供给到腔室2内的情况下的稳定时间。测定结果如表1所示。Set the flow ratio of helium, hydrogen chloride gas and SF gas as processing gas to be 2:1:1, the total flow rate is 5slm, the capacity l0 of chamber 2 is 23101, and the capacity l1 of processing gas tank 33 is 3l , the set pressure P0 in the chamber 2 is 23.3Pa (0.175Torr), and the following cases are measured respectively, the pressure P1 of the processing gas filled in the processing gas tank 33 is 26.7kPa (200Torr) (Example 1); the case of 53.3 kPa (400 Torr) (Example 2); and the case of 80.0 kPa (600 Torr) (Example 3). In addition, as a comparative example, the stabilization time was measured when only the processing gas from the processing gas supply sources 30 , 31 , and 32 was supplied into the chamber 2 without using the processing gas tank 33 . The measurement results are shown in Table 1.

表1Table 1

 填充时间(sec)Fill time(sec)  稳定时间(sec)Stabilization time (sec) 实施例1Example 1  2 2  1414 实施例2Example 2  55  1010 实施例3Example 3  1010  77 比较例comparative example  1515

如表1所示,可以确认,在实施例1、2、3中,与比较例相比稳定时间变短。即、可以确认,通过使用等离子体蚀刻装置1,与未使用处理气体罐33的现有技术的等离子体蚀刻装置的情况相比,则能够缩短稳定时间。As shown in Table 1, it was confirmed that in Examples 1, 2, and 3, the stabilization time was shorter than that of the comparative example. That is, it was confirmed that by using the plasma etching apparatus 1 , the stabilization time can be shortened compared to the case of the conventional plasma etching apparatus not using the process gas tank 33 .

另外,可以确认,虽然被填充在处理气体罐33中的处理气体的压力越低填充时间越短,但是被填充在处理气体罐33中的处理气体的压力越高则稳定时间越短,并且压力为80.0kPa的情况与压力为26.7kPa的情况相比大约变为一半。这也是因为,如果被填充在处理气体罐33内的处理气体的压力低,则从处理气体供给源30、31、32被供给腔室2内的处理气体会通过第二处理气体流路37而流入处理气体罐33中。因此,通过测定从处理气体罐33向腔室2内开始供给处理气体前后的处理气体流通部件35内的压力变化得出以下结果:就从处理气体罐33向腔室2内刚刚开始供给处理气体之后的处理气体流通部件35内的压力来说,如图3(a)的箭头部分所示,被填充在处理气体罐33中的处理气体的压力P1为26.7kPa的情况下,接近稳定时的处理气体流通部件35内的压力29.9kPa(224Torr),如图3(b)的箭头部分所示,被填充在处理气体罐33中的处理气体的压力P1不足29.9kPa例如为17.9kPa(135Torr)的情况下,比稳定时的处理气体流通部件35内的压力小,如图3(c)的箭头部件所示,被填充在处理气体罐33中的处理气体的压力P1比29.9kPa还大、例如为53.3kPa的情况下,比稳定时的处理气体流通部件35内的压力还大。另外,在被填充于处理气体罐33中的处理气体的压力P1为17.9kPa的情况下,与26.7kPa的情况相比,稳定时间延长2秒之多,即,其结果为,比未使用处理气体罐33而仅向腔室2内供给来自处理气体供给源30、31、32的处理气体时的稳定时间还长。因此,在第二处理气体流路37(38)兼作为用于将处理气体送入处理气体罐33(34)中的流路、以及用于将处理气体从处理气体罐33(34)中送出的流路的情况下,如果使被填充在处理气体罐33中的处理气体的压力比处理气体流通部件35内的压力高,那么,不仅能够防止处理气体流入处理气体罐33、34中,而且,越是提高被填充在处理气体罐33中的处理气体的压力,则越能够缩短稳定时间。In addition, it was confirmed that the lower the pressure of the processing gas filled in the processing gas tank 33, the shorter the filling time, but the higher the pressure of the processing gas filled in the processing gas tank 33, the shorter the stabilization time, and the pressure The case where the pressure is 80.0 kPa is about half that of the case where the pressure is 26.7 kPa. This is also because, if the pressure of the processing gas filled in the processing gas tank 33 is low, the processing gas supplied to the chamber 2 from the processing gas supply sources 30 , 31 , and 32 passes through the second processing gas flow path 37 . It flows into the processing gas tank 33 . Therefore, by measuring the pressure change in the processing gas circulation member 35 before and after the processing gas supply from the processing gas tank 33 into the chamber 2 is started, the following results are obtained: In terms of the pressure in the subsequent processing gas circulation part 35, as shown by the arrow portion in FIG . The pressure in the processing gas circulation part 35 is 29.9 kPa (224 Torr), as shown by the arrow part in FIG . 135 Torr), the pressure in the processing gas circulation part 35 is smaller than that at the time of stabilization, as shown by the arrow parts in FIG . Even higher, for example, 53.3 kPa, is higher than the pressure inside the process gas flow member 35 at a steady state. In addition, when the pressure P1 of the processing gas filled in the processing gas tank 33 is 17.9 kPa, the stabilization time is as much as 2 seconds longer than in the case of 26.7 kPa. When the processing gas tank 33 is used and only the processing gas from the processing gas supply sources 30 , 31 , and 32 is supplied into the chamber 2 , the stabilization time is longer. Therefore, the second processing gas flow path 37 (38) also serves as a flow path for sending the processing gas into the processing gas tank 33 (34) and as a flow path for sending the processing gas out of the processing gas tank 33 (34). In the case of a flow path, if the pressure of the processing gas filled in the processing gas tank 33 is higher than the pressure in the processing gas flow member 35, not only can the processing gas be prevented from flowing into the processing gas tanks 33, 34, but also , the higher the pressure of the processing gas filled in the processing gas tank 33 is, the more the stabilization time can be shortened.

