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CN101095022A - Assembly of heat exchangers and a cryogenic distillation apparatus incorporating the same - Google Patents

Assembly of heat exchangers and a cryogenic distillation apparatus incorporating the same Download PDF

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Publication number
CN101095022A
CN101095022A CNA2005800456422A CN200580045642A CN101095022A CN 101095022 A CN101095022 A CN 101095022A CN A2005800456422 A CNA2005800456422 A CN A2005800456422A CN 200580045642 A CN200580045642 A CN 200580045642A CN 101095022 A CN101095022 A CN 101095022A
Authority
CN
China
Prior art keywords
heat exchanger
exchanger body
fluid
group
heat
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CNA2005800456422A
Other languages
Chinese (zh)
Other versions
CN100590374C (en
Inventor
P·卡瓦涅
A·吉亚尔
P·勒博
D·古尔丹
M·瓦格纳
F·茹达斯
J-M·佩龙
B·索尼耶
D·阿弗鲁
I·瑙德
I·莱沃
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Nordon Cryogenic Technique Corp
LAir Liquide SA pour lEtude et lExploitation des Procedes Georges Claude
Original Assignee
Nordon Cryogenic Technique Corp
LAir Liquide SA pour lEtude et lExploitation des Procedes Georges Claude
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Filing date
Publication date
Application filed by Nordon Cryogenic Technique Corp, LAir Liquide SA pour lEtude et lExploitation des Procedes Georges Claude filed Critical Nordon Cryogenic Technique Corp
Publication of CN101095022A publication Critical patent/CN101095022A/en
Application granted granted Critical
Publication of CN100590374C publication Critical patent/CN100590374C/en
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    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F28—HEAT EXCHANGE IN GENERAL
    • F28D—HEAT-EXCHANGE APPARATUS, NOT PROVIDED FOR IN ANOTHER SUBCLASS, IN WHICH THE HEAT-EXCHANGE MEDIA DO NOT COME INTO DIRECT CONTACT
    • F28D9/00—Heat-exchange apparatus having stationary plate-like or laminated conduit assemblies for both heat-exchange media, the media being in contact with different sides of a conduit wall
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/0204—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream characterised by the feed stream
    • F25J3/0223—H2/CO mixtures, i.e. synthesis gas; Water gas or shifted synthesis gas
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/0228—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream characterised by the separated product stream
    • F25J3/0252—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream characterised by the separated product stream separation of hydrogen
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/0228—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream characterised by the separated product stream
    • F25J3/0261—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream characterised by the separated product stream separation of carbon monoxide
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/0295—Start-up or control of the process; Details of the apparatus used, e.g. sieve plates, packings
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04006—Providing pressurised feed air or process streams within or from the air fractionation unit
    • F25J3/04078—Providing pressurised feed air or process streams within or from the air fractionation unit providing pressurized products by liquid compression and vaporisation with cold recovery, i.e. so-called internal compression
    • F25J3/0409—Providing pressurised feed air or process streams within or from the air fractionation unit providing pressurized products by liquid compression and vaporisation with cold recovery, i.e. so-called internal compression of oxygen
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04151—Purification and (pre-)cooling of the feed air; recuperative heat-exchange with product streams
    • F25J3/04187—Cooling of the purified feed air by recuperative heat-exchange; Heat-exchange with product streams
    • F25J3/04218—Parallel arrangement of the main heat exchange line in cores having different functions, e.g. in low pressure and high pressure cores
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04151—Purification and (pre-)cooling of the feed air; recuperative heat-exchange with product streams
    • F25J3/04187—Cooling of the purified feed air by recuperative heat-exchange; Heat-exchange with product streams
    • F25J3/0423—Subcooling of liquid process streams
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04151—Purification and (pre-)cooling of the feed air; recuperative heat-exchange with product streams
    • F25J3/04187—Cooling of the purified feed air by recuperative heat-exchange; Heat-exchange with product streams
    • F25J3/04236—Integration of different exchangers in a single core, so-called integrated cores
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04406—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air using a dual pressure main column system
    • F25J3/04412—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air using a dual pressure main column system in a classical double column flowsheet, i.e. with thermal coupling by a main reboiler-condenser in the bottom of low pressure respectively top of high pressure column
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04763—Start-up or control of the process; Details of the apparatus used
    • F25J3/04866—Construction and layout of air fractionation equipments, e.g. valves, machines
    • F25J3/04872—Vertical layout of cold equipments within in the cold box, e.g. columns, heat exchangers etc.
