CN100526821C - Thin film type optical fiber temperature sensor and its temperature sensing method - Google Patents
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Abstract
本发明涉及光学测量仪器领域,其目的在于克服现有技术中的缺点,提供一种温度感应灵敏,可靠性高的薄膜型光纤温度传感器及其温度感应方法。其结构是包括一段光纤,光纤具有一个光信号入射端面和光信号出射端面,在光信号出射端面上镀制一层反射率随温度变化而变化的光学薄膜。薄膜型光纤温度传感器主要是利用光学薄膜介质的折射率随着温度变化而变化的特性,进而影响到特定波长光波的反射率或透射率变化而构成的一种新型光纤温度传感器。
The invention relates to the field of optical measuring instruments, and aims at overcoming the shortcomings in the prior art, and providing a thin-film optical fiber temperature sensor with sensitive temperature sensing and high reliability and a temperature sensing method thereof. Its structure includes a section of optical fiber, the optical fiber has an optical signal incident end face and an optical signal output end face, and an optical thin film whose reflectivity changes with temperature is plated on the optical signal output end face. The thin-film optical fiber temperature sensor is a new type of optical fiber temperature sensor that mainly utilizes the characteristics that the refractive index of the optical thin film medium changes with temperature, and then affects the reflectivity or transmittance of specific wavelength light waves.
Description
技术领域 technical field
本发明涉及光学测量仪器领域,更具体的说是一种薄膜型光纤温度传感器及其温度感应方法。The invention relates to the field of optical measuring instruments, in particular to a film-type optical fiber temperature sensor and a temperature sensing method thereof.
技术背景 technical background
在强电磁场和高电压系统中,温度是需要测量和控制的重要物理量之一,传统的电测技术如热电偶等由于具有电磁噪声和产生短路引起爆炸等危险而无法使用。光纤温度传感器具有电绝缘性能好、抗强电磁干扰、使用安全可靠、体积小、重量轻,特别适用于强电磁场、高电压以及有毒有害、易燃易爆等恶劣环境下使用,有着广阔的应用前景。In a strong electromagnetic field and high voltage system, temperature is one of the important physical quantities that need to be measured and controlled. Traditional electrical measurement techniques such as thermocouples cannot be used due to electromagnetic noise and dangers such as short circuits and explosions. The fiber optic temperature sensor has good electrical insulation performance, anti-strong electromagnetic interference, safe and reliable use, small size, and light weight. It is especially suitable for use in harsh environments such as strong electromagnetic fields, high voltage, toxic, harmful, flammable and explosive, and has a wide range of applications. prospect.
目前国内外对于光纤温度传感器的研究分为两个方向。第一类就是传光型光纤温度传感器。传光型把光的强度(吸收,热辐射,折射率变化,散射),波长(荧光,光致发光),偏振面(双折射),时间变化(荧光)等当作温度信号,只是利用光纤传输光的信道作用,在光纤的一个端面上配置另外的温度敏感器件,并与光纤耦合起来,构成光纤传感器。第二类就是传感型光纤温度传感器,是利用相位(干涉),强度(散射)作为温度信号,利用光纤自身所具有的物理参数随着温度变化而变化的特性构成光纤传感器。传光型传感器虽然对温度检测的灵敏度较差,但可靠性高,其中利用荧光吸收,热辐射的光纤温度传感器已达到实用水平。传感型光纤温度传感器的灵敏度高,但由于对温度以外的压力,振动等机械量的变化也很敏感,因此,其可靠性是尚未解决的问题。At present, the research on optical fiber temperature sensor at home and abroad is divided into two directions. The first type is the light-transmitting fiber optic temperature sensor. The light transmission type regards the intensity of light (absorption, thermal radiation, refractive index change, scattering), wavelength (fluorescence, photoluminescence), polarization plane (birefringence), time change (fluorescence), etc. as temperature signals, but only uses optical fiber For the channel function of transmitting light, another temperature-sensitive device is arranged on one end face of the optical fiber, and coupled with the optical fiber to form an optical fiber sensor. The second type is the sensor-type optical fiber temperature sensor, which uses phase (interference) and intensity (scattering) as temperature signals, and uses the characteristics of the physical parameters of the optical fiber itself to change with temperature to form an optical fiber sensor. Although the light transmission type sensor has poor sensitivity to temperature detection, it has high reliability. Among them, the optical fiber temperature sensor using fluorescence absorption and thermal radiation has reached the practical level. Sensing-type optical fiber temperature sensor has high sensitivity, but it is also very sensitive to changes in mechanical quantities other than temperature, such as pressure and vibration, so its reliability is an unresolved problem.
