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CN101056697A - 静态混合器 - Google Patents

静态混合器 Download PDF

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Publication number
CN101056697A
CN101056697A CNA2005800349401A CN200580034940A CN101056697A CN 101056697 A CN101056697 A CN 101056697A CN A2005800349401 A CNA2005800349401 A CN A2005800349401A CN 200580034940 A CN200580034940 A CN 200580034940A CN 101056697 A CN101056697 A CN 101056697A
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shear plate
static mixer
mixer
passage
shear
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CN101056697B (zh
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威廉·A·凯勒
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Medmis Switzerland Ag
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Mixpac Systems AG
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B05—SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05C—APPARATUS FOR APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05C17/00—Hand tools or apparatus using hand held tools, for applying liquids or other fluent materials to, for spreading applied liquids or other fluent materials on, or for partially removing applied liquids or other fluent materials from, surfaces
    • B05C17/005—Hand tools or apparatus using hand held tools, for applying liquids or other fluent materials to, for spreading applied liquids or other fluent materials on, or for partially removing applied liquids or other fluent materials from, surfaces for discharging material from a reservoir or container located in or on the hand tool through an outlet orifice by pressure without using surface contacting members like pads or brushes
    • B05C17/00503—Details of the outlet element
    • B05C17/00506—Means for connecting the outlet element to, or for disconnecting it from, the hand tool or its container
    • B05C17/00509—Means for connecting the outlet element to, or for disconnecting it from, the hand tool or its container of the bayonet type
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F25/40—Static mixers
    • B01F25/42—Static mixers in which the mixing is affected by moving the components jointly in changing directions, e.g. in tubes provided with baffles or obstructions
    • B01F25/421—Static mixers in which the mixing is affected by moving the components jointly in changing directions, e.g. in tubes provided with baffles or obstructions by moving the components in a convoluted or labyrinthine path
    • B01F25/423—Static mixers in which the mixing is affected by moving the components jointly in changing directions, e.g. in tubes provided with baffles or obstructions by moving the components in a convoluted or labyrinthine path by means of elements placed in the receptacle for moving or guiding the components
    • B01F25/4233—Static mixers in which the mixing is affected by moving the components jointly in changing directions, e.g. in tubes provided with baffles or obstructions by moving the components in a convoluted or labyrinthine path by means of elements placed in the receptacle for moving or guiding the components using plates with holes, the holes being displaced from one plate to the next one to force the flow to make a bending movement
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F25/40—Static mixers
    • B01F25/42—Static mixers in which the mixing is affected by moving the components jointly in changing directions, e.g. in tubes provided with baffles or obstructions
    • B01F25/43—Mixing tubes, e.g. wherein the material is moved in a radial or partly reversed direction
    • B01F25/431—Straight mixing tubes with baffles or obstructions that do not cause substantial pressure drop; Baffles therefor
    • B01F25/4312—Straight mixing tubes with baffles or obstructions that do not cause substantial pressure drop; Baffles therefor having different kinds of baffles, e.g. plates alternating with screens
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F25/40—Static mixers
    • B01F25/42—Static mixers in which the mixing is affected by moving the components jointly in changing directions, e.g. in tubes provided with baffles or obstructions
    • B01F25/43—Mixing tubes, e.g. wherein the material is moved in a radial or partly reversed direction
    • B01F25/431—Straight mixing tubes with baffles or obstructions that do not cause substantial pressure drop; Baffles therefor
    • B01F25/4314—Straight mixing tubes with baffles or obstructions that do not cause substantial pressure drop; Baffles therefor with helical baffles
    • B01F25/43141—Straight mixing tubes with baffles or obstructions that do not cause substantial pressure drop; Baffles therefor with helical baffles composed of consecutive sections of helical formed elements
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F25/40—Static mixers
    • B01F25/45—Mixers in which the materials to be mixed are pressed together through orifices or interstitial spaces, e.g. between beads
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F25/40—Static mixers
    • B01F25/45—Mixers in which the materials to be mixed are pressed together through orifices or interstitial spaces, e.g. between beads
    • B01F25/452—Mixers in which the materials to be mixed are pressed together through orifices or interstitial spaces, e.g. between beads characterised by elements provided with orifices or interstitial spaces
    • B01F25/4521—Mixers in which the materials to be mixed are pressed together through orifices or interstitial spaces, e.g. between beads characterised by elements provided with orifices or interstitial spaces the components being pressed through orifices in elements, e.g. flat plates or cylinders, which obstruct the whole diameter of the tube
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B05—SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05C—APPARATUS FOR APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05C17/00—Hand tools or apparatus using hand held tools, for applying liquids or other fluent materials to, for spreading applied liquids or other fluent materials on, or for partially removing applied liquids or other fluent materials from, surfaces
    • B05C17/005—Hand tools or apparatus using hand held tools, for applying liquids or other fluent materials to, for spreading applied liquids or other fluent materials on, or for partially removing applied liquids or other fluent materials from, surfaces for discharging material from a reservoir or container located in or on the hand tool through an outlet orifice by pressure without using surface contacting members like pads or brushes
    • B05C17/00503—Details of the outlet element
    • B05C17/00506—Means for connecting the outlet element to, or for disconnecting it from, the hand tool or its container
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F2101/00—Mixing characterised by the nature of the mixed materials or by the application field
    • B01F2101/22—Mixing of ingredients for pharmaceutical or medical compositions
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F2101/00—Mixing characterised by the nature of the mixed materials or by the application field
    • B01F2101/2305—Mixers of the two-component package type, i.e. where at least two components are separately stored, and are mixed in the moment of application