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04763—Start-up or control of the process; Details of the apparatus used
    • F25J3/04866—Construction and layout of air fractionation equipments, e.g. valves, machines
    • F25J3/0489—Modularity and arrangement of parts of the air fractionation unit, in particular of the cold box, e.g. pre-fabrication, assembling and erection, dimensions, horizontal layout "plot"
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04763—Start-up or control of the process; Details of the apparatus used
    • F25J3/04866—Construction and layout of air fractionation equipments, e.g. valves, machines
    • F25J3/04945—Details of internal structure; insulation and housing of the cold box
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J5/00—Arrangements of cold exchangers or cold accumulators in separation or liquefaction plants
    • F25J5/002—Arrangements of cold exchangers or cold accumulators in separation or liquefaction plants for continuously recuperating cold, i.e. in a so-called recuperative heat exchanger
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F28—HEAT EXCHANGE IN GENERAL
    • F28D—HEAT-EXCHANGE APPARATUS, NOT PROVIDED FOR IN ANOTHER SUBCLASS, IN WHICH THE HEAT-EXCHANGE MEDIA DO NOT COME INTO DIRECT CONTACT
    • F28D9/00—Heat-exchange apparatus having stationary plate-like or laminated conduit assemblies for both heat-exchange media, the media being in contact with different sides of a conduit wall
    • F28D9/0093—Multi-circuit heat-exchangers, e.g. integrating different heat exchange sections in the same unit or heat-exchangers for more than two fluids
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F28—HEAT EXCHANGE IN GENERAL
    • F28F—DETAILS OF HEAT-EXCHANGE AND HEAT-TRANSFER APPARATUS, OF GENERAL APPLICATION
    • F28F9/00—Casings; Header boxes; Auxiliary supports for elements; Auxiliary members within casings
    • F28F9/26—Arrangements for connecting different sections of heat-exchange elements, e.g. of radiators
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2290/00—Other details not covered by groups F25J2200/00 - F25J2280/00
    • F25J2290/30—Details about heat insulation or cold insulation
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2290/00—Other details not covered by groups F25J2200/00 - F25J2280/00
    • F25J2290/40—Vertical layout or arrangement of cold equipments within in the cold box, e.g. columns, condensers, heat exchangers etc.
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2290/00—Other details not covered by groups F25J2200/00 - F25J2280/00
    • F25J2290/42—Modularity, pre-fabrication of modules, assembling and erection, horizontal layout, i.e. plot plan, and vertical arrangement of parts of the cryogenic unit, e.g. of the cold box
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2290/00—Other details not covered by groups F25J2200/00 - F25J2280/00
    • F25J2290/50—Arrangement of multiple equipments fulfilling the same process step in parallel
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F28—HEAT EXCHANGE IN GENERAL
    • F28F—DETAILS OF HEAT-EXCHANGE AND HEAT-TRANSFER APPARATUS, OF GENERAL APPLICATION
    • F28F2270/00—Thermal insulation; Thermal decoupling

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  • Engineering & Computer Science (AREA)
  • Physics & Mathematics (AREA)
  • Mechanical Engineering (AREA)
  • Thermal Sciences (AREA)
  • General Engineering & Computer Science (AREA)
  • Health & Medical Sciences (AREA)
  • Emergency Medicine (AREA)
  • Separation By Low-Temperature Treatments (AREA)
  • Heat-Exchange Devices With Radiators And Conduit Assemblies (AREA)

Abstract

Heat exchange assembly comprising at least one first and one second heat exchange body (5, 7), each body being of the plate heat exchanger type, comprising a plurality of metal plates of substantially similar contour extending along a first dimension or length and a second dimension or width, spaced from and arranged in parallel rows to one another along a third dimension or thickness and sealing means bounding flattened passages with the said plates, forming at least one passage of a first type and at least one passage of a second type, the sealing means allocated to each passage releasing one fluid inlet and one fluid outlet, characterized in that one side bounded by a width and a thickness of at least one first heat exchange body is located at least partially opposite a side bounded by a width and a thickness of at least one second heat exchange body, the two sides being separated by insulating material (I).

Description

Heat exchangers and the cryogenic distillation apparatus that is combined with this sub-assembly
Technical field
The present invention relates to a kind of heat exchangers, a kind of cryogenic distillation apparatus that is combined with this heat exchangers, and a kind of cryogenic distillation method that uses this heat exchangers.
Background technology
Be air distillation, cool air to very low temperature.Heat exchange for restriction and external environment, by one or more heat-insulating materials (as perlite, rock wool etc.) each tower and heat exchanger are incubated, come from this each tower and heat exchanger that the fluid of gas takes place by separating/liquefying of each stage in the air, because this heat-insulating material of mechanical reason is contained in the macrostructure that generally is called ice chest (cold box).
The size of these ice chests depends on the quantity of tower, the quantity of heat exchanger, the size that also depends on tower and heat exchanger, depend on each pipeline and other additional low-temperature device, depend on all these low-temperature devices distance of needed heat-insulating material and the external structure of holding heat-insulating material each other.
Under many situations, for this air separation equipment, reason for quality and control, advantageously, these comprise following vitals in special prefabrication---be tower, all or nearly all additional low-temperature device and cryogenic pipe, also comprise heat exchanger---structure, the configuration that limits simultaneously these " cold box package " as far as possible transports between the local and final place of installing of making being suitable for.
The heat exchanger body of the air that is sent to air separation equipment is cooled off in two kinds of different being used for of known use.FR-A-2 846 077, US-A-4 555 256, described a kind of first heat exchanger body that is used under high pressure cooling off and adds hot fluid and a kind of being used among EP-A-0 044 679 and the EP-A-0 042676 and depressed cooling and adding second heat exchanger body of hot fluid.
The present invention be applicable to fully restriction accommodate heat-insulating material external structure size and no matter the air-treatment ability of the type of separation of being considered and this separative element, and, be applicable to the capacity limit of the separation equipment that enlarges factory-prefabricated with regard to cold box package.
