CN101095814A - Liposoluble effective extracts from onion white and the extracting method thereof - Google Patents
Liposoluble effective extracts from onion white and the extracting method thereof Download PDFInfo
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- CN101095814A CN101095814A CNA2006100195378A CN200610019537A CN101095814A CN 101095814 A CN101095814 A CN 101095814A CN A2006100195378 A CNA2006100195378 A CN A2006100195378A CN 200610019537 A CN200610019537 A CN 200610019537A CN 101095814 A CN101095814 A CN 101095814A
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- 239000000284 extract Substances 0.000 title claims abstract description 39
- 235000002732 Allium cepa var. cepa Nutrition 0.000 title claims abstract description 19
- 238000000034 method Methods 0.000 title claims abstract description 16
- 241000234282 Allium Species 0.000 title claims description 18
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims abstract description 47
- 239000002904 solvent Substances 0.000 claims abstract description 32
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 claims abstract description 20
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 17
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 claims abstract description 14
- 238000001914 filtration Methods 0.000 claims abstract description 12
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 claims abstract description 8
- 239000002994 raw material Substances 0.000 claims abstract description 6
- 239000003208 petroleum Substances 0.000 claims description 17
- 238000001035 drying Methods 0.000 claims description 10
- 239000000796 flavoring agent Substances 0.000 claims description 8
- 235000019634 flavors Nutrition 0.000 claims description 7
- 239000012141 concentrate Substances 0.000 claims description 3
- 238000004108 freeze drying Methods 0.000 claims description 3
- 238000010792 warming Methods 0.000 claims description 2
- 244000291564 Allium cepa Species 0.000 abstract description 11
- 238000000605 extraction Methods 0.000 abstract description 5
- 239000000341 volatile oil Substances 0.000 abstract description 5
- -1 ligarine Chemical compound 0.000 abstract description 4
- 208000024172 Cardiovascular disease Diseases 0.000 abstract description 2
- 230000000694 effects Effects 0.000 abstract description 2
- 150000004676 glycans Chemical class 0.000 abstract description 2
- 229920001282 polysaccharide Polymers 0.000 abstract description 2
- 239000005017 polysaccharide Substances 0.000 abstract description 2
- 239000011782 vitamin Substances 0.000 abstract description 2
- 229940088594 vitamin Drugs 0.000 abstract description 2
- 229930003231 vitamin Natural products 0.000 abstract description 2
- 235000013343 vitamin Nutrition 0.000 abstract description 2
- 150000003722 vitamin derivatives Chemical class 0.000 abstract description 2
- 239000007788 liquid Substances 0.000 abstract 2
- 150000001875 compounds Chemical class 0.000 abstract 1
- 235000011389 fruit/vegetable juice Nutrition 0.000 abstract 1
- 238000002791 soaking Methods 0.000 abstract 1
- 229930002600 steroidal saponin Natural products 0.000 abstract 1
- 239000000243 solution Substances 0.000 description 15
- GMBQZIIUCVWOCD-WWASVFFGSA-N Sarsapogenine Chemical compound O([C@@H]1[C@@H]([C@]2(CC[C@@H]3[C@@]4(C)CC[C@H](O)C[C@H]4CC[C@H]3[C@@H]2C1)C)[C@@H]1C)[C@]11CC[C@H](C)CO1 GMBQZIIUCVWOCD-WWASVFFGSA-N 0.000 description 14
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 12
- 235000001270 Allium sibiricum Nutrition 0.000 description 9
- 239000000523 sample Substances 0.000 description 9
- ZRSNZINYAWTAHE-UHFFFAOYSA-N p-methoxybenzaldehyde Chemical compound COC1=CC=C(C=O)C=C1 ZRSNZINYAWTAHE-UHFFFAOYSA-N 0.000 description 8
- RTMWIZOXNKJHRE-UHFFFAOYSA-N Tigogenin Natural products CC1COC2CC(C)(OC12)C3CCC4C5CCC6CC(O)CCC6(C)C5CCC34C RTMWIZOXNKJHRE-UHFFFAOYSA-N 0.000 description 7
- 239000000126 substance Substances 0.000 description 6
- 241001280436 Allium schoenoprasum Species 0.000 description 5
- 238000010521 absorption reaction Methods 0.000 description 5
- WQLVFSAGQJTQCK-UHFFFAOYSA-N diosgenin Natural products CC1C(C2(CCC3C4(C)CCC(O)CC4=CCC3C2C2)C)C2OC11CCC(C)CO1 WQLVFSAGQJTQCK-UHFFFAOYSA-N 0.000 description 5