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  • Chemical & Material Sciences (AREA)
  • Dispersion Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Processing And Handling Of Plastics And Other Materials For Molding In General (AREA)

Abstract

用于两种成分的静态混合器，包括具有入口部分(4)的壳体(3)和设置在该壳体中的混合元件。已知的混合器使用混合器螺旋作为混合元件。本发明的混合器的特征在于至少其中一个混合元件配置成圆盘形的剪切板(7、7A)，所述剪切板的每个盘(8)中具有通道(10、10A)。这种剪切元件允许即使量非常小也能混合，其可能是逐滴分配，因为在排出期间在剪切板的通道附近产生较高的剪切速率，并且在混合器的排出端产生涡流，这种混合器在医药领域是特别有利的。

Description

静态混合器
技术领域
本发明涉及根据权利要求1的前序部分所述的用于两种成分的静态混合器，其包括入口部分和内部设置有混合元件的壳体。
背景技术
很长时间以来就已经知道通过静态混合器来混合两种物质，大部分静态混合器包括如在本发明申请人的US-A-5 609 271中所述的螺旋混合元件。在这种原理中，两种物质通过重复的移动而彼此混合。为了实现高质量的混合，混合器的不同参数以多种方式来确定，例如混合元件的几何形状、混合元件的数目和混合器直径。在静态类型的混合器中，层流通常用于具有中粘性到高粘性的介质。这同样适用于具有例如1-2mm的非常小直径的混合器以及具有低粘性的成分。
特别地，如果待混合量非常小，例如在逐滴分配的情形中，使用具有传统混合元件的混合器是有问题的，因为特别是对于具有不同粘性及相应的表面张力的成分而言，不再能够获得足够彻底的混合效果。特别是在医药领域，这可能会导致严重的问题。
而且，在现有技术中已知的是具有带一个或多个孔的盘状混合元件的混合器。
GB-A-1 188 516公开了一种具有一叠盘的混合器，这些盘设置在混合器壳体中并具有相应的孔，这些盘设置为使得这些孔互相之间转动偏移了180°。
US-A-2 125 245公开了一种具有板的乳剂装置，这些板设置在壳体中并且每个板具有多个小开口或者一个较大开口。
US-A-5 968 018公开了一种具有一叠盘的细胞分离设备，这些盘每个具有一个孔，这些盘设置为使得这些孔互相之间转动偏移180°。
US-A1-2003/0179648公开了一种具有混合室的混合器，在混合室之间可设置传统的混合螺旋等。
US-A-4 068 830公开了一种带有混合螺旋的传统的混合器，在混合螺旋之间设置有穿孔板。
这些混合器中没有一个针对小分配体积。
发明内容
在现有技术的基础上，本发明的目的是提供一种具有混合元件的混合器，该混合器在非常小分配体积时同样确保两种物质彻底混合。
附图说明
下面将参照示例性实施方式的附图更详细地解释本发明。
图1示出了根据本发明的混合器的剖视图；
图2示出了图1的放大细节；
图3示出了图2的俯视图；
图4示出了图1的混合元件的立体图；和
图5示意性地示出了一种实施方式变型。
具体实施方式
图1示出了根据本发明的混合器1的纵向剖视面，该混合器紧固到两成分筒2并且具有带有入口部分4的壳体3。在圆筒形的壳体部分5中设置有不同类型的混合元件。在混合元件的中间部分，设置有传统的混合螺旋6，该混合螺旋的两侧是新型的混合元件7，还参见图2和3。