下面,对等离子体蚀刻装置的其它实施方式进行说明。Next, other embodiments of the plasma etching apparatus will be described.

图4是作为本发明所涉及的气体处理装置的其它实施方式的等离子体蚀刻装置的大致截面图。4 is a schematic cross-sectional view of a plasma etching apparatus as another embodiment of the gas processing apparatus according to the present invention.

如图4所示,等离子体蚀刻装置1`是将等离子体蚀刻装置1中的处理气体供给机构3的第二处理气体流路37、38的送入流路37a、38a以及旁通流路39变形后的例子,对于与等离子体蚀刻装置1相同的部位标注相同的符号并省略其说明。等离子体蚀刻装置1`中的处理气体供给机构3`的第二处理气体流路37`(38`)的向处理气体罐33(34)的送入流路37a`(38a`)包括:分支送入流路37e、37f、37g(38e、38f、38g),这些分支送入流路是一个端部或者上游侧端部从导入分支流路37i、37j、37k而继续分支的,而这些导入分支流路按照分别从供给源连接流路36a、36b、36c的比质量流量控制器36d、36e、36f还靠向上游的上游侧分支的方式而设置;以及分支送入流路37e、37f、37g(38e、38f、38g)的另一个端部或下游侧端部相互合流并且与处理气体罐33(34)连接着的合流送入流路37h(38h)。在导入分支流路37i、37j、37k中分别设置有质量流量控制器37l、37m、37n,在分支送入流路37e、37f、37g、38e、38f、38g中分别设置有阀37o、37p、37q、38o、38p、38q。As shown in FIG. 4 , the plasma etching apparatus 1 ′ is a process gas supply mechanism 3 in the plasma etching apparatus 1. In the modified example, the same reference numerals are assigned to the same parts as those of the plasma etching apparatus 1, and description thereof will be omitted. The feeding flow path 37a' (38a') of the second processing gas flow path 37' (38') of the processing gas supply mechanism 3' in the plasma etching apparatus 1' to the processing gas tank 33 (34) includes: Sending flow paths 37e, 37f, 37g (38e, 38f, 38g), these branch sending flow paths are branched from one end or the upstream side end from the introduction branch flow path 37i, 37j, 37k, and these introduction flow paths The branch flow path is provided in such a way that it branches from the upstream side of the supply source connection flow path 36a, 36b, 36c to the upstream side of the mass flow controller 36d, 36e, 36f; and the branch feed flow path 37e, 37f, The other ends or the downstream ends of 37g (38e, 38f, 38g) merge with each other and are connected to the merged flow path 37h (38h) connected to the process gas tank 33 (34). Mass flow controllers 37l, 37m, 37n are respectively provided in the introduction branch flow paths 37i, 37j, 37k, and valves 37o, 37p, 37p, 37p, 37q, 38o, 38p, 38q.