- NWMIYTWHUDFRPL-UHFFFAOYSA-N sapogenin Natural products COC(=O)C1(CO)C(O)CCC2(C)C1CCC3(C)C2CC=C4C5C(C)(O)C(C)CCC5(CCC34C)C(=O)O NWMIYTWHUDFRPL-UHFFFAOYSA-N 0.000 description 5
- 235000010167 Allium cepa var aggregatum Nutrition 0.000 description 4
- 244000016163 Allium sibiricum Species 0.000 description 4
- 238000003556 assay Methods 0.000 description 4
- 229960004756 ethanol Drugs 0.000 description 4
- 150000003431 steroids Chemical class 0.000 description 4
- 239000000470 constituent Substances 0.000 description 3
- 239000000843 powder Substances 0.000 description 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- 238000002835 absorbance Methods 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 229960000935 dehydrated alcohol Drugs 0.000 description 2
- 230000035558 fertility Effects 0.000 description 2
- 239000000706 filtrate Substances 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 239000013558 reference substance Substances 0.000 description 2
- 239000012488 sample solution Substances 0.000 description 2
- 239000012086 standard solution Substances 0.000 description 2
- 239000001117 sulphuric acid Substances 0.000 description 2
- 235000011149 sulphuric acid Nutrition 0.000 description 2
- 206010000087 Abdominal pain upper Diseases 0.000 description 1
- 206010010774 Constipation Diseases 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 206010019233 Headaches Diseases 0.000 description 1
- 206010061217 Infestation Diseases 0.000 description 1
- 241001349804 Juncus alpinoarticulatus Species 0.000 description 1
- 208000002720 Malnutrition Diseases 0.000 description 1
- 208000002193 Pain Diseases 0.000 description 1
- 208000037386 Typhoid Diseases 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 238000004737 colorimetric analysis Methods 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 208000001848 dysentery Diseases 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 235000013355 food flavoring agent Nutrition 0.000 description 1
- 238000007710 freezing Methods 0.000 description 1
- 230000008014 freezing Effects 0.000 description 1
- 231100000869 headache Toxicity 0.000 description 1
- 239000002932 luster Substances 0.000 description 1
- 230000001071 malnutrition Effects 0.000 description 1
- 235000000824 malnutrition Nutrition 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000002398 materia medica Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 208000015380 nutritional deficiency disease Diseases 0.000 description 1
- 230000003071 parasitic effect Effects 0.000 description 1
- 239000000419 plant extract Substances 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 238000000194 supercritical-fluid extraction Methods 0.000 description 1
- 208000011580 syndromic disease Diseases 0.000 description 1
- 201000008297 typhoid fever Diseases 0.000 description 1
- 235000013311 vegetables Nutrition 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
- 238000005303 weighing Methods 0.000 description 1
- 239000002023 wood Substances 0.000 description 1
- 230000037303 wrinkles Effects 0.000 description 1
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- Medicines Containing Plant Substances (AREA)
Abstract
The invention discloses a scallion stalk fat-soluble effective extract and the extraction method. The method comprises following steps: disintegrating one or the combination of dry scallion stalk or dry onion juice or dry onion, cold soaking or warm extracting with one of ether, ligarine, chloroform, acetic acid ethyl ester, butanol and ethanol for 1-24 hours, filtering extraction liquid, condensing extraction liquid to remove solvent and getting fat soluble effective extract. The ratio between said raw material and solvent is 1g: 6-15ml, the relative density of said fat soluble effective extract at 20 Deg. C is 0.8000-0.9000; the refractive index at 20 Deg. C is 1.2500-1.4500.The main component in said fat soluble extract comprises volatile oil, steroidal saponins compound, chromocor compound, vitamin and polysaccharide. The extract effect for treating cardiovascular disease is distinctive. The extraction process is simple, controllable and stable.