新型混合元件7设计为剪切板并包括盘8，该盘紧固到轴毂9并具有通道10。特别如图2所示，通道10设置在使得每个通道相对于相邻通道转动偏离例如180°。通道的形状选择为使得液体分别承受高速度或者剪切应力，从而形成后续的涡流并确保即使最小量也会有较好的混合。然而，具体形状不限制于所示出的形状并可与其不同。
在由多个剪切板施加的剪切和回旋作用后，在下面的传统混合螺旋中开始通过移动进行混合的过程，以便实现各成分在整个横截面上可能的最佳扩散。
在根据图1的示例性实施方式中，如从入口处观察，四个剪切板后是五个传统的混合螺旋，随后又是四个剪切板。在图5中，示出另一顺序，其中例如五个螺旋后是四个剪切板，接着又是五个混合螺旋。这两种示例性实施方式的意思是表示混合螺旋和剪切板可按需组合，使得混合器能够最优地适用于待混合的材料并适用于几何形状条件。
在混合器的入口部分4中，混合器包括两个入口11和12，所述两个入口在该示例性实施方式中被推入到筒2的出口13和14中。混合器入口部分4还包括筒上的锁定元件15和混合器入口部分上相应的锁定元件16。锁定元件还可具有卡口类型。
在图4中，在立体图中示出不同的混合元件，其中可以看出带通道10的剪切板7和传统的螺旋6。在图4中，可看到在该实施例中，第一剪切板7A的板通道10A与入口11和12的排出口对准。从而，剪切板通道10的纵轴线基本上与两个入口的排出口的连接线一致。然而，剪切板通道的纵轴线相对于出口的指向也可以不同，例如与其垂直。
还示出混合器入口部分由连接构件20连接到混合元件，并可与其一体地形成为单件。
来自筒2的两个存储容器17和18的两种物质在压力下传送到混合器入口。在连接构件20和第一剪切板之间的空间19内，两种物质相遇并一起受压而通过剪切板7A的通道10A。剪切板通道的形状影响剪切应力以及涡流的形成，并且可提供两种物质更好的混合。
正如引言中所指出的那样，能够合适地使用具有合适通道的混合板用于具有不同粘性的混合介质，特别是非常小的量需要逐滴分配时。更具体地，混合元件的直径可以是约1mm的量级。
本发明，即剪切板的设置，不限制于示例性的圆柱形状。混合器壳体及其容纳混合元件的中空部分，还有混合元件和剪切板都可具有其它形状和横截面，例如矩形或正方形。而且，剪切板可包括一个以上的剪切板通道，并且通道的形状例如可为圆形、椭圆形或者楔形、矩形、或三角形。

Claims (5)

1.用于两种成分的静态混合器，包括具有入口部分的壳体和设置在所述壳体中的混合元件，其中至少一个混合元件是混合螺旋，其特征在于，额外地设置有至少一组包括至少两个盘形剪切板(7、7A)形式的混合元件，所述剪切板的每个盘(8)具有至少一个通道(10、10A)。
2.根据权利要求1所述的静态混合器，其特征在于，所述混合器壳体包括一组剪切板(7)，相继的剪切板的通道(10、10A)相互转动偏移一个角度。
3.根据权利要求2所述的静态混合器，其特征在于，所述角度为180°。
4.根据权利要求1到3中任一项所述的静态混合器，其特征在于，剪切板的组和混合螺旋的组彼此交替地设置。
5.根据权利要求1到4中任一项所述的静态混合器，其特征在于，入口侧上的第一剪切板(7A)的通道(10A)与混合器入口(11、12)的排出口对准，所述剪切板通道(10A)的纵轴线基本上与这两个入口的排出口之间的连接线一致或者与其垂直。
CN2005800349401A 2004-10-15 2005-10-11 静态混合器 Active CN101056697B (zh)