处理气体供给机构3`中的旁通流路39`的一侧或者说上游侧分支并分别与合流送入流路37h、38h连接,并在各个分支部上设置有阀39b、39c。One side or the upstream side of the bypass flow path 39' in the processing gas supply mechanism 3' is branched and connected to the merged flow path 37h, 38h, respectively, and valves 39b, 39c are provided on each branch.

在采用这种方式构成的处理气体供给机构3`中,从He气体供给源30、HCl气体供给源31以及SF6气体供给源32经由第一处理气体流通部件35而向腔室2内供给氦气、氯化氢气体以及SF6气体,与此同时,能够从He气体供给源30、HCl气体供给源31以及SF6气体供给源32经由第二处理气体流路37`(38`)向处理气体罐33(34)填充氦气、氯化氢气体以及SF6气体,并且,能够通过各个质量流量控制器36d、36e、36f、37l、37m、37n以及各阀36g、36h、36i、37o(38o)、37p(38p)、37q(38q)来分别调整被供给腔室2内的氦气的流量、氯化氢气体的流量、SF6气体的流量、被送给处理气体罐33(34)的氦气的流量、氯化氢气体的流量、SF6气体的流量。另外,使旁通流路39`分支而分别与合流送入流路37h、38h连接,这样,则能够分别排出包括合流送入流路37h的第二处理气体流路37`内的处理气体与包括合流送入流路38h的第二处理气体流路38`内的处理气体。因此,将预先被填充在处理气体罐33(34)中的由规定种类及比例组成的处理气体、以及来自处理气体供给源30、31、32的由规定种类及比率组成的处理气体供给腔室2内,进行某种处理,由于与此同时,能够将在下一处理中所使用的、由与规定种类及比例不同的种类以及/或者比例组成的处理气体填充在处理气体罐34(33)中,所以能够连续进行所使用的处理气体种类或比率等不同的三种以上的处理。In the processing gas supply mechanism 3' configured in this way, helium is supplied into the chamber 2 from the He gas supply source 30, the HCl gas supply source 31, and the SF 6 gas supply source 32 via the first processing gas circulation member 35. gas, hydrogen chloride gas, and SF 6 gas, and at the same time, from He gas supply source 30, HCl gas supply source 31 and SF 6 gas supply source 32 to the process gas tank via the second process gas flow channel 37'(38') 33 (34) fill helium gas, hydrogen chloride gas and SF 6 gas, and can pass through each mass flow controller 36d, 36e, 36f, 37l, 37m, 37n and each valve 36g, 36h, 36i, 37o (38o), 37p (38p), 37q (38q) to adjust respectively the flow rate of the helium gas supplied to the chamber 2, the flow rate of the hydrogen chloride gas, the flow rate of the SF gas, the flow rate of the helium gas sent to the processing gas tank 33 (34), The flow rate of hydrogen chloride gas and the flow rate of SF 6 gas. In addition, by branching the bypass flow path 39' and connecting it to the merged feeding flow paths 37h and 38h, respectively, the processing gas and the gas in the second processing gas flow path 37' including the merged feeding flow path 37h can be discharged separately. The processing gas included in the second processing gas flow path 38' that is confluently sent into the flow path 38h. Therefore, the processing gas composed of a predetermined type and ratio filled in the processing gas tank 33 (34) in advance, and the processing gas composed of a predetermined type and ratio from the processing gas supply sources 30, 31, 32 are supplied to the chamber. 2, a certain processing is performed, because at the same time, the processing gas used in the next processing can be filled in the processing gas tank 34 (33) by a different type and/or ratio from the specified type and ratio. , Therefore, three or more types of processing different in the type and ratio of the processing gas to be used can be continuously performed.