Summary of the invention
An object of the present invention is to provide a heat exchangers, this sub-assembly comprises at least one first heat exchanger body and one second heat exchanger body, each heat exchanger body is the heat-exchangers of the plate type type and comprises: a plurality of have a metallic plate of similar profile basically, these metallic plates extend along first direction or length and second direction or width, along third direction or thickness at each interval, be provided with in parallel to each other; And sealing device, sealing device and above-mentioned plate limit flat channel together, form the passage of at least one first kind and the passage of at least one second type, the sealing device that is allocated in each passage forms (releasing) fluid inlet and a fluid issuing, an import of first heat exchanger body is connected to first conveyance conduit (delivery line) that is used for fluid to be cooled, an outlet of first heat exchanger body is connected to first collecting loop (collecting line) that is used for cooled fluid, another import of first heat exchanger body is connected to first conveyance conduit that is used for fluid to be heated, another outlet of first heat exchanger body is connected to one and is used to heat first collecting loop of fluid afterwards, an import of second heat exchanger body is connected to a conveyance conduit that is used for fluid to be cooled, an outlet of second heat exchanger body is connected to a collecting loop that is used for cooled fluid, another import of second heat exchanger body is connected to a conveyance conduit that is used for fluid to be heated, another outlet of second heat exchanger body is connected to one and is used to heat the collecting loop of fluid afterwards, it is characterized in that, the relative at least in part configuration in side that the side that is limited by the width of at least one first heat exchanger body and thickness and width and the thickness by at least one second heat exchanger body limit, these two sides are separated by heat-insulating material.
According to other optional aspect:
At least one heat exchanger body of-the second group of heat exchanger is connected to a fluid-transporting tubing that is not connected with any heat exchanger body of first group of heat exchanger, and alternatively, at least one heat exchanger body of second group of heat exchanger is connected to a fluid collecting loop that is not connected with any heat exchanger body of first group of heat exchanger;
-the first heat exchanger body forms the part of first group of heat exchanger of the heat exchanger body with at least three arrangements of embarking on journey basically, at least two first heat exchanger body of first group of heat exchanger are connected to first conveyance conduit that is used for fluid to be cooled abreast at least, first conveyance conduit that is used for fluid to be heated, be used to heat first collecting loop of back fluid, be used to cool off first collecting loop of back fluid, and/or, second heat exchanger body forms the part of second group of heat exchanger with at least three heat exchanger body of arranging of embarking on journey basically, and at least two second heat exchanger body of second group of heat exchanger are parallel to be connected to the conveyance conduit that at least one is used for fluid to be cooled, at least one is used for the conveyance conduit of fluid to be heated, at least one is used to cool off the collecting loop of back fluid and is connected to the collecting loop that is used to heat the back fluid at least;
An import of-the second heat exchanger body is connected to first conveyance conduit that is used for fluid to be cooled and/or first conveyance conduit that is used for fluid to be heated;
An import of-the second heat exchanger body is connected to that of being different from first conveyance conduit that is used for fluid to be cooled is used for the conveyance conduit of fluid to be cooled and/or another import of second heat exchanger body is connected to a conveyance conduit that is used for fluid to be heated that is different from first conveyance conduit that is used for fluid to be heated;
-this sub-assembly comprises and the passage of second heat exchanger body liquid conducting pipes that be connected, that be used for liquid is sent at least one second heat exchanger body that described passage is connected with the outlet that back liquid is evaporated near being used to of an import that is positioned at gas to be cooled;
At least one first heat exchanger body of-(first group of heat exchanger) only is connected at least one gas transmission pipeline and/or at least one is used for the pipeline of liquid to be cooled;
-at least one heat exchanger body is arranged between the side positioned opposite to each other of first heat exchanger body and second heat exchanger body.
The heat exchanger body of " arrangement (aligned) of embarking on journey " longitudinally is arranged side by side each other.
Term " liquid " comprises pseudo-liquid (psuedo-liquids), the just liquid on critical pressure.
" liquid injection " means that a kind of cryogenic liquid is injected into Tower System, and purpose is to absorb heat.
Another object of the present invention provides a kind of equipment that is used for the cryogenic separation of admixture of gas, and this equipment comprises elution unit (stripping unit), as described sub-assembly of one of claim 1-8 and Tower System, be used for admixture of gas is sent to the device of above-mentioned elution unit, be used for the admixture of gas after the elution is sent to heat exchangers so that the admixture of gas after this elution is cooled to the device of at least one pressure at least in one of heat exchanger body of first and second groups of heat exchangers, each the device that is used for that at least some admixture of gas that cools off are sent to the device of Tower System and is used at least a product from Tower System is sent to first and second heat exchanger body at least one of first and second heat exchanger body.
According to other optional aspect of the present invention, this equipment comprises:
-be used for that the liquid flow a kind of component, pressurization that is rich in admixture of gas delivered to the device of (second group of heat exchanger) at least one second heat exchanger body and the gas that is used for being rich in a kind of component of admixture of gas is sent to the device of (first group of heat exchanger) first heat exchanger body;
-at least one heat exchanger body, described at least one heat exchanger body constitutes a subcooler, and this subcooler is positioned over the below of the heat exchanger body of first group of heat exchanger, preferably is placed on the below of the heat exchanger body of second group of heat exchanger;
-reboiler-condenser and be used for a kind of treat condensed gas and a kind of liquid to be evaporated that comes from the Tower System that comes from Tower System is delivered to device wherein, above-mentioned reboiler-condenser is positioned at the top of the heat exchanger body of the outside of any tower of system, second group of heat exchanger, is preferably located in the top of the heat exchanger body of first group of heat exchanger.