Description
Technical field
The invention belongs to plant extract and extracting method, being specifically related to a kind of is the extract and the extracting method of the very light blue liposoluble substance of raw material with very light blue or dried Sucus Allii Fistulosi or full Herba Alii fistulosi, specifically adopts solvent method to extract.
Background technology
Very light blue title is according to the medicinal custom of history, and so the dispersing wind-cold exterior syndrome is all with very light blue and name.Its source is the fresh bulb of liliaceous plant shallot Allium fisturosum L.var.caespitosum Makio or chive Allium schoenoprasum.The four seasons can gather, and clean using fresh herb.Herba Alii fistulosi beginning alpine rush or palm-bark rain cape be stated from { Newly Revised Canon of Materia Medica } " its human world food Herba Alii fistulosi has 2 kinds again, and the Herba Alii fistulosi of freezing is arranged, and is promptly not dead through the winter, divide stem to plant to transplant and loss of fecundity also; Chinese Herba Alii fistulosi is arranged again, and the winter is that leaf is withered ", the former is like shallot, and the latter is like chive.The Compendium of Material Medica cloud: " shallot is kind Herba Alii fistulosi ..., stem is soft and fine and fragrant, can be through the winter, wooden Herba Alii fistulosi of Chinese Herba Alii fistulosi, its stem is thick and stiff, so the wood name is arranged.The shallot loss of fecundity, Chinese Herba Alii fistulosi spring end is bloomed into clump, Bluish white, its sub-acrid in the mouth, darkish complexion has wrinkle, makes 3 flaps. describe according to it, the person like shallot, the latter is like Herba Alii fistulosi.Very light bluely be distributed widely in the Northern Hemisphere, the centuries, very light blue in the Middle East and the Far East Area extensively cultivate, very light blue abundant in china natural resources, be mainly used in vegetable and flavoring agent.And do not have the report of the effective extract in the fresh bulb of open shallot Allium fisturosum L.var.caespitosum Makio of document or chive Allium schoenoprasum at present.
Summary of the invention
The object of the present invention is to provide liposoluble effective extracts and extracting method thereof in the fresh bulb of a kind of shallot Allium fisturosum L.var.caespitosum Makio or chive Allium schoenoprasum, adopt solvent method to extract.
The technical scheme that realizes one of the object of the invention is: lipophilic effective extract of Chinese green onion, it is after one or more the combination in exsiccant very light blue or dried Sucus Allii Fistulosi or the dry full Herba Alii fistulosi is pulverized, adopt a kind of solvent cold soak or heat in ether, petroleum ether, petroleum ether, chloroform, ethyl acetate, butanols and the ethanol to carry 1～24 hour, filtering extracting solution, extracting solution concentrated remove solvent, promptly get fat-soluble live part extract; The w/v of described raw material and solvent is: 1g: 6～15ml, and described fat-soluble live part extract is 0.8000～0.9000 20 ℃ of relative densities; Index of refraction is 1.2500～1.4000 at D20 ℃.
Two the technical scheme that realizes the object of the invention is: the extracting method of lipophilic effective extract of Chinese green onion, it is after one or more the combination in exsiccant very light blue or dried Sucus Allii Fistulosi or the dry full Herba Alii fistulosi is pulverized, adopt a kind of solvent cold soak or heat in ether, petroleum ether, chloroform, ethyl acetate, butanols and the ethanol to carry 1～24 hour, filtering extracting solution, extracting solution concentrated remove solvent, promptly get fat-soluble live part extract; The w/v of described raw material and solvent is: 1g: 6～15ml.
It is to adopt petroleum ether (30～60 ℃) to extract.
It is to adopt a kind of solvent in petroleum ether (60～90 ℃), chloroform, ethyl acetate, butanols and the ethanol to extract.
Described extracting solution concentrates and to remove solvent and be: be evaporated to no above-mentioned solvent at 25～60 ℃ of temperature, pressure 0.08～0.095Mpa and distinguish the flavor of.