再者,在本实施方式中,使分支送入流路37e、38e、37f、38f、37g、38g经由导入分支流路37i、37j、37k从供给源连接流路36a、36b、36c分支,但是,也可以不通过导入分支流路37i、37j、37k而从供给源连接流路36a、36b、36c直接分支。在这种情况下,能够在分支送入流路37e、38e、37f、38f、37g、38g中分别设置质量流量控制器。Furthermore, in the present embodiment, the branch supply flow paths 37e, 38e, 37f, 38f, 37g, and 38g are branched from the supply source connection flow paths 36a, 36b, and 36c via the introduction branch flow paths 37i, 37j, and 37k. , may directly branch from the supply source connecting flow paths 36a, 36b, 36c without passing through the introduction branch flow paths 37i, 37j, 37k. In this case, mass flow controllers can be provided in each of the branch feeding channels 37e, 38e, 37f, 38f, 37g, and 38g.

图5表示在等离子体蚀刻装置1中所设置着的处理气体供给机构3的供给源连接流路的变形例。FIG. 5 shows a modified example of the supply source connection flow path of the processing gas supply mechanism 3 provided in the plasma etching apparatus 1 .

为了在短时间内从处理气体供给源30、31、32向处理气体罐33、34填充处理气体,优选采用能够适用大流量的部件构成在供给源连接流路36a、36b、36c中所设置的质量流量控制器以及阀,从而按照大流量向处理气体罐33、34供给处理气体。但是,为了提高基板G的处理质量,必须细致地调整从处理气体供给源30、31、32供给至腔室2内的处理气体的流量,如果在供给源连接流路36a、36b、36c中设置能够适用大流量的质量流量控制器,那么就无法对流量进行微妙的调整,有可能使基板G的处理质量下降。因此,如图5所示,在各供给源连接流路36a、36b、36c中,使其分支为使来自处理气体供给源30、31、32的处理气体贮存或填充在处理气体罐33、34中时而使其流通的贮存用流路36j、36k、36l;以及在将来自处理气体供给源30、31、32的处理气体供给腔室2内时使其流通的供给用流路36m、36n、36o,进行设置,在贮存用流路36j、36k、36l中分别设置能够适用大流量的质量流量控制器36p以及阀36q,并且,在供给用流路36m、36n、36o中分别设置能够进行微调的例如小流量用的质量流量控制器36r以及阀36s。通过采用这种构造,能够在按照短时间向处理气体罐33、34中填充处理气体的同时细致地调整被供给到腔室2内的处理气体的流量。In order to fill the processing gas tanks 33, 34 with processing gas from the processing gas supply sources 30, 31, 32 in a short time, it is preferable to use parts that can apply a large flow rate to configure the supply source connecting channels 36a, 36b, 36c. mass flow controllers and valves to supply processing gas to the processing gas tanks 33 and 34 at a large flow rate. However, in order to improve the processing quality of the substrate G, the flow rate of the processing gas supplied from the processing gas supply source 30, 31, 32 to the chamber 2 must be finely adjusted. If a mass flow controller is applicable to a large flow rate, fine adjustment of the flow rate cannot be performed, and the processing quality of the substrate G may be deteriorated. Therefore, as shown in FIG. 5 , in each supply source connection channel 36 a , 36 b , 36 c , it is branched so that the processing gas from the processing gas supply source 30 , 31 , 32 is stored or filled in the processing gas tank 33 , 34 The storage flow paths 36j, 36k, 36l are used to circulate during the middle; and the supply flow paths 36m, 36n, 36o, to set up, in the storage flow paths 36j, 36k, 36l, respectively set a mass flow controller 36p and a valve 36q that can be applied to a large flow rate, and in the supply flow paths 36m, 36n, 36o, respectively set a For example, mass flow controller 36r and valve 36s for small flow. By employing such a configuration, it is possible to finely adjust the flow rate of the processing gas supplied into the chamber 2 while filling the processing gas tanks 33 and 34 with the processing gas in a short time.