Another object of the present invention provides a kind of equipment that is used for the cryogenic separation of admixture of gas, this equipment comprises the elution unit, the sub-assembly that comprises at least one first heat exchanger and one second heat exchanger, Tower System, be used for this admixture of gas is sent to the device of elution unit, be used for the admixture of gas after the elution is sent to heat exchangers so that the admixture of gas after this elution is cooled to the device of at least one pressure at least in one of first and second heat exchanger body, be used at least some admixture of gas that cools off at least one first and second heat exchanger body are sent to the device of Tower System, be used for to be sent to from least a product that Tower System produces each the device first and second heat exchanger body, it is characterized in that, first heat exchanger is positioned at second heat exchanger top, be preferably located in second heat exchanger directly over.
According to of the present invention one optional aspect, this equipment comprises the device that is used for the liquid that comes from a tower of Tower System is delivered to second heat exchanger that this liquid is evaporated therein, and the device that is used for collecting the liquid that is evaporated, and be not used in the device of collecting the liquid that is evaporated from first heat exchanger from second heat exchanger.
Another aspect of the present invention provides a kind of method that is used at a kind of equipment admixture of gas being carried out cryogenic separation, this equipment comprises: the elution unit, as the described heat exchangers of one of claim 1-8, and Tower System, in this equipment, this admixture of gas is sent to the elution unit, admixture of gas after the elution is sent at least one first heat exchanger body to be cooled at least one pressure therein, admixture of gas after the elution is sent at least one second heat exchanger body to be cooled at least one pressure therein, the admixture of gas that cools off in first heat exchanger body is sent to Tower System, the admixture of gas that cools off in second heat exchanger body is sent to Tower System, at least a fluid is sent at least one first heat exchanger body from Tower System, at least a fluid is sent at least one second heat exchanger body from Tower System, it is characterized in that, first heat exchanger body (at least one in first heat exchanger body) comprises circulation of fluid, at least a pressure that is higher than threshold value that is in this circulation of fluid, second heat exchanger body (at least one in second heat exchanger body) comprises the circulation of fluid that only is in the pressure that is lower than this threshold value.
At least one first heat exchanger body is positioned at the top of one second heat exchanger body.Preferably, the heat exchanger body of all first group of heat exchangers all is positioned at the top of the heat exchanger body of all second group of heat exchangers.
Another aspect of the present invention provides a kind of method that is used at a kind of equipment admixture of gas being carried out cryogenic separation, this equipment comprises: the elution unit, as the described heat exchangers of one of claim 1-8, and Tower System, in this equipment, this admixture of gas is sent to the elution unit, admixture of gas after the elution is sent at least one first heat exchanger body to be cooled at least one pressure therein, admixture of gas after the elution is sent at least one second heat exchanger body to be cooled at least one pressure therein, the admixture of gas that cools off in first heat exchanger body is sent to Tower System, the admixture of gas that cools off in second heat exchanger body is sent to Tower System, at least a fluid is sent at least one first heat exchanger body to be heated therein from Tower System, and at least a fluid is sent at least one second heat exchanger body to be heated therein from Tower System, it is characterized in that, first heat exchanger body (at least one in first heat exchanger body) only comprises recyclegas and/or at least a circulating fluid that is cooled, and second heat exchanger body (at least one in second heat exchanger body) comprises at least a circulation of fluid, this circulation of fluid comes from Tower System, and evaporates in this second heat exchanger body.
At least one first heat exchanger body is positioned at the top of one second heat exchanger body.Preferably, the heat exchanger body of all first group of heat exchangers all is positioned at the top of the heat exchanger body of all second group of heat exchangers.
Another aspect of the present invention provides a kind of method that is used at a kind of equipment admixture of gas being carried out cryogenic separation, this equipment comprises: the elution unit, the heat exchangers that comprises one first heat exchanger and one second heat exchanger, and Tower System, wherein, this admixture of gas is sent to the elution unit, admixture of gas after the elution is sent at least one first heat exchanger body to be cooled at least one pressure therein, admixture of gas after the elution is sent at least one second heat exchanger body to be cooled at least one pressure therein, the admixture of gas that cools off in first heat exchanger body is sent to Tower System, the admixture of gas that cools off in second heat exchanger body is sent to Tower System, at least a fluid is sent at least one first heat exchanger body from Tower System, at least a fluid is sent at least one second heat exchanger body from Tower System, first heat exchanger body (at least one in first heat exchanger body) comprises circulation of fluid, at least a in this circulation of fluid is in a pressure that is higher than threshold value, and second heat exchanger body (at least one in second heat exchanger body) comprises the circulation of fluid that all is in the pressure that is lower than this threshold value, it is characterized in that first heat exchanger is positioned at the top of second heat exchanger.