Main component contains volatile oil, steroid saponin compound, chromocor compound, vitamin, polysaccharide etc. in the described liposoluble effective extracts.Nature and flavor suffering, temperature; Function is for delivering, activate yang, detoxifying.Be used for the headache of typhoid fever cold and heat, YIN-cold stomachache, the malnutrition due to parasitic infestation internal resistance, constipation and anuresis, dysentery, pain is swollen.Aspects such as cardiovascular disease there is significant curative effect.Its extracting method is simple, and is easy to control, stable.
The specific embodiment
This extract is the liposoluble effective extracts of shallot Allium fisturosum L.var.caespi-tosumMakio or chive Allium schoenoprasum L., and it can be above-mentioned fresh bulb or bright Sucus Allii Fistulosi or fresh full Herba Alii fistulosi, after drying, passes through CO again
2The supercritical extraction separation and Extraction.Drying wherein very light blue or Sucus Allii Fistulosi or full Herba Alii fistulosi can adopt micro-wave drying method; The temperature that is microwave drying is 20～60 ℃; The microwave drying time is 15min～5h, and vacuum is 0.085～0.095Mpa.Also can adopt: freeze-drying; Promptly at-30～-50 ℃ of pre-freeze 24h, dividing plate to 0 ℃ dry 12h is heightened then with-30～-50 ℃ of dry 12h in the back, is warming up to 10 ℃ of dry 6h after finishing again, gives birth to 20 ℃ of dry 6h at last.
After one or more combination in above-mentioned exsiccant very light blue or dried Sucus Allii Fistulosi or the dry full Herba Alii fistulosi pulverized, extract with solvent.
Embodiment 1
Use ether 60～150ml merceration after 1～24 hour above-mentioned powder 10g, filtering extracting solution is evaporated to no above-mentioned solvent flavor with extracting solution at 25～60 ℃ of temperature, pressure 0.08～0.095Mpa, promptly gets fat-soluble live part extract.
The consumption of above-mentioned solvent ether can be according to production requirement, can select between 60～150ml to select arbitrarily any interval value within some points such as 60ml, 80ml, 88ml, 95.6ml, 160ml or the 60～150ml, as the consumption between 65～130ml, the 60～100ml etc.; The described merceration time can select some points or the interval value within 1～24 hour to select arbitrarily between 1～24 hour.
Embodiment 2
After above-mentioned powder 10g extracted 1～24 hour with petroleum ether 60～150ml of 30～60 ℃, filtering extracting solution, extracting solution is evaporated to no above-mentioned solvent flavor at 25～60 ℃ of temperature, pressure 0.08～0.095Mpa, promptly gets fat-soluble live part extract.
A kind of conventional requirement during said extracted can adopt merceration or seepage or heat to carry to wait is carried out; The consumption of petroleum ether can be selected any some points between 60～150ml, as 60ml, 80ml, 88ml, 95.6ml, 160ml etc. or be chosen in any interval value within 60～150ml, and as 60～120ml, 70～140ml etc.
Embodiment 3
After above-mentioned powder 10g extracted 1～24 hour with a kind of 60～150ml in the petroleum ether of ethanol, chloroform, ethyl acetate, butanols and 60～90 ℃, filtering extracting solution, extracting solution is evaporated to no above-mentioned solvent flavor at 25～60 ℃ of temperature, pressure 0.08～0.095Mpa, promptly gets fat-soluble live part extract.
A kind of conventional requirement during said extracted can adopt merceration or seepage or heat to carry to wait is carried out, the consumption of solvent can be selected any some points between 60～150ml, as 65ml, 75ml, 90ml, 100ml, 150ml or be chosen in interval value within 60～150ml, as 70～100ml, 76～160ml etc.
The spissated temperature of extracting solution can be selected some points arbitrarily in the foregoing description between 25～60 ℃, and pressure can be selected some points arbitrarily between 0.08～0.095Mpa.
The filtration of extracting solution can be adopted one or many, after the multiple times of filtration, the filtering filtrate of each time is mixed the back reconcentration remove solvent.
Use it for anything else fully through extracting the filtrate of filtering gained in the foregoing description.