以上,说明了本发明的最佳实施方式,但是,本发明并不局限于上述实施方式,可以有各种各样的改变。在上述实施方式中,对应用在向下部电极施加高频电力的RIE式的电容耦合型平行平板等离子体蚀刻装置中的例子进行了说明,但是,并不局限于此,也能够应用在灰化、CVD成膜等其它的等离子体处理装置中,而且,也能应用在将基板等被处理体收容在处理容器内进行气体处理的、等离子体处理装置以外的一般气体装置中。另外,在上述实施方式中,对应用在FPD用的玻璃基板的处理中的例子进行了说明,但并不局限于此,即能应用在半导体基板等一般的基板处理中,也能应用在基板以外的被处理体的处理中。As mentioned above, the best embodiment of this invention was described, However, this invention is not limited to the said embodiment, Various changes are possible. In the above-mentioned embodiments, an example of application to an RIE-type capacitively coupled parallel-plate plasma etching apparatus that applies high-frequency power to the lower electrode has been described. , CVD film formation, and other plasma processing apparatuses, and can also be applied to general gas apparatuses other than plasma processing apparatuses that house a substrate such as a substrate in a processing container and perform gas processing. In addition, in the above-mentioned embodiments, an example of application to the processing of glass substrates for FPDs has been described, but the present invention is not limited to this, and it can be applied to general substrate processing such as semiconductor substrates, and can also be applied to substrates. Other than the processed objects are being processed.

Claims (14)