发明内容 Contents of the invention
本发明的目的在于克服现有技术中的缺点,提供一种温度感应灵敏,可靠性高的薄膜型光纤温度传感器及其温度感应方法。The purpose of the present invention is to overcome the shortcomings in the prior art, and provide a thin-film optical fiber temperature sensor with sensitive temperature sensing and high reliability and a temperature sensing method thereof.
首先本发明公开了一种薄膜型光纤温度传感器,结构是包括一段光纤,光纤具有一个光信号入射端面和光信号出射端面,在光信号出射端面上镀制一层反射率随温度变化而变化的光学薄膜。薄膜型光纤温度传感器主要是利用光学薄膜介质的折射率随着温度变化而变化的特性,进而影响到特定波长光波的反射率或透射率变化而构成的一种新型光纤温度传感器。本发明使用时不会受到在温度的测量过程中产生的强电磁场或高电压影响,同时具有传感型光纤温度传感器的灵敏度,而且由于光学薄膜厚度十分小,因此本发明不会受到外界压力,振动等机械量的影响,具有很高的稳定性。First of all, the invention discloses a film-type optical fiber temperature sensor. The structure includes a section of optical fiber. The optical fiber has an optical signal incident end face and an optical signal output end face. film. The thin-film optical fiber temperature sensor is a new type of optical fiber temperature sensor that mainly utilizes the characteristics that the refractive index of the optical thin film medium changes with temperature, and then affects the reflectivity or transmittance of specific wavelength light waves. When the present invention is used, it will not be affected by the strong electromagnetic field or high voltage generated during the temperature measurement process, and has the sensitivity of the sensor-type optical fiber temperature sensor, and because the thickness of the optical film is very small, the present invention will not be subjected to external pressure. Influenced by mechanical quantities such as vibration, it has high stability.
本发明进一步提供一种适用所述薄膜型光纤温度传感器的温度感应方法,通过获得在光纤端面的光学薄膜的反射率或透过率,根据光学薄膜反射率或透过率随外界温度变化的曲线获得外界温度。这不同于现有传感型光纤温度传感器,是利用相位(干涉),强度(散射)作为温度信号,利用光纤自身性质随温度的变化而变化来获得温度,这也决定了本发明所具有的稳定性优势。所述光学薄膜反射率或透过率随外界温度变化的曲线是通过在标定温度下测量特定波长反射率或透过率的变化,并将多组相对应的数据在坐标系上拟合得到的定标曲线。采用标定温度的方法来获得定标曲线的方式是最直接的一种方式,而且也是最符合每个具体温度传感器自身特点的一种方式,能够进一步减少由于工艺原因所产生的误差。The present invention further provides a temperature sensing method suitable for the film-type optical fiber temperature sensor, by obtaining the reflectance or transmittance of the optical film on the end face of the optical fiber, according to the curve of the reflectance or transmittance of the optical film with the external temperature Get the outside temperature. This is different from the existing sensor-type optical fiber temperature sensor, which uses phase (interference) and intensity (scattering) as temperature signals, and uses the properties of the optical fiber itself to change with temperature to obtain temperature, which also determines the advantages of the present invention. Stability advantage. The curve of the reflectance or transmittance of the optical film changing with the external temperature is obtained by measuring the change of the reflectance or transmittance of a specific wavelength at the calibration temperature and fitting multiple sets of corresponding data on the coordinate system calibration curve. It is the most direct way to obtain the calibration curve by calibrating the temperature, and it is also a way that is most in line with the characteristics of each specific temperature sensor, which can further reduce the error caused by the process.