Another aspect of the present invention provides a kind of method that is used at a kind of equipment admixture of gas being carried out cryogenic separation, this equipment comprises: the elution unit, the heat exchangers that comprises first and second heat exchanger, and Tower System, wherein, this admixture of gas is sent to the elution unit, admixture of gas after the elution is sent at least one first heat exchanger body to be cooled at least one pressure therein, admixture of gas after the elution is sent at least one second heat exchanger body to be cooled at least one pressure therein, the admixture of gas that cools off in first heat exchanger is sent to Tower System, the admixture of gas that cools off in second heat exchanger is sent to Tower System, at least a fluid is sent at least one first heat exchanger to be heated therein from Tower System, and at least a fluid is sent at least one second heat exchanger to be heated therein from Tower System, first heat exchanger (at least one in first heat exchanger) includes only recyclegas (and/or at least a circulating fluid that is cooled therein), and second heat exchanger (at least one in second heat exchanger) comprises at least a circulation of fluid that flows out from Tower System, this circulation of fluid is evaporated in this second heat exchanger, it is characterized in that first heat exchanger is positioned at the top of second heat exchanger.
According to other optional aspect:
-admixture of gas is that air or the gas that contains air or a kind of key component are the admixture of gas of hydrogen and/or carbon monoxide and/or methane and/or nitrogen;
-this admixture of gas is an air, Tower System comprises thermally coupled at least one medium pressure column and lower pressure column together, and liquid oxygen evaporates at least one mat woven of fine bamboo strips two heat exchangers main body to form oxygen, alternatively, does not evaporate in any first heat exchanger body;
-liquid oxygen is cooled at least one first heat exchanger body, alternatively, does not cool off in any second heat exchanger body;
Although-liquid also may be in some local bottom horizontal flow sheet, liquid flow direction is vertical basically in first and/or second heat exchanger body.
The floor space that heat exchanger takies is totally greater than set of columns.One is limited this Method for Area that hampers " packing " mode is can be received and do not hamper the heat exchanger of distillation, typically as gas heat-exchanger, be placed on the heat exchanger that those can not be received, typically as the top of the heat exchanger of liquid or liquid evaporation.Like this, floor space obviously reduces.
Can not implement if comprise single manner of packing of tower and heat exchanger, the independent packaging of stacked heat exchanger may be favourable.
Do not adopt above-mentioned packing notion and just to reducing air or gas such as H 2The floor space of the cryogenic separation unit of/CO also can adopt this mode.
Description of drawings
Describe the present invention in detail with reference to Fig. 1-6.
Fig. 1-3 illustrates from different perspectives according to sub-assembly of the present invention;
Fig. 1 illustrates the front portion of this sub-assembly, and Fig. 2 illustrates the sub-assembly that Fig. 1 is transferred to different angles, and Fig. 3 illustrates the rear portion of the sub-assembly identical with Fig. 1;
Fig. 4 illustrates in greater detail the front view of the bottom of the sub-assembly among Fig. 1, and Fig. 5 illustrates the rear portion of Fig. 4;
Fig. 6 illustrates according to combination of the present invention, and this combination is combined in the air separation equipment by the sub-assembly shown in the aforementioned figures and forms.
The specific embodiment
Fig. 1-3 illustrates according to heat exchangers of the present invention, and this heat exchangers comprises that 1,2, the first groups of heat exchangers 1 of two groups of heat exchangers rest on the ground at least 10 meters or 15 meters, and second group of heat exchanger 2 is positioned at below first group of heat exchanger.
First group of heat exchanger 1 is placed on the stainless steel frame 3, and the leg of this framework is seated on the bottom of cold box package, and second group of heat exchanger is positioned at the inner or first group of heat exchanger bottom of framework, supports first group of heat exchanger simultaneously.If can more effectively carry out thermal insulation between heat exchanger block that forms by first group of heat exchanger and the heat exchanger block that forms by second group of heat exchanger, then the heat exchanger block that is formed by first group of heat exchanger also can be placed on the heat exchanger block that is formed by second group of heat exchanger, this is because the hottest part of the coldest part of first group of heat exchanger and second group of heat exchanger relatively is provided with, when work, one of them is in about environment temperature, and another is in low temperature.Cold box package is filled with heat-insulating material I.
Two first heat exchanger body 5 are formed the heat exchanger body of embarking on journey and arranging of first group of heat exchanger 1.These two substantially the same heat exchanger body 5 are heat-exchangers of the plate type types, comprise a plurality of metallic plates of similar profile basically that have, these metallic plates extend along first direction or length and second direction or width, along third direction or thickness at each interval, be provided with in parallel to each other.Sealing device limits flat channel with above-mentioned plate, forms four types passage, and these passages do not extend along the whole length of heat exchanger body.To every type passage, the sealing device that is allocated in each passage forms a fluid inlet and a fluid issuing at the two ends of this passage.The first import E1 in the hot junction of each first heat exchanger body 5 is connected to a conveyance conduit D AIR MP who is used for pressure air to be cooled, and the first outlet S1 in the centre position of each first heat exchanger body is connected to one and is used for the cooled collecting loop C AIR MP that presses air.The second import E2 in the centre position of each first heat exchanger body 5 is connected to a conveyance conduit DNR who is used for useless nitrogen to be heated, is connected to the collecting loop CNR of useless nitrogen after being used to heat at the second outlet S2 in the hot junction of each first heat exchanger body 5.
Because each heat exchanger body 5 of first group of heat exchanger 1 also has the function of subcooler, the coldest part of each heat exchanger body 5 particularly, be connected to a conveyance conduit DOL who is used for liquid oxygen to be cooled at the triple feed inlet E3 of each first heat exchanger body, 5 cold junction, the 3rd outlet S3 of first heat exchanger body is connected to a collecting loop COL who is used for cooled liquid oxygen, be connected to a conveyance conduit DLL who is used for nitrogen-rich liquid to be cooled at the 4th import E4 of each first heat exchanger body, 5 cold junction, the 4th outlet S4 of first heat exchanger body is connected to a collecting loop CLL who is used for cooled nitrogen-rich liquid.