1. handle gas supply mechanism for one kind, it is characterized in that,
It handles gas according to the mode that is housed in the handled object enforcement predetermined processing in the container handling is supplied with in said container handling, this processing gas supply mechanism comprises:
Be used in said container handling, supplying with the processing gas supply source of handling gas;
Be used for temporary transient processing gas tank of storing from the processing gas of said processing gas supply source; With
To supply with said processing gas tank from the processing gas of said processing gas supply source, and the processing gas in the said processing gas tank will be supplied with the processing gas communication parts in the said container handling,
Handle gas and temporarily be stored in the said processing gas tank, and in said container handling, supply with from said processing gas tank from said processing gas supply source,
Said processing gas communication parts comprise: the first processing gas flow path that is being connected with said processing gas supply source and said container handling; And from said first handle gas flow path branch and be connected with said processing gas tank second handle gas flow path,
Said processing gas supply mechanism is also supplied with in said container handling from said processing gas supply source and is handled gas,
Said processing gas tank is provided with a plurality of, and, it is corresponding with the quantity of said processing gas tank and be provided with a plurality of said second and handle gas flow paths,
Each said second processing gas flow path has the stream of sending into that is used for processing gas is sent into said processing gas tank respectively; And be used for seeing stream off from what said processing gas tank was seen off with handling gas.
2. a gas treatment equipment is characterized in that, comprising:
Accommodate the container handling of handled object;
In said container handling, supply with the processing gas supply mechanism of handling gas; And
To carrying out the exhaust unit of exhaust in the said container handling, and,
Under the state that handled object is housed in the said container handling, utilize said exhaust unit to carry out exhaust, utilize said processing gas supply mechanism to supply with simultaneously and handle gas, handled object is implemented predetermined processing,
Said processing gas supply mechanism comprises:
Be used in said container handling, supplying with the processing gas supply source of handling gas;
Be used for temporary transient processing gas tank of storing from the processing gas of said processing gas supply source; With
To supply with said processing gas tank from the processing gas of said processing gas supply source, and the processing gas in the said processing gas tank will be supplied with the processing gas communication parts in the said container handling,
Handle gas and temporarily be stored in the said processing gas tank, and in said container handling, supply with from said processing gas tank from said processing gas supply source,
Said processing gas communication parts comprise: the first processing gas flow path that is being connected with said processing gas supply source and said container handling; And from said first handle gas flow path branch and be connected with said processing gas tank second handle gas flow path,
Said processing gas supply mechanism is also supplied with in said container handling from said processing gas supply source and is handled gas,
Said processing gas tank is provided with a plurality of, and, it is corresponding with the quantity of said processing gas tank and be provided with a plurality of said second and handle gas flow paths,
Each said second processing gas flow path has the stream of sending into that is used for processing gas is sent into said processing gas tank respectively; And be used for seeing stream off from what said processing gas tank was seen off with handling gas.
3. gas treatment equipment according to claim 2 is characterized in that,
Comprise the control part of controlling said processing gas supply mechanism,
Said control part is controlled as follows: make and handle gas and supply with in said container handling through the said stream of seeing off from the part of said a plurality of processing gas tank, make simultaneously handle gas from said processing gas supply source through said send into stream be stored in the remaining part of said a plurality of processing gas tank or all.
4. gas treatment equipment according to claim 2 is characterized in that,
Said second handles gas flow path has the stream of sending into that is used for processing gas is sent into said processing gas tank respectively; And be used for seeing stream with handling gas off from what said processing gas tank was seen off,
Be provided with a plurality of said processing gas supply sources to supply with different multiple processing gas; And; Said first handles gas flow path has and is branched off into supply source a plurality of and that be connected with the said body supply source of regulating the flow of vital energy accordingly everywhere with the quantity of said processing gas supply source and connects stream
Said second handle gas flow path said send into stream be from said first handle gas flow path said each supply source connect stream branch.
5. gas treatment equipment according to claim 4 is characterized in that,
Comprise the control part of controlling said processing gas supply mechanism,
Said control part is controlled as follows: the processing gas be made up of regulation kind and ratio is seen off after stream supplies with in said container handling through said from said processing gas tank; Make the processing gas formed by said regulation kind and ratio from the part of said a plurality of processing gas supply sources or all handle gas flow path and in said container handling, supply with through said first; Meanwhile; Make the processing gas of forming by the kind different and/or ratio, be stored in the said processing gas tank through the said stream of sending into from part or all of said a plurality of processing gas supply sources with said regulation kind and ratio.
6. gas treatment equipment according to claim 2 is characterized in that,
Be provided with a plurality of said processing gas tank, and, it is corresponding with the quantity of said processing gas tank and be provided with a plurality of said second and handle gas flow paths,
Said each second processing gas flow path has the stream of sending into that is used for processing gas is sent into said processing gas tank respectively; And be used for seeing stream with handling gas off from what said processing gas tank was seen off,
Be provided with a plurality of said processing gas supply sources to supply with different multiple processing gas; And; Said first handles gas flow path has and is branched off into supply source a plurality of and that be connected with the said body supply source of regulating the flow of vital energy accordingly everywhere with the quantity of said processing gas supply source and connects stream
Said each second handle gas flow path said send into stream be from said first handle gas flow path said each supply source connect stream branch.
7. gas treatment equipment according to claim 6 is characterized in that,
Comprise the control part of controlling said processing gas supply mechanism,
Said control part is controlled as follows: the processing gas of being made up of regulation kind and ratio is supplied with in said container handling through the said stream of seeing off from the part of said a plurality of processing gas tank; And make the processing gas formed by said regulation kind and ratio from the part of said a plurality of processing gas supply sources or all handle gas flow path and in said container handling, supply with through said first; Meanwhile; Make the processing gas of forming by the kind different and/or ratio, send into stream to be stored in said a plurality of processing gas tank remaining part or all through said from part or all of said a plurality of processing gas supply sources with said regulation kind and ratio.