上述方法具体包括以下步骤:The above method specifically includes the following steps:
①将薄膜型光纤温度传感器置于被探测的温度环境中,光信号从光纤的光信号入射端面入射;① Place the film-type optical fiber temperature sensor in the temperature environment to be detected, and the optical signal is incident from the optical signal incident end face of the optical fiber;
②探测光信号在镀制在光纤光信号出射端面上的光学薄膜的反射光强或透射光强;②Detect the reflected light intensity or transmitted light intensity of the optical signal on the optical film plated on the output end surface of the optical fiber optical signal;
③计算光学薄膜的反射率或透射率;③ Calculate the reflectance or transmittance of the optical film;
④根据上述的反射率或透射率对应光学薄膜反射率或透过率随外界温度变化的曲线,获得被探测环境的温度。④ Obtain the temperature of the detected environment according to the above-mentioned curve of reflectance or transmittance corresponding to the reflectance or transmittance of the optical film as a function of external temperature.
本发明方法简单容易实现,而且适用于采用计算机进行测量和计算,有利于提高测量系统的自动化程度,使得温度测量更加简易且人性化。The method of the invention is simple and easy to realize, and is suitable for measuring and calculating with a computer, which is beneficial to improving the degree of automation of the measuring system, and makes temperature measurement easier and more humanized.
上述薄膜型光纤温度传感器的传感端是通过在光纤端面镀制的光学薄膜组成的,为使得反射率或透过率曲线具有良好的线性度,便于测量。本发明选择了截止滤光膜层结构作为在光纤端面镀膜的标准。The sensing end of the above-mentioned film-type optical fiber temperature sensor is composed of an optical film plated on the end face of the optical fiber, so that the reflectance or transmittance curve has good linearity and is convenient for measurement. The present invention selects the cut-off filter film layer structure as the standard for coating the optical fiber end face.
所述光学薄膜的膜系结构为或,H表示光学厚度为四分之一膜系的中心波长的高折射率层,L表示光学厚度为四分之一中心波长的低折射率层。m为基本周期的重复次数,一般为5<m<10,可以根据具体采用的镀膜机而定,采用现有通用的镀膜机,其最佳数值为6或7。截止滤光膜层由高、低折射率的材料组成,环境温度对光学薄膜器件温度稳定性的影响主要是通过改变光学薄膜器件的光学常数(n,k,d)来实现的。在可见、近红外波段,所述低折射率介质层和高折射率层材料采用氧化物、氟化物、硫化物或碲化物。这类材料的折射率温度系数和其热膨胀系数相当,其温度漂移主要由折射率n和几何厚度d共同作用决定,影响主要由折射率n和几何厚度d共同作用决定。对折射率温度系数比较大的材料,光学薄膜器件的温度漂移主要由折射率n的变化引起的。所述低折射率层材料为SiO2、NaF或MgF2,高折射率层材料为TiO2、PbTe或ZeS,截止滤光膜层的光谱性能由各层膜的折射率和厚度决定。环境温度的变化时,所述光学薄膜的光学特性会随着环境温度的变化而发生变化。这种变化主要表征为光学薄膜的峰值透过率发生变化,截止波长或中心波长的位置发生漂移,带宽改变等。The film system structure of described optical thin film is or , H represents the high refractive index layer whose optical thickness is a quarter of the central wavelength of the film system, and L represents the low refractive index layer whose optical thickness is a quarter of the central wavelength. m is the number of repetitions of the basic cycle, generally 5<m<10, which can be determined according to the specific coating machine used, and the best value is 6 or 7 if the existing general coating machine is used. The cut-off filter layer is composed of high and low refractive index materials. The influence of ambient temperature on the temperature stability of optical thin film devices is mainly realized by changing the optical constants (n, k, d) of optical thin film devices. In the visible and near-infrared bands, the low refractive index medium layer and the high refractive index layer are made of oxide, fluoride, sulfide or telluride. The temperature coefficient of the refractive index of this kind of material is equivalent to its thermal expansion coefficient, and its temperature drift is mainly determined by the joint action of the refractive index n and the geometric thickness d, and the influence is mainly determined by the joint action of the refractive index n and the geometric thickness d. For materials with a relatively large temperature coefficient of refractive index, the temperature drift of optical thin film devices is mainly caused by the change of refractive index n. The material of the low refractive index layer is SiO 2 , NaF or MgF 2 , the material of the high refractive index layer is TiO 2 , PbTe or ZeS, and the spectral performance of the cut-off filter film layer is determined by the refractive index and thickness of each film. When the ambient temperature changes, the optical properties of the optical film will change with the change of the ambient temperature. This change is mainly characterized by a change in the peak transmittance of the optical film, a shift in the position of the cut-off wavelength or center wavelength, and a change in bandwidth.
