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CN100593727C - Apparatus based on magnetofluid refraction index changing and detecting magnetic variation - Google Patents

Apparatus based on magnetofluid refraction index changing and detecting magnetic variation Download PDF

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CN100593727C
CN100593727C CN200810037409A CN200810037409A CN100593727C CN 100593727 C CN100593727 C CN 100593727C CN 200810037409 A CN200810037409 A CN 200810037409A CN 200810037409 A CN200810037409 A CN 200810037409A CN 100593727 C CN100593727 C CN 100593727C
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magnetic field
refractive index
light source
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changes
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CN101281237A (en
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狄子昀
陈险峰
刘婷
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Shanghai Jiao Tong University
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Abstract

The invention discloses an apparatus for testing magnetic variation based on the refractive index change of magnetofluid, including a first light source output device, a transmission apparatus, a magnetic field testing device and a first receiving detecting device. The magnetic field testing device includes a refractive index testing device, an electric magnet, a long cycle optical fiber grating and a magnetofluid sample. The long cycle optical fiber grating is arranged in the capillary pipe filled with magnetofluid, and then arranged between two magnetic poles of the electric magnet. A transmission apparatus is used to connect the first light source output device, the magnetic field testing device and the first receiving detecting device, the light output from the first light source output device spreads in the transmission apparatus, the light signal passing through the magnetic field testing device is then received by the first receiving detecting device. The inventive apparatus fortesting magnetic variation based on the refractive index change of magnetofluid under the function of magnetic field in the normal temperature, has very high sensitivity, reaching 0.0025nm/Gs, and the operating region of the apparatus can be from 0Gs to 1500Gs.

Description

基于磁流体折射率改变检测磁场变化的装置 Device for detecting changes in magnetic field based on changes in the refractive index of ferrofluid

技术领域 technical field

本发明涉及的是一种物理光电技术领域的检测装置,具体是一种磁场作用下基于磁流体折射率改变从而检测磁场变化的装置。The invention relates to a detection device in the field of physical optoelectronic technology, in particular to a device for detecting changes in a magnetic field based on a change in the refractive index of a magnetic fluid under the action of a magnetic field.

背景技术 Background technique

在光通讯中,可调谐光纤器件是非常有用的。长周期光纤光栅能将光纤纤芯的光耦合到包层,它对包覆在其外包层的材料折射率敏感,所以可被用来进行可调谐滤波和带阻。在理论和实验上,人们已经研究了通过改变长周期光栅外包层的折射率来改变长周期光栅的光学性能。长周期光栅外包层折射率的改变可以通过置于毛细管中的长周期光栅外围的液滴来实现。有多种方法可以对液滴进行操作,如:电化学效应、电毛细压力和电湿激励法,等。通过电湿泵浦和流体腔的循环,可以实现动态调节长周期光栅的光学性质,使其具有开关和滤波器的特性。In optical communication, tunable optical fiber devices are very useful. Long-period fiber gratings can couple light from the fiber core to the cladding. It is sensitive to the refractive index of the material cladding it, so it can be used for tunable filtering and band rejection. Theoretically and experimentally, people have studied how to change the optical properties of LPFGs by changing the refractive index of the outer cladding of LPFGs. The change of the refractive index of the outer cladding of the LPFG can be realized by liquid droplets placed on the periphery of the LPFG in the capillary. There are various methods to manipulate droplets, such as: electrochemical effects, electrocapillary pressure, and electrowetting excitation methods, etc. Through the electrowetting pumping and the circulation of the fluid cavity, the optical properties of the LPFG can be dynamically adjusted, so that it has the characteristics of a switch and a filter.