8. according to each described gas treatment equipment in the claim 2~7, it is characterized in that,
Said first handles gas flow path has respectively: when making processing gas from said processing gas supply source be stored in the said processing gas tank and make the storage of its circulation use stream; And when will supplying with in the said container handling and make the supply of its circulation use stream from the processing gas of said processing gas supply source.
9. according to each described gas treatment equipment in the claim 2~7, it is characterized in that,
Said exhaust unit has the exhaust flow path that a plurality of and said container handling is being connected; And through said exhaust flow path to carrying out the exhaust apparatus of exhaust in the said container handling,
On the part in said processing gas communication parts and the said a plurality of exhaust flow paths, be connected bypass flow path, the processing gas that constitutes in the said processing gas communication parts can be by said exhaust unit discharge through said bypass flow path,
The said exhaust flow path that is connecting said bypass flow path also leans on the upstream side at the upper reaches to open and close freely at the connecting portion than itself and said bypass flow path.
10. according to each described gas treatment equipment in the claim 2~7, it is characterized in that,
In said container handling, also possess plasma and generate mechanism, it generates the plasma of the processing gas of being supplied with by said processing gas supply mechanism,
Said predetermined process is being to use the Cement Composite Treated by Plasma of the plasma of handling gas.
11. handle the gas supply method for one kind, it is characterized in that,
It handles gas according to the mode that is housed in the handled object enforcement predetermined processing in the container handling is supplied with in said container handling, prepare:
Be used in said container handling, supplying with the processing gas supply source of handling gas;
Be used for temporary transient a plurality of processing gas tank of storing from the processing gas of said processing gas supply source; With
To supply with said processing gas tank from the processing gas of said processing gas supply source; And the processing gas in the said processing gas tank supplied with the processing gas communication parts in the said container handling; To handle gas temporarily is stored in the said processing gas tank from said processing gas supply source; And in said container handling, supply with from said processing gas tank
In advance by the first processing gas flow path that is being connected with said processing gas supply source and said container handling; And from said first handle gas flow path branch and be connected with said processing gas tank second handle gas flow path and constitute said processing gas communication parts,
Prepare a plurality of said second accordingly with the quantity of said processing gas tank and handle gas flow path, each said second processing gas flow path has the stream of sending into that is used for processing gas is sent into said processing gas tank respectively; And be used for seeing stream with handling gas off from what said processing gas tank was seen off,
Also in said container handling, supply with and handle gas from said processing gas supply source.
12. processing gas supply method according to claim 11 is characterized in that,
A plurality of said processing gas tank are set, and corresponding with the quantity of said processing gas tank and be provided with a plurality of said second and handle gas flow paths,
Have respectively and be used for sending handling gas into the stream of sending into of said processing gas tank; And be used for seeing stream with handling gas off from what said processing gas tank was seen off, constitutes said each second processing gas flow path,
In said container handling, supply with processing gas from the part of said a plurality of processing gas tank through the said stream of seeing off; Simultaneously, from said processing gas supply source through the said stream storage at body of regulating the flow of vital energy or all of sending in the remaining part of said a plurality of processing gas tank.
13. processing gas supply method according to claim 11 is characterized in that,
Have respectively and be used for sending handling gas into the stream of sending into of said processing gas tank; And be used for seeing stream with handling gas off from what said processing gas tank was seen off, constitute said second and handle gas flow path,
A plurality of said processing gas supply sources are set to supply with different multiple processing gas; And; Handling gas flow path with said first constitutes to have and is branched off into supply source a plurality of and that be connected with the said body supply source of regulating the flow of vital energy accordingly everywhere with the quantity of said processing gas supply source and connects stream
With said said each supply source connection stream branch that sends into stream from the said first processing gas flow path of the said second processing gas flow path,
From said processing gas tank through said see stream off and in said container handling, supply with the processing gas of forming by regulation kind and ratio after; From said a plurality of processing gas supply sources a part or all through said first the processing gas flow path in said container handling, supply with the processing gas of forming by said regulation kind and ratio; Meanwhile, from the part of said a plurality of processing gas supply sources or all said processing gas tank, store the processing gas of forming by the kind different and/or ratio with said regulation kind and ratio through the said stream of sending into.
14. processing gas supply method according to claim 11 is characterized in that,
A plurality of said processing gas tank are set, and corresponding with the quantity of said processing gas tank and be provided with a plurality of said second and handle gas flow paths,
Have respectively and be used for sending handling gas into the stream of sending into of said processing gas tank; And be used for seeing stream with handling gas off from what said processing gas tank was seen off, constitutes said each second processing gas flow path,
A plurality of said processing gas supply sources are set to supply with different multiple processing gas; And; Handling gas flow path with said first constitutes to have and is branched off into supply source a plurality of and that be connected with the said body supply source of regulating the flow of vital energy accordingly everywhere with the quantity of said processing gas supply source and connects stream
With said said each supply source connection stream branch that sends into stream from the said first processing gas flow path of the said second processing gas flow path,
In said container handling, supply with the processing gas of forming by regulation kind and ratio from the part of said a plurality of processing gas tank through the said stream of seeing off; And from said a plurality of processing gas supply sources a part or all through said first the processing gas flow path in said container handling, supply with the processing gas of forming by said regulation kind and ratio; Meanwhile, from the part of said a plurality of processing gas supply sources or all through the said stream of sending at said a plurality of processing gas tank the remaining processing gas that storage is made up of the kind different with said regulation kind and ratio and/or ratio part or all.
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