The said extracted thing is measured:
The physicochemical constant of fat-soluble effective site is through the repeated detection analysis:
(1) extracts percentage rate (g/g): 1.20%～6%
(2) color and luster: yellowish-brown
(3) relative density (20 ℃): 0.8000～0.9000 interval interior any value.
(4) index of refraction (D20 ℃): 1.2500～1.4500 interval interior any values.
Fat-soluble effective site volatile oil contents is measured
Adopt the assay method of Chinese Pharmacopoeia volatile oil to measure
Sample determination: precision is measured quantity of sample, presses 57 pages of mensuration of 2005 editions appendix of Chinese Pharmacopoeia, and volatile oil content is 0.01～0.05%.
The assay of steroid sapogenin
Adopt colorimetry to measure sapogenin constituents content, the reaction of main at present employing anisaldehyde is carried out quantitatively, is that standard substance are found out sample and standard substance maximum absorption band by UV scanning with the Sarsasapogenin.And, make standard curve with the Sarsasapogenin standard substance at the maximum absorption band place, come the content of steroid sapogenin constituents in the working sample with this.
Key instrument and reagent
CARY 50 Scan UV-Visible Spectrophotometer；
Anisaldehyde, methanol, concentrated hydrochloric acid, concentrated sulphuric acid, petroleum ether (60～90 ℃) and dehydrated alcohol are analytical pure;
The Sarsasapogenin reference substance
The mensuration of maximum absorption band
Accurately draw a certain amount of Sarsasapogenin standard solution, volatilize solvent, and adding 0.5ml anisaldehyde solution (anisaldehyde: concentrated sulphuric acid: dehydrated alcohol=0.1: 1: 18.9), boiling water bath 15min, ice bath 10min adds methanol constant volume to 10ml.Thereby in 200～700nm scope, carry out UV scanning by ultraviolet scanner and determine its maximum absorption band.In kind sample solution is done chromogenic reaction; Compare then, sample and standard substance all are equipped with absorption maximum in 420nm place identical bits.
The assay of steroid sapogenin constituents
The preparation of reference substance solution: precision takes by weighing 2mg Sarsasapogenin standard substance, uses dissolve with methanol, and is fixed molten to the 2ml volumetric flask, standby.
The preparation of standard curve: draw 0.15ml, 0.20ml, 0.25ml, 0.30ml, 0.35ml standard solution respectively, add methanol constant volume to 10ml, measure as stated above, get standard curve linear equation Y=0.7946x+0.1229 R2=0.9980, the result shows: Sarsasapogenin is good in 0.015～0.035mg scope internal linear relation.
| Sample volume (ml) | 0.15 | 0.20 | 0.25 | 0.30 | 0.35 |
| Concentration (mg/ml) | 0.015 | 0.020 | 0.025 | 0.030 | 0.035 |
| Absorbance | 0.239 | 0.286 | 0.322 | 0.361 | 0.400 |
The assay of sample
Precision is measured quantity of sample solution, measures its absorbance as stated above, and the standard curve by Sarsasapogenin calculates sample size, and steroid sapogenin contains 15～30% in the sample
Lipophilic effective extract of Chinese green onion has high medical value.
Claims (10)
1, a kind of extracting method of lipophilic effective extract of Chinese green onion, it is after one or more the combination in exsiccant very light blue or dried Sucus Allii Fistulosi or the dry full Herba Alii fistulosi is pulverized, adopt a kind of solvent cold soak or heat in ether, petroleum ether, petroleum ether, chloroform, ethyl acetate, butanols and the ethanol to carry 1～24 hour, filtering extracting solution, extracting solution concentrated remove solvent, promptly get fat-soluble live part extract; The w/v of described raw material and solvent is: 1g: 6～15ml.
2, the extracting method of lipophilic effective extract of Chinese green onion according to claim 1, it is characterized in that described extracting solution concentrates removes solvent and is: be evaporated to no above-mentioned solvent at 25～60 ℃ of temperature, pressure 0.08～0.095Mpa and distinguish the flavor of.
3, the extracting method of lipophilic effective extract of Chinese green onion according to claim 1 is characterized in that it is to adopt 30～60 ℃ petroleum ether to extract.
4, the extracting method of lipophilic effective extract of Chinese green onion according to claim 1 is characterized in that it is to adopt 60～90 ℃ petroleum ether solvent to extract.