磁流体(或称做:磁性液体,磁液,铁磁流体,磁性胶体,磁性流体)是由纳米级的强磁性颗粒弥散于某种液体之中所形成的稳定的胶体体系,它既具有固体物质的磁性,又具有液体的流动性,是一种新型的功能材料,受到人们的日益重视,其应用已深入到电子,能源,国防军工,冶金机械,化工环保,仪器仪表,医疗卫生等方面,收效十分显著。而直到二十世纪末才有学者对磁流体的新型光学性质(如:光学透过率、磁致变色效应、热光效应,等性质)进行研究。近年来,随着集成光学、光子器件的迅猛发展,以及磁流体在光学领域潜在应用的发现,一些研究者开始重视磁流体的光学性质,并且提出了基于磁流体的光子器件,如光开关、光调制器、磁场或电场传感器、可调谐光栅和粗波分复用器,等。Magnetic fluid (or called: magnetic liquid, ferrofluid, ferrofluid, magnetic colloid, magnetic fluid) is a stable colloidal system formed by nano-scale strong magnetic particles dispersed in a certain liquid. It has both solid The magnetism of the substance and the fluidity of the liquid are a new type of functional material, which has been paid more and more attention by people. Its application has penetrated into electronics, energy, national defense and military industry, metallurgical machinery, chemical environmental protection, instrumentation, medical and health care, etc. , the effect is very significant. It was not until the end of the 20th century that scholars studied the new optical properties of magnetic fluids (such as: optical transmittance, magnetochromic effect, thermo-optic effect, etc.). In recent years, with the rapid development of integrated optics and photonic devices, and the discovery of the potential application of magnetic fluid in the field of optics, some researchers have begun to pay attention to the optical properties of magnetic fluid, and proposed photonic devices based on magnetic fluid, such as optical switches, Optical modulators, magnetic or electric field sensors, tunable gratings and coarse wavelength division multiplexers, etc.

经对现有技术的文献检索发现,S.Y.Yang等在《Applied PhysicsLetters》(应用物理学报)2004年上发表的“Origin and applications ofmagnetically tunable refractive index of magnetic fluid films”,(磁流体薄膜磁致折射率可调的起源及应用),该文中提出第一次全面提出了,利用磁流体薄膜折射率差随磁场大小变化的特性进行光传感,其不足在于:由于所使用的将磁流体灌入光纤包层的实验方案调制现象不是非常明显,传输损耗仅为1.13%,很难满足高精度的磁场测量要求,很难在现实生活中有太多的应用。After searching the literature of the prior art, it was found that "Origin and applications of magnetically tunable refractive index of magnetic fluid films" published by S.Y.Yang et al. in "Applied Physics Letters" (Journal of Applied Physics) in 2004, (Magneto-induced refractive index of magnetic fluid film Adjustable origin and application), this paper proposes for the first time to comprehensively propose the use of the characteristics of the change of the refractive index difference of the magnetic fluid film with the size of the magnetic field for optical sensing. The modulation phenomenon of the experimental scheme of the cladding is not very obvious, and the transmission loss is only 1.13%. It is difficult to meet the requirements of high-precision magnetic field measurement, and it is difficult to have too many applications in real life.

发明内容 Contents of the invention

本发明针对现有技术的不足,提供一种基于磁流体折射率改变检测磁场变化的装置,使其通过磁场作用在磁流体的方法来实现调节长周期光纤光栅光学性质的目的。磁流体的折射率可以通过施加外部磁场来调节。当具有适当折射率的磁流体在长周期光栅外包层时,长周期光栅的光学性质就得到了调节,进而可实现滤波器和光开关的功能。The present invention aims at the deficiencies of the prior art, and provides a device for detecting changes in the magnetic field based on the change of the refractive index of the magnetic fluid, so that the purpose of adjusting the optical properties of the long-period fiber grating can be achieved through the method that the magnetic field acts on the magnetic fluid. The refractive index of ferrofluids can be tuned by applying an external magnetic field. When the magnetic fluid with proper refractive index is coated on the outer layer of the LPFG, the optical properties of the LPFG can be adjusted, and then the functions of filter and optical switch can be realized.