本发明相对于现有技术具有以下突出的实质性特点和显著的进步。Compared with the prior art, the present invention has the following outstanding substantive features and remarkable progress.
1.本发明公开的传感器结构具有体积小、重量轻的优点,特别适用于强电磁场、高电压等恶劣环境下的温度测量;1. The sensor structure disclosed in the present invention has the advantages of small size and light weight, and is especially suitable for temperature measurement in harsh environments such as strong electromagnetic fields and high voltages;
2.具有很高的灵敏度和良好的重复性和温度稳定性;2. High sensitivity and good repeatability and temperature stability;
3.本发明方法简单易于实施,能够适用于计算机控制,降低误差。3. The method of the present invention is simple and easy to implement, and can be applied to computer control to reduce errors.
附图说明 Description of drawings
图1本发明传感器的膜系反射率曲线;The film system reflectivity curve of Fig. 1 sensor of the present invention;
图2为薄膜的反射率-温度关系曲线;Fig. 2 is the reflectance-temperature relational curve of film;
图3为本发明传感器结构示意图;Fig. 3 is a schematic structural diagram of the sensor of the present invention;
图4为传感器测量系统原理图;Figure 4 is a schematic diagram of the sensor measurement system;
图5为光纤传感器的反射率-温度关系曲线。Fig. 5 is the reflectivity-temperature relation curve of the optical fiber sensor.
具体实施方式 Detailed ways
以下结合附图对本发明做进一步详细的说明。The present invention will be described in further detail below in conjunction with the accompanying drawings.
原理说明Principle Description
带通截止滤光膜层结构的截止波长可表述成:The cut-off wavelength of the band-pass cut-off filter film layer structure can be expressed as:
其中λ0是一个参考波长。where λ 0 is a reference wavelength.
其截止带宽度为:Its cut-off band width is:
相应的透射率为:The corresponding transmittance is:
从上面可以看出Δg是关于ηH和ηL的函数,而当正入射时,ηH=nH,ηL=nL。而nH和nL又是温度T的函数,那么截止带宽度Δg也是温度T的函数,可以写成如下形式:It can be seen from the above that Δg is a function of η H and η L , and when it is normal incidence, η H =n H , η L =n L . And n H and n L are functions of temperature T, then the cut-off band width Δg is also a function of temperature T, which can be written as follows:
Δg=f(T) (4)Δg=f(T) (4)
对上式求微分,得,Differentiate the above formula to get,
当温度变化时,截止带宽度会发生变化,特定波长处的反射率也会发生变化。一般材料的折射率随温度变化的规律成线性关系,透射率曲线边沿处的反射率随温度的变化也成线性关系。基于这个变化特性,本发明设计出一种新型的薄膜型光纤传感器。When the temperature changes, the cut-off band width changes, as does the reflectivity at a specific wavelength. Generally, the refractive index of a material has a linear relationship with the change of temperature, and the reflectivity at the edge of the transmittance curve also has a linear relationship with the change of temperature. Based on this change characteristic, the present invention designs a novel thin-film optical fiber sensor.