Be understood that easily at least one heat exchanger body of first group of heat exchanger can be carried out the function of subcooler, thereby make that this sub-assembly is compacter.In fact, do not carry out the situation of above-mentioned functions in the heat exchanger body of first group of heat exchanger, subcooler can be made of at least one heat exchanger that independently, preferably is placed between first group of heat exchanger and the second group of heat exchanger.Concerning the said equipment, also can not comprise subcooler.
It is also to be understood that the heat exchanger of first group of heat exchanger needn't be identical, and particularly, be not all to flow through identical fluid.
Four second heat exchanger body 7 are formed second group of heat exchanger 2 of the heat exchanger body that having embarks on journey arranges, and this second group of heat exchanger is bearing in the top slightly of the bottom of cold box package by framework 3.In these four essentially identical heat exchanger body 7 each all is the heat-exchangers of the plate type type, comprise a plurality of metallic plates of similar profile basically that have, these metallic plates extend along first direction or length and second direction or width, along third direction or thickness at each interval, be provided with in parallel to each other.Sealing device limits flat channel with above-mentioned plate, forms passage five types, that extend along the whole length of heat exchanger body.To every type passage, the sealing device that is allocated in each passage forms a fluid inlet and a fluid issuing at its two ends.One first import E1 ' in the hot junction of each second heat exchanger body 7 is connected to a conveyance conduit D1 AIR HP who is used to cool air to first high pressure, is connected to a collecting loop C2 AIR HP who is used for cooled pressure-air at the first outlet S1 ' of the cold junction of each second heat exchanger body 7.The second import E2 ' in the hot junction of each second heat exchanger body 7 is connected to a conveyance conduit D2 AIR HP who is used to cool air to second high pressure, is connected to a collecting loop C1 AIR HP who is used for cooled pressure-air at the second outlet S2 ' of the cold junction of each second heat exchanger body.Be connected to a conveyance conduit DNR ' who is used for useless nitrogen to be heated at the triple feed inlet E3 ' of the cold junction of each second heat exchanger body 7, be connected to the collecting loop CNR ' of useless nitrogen after being used to heat at the 3rd outlet S3 ' in the hot junction of each second heat exchanger body 7.
Unlike first group of heat exchanger, the heat exchanger body 7 of second group of heat exchanger is connected to a nitrogen gas delivery-line and a liquid oxygen line.Be connected to a conveyance conduit DN who is used for nitrogen to be heated at the 4th import E4 ' of each second heat exchanger body, 7 cold junction, be connected to the collecting loop CN of useless nitrogen after being used to heat at the 4th outlet S4 ' in each second heat exchanger body, 7 hot junction.Be connected to a conveyance conduit DOL who is used for liquid oxygen to be evaporated at the 5th import E5 ' of each second heat exchanger body, 7 cold junction, be connected to the collecting loop COG of oxygen after being used to evaporate at the 5th outlet S5 ' in each second heat exchanger body, 7 hot junction.
The heat exchanger body that will be further appreciated that second group of heat exchanger needn't be identical, particularly, is not all to flow through identical fluid.
Two main distinctions between the heat exchanger body of the heat exchanger body of first group of heat exchanger and second group of heat exchanger are:
The first, arbitrary fluid to be evaporated is sent at least one, the heat exchanger body of second group of preferably all heat exchangers.Like this, the heat exchanger body of first group of heat exchanger comprises the passage that is used for the liquid oxygen evaporation is for example arrived several pressure of at least a type.They also can comprise the passage that is used to evaporate liquid nitrogen.
The second, arbitrary fluid to be cooled or heating is sent in second group of heat exchanger under being higher than the pressure of given threshold value.This second group of heat exchanger obviously also can receive the fluid of lower pressure, but these heat exchanger body are intended to use down for high pressure.This threshold value can be 30bar abs, 20bar abs or 15bar abs.
For first group of heat exchanger 1 and second group of heat exchanger 2, heat exchanger body 5 and 7 and their distribution and collecting loop must be by perlite or rock wool I insulation.Every group of heat exchanger can be placed in the single ice chest 4 that includes only heat exchanger and at least some affluxs, conveyance conduit, perhaps two groups of heat exchangers can be placed on common, include only in the ice chest of heat exchanger body and their afflux, conveyance conduit, perhaps two groups of heat exchangers can be placed in the common ice chest together with the air separation Tower System.
Fig. 4 and Fig. 5 illustrate in greater detail the bottom of sub-assembly.
As describing among the EP-A-1 230 522, a kind of reboiler-condenser that is used for two air separation (double air separation column) of evaporation pressure nitrogen under the situation of Low Pressure Oxygen can be arranged in the tower outside.In this case, above-mentioned reboiler-condenser can be placed on as two groups of heat exchangers 1 and 2 in the same ice chest 4 above first group of heat exchanger 1 or between two groups of heat exchangers.By this way, all elements (heat exchanger, reboiler-condenser) that provided by same manufacturing firm are placed in the individual packaging, and this packing can directly be provided to installs ground.Be understandable that, each element (overhead heat exchanger, bottom heat exchanger and, optionally, reboiler) can both one independently in the ice chest by heat insulation, perhaps several being placed in the common ice chest in these elements.