本发明是通过以下技术方案实现的,本发明包括:第一光源输出装置、传输装置、磁场测试装置以及第一接收检测装置。磁场测试装置中包括了折射率测试装置,电磁铁,长周期光纤光栅,以及磁流体样品。长周期光纤光栅置于装有磁流体的毛细管后,置于电磁铁的两个磁极中间。第一光源输出装置、磁场测试装置以及第一接收检测装置之间使用传输装置连接,第一光源输出装置输出的光在传输装置内几乎无损耗传播,经过磁场测试装置后光信号被第一接收检测装置接收。折射率测试装置和磁流体样品连接在一起。以上所有部件之间的连接均通过光纤实现。The present invention is realized through the following technical solutions, and the present invention includes: a first light source output device, a transmission device, a magnetic field testing device and a first receiving and detecting device. The magnetic field test device includes a refractive index test device, an electromagnet, a long-period fiber grating, and a magnetic fluid sample. The long-period fiber grating is placed behind the capillary filled with magnetic fluid, and placed between the two magnetic poles of the electromagnet. The first light source output device, the magnetic field testing device, and the first receiving and detecting device are connected by a transmission device. The light output by the first light source output device propagates almost without loss in the transmission device. After passing through the magnetic field testing device, the optical signal is received by the first receiver. The detection device receives. The refractive index testing device and the ferrofluid sample are connected together. The connections between all the above components are realized by optical fiber.

所述第一光源输出装置为放大自发辐射光源。The first light source output device is an amplified spontaneous radiation light source.

所述传输装置为标准通信波长单模光纤。The transmission device is a standard communication wavelength single-mode optical fiber.

所述第一接收检测装置为光谱分析仪。The first receiving and detecting device is a spectrum analyzer.

所述折射率测试装置由第二光源输出装置,耦合器,以及第二接收检测装置组成,用于测量磁流体样品在磁场下的折射率变化。这些部件之间均通过光纤连接,折射率测试装置中的耦合器将入射光引导到光纤端面,并且用光纤来收集后向反射光。耦合器的输入端连接第二光源输出装置,耦合器的输入端将入射光引导到光纤端面处的光纤-磁流体样品界面上,反射回来的光功率第二接收检测装置检测接受。The refractive index testing device is composed of a second light source output device, a coupler, and a second receiving and detecting device, and is used to measure the change of the refractive index of the ferrofluid sample under a magnetic field. These components are connected by optical fibers, and the coupler in the refractive index test device guides the incident light to the end face of the optical fiber, and uses the optical fiber to collect the back reflected light. The input end of the coupler is connected to the second light source output device, and the input end of the coupler guides the incident light to the fiber-magnetic fluid sample interface at the end face of the fiber, and the reflected light power is detected by the second receiving and detecting device.

所述第二光源输出装置为输出功率稳定、通信波段的激光器。The second light source output device is a laser with stable output power and communication band.

所述第二光源检测装置为通信波段的光功率计。The second light source detection device is an optical power meter in the communication band.

本发明工作时,将所述的长周期光纤光栅置入毛细管中,并在毛细管中注入磁流体,使得长周期光纤光栅置于磁流体环境中。由于长周期光纤光栅的中心衰减波长对于其周围折射率的变化相当敏感。因此,当存在磁场时,磁流体样品的折射率发生改变,使得检测到的中心衰减波长发生漂移。以此,通过检测到的中心波长漂移值可以探测到磁流体在磁场作用下折射率变化情况。另外,通过折射率测试装置,可以探测到所加磁场的大小。从而,达到精确检测磁场的效果。When the present invention works, the long-period optical fiber grating is put into the capillary, and magnetic fluid is injected into the capillary, so that the long-period optical fiber grating is placed in the magnetic fluid environment. Because the central attenuation wavelength of the long period fiber grating is quite sensitive to the change of its surrounding refractive index. Therefore, when a magnetic field is present, the refractive index of the ferrofluid sample changes, causing the detected central attenuation wavelength to shift. In this way, the change of the refractive index of the magnetic fluid under the action of a magnetic field can be detected through the detected central wavelength drift value. In addition, the magnitude of the applied magnetic field can be detected by means of a refractive index testing device. Thus, the effect of accurately detecting the magnetic field is achieved.

本发明在常温条件下实现了磁场作用下磁流体折射率改变在检测磁场中的应用。在工作范围内,其灵敏度极高,达到了0.0025nm/Gs。该发明适用于小范围高精度的温度测量或者常温范围内的精确温度甄别,且结构简单,易于集成。The invention realizes the application of the change of the refraction index of the magnetic fluid under the action of the magnetic field in the detection of the magnetic field under normal temperature conditions. In the working range, its sensitivity is extremely high, reaching 0.0025nm/Gs. The invention is suitable for small-scale high-precision temperature measurement or accurate temperature discrimination in the normal temperature range, and has a simple structure and is easy to integrate.