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EP (1) EP1799336B9 (zh)
JP (1) JP2008516745A (zh)
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DE (1) DE502005007759D1 (zh)
ES (1) ES2329491T3 (zh)
WO (1) WO2006039827A1 (zh)

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CN101371975B (zh) * 2008-09-26 2010-06-09 沈阳化工学院 多流道螺旋静态混合器
CN102089084A (zh) * 2008-07-14 2011-06-08 药物混合系统股份公司 包含带袋的筒的分配组件
CN102182496A (zh) * 2011-03-21 2011-09-14 西安西科煤矿安全通风防灭火研究所有限公司 用于煤矿防灭火的泡沫发生器
CN102182497A (zh) * 2011-03-21 2011-09-14 西安西科煤矿安全通风防灭火研究所有限公司 用于煤矿防灭火的泡沫制备装置
CN102458628A (zh) * 2009-06-05 2012-05-16 药物混合系统股份公司 用于产生由至少三种组分组成的混合物的混合装置
CN104582823A (zh) * 2012-08-21 2015-04-29 药物混合系统股份公司 用于排料单元的混合设备
CN104548988A (zh) * 2014-11-04 2015-04-29 华文蔚 一种用于两种液态成分静态混合的方法
CN106422832A (zh) * 2016-11-21 2017-02-22 浙江福立分析仪器股份有限公司 一种用于液相色谱系统的高压静态混合器及液体混合方法
CN107921386A (zh) * 2015-08-28 2018-04-17 苏舍米克斯帕克有限公司 静态混合器、装配静态混合器的方法和分送设备
CN108607484A (zh) * 2018-05-10 2018-10-02 南京师范大学 一种新型表面摩擦更新静态混合反应器
CN114832706A (zh) * 2022-04-15 2022-08-02 杭州正创新材料有限公司 硅酮胶生产用静态混合装置

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CN102089084A (zh) * 2008-07-14 2011-06-08 药物混合系统股份公司 包含带袋的筒的分配组件
CN102089084B (zh) * 2008-07-14 2014-12-10 药物混合系统股份公司 包含带袋的筒的分配组件
CN101371975B (zh) * 2008-09-26 2010-06-09 沈阳化工学院 多流道螺旋静态混合器
CN102458628A (zh) * 2009-06-05 2012-05-16 药物混合系统股份公司 用于产生由至少三种组分组成的混合物的混合装置
CN102182496A (zh) * 2011-03-21 2011-09-14 西安西科煤矿安全通风防灭火研究所有限公司 用于煤矿防灭火的泡沫发生器
CN102182497A (zh) * 2011-03-21 2011-09-14 西安西科煤矿安全通风防灭火研究所有限公司 用于煤矿防灭火的泡沫制备装置
CN104582823A (zh) * 2012-08-21 2015-04-29 药物混合系统股份公司 用于排料单元的混合设备
CN104582823B (zh) * 2012-08-21 2017-02-22 药物混合系统股份公司 用于排料单元的混合设备
CN104548988A (zh) * 2014-11-04 2015-04-29 华文蔚 一种用于两种液态成分静态混合的方法
CN107921386A (zh) * 2015-08-28 2018-04-17 苏舍米克斯帕克有限公司 静态混合器、装配静态混合器的方法和分送设备
CN106422832A (zh) * 2016-11-21 2017-02-22 浙江福立分析仪器股份有限公司 一种用于液相色谱系统的高压静态混合器及液体混合方法
CN108607484A (zh) * 2018-05-10 2018-10-02 南京师范大学 一种新型表面摩擦更新静态混合反应器
CN114832706A (zh) * 2022-04-15 2022-08-02 杭州正创新材料有限公司 硅酮胶生产用静态混合装置

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JP2008516745A (ja) 2008-05-22
DE502005007759D1 (de) 2009-09-03
CN101056697B (zh) 2011-10-26
WO2006039827A1 (de) 2006-04-20
EP1799336B1 (de) 2009-07-22
US20080056065A1 (en) 2008-03-06
EP1799336A1 (de) 2007-06-27
ES2329491T3 (es) 2009-11-26

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