Sub-assembly shown in the accompanying drawing is applicable in the low temperature distillation air separation equipment that is attached to as shown in Figure 6 as described above.Here, heat exchangers is shown the discrete component 12 that comprises first group of heat exchanger 1 and second group of heat exchanger 2.
Fig. 6 illustrates according to air separation equipment of the present invention, and especially, heat exchangers as previously described is combined in the low temperature distillation air separation equipment that uses double tower.Should be understood that the present invention is not limited to this two-column plant, but can be applicable to single tower, three towers and use other type tower such as the equipment of argon air tower or mixture tower.
Fig. 6 just schematically, especially, does not accurately illustrate fluid inlet and outlet in the sub-assembly 1 and 2 that is shown two heat exchanger blocks.Part 1 comprises at least one heat exchanger body, and part 2 comprises at least one heat exchanger body.For this embodiment, should be taken into account that each part comprises a series of substantially the same heat exchanger body.
During being compressed in a main compressor MAC, air to be separated presses to press air AIR MP in forming.The pressure of this air remainder is supercharged to earlier one first high pressure with formation high-pressure spray 1 AIR HP in booster compressor S1, and the pressure of this air remainder is supercharged to one second high pressure to form stream 2 AIR HP in booster compressor S2.In baric flow AIR MP be sent to resting on the ground at least tens meters the part 1 of heat exchangers, and high-pressure spray 1 AIR HP and 2AIR HP are sent in the bottom part 2 that rest on the ground 1 meter at least.The middle part of air stream of pressing can be sent in the bottom part 2.
In press air in the heat exchanger body of first group of heat exchanger 1, to be cooled to an intermediate point, be sent to then in the chamber of medium pressure column MP of two air separation.
Should be appreciated that, the device that is used to absorb heat is not shown in order to simplify accompanying drawing.The described device that is used for absorbing heat can be the pressure air turbine or the nitrogen turbine that enter to air separation, injects to replenish by liquid when needs.
Pressure-air is liquefied in the heat exchanger body of second group of heat exchanger, is sent to then in one of double tower or all towers.
Liquid oxygen flows out from the chamber of lower pressure column, is divided into two plumes.Part OL be sent in the coldest part of heat exchanger body of first group of heat exchanger with before being sent to holder S by cold excessively.Remainder is sucked to be formed on 20bar abs at least or the stream OLP under the 30bar abs pressure at least.This stream OLP evaporates in the heat exchanger body of second group of heat exchanger to produce stream OG.
The middle nitrogen N of pressing flows out at the top of medium pressure column, is sent in the heat exchanger body of second group of heat exchanger, is heated in this heat exchanger body to form product N.
The nitrogen that flows out at the top of lower pressure column is divided into two plumes, and a part of NR is sent in first group of heat exchanger 1, and remainder NR ' is sent in second group of heat exchanger 2.This two plume is heated, and is sent to then and recycles or arrange atmosphere.
Cold excessively in the coldest part of middle pressure nitrogen-rich liquid stream LL in the heat exchanger body of first group of heat exchanger 1, reflux to be used as in the top that is sent to lower pressure column then.

Claims (10)

1, a kind of heat exchangers, comprise at least one first heat exchanger body and one second heat exchanger body (5,7), each heat exchanger body is the heat-exchangers of the plate type type and comprises: a plurality of have a metallic plate of similar profile basically, these metallic plates extend along first direction or length and second direction or width, along third direction or thickness at each interval, be provided with in parallel to each other; And sealing device, the sealing device limits flat channel with described plate, form the passage of at least one first kind and the passage of at least one second type, the sealing device that is allocated in each passage forms a fluid inlet and a fluid issuing, an import (E1) of first heat exchanger body is connected to first conveyance conduit (D AIR MP) that is used for fluid to be cooled, an outlet (S1) of first heat exchanger body is connected to first collecting loop (C AIRMP) that is used for cooled fluid, another import of first heat exchanger body is connected to first conveyance conduit (DNR) that is used for fluid to be heated, another outlet of first heat exchanger body is connected to one and is used to heat first collecting loop (CNR) of fluid afterwards, an import of second heat exchanger body is connected to a conveyance conduit (D1 AIR HP who is used for fluid to be cooled, D2 AIR HP), an outlet of second heat exchanger body is connected to a collecting loop (C1 AIR HP who is used for cooled fluid, C2 AIR HP), another import of second heat exchanger body is connected to a conveyance conduit that is used for fluid to be heated (DNR '), another outlet of second heat exchanger body is connected to a collecting loop that is used to heat the back fluid (CNR '), it is characterized in that, the relative at least in part configuration in side that the side that is limited by the width of at least one first heat exchanger body and thickness and width and the thickness by at least one second heat exchanger body limit, these two sides are separated by heat-insulating material (I).
2, sub-assembly according to claim 1, it is characterized in that, at least one heat exchanger body (7) in second group of heat exchanger is connected to not at least one fluid-transporting tubing (the D1 AIR HP that is connected with any heat exchanger body in first group of heat exchanger, D2 AIR HP), alternatively, at least one heat exchanger body of second group of heat exchanger is connected to not the fluid collecting loop (C1 AIR HP, C2 AIRHP) that is connected with any heat exchanger body in first group of heat exchanger.