附图说明 Description of drawings

图1为本发明结构示意图。Fig. 1 is a schematic diagram of the structure of the present invention.

具体实施方式 Detailed ways

下面结合附图对本发明的实施例作详细说明:本实施例在以本发明技术方案为前提下进行实施,给出了详细的实施方式和具体的操作过程,但本发明的保护范围不限于下述的实施例。The embodiments of the present invention are described in detail below in conjunction with the accompanying drawings: this embodiment is implemented on the premise of the technical solution of the present invention, and detailed implementation methods and specific operating procedures are provided, but the protection scope of the present invention is not limited to the following the described embodiment.

如图1所示,本实施例为一种基于磁流体折射率改变检测磁场变化的装置:第一光源输出装置1、传输装置2、磁场测试装置以及第一接收检测装置9。As shown in FIG. 1 , this embodiment is a device for detecting changes in magnetic field based on changes in the refractive index of magnetic fluid: a first light source output device 1 , a transmission device 2 , a magnetic field testing device, and a first receiving and detecting device 9 .

磁场测试装置中包括了折射率测试装置,电磁铁3,长周期光纤光栅4,以及磁流体样品5。长周期光纤光栅4置于装有磁流体5的毛细管后,置于电磁铁3的两个磁极中间。第一光源输出装置1、磁场测试装置以及第一接收检测装置9之间使用传输装置2连接,第一光源输出装置1输出的光在传输装置2内几乎无损耗传播,经过磁场测试装置后光信号被第一接收检测装置9接收。The magnetic field testing device includes a refractive index testing device, an electromagnet 3 , a long period fiber grating 4 , and a magnetic fluid sample 5 . The long-period fiber grating 4 is placed behind the capillary filled with the magnetic fluid 5 and placed between the two magnetic poles of the electromagnet 3 . The transmission device 2 is used to connect the first light source output device 1, the magnetic field testing device, and the first receiving and detecting device 9. The light output by the first light source output device 1 propagates almost without loss in the transmission device 2. After passing through the magnetic field testing device, the light The signal is received by the first reception detection means 9 .

所述折射率测试装置由第二光源输出装置7,耦合器6,以及第二接收检测装置8组成,用于测量磁流体样品在磁场下的折射率变化。折射率测试装置中光纤耦合器6将入射光引导到光纤端面,并且用光纤来收集后向反射光。耦合器6的输入端连接第二光源输出装置7,耦合器的输入端将入射光引导到光纤端面处的光纤-磁流体样品5界面上,反射回来的光功率第二接收检测装置8检测接收。The refractive index testing device is composed of a second light source output device 7, a coupler 6, and a second receiving and detecting device 8, and is used to measure the refractive index change of the ferrofluid sample under a magnetic field. The optical fiber coupler 6 in the refractive index testing device guides the incident light to the end face of the optical fiber, and uses the optical fiber to collect the retroreflected light. The input end of the coupler 6 is connected to the second light source output device 7, and the input end of the coupler guides the incident light to the optical fiber-magnetic fluid sample 5 interface at the end face of the optical fiber, and the second receiving and detecting device 8 detects and receives the light power reflected back. .

上述部件之间均通过光纤连接。All the above components are connected by optical fibers.

所述第一光源输出装置1为放大自发辐射光源。The first light source output device 1 is an amplified spontaneous emission light source.

所述传输装置2为单模光纤。The transmission device 2 is a single-mode optical fiber.

所述第一接收检测装置9为光谱分析仪。The first receiving and detecting device 9 is a spectrum analyzer.

所述电磁铁装置3为磁场大小可通过供电电流的大小来改变磁场大小的电磁铁。The electromagnet device 3 is an electromagnet whose magnetic field can be changed by the magnitude of the supply current.

所述长周期光纤光栅4为光栅周期为400μm,空气中中心波长为1540.5nm的长周期光纤光栅。The long-period fiber grating 4 is a long-period fiber grating with a grating period of 400 μm and a central wavelength of 1540.5 nm in air.