5, a kind of lipophilic effective extract of Chinese green onion, it is after one or more the combination in exsiccant very light blue or dried Sucus Allii Fistulosi or the dry full Herba Alii fistulosi is pulverized, the combination solvent merceration or the heat of one or more in employing ether, petroleum ether, petroleum ether, chloroform, ethyl acetate, butanols and the ethanol are carried 1～24 hour, filtering extracting solution, extracting solution concentrated remove solvent, promptly get fat-soluble live part extract; The w/v of described raw material and solvent is: 1g: 6～15ml, and described fat-soluble live part extract is 0.8000～0.9000 20 ℃ of relative densities; Index of refraction is 1.2500～1.4500 at D20 ℃.
6, as lipophilic effective extract of Chinese green onion as described in the claim 5, it is characterized in that: described extracting solution concentrates and removes solvent and be: be evaporated to no above-mentioned solvent at 25～60 ℃ of temperature, pressure 0.08～0.095Mpa and distinguish the flavor of.
7,, it is characterized in that it is to adopt 30～60 ℃ petroleum ether to extract to obtain as lipophilic effective extract of Chinese green onion as described in the claim 5.
8,, it is characterized in that it is to adopt 60～90 ℃ petroleum ether solvent to extract to obtain as lipophilic effective extract of Chinese green onion as described in the claim 5.
9, the extracting method of lipophilic effective extract of Chinese green onion or as lipophilic effective extract of Chinese green onion as described in the claim 5 according to claim 1 is characterized in that the drying means of described exsiccant very light blue or dried Sucus Allii Fistulosi or dry full Herba Alii fistulosi is: micro-wave drying method; The temperature of described micro-wave drying method is 20～60 ℃; The microwave drying time is 15min～5h, and vacuum is 0.085～0.095Mpa.
10, the extracting method of lipophilic effective extract of Chinese green onion or as lipophilic effective extract of Chinese green onion as described in the claim 5 according to claim 1 is characterized in that the drying means of described exsiccant very light blue or dried Sucus Allii Fistulosi or dry full Herba Alii fistulosi is: freeze-drying; Described freeze-drying is: at-30～-50 ℃ of pre-freeze 24h, dividing plate to 0 ℃ dry 12h is heightened then with-30～-50 ℃ of dry 12h in the back, is warming up to 10 ℃ of dry 6h after finishing again, gives birth to 20 ℃ of dry 6h at last.
Priority Applications (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNA2006100195378A CN101095814A (en) | 2006-06-30 | 2006-06-30 | Liposoluble effective extracts from onion white and the extracting method thereof |
| PCT/CN2007/001947 WO2008003226A1 (en) | 2006-06-30 | 2007-06-21 | Caulis allii fistulosum extract and the use in modulating blood-lipids and lowering cholesterols thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNA2006100195378A CN101095814A (en) | 2006-06-30 | 2006-06-30 | Liposoluble effective extracts from onion white and the extracting method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN101095814A true CN101095814A (en) | 2008-01-02 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNA2006100195378A Pending CN101095814A (en) | 2006-06-30 | 2006-06-30 | Liposoluble effective extracts from onion white and the extracting method thereof |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101919437A (en) * | 2010-09-26 | 2010-12-22 | 福建农林大学 | Microwave Vacuum Drying Technology of Shallot |
| CN103181401A (en) * | 2013-02-26 | 2013-07-03 | 安徽师范大学 | Algistat |
| CN103229857A (en) * | 2013-04-25 | 2013-08-07 | 西华大学 | Quenching and extracting process of onion oil and garlic oil |
-
2006
- 2006-06-30 CN CNA2006100195378A patent/CN101095814A/en active Pending
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101919437A (en) * | 2010-09-26 | 2010-12-22 | 福建农林大学 | Microwave Vacuum Drying Technology of Shallot |
| CN103181401A (en) * | 2013-02-26 | 2013-07-03 | 安徽师范大学 | Algistat |
| CN103229857A (en) * | 2013-04-25 | 2013-08-07 | 西华大学 | Quenching and extracting process of onion oil and garlic oil |
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