3, sub-assembly according to claim 1 and 2, it is characterized in that, first heat exchanger body (5) constitutes the part of first group of heat exchanger (1) of the heat exchanger body with at least three arrangements of embarking on journey basically, at least two first heat exchanger body of first group of heat exchanger are connected to first conveyance conduit that is used for fluid to be cooled abreast at least, first conveyance conduit that is used for fluid to be heated, be used to heat first collecting loop of back fluid, and first collecting loop that is used to cool off the back fluid, and/or second heat exchanger body (7) constitute the part of second group of heat exchanger (2) with at least three heat exchanger body of arranging of embarking on journey basically, at least two second heat exchanger body of second group of heat exchanger are connected to the conveyance conduit that at least one is used for fluid to be cooled abreast, at least one is used for the conveyance conduit of fluid to be heated, at least one is used to cool off the collecting loop of back fluid and is connected to the collecting loop that is used to heat the back fluid at least.
According to claim 1,2 or 3 described sub-assemblies, it is characterized in that 4, an import of at least one second heat exchanger body (7) is connected to first conveyance conduit that is used for fluid to be cooled, and/or be used for first conveyance conduit of fluid to be heated.
5, according to claim 1,2,3 or 4 described sub-assemblies, it is characterized in that, an import of at least one second heat exchanger body (7) is connected to a conveyance conduit that is used for fluid to be cooled that is different from first conveyance conduit that is used for fluid to be cooled, and/or another import of second heat exchanger body is connected to a conveyance conduit that is used for fluid to be heated that is different from first conveyance conduit that is used for fluid to be heated.
6, according to the described sub-assembly of one of claim 1 to 6, it is characterized in that, described sub-assembly comprises the liquid conducting pipes that is connected with the passage of second heat exchanger body, be used for liquid is sent at least one second heat exchanger body (7), and described passage is connected with the outlet that back liquid is evaporated near being used to of an import that is positioned at gas to be cooled.
According to the described sub-assembly of one of claim 1 to 6, it is characterized in that 7, (first group of heat exchanger) at least one first heat exchanger body (5) only is connected at least one gas transmission pipeline and/or at least one is used for the pipeline of liquid to be cooled.
8, according to the described sub-assembly of one of aforementioned claim, it is characterized in that, comprise the heat exchanger body between at least one side positioned opposite to each other that is arranged on first heat exchanger body and second heat exchanger body.
9, a kind of cryogenic separation that is used for admixture of gas, this equipment comprises the elution unit, as the described sub-assembly of one of claim 1 to 8, Tower System, be used for admixture of gas is sent to the device of elution unit, be used for the admixture of gas after the elution is sent to heat exchangers so that the admixture of gas after this elution at least in first and second heat exchanger body (5,7) be cooled to the device of at least one pressure one of, be used at least some in first and second heat exchanger body (5,7) admixture of gas that cools off at least one in is sent to the device of Tower System, be used for to be sent to from least a product that Tower System produces the device (DNR, DNR ') in each the heat exchanger body of first group of heat exchanger and second group of heat exchanger.
10, cryogenic separation according to claim 9, it is characterized in that, comprise being used for liquid flow pressurization, a kind of component of being rich in admixture of gas is delivered to the device of (second group of heat exchanger (2)) at least one second heat exchanger body (7), and the device that is used for a kind of gas that is rich in a kind of component of admixture of gas is sent to (first group of heat exchanger (1)) at least one first heat exchanger body (5).
CN200580045642A 2004-12-30 2005-12-23 Heat exchanger assembly and cryogenic distillation apparatus incorporating same Active CN100590374C (en)

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
FR0414070A FR2880418B1 (en) 2004-12-30 2004-12-30 HEAT EXCHANGER ASSEMBLY, CRYOGENIC DISTILLATION APPARATUS INCORPORATING SUCH ASSEMBLY, AND CRYOGENIC DISTILLATION METHOD USING SUCH ASSEMBLY
FR0414070 2004-12-30
FR0550288A FR2881515A1 (en) 2004-12-30 2005-02-01 Heat exchange assembly for cryogenic gaseous mixture separation apparatus, has exchange bodies each comprising inlets and outlets connected to distribution and collecting lines, where lines and bodies are isolated by perlite or rock wool
FR0550288 2005-02-01

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CN109954367A (en) * 2017-12-14 2019-07-02 乔治洛德方法研究和开发液化空气有限公司 It is separated by distillation the sealing cover of the equipment of gaseous mixture and the equipment including sealing cover
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CN102706097B (en) * 2011-03-25 2016-06-01 林德股份公司 The equipment of low temperature air separating
CN104641197A (en) * 2012-09-19 2015-05-20 乔治洛德方法研究和开发液化空气有限公司 Heat exchanger and method for the installation of a gas separation unit comprising such heat exchangers
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FR2880418B1 (en) 2007-04-27
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FR2880418A1 (en) 2006-07-07
JP4991561B2 (en) 2012-08-01
FR2881515A3 (en) 2006-08-04
US20090211295A1 (en) 2009-08-27
EP1834143A1 (en) 2007-09-19
WO2006069983A1 (en) 2006-07-06
FR2881515A1 (en) 2006-08-04

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