所述磁流体5为密度为1.2g/ml的水基磁流体。The magnetic fluid 5 is a water-based magnetic fluid with a density of 1.2 g/ml.

所述耦合器6为3dB的耦合器。The coupler 6 is a 3dB coupler.

所述第二光源输出装置7为功率1mW,中心波长1550nm激光器。The second light source output device 7 is a laser with a power of 1 mW and a center wavelength of 1550 nm.

所述第二接收检测装置8为通信波段1550nm光功率计。The second receiving and detecting device 8 is a communication band 1550nm optical power meter.

本实施例工作时,将所述的长周期光纤光栅4置入毛细管中,并在毛细管中注入磁流体5,使得长周期光纤光栅4置于磁流体5环境中。由于长周期光纤光栅4的中心衰减波长对于其周围折射率的变化相当敏感。因此,当存在磁场时,磁流体5样品的折射率发生改变,使得检测到的中心衰减波长发生漂移。通过检测到的中心波长漂移值可以探测到磁流体5在磁场作用下折射率变化情况。另外,通过折射率测试装置,可以探测到所加磁场的大小。从而,达到精确检测磁场的效果。本实施例首先选用了光栅周期为400μm,空气中中心波长为1540.5nm的长周期光纤光栅4,并且置于密度为1.2g/ml的水基磁流体5中,在通过外部施加磁场装置改变磁场的过程中,接收检测装置9接收到的中心衰减波长变化明显。装置工作区域中心在25摄氏度左右,灵敏度达到了0.0025nm/Gs,实验结果与理论预测吻合。本实施例通过施加磁场改变磁流体5的折射率,从而改变了长周期光纤光栅4的中心波长位置,从1528.4nm移动到了1532.2nm,由此探测到的磁场的变化范围为0到1500Gs。实验得出的磁场与中心波长的关系为:When this embodiment works, the long-period fiber grating 4 is put into the capillary, and the magnetic fluid 5 is injected into the capillary, so that the long-period fiber grating 4 is placed in the environment of the magnetic fluid 5 . Since the central attenuation wavelength of the long-period fiber grating 4 is quite sensitive to changes in the surrounding refractive index. Therefore, when a magnetic field exists, the refractive index of the sample of the magnetic fluid 5 changes, so that the detected central attenuation wavelength shifts. The change of the refractive index of the magnetic fluid 5 under the action of the magnetic field can be detected through the detected central wavelength drift value. In addition, the magnitude of the applied magnetic field can be detected by means of a refractive index testing device. Thus, the effect of accurately detecting the magnetic field is achieved. In this embodiment, a long-period fiber grating 4 with a grating period of 400 μm and a central wavelength of 1540.5 nm in air is first selected, and placed in a water-based magnetic fluid 5 with a density of 1.2 g/ml, and the magnetic field is changed by an external magnetic field device During the process, the center attenuation wavelength received by the receiving and detecting device 9 changes significantly. The center of the working area of the device is around 25 degrees Celsius, and the sensitivity reaches 0.0025nm/Gs. The experimental results are consistent with the theoretical predictions. In this embodiment, the refractive index of the magnetic fluid 5 is changed by applying a magnetic field, thereby changing the center wavelength position of the long-period fiber grating 4 from 1528.4 nm to 1532.2 nm, and the detected magnetic field ranges from 0 to 1500 Gs. The experimentally obtained relationship between the magnetic field and the central wavelength is:

λ=[nco-(-5.49121×10-6×H+1.43255)]×Λ.λ=[n co -(-5.49121×10 -6 ×H+1.43255)]×Λ.

本实施例在常温条件下实现了磁场作用下磁流体折射率改变在检测磁场中的应用。在工作范围内,其灵敏度极高,达到了0.0025nm/Gs。该发明适用于小范围高精度的温度测量或者常温范围内的精确温度甄别。且结构简单,易于集成。This embodiment realizes the application of the change of the refractive index of the magnetic fluid under the action of the magnetic field in the detection of the magnetic field under the condition of normal temperature. In the working range, its sensitivity is extremely high, reaching 0.0025nm/Gs. The invention is suitable for small-scale high-precision temperature measurement or accurate temperature discrimination in the normal temperature range. And the structure is simple and easy to integrate.