考虑到一般所设计的传感器所用光信号的中心波长为1310nm,所以在裸光纤端面镀膜中,要使得1310nm附近的反射率曲线具有良好的线性度。本发明选择了截止滤光片的膜层结构作为在光纤端面镀膜的标准。选择TiO2作为高折射率材料,SiO2作为低折射率材料,并且先选定膜系的中心波长为1080nm。入射介质为玻璃,透射介质是空气。膜系结构为。通过模拟计算,得出不同波长下的反射率曲线,如图1所示。该膜系的反射率曲线在1310nm附近有着良好的线性度。选定这段曲线作为传感器的工作区域。当温度产生变化时候,由于材料折射率的变化,这段曲线会产生漂移,从而使得特定波长处的透过率也产生相应的变化,如图2所示,其中T1<T2<T3且T3-T2=T2-T1。通过标定温度与特定波长下透过率的变化关系,可以得到一条定标曲线。利用定标曲线,当测得透过率的值,便可找到相对应的温度,从而达到传感温度的作用。将前面设计的膜系结构镀制在单模光纤端面上,制备出设计的薄膜型光纤温度传感器。Considering that the center wavelength of the optical signal used by the generally designed sensor is 1310nm, in the coating on the end face of the bare optical fiber, the reflectivity curve near 1310nm should have good linearity. The present invention selects the film layer structure of the cut-off filter as the standard for coating the end face of the optical fiber. Choose TiO 2 as the high refractive index material, SiO 2 as the low refractive index material, and first select the central wavelength of the film system as 1080nm. The incident medium is glass and the transmitted medium is air. The film structure is . Through simulation calculation, the reflectance curves at different wavelengths are obtained, as shown in Fig. 1 . The reflectance curve of this film system has good linearity around 1310nm. Select this curve as the working area of the sensor. When the temperature changes, due to the change of the refractive index of the material, this curve will drift, so that the transmittance at a specific wavelength will also change accordingly, as shown in Figure 2, where T 1 <T 2 <T 3 And T 3 -T 2 =T 2 -T 1 . A calibration curve can be obtained by calibrating the relationship between temperature and transmittance at a specific wavelength. Using the calibration curve, when the value of the transmittance is measured, the corresponding temperature can be found, so as to achieve the function of sensing temperature. The previously designed film structure was plated on the end face of the single-mode optical fiber to prepare the designed film-type optical fiber temperature sensor.
光纤温度传感器的结构如图3所示,传感器由镀在裸光纤1端面的高、低折射率周期薄膜2组成,膜系结构为高折射率材料为TiO2,低折射率材料为SiO2,基本周期的重复次数为6,选定膜系的中心波长为1080nm。膜系的反射率曲线如前面所述的图2所示,膜系的透过率曲线在1260nm到1360nm间有较好的线性度。当温度变化时,膜系的光谱特性将发生变化,其中1260nm到1360nm间的反射率与温度的变化曲线具有比较好的线性。通过测量传感器的反射率,将得到传感器探测到的外界温度。The structure of the optical fiber temperature sensor is shown in Figure 3. The sensor is composed of high and low refractive index
利用本发明所述的传感器,按照图4搭建传感器模拟实验测量系统。在本实验系统中,选用中心波长为1310nm的LD光源3作为信号源,3dB耦合器4和Newport公司生产的1830-C型光电探测器5。LD光源3发出的光经3dB耦合器4进入本发明的薄膜型光纤温度传感器6,薄膜型光纤温度传感器6的反射光将再次通过3dB耦合器4的而进入光电探测器5,反射光信号经光电探测器5探测到。耦合器4的另一支插入折射率匹配液8中以消除端面反射。把薄膜型光纤温度传感器6放进水浴锅9中,通过改变水浴锅9的温度来改变其环境温度,薄膜型光纤温度传感器6的温度可以直接从水温中读出。实验发现,当薄膜型光纤温度传感器6的温度变化时,光电探测器5探测到的光强也在改变,而且反射率的变化跟薄膜型光纤温度传感器6的温度变化成比较好的线性关系。将得到的数据通过计算机7进行分析就可以得出薄膜型光纤温度传感器6探测到的温度值。在实际使用中要先对设计的薄膜型光纤温度传感器6进行温度测量定标。Utilize the sensor described in the present invention, set up the sensor simulation experiment measuring system according to Fig. 4. In this experimental system, the LD
基于上面所测的特定波长出的光纤透射率与温度的线性关系,按照图4的实验系统图进行了薄膜型光纤温度传感器6的实验。测得的1310nm的薄膜型光纤温度传感器6的反射率与温度的关系曲线,如图5所示。实验结果表明,本发明的传感器的测量精度能达到1℃,在多次测量中也显示了良好的稳定性和重复性。如果通过选用更高的折射率温度系数材料如碲化铅、硫化锌等,本发明的测量精度将会进一步得到提高。Based on the measured linear relationship between the optical fiber transmittance at a specific wavelength and the temperature, the experiment of the thin-film optical
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