Claims (7)

1.一种基于磁流体折射率改变检测磁场变化的装置,包括:第一光源输出装置、传输装置、磁场测试装置以及第一接收检测装置,其特征在于,所述磁场测试装置包括折射率测试装置、电磁铁、长周期光纤光栅以及磁流体样品,长周期光纤光栅置于装有磁流体的毛细管后,置于电磁铁的两个磁极中间,第一光源输出装置、磁场测试装置以及第一接收检测装置之间使用传输装置连接,第一光源输出装置输出的光在传输装置内传播,经过磁场测试装置后光信号被第一接收检测装置接收,折射率测试装置和磁流体样品连接在一起,以上所有部件之间的连接均通过光纤实现。1. A device for detecting magnetic field changes based on the refractive index of the magnetic fluid, comprising: a first light source output device, a transmission device, a magnetic field testing device and a first receiving and detecting device, wherein the magnetic field testing device includes a refractive index testing device device, electromagnet, long-period fiber grating and ferrofluid sample, the long-period fiber grating is placed behind the capillary tube containing the ferrofluid, and placed between the two magnetic poles of the electromagnet, the first light source output device, the magnetic field testing device and the first The receiving and detecting devices are connected by a transmission device, the light output by the first light source output device propagates in the transmission device, and the optical signal is received by the first receiving and detecting device after passing through the magnetic field testing device, and the refractive index testing device and the ferrofluid sample are connected together , the connections between all the above components are realized by optical fiber. 2.根据权利要求1所述的基于磁流体折射率改变检测磁场变化的装置,其特征是,所述折射率测试装置由第二光源输出装置、耦合器以及第二接收检测装置组成,这些部件之间均通过光纤连接,耦合器将入射光引导到光纤端面,并且用光纤来收集后向反射光,耦合器的输入端连接第二光源输出装置,耦合器的输入端将入射光引导到光纤端面处的光纤-磁流体样品界面上,反射回来的光功率由第二接收检测装置检测接受。2. The device for detecting changes in the magnetic field based on changes in the refractive index of the magnetic fluid according to claim 1, wherein the refractive index testing device is composed of a second light source output device, a coupler and a second receiving and detecting device, and these components They are all connected by optical fiber. The coupler guides the incident light to the end face of the optical fiber, and uses the optical fiber to collect the retroreflected light. The input end of the coupler is connected to the second light source output device, and the input end of the coupler guides the incident light to the optical fiber. On the optical fiber-magnetic fluid sample interface at the end face, the reflected optical power is detected and accepted by the second receiving and detecting device. 3.根据权利要求2所述的基于磁流体折射率改变检测磁场变化的装置,其特征是,所述第二光源输出装置为通信波段激光器。3 . The device for detecting changes in magnetic field based on changes in the refractive index of the magnetic fluid according to claim 2 , wherein the second light source output device is a communication band laser. 4 . 4.根据权利要求2所述的基于磁流体折射率改变检测磁场变化的装置,其特征是,所述第二光源检测装置为通信波段的光功率计。4 . The device for detecting changes in magnetic field based on changes in the refractive index of ferrofluid according to claim 2 , wherein the second light source detection device is an optical power meter in a communication band. 5.根据权利要求1所述的基于磁流体折射率改变检测磁场变化的装置,其特征是,所述第一光源输出装置为放大自发辐射光源。5 . The device for detecting changes in magnetic field based on changes in the refractive index of ferrofluid according to claim 1 , wherein the first light source output device is an amplified spontaneous emission light source. 6 . 6.根据权利要求1所述的基于磁流体折射率改变检测磁场变化的装置,其特征是,所述传输装置为通信波段使用的单模光纤。6 . The device for detecting changes in magnetic field based on changes in the refractive index of ferrofluid according to claim 1 , wherein the transmission device is a single-mode optical fiber used in the communication band. 7.根据权利要求1所述的基于磁流体折射率改变检测磁场变化的装置,其特征是,所述第一接收检测装置为光谱分析仪。7 . The device for detecting changes in magnetic field based on changes in the refractive index of ferrofluid according to claim 1 , wherein the first receiving and detecting device is a spectrum analyzer.
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