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CN100409917C - Trace element activity analysis and extraction method and device - Google Patents

Trace element activity analysis and extraction method and device Download PDF

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CN100409917C
CN100409917C CNB2004100481436A CN200410048143A CN100409917C CN 100409917 C CN100409917 C CN 100409917C CN B2004100481436 A CNB2004100481436 A CN B2004100481436A CN 200410048143 A CN200410048143 A CN 200410048143A CN 100409917 C CN100409917 C CN 100409917C
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林松辉
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Abstract

The invention relates to a method and a device for analyzing and extracting the activity of trace elements, wherein the device comprises: a filter device; a preheating device is communicated with the filtering device; an extraction tank communicated with the preheating device and filled with material; the activation tank is communicated with the extraction tank and is filled with ozone; an ozone generator, which is communicated with the extraction tank and the activation tank and provides an ozone source; a high pressure oxygen generator, which is communicated with the extraction tank and provides a high pressure oxygen source; a filtering storage tank which is communicated with the activation tank for filtering and storing; the extraction method includes mixing ozone, high pressure oxygen and water, and ultrasonic diathermy, and at normal temperature, its high decomposition capacity and forced permeability are used to stabilize the physical property of extracted matter, make nutrients not easy to be lost, and make the extracted matter possess high pharmacological activity.

Description

微量元素活性分析萃取方法及其装置 Extraction method and device for trace element activity analysis

技术领域 technical field

本发明为一种微量元素活性分析萃取方法及其装置,可在常温下进行,使萃取的物质物性稳定,营养素成份不易流失,萃取成份较高及药理活性完整的方法与装置。The present invention is a trace element activity analysis and extraction method and its device, which can be carried out at normal temperature, so that the physical properties of the extracted substance are stable, the nutrient components are not easy to lose, the method and the device have high extraction components and complete pharmacological activity.

背景技术 Background technique

人体及所有其它生命有机体都需要特定的营养素来维持身体组织的健全,并提供活动所需的热量。一般所指的营养素包含两大类:一是巨量营养素,包括蛋白质、碳水化合物及脂肪,用以供应热量及组织物质;另一种为微量营养素,其需要量极微,包括微生素以及矿物质,虽不能供应热量,但在体内的生化代谢上却扮演相当重要的角色。The human body, and all other living organisms, require specific nutrients to maintain the health of body tissues and provide the calories needed for activity. The nutrients generally referred to include two categories: one is macronutrients, including protein, carbohydrates and fats, which are used to supply calories and tissue substances; the other is micronutrients, which require very small amounts, including micronutrients and Although minerals cannot supply calories, they play a very important role in the biochemical metabolism in the body.

所谓的微量元素是指在人体内的组织组成与需要均很微量,一般低于一百毫克或低至微克,却是巨量营养要素的生化代谢及功能执行上所必需,若无矿物质与微量元素的存在,体内微生素、酵素以及辅酵素的作用将会完全丧失。这些微量元素包括锌、铜、锰、铁、钴、氟、钼、碘、硼、铬、硅、硒、锗、钒、镓、镍、锡、镧、锂。The so-called trace elements refer to very small amounts of tissue composition and requirements in the human body, generally less than 100 mg or as low as micrograms, but they are necessary for the biochemical metabolism and function execution of macronutrients. Without minerals and With the existence of trace elements, the functions of microorganisms, enzymes and coenzymes in the body will be completely lost. These trace elements include zinc, copper, manganese, iron, cobalt, fluorine, molybdenum, iodine, boron, chromium, silicon, selenium, germanium, vanadium, gallium, nickel, tin, lanthanum, lithium.

在人体内,微量元素通常与有机化合物(主要是蛋白质形成复合物,例如,铁与蛋白质形成运铁蛋白质,用来运送及储存铁;血红素中结合的铁离子,本身为活性中心,能与蛋白质及氧分子结合,负责氧的运送;锌是脱氢酵素及磷酸水解酵素的组成成份;细胞氧化酵素同时需要铜及铁。In the human body, trace elements usually form complexes with organic compounds (mainly proteins, for example, iron and proteins form transferrin, which is used to transport and store iron; iron ions bound in heme itself are active centers and can interact with The combination of protein and oxygen molecules is responsible for the transportation of oxygen; zinc is a component of dehydrogenase and phosphohydrolase; cell oxidative enzymes need both copper and iron.

在过去五十年当中,微量元素的生物功能以及因为缺乏微量元素引发疾病的相关研究进展快速,重要性因而日益提升。一般而言,缺乏微量元素均会造成健康上的问题,如缺铁引起贫血症、缺碘出现甲状腺肿大即是最典型的例子。大部份人则是因为蛋白质与卡路里的吸收不平衡而造成各种苦痛,或因微量元素摄取不足而造成多种疾病。虽然营养不良及肌饿主要出在亚洲、非洲及拉丁美洲的部份贫穷地区,但是几种微量元素包括锌、铜、硒的缺乏,已在全世界各地(包括富裕地区普遍发生。一般人都认为微量元素如铬、铜、锰及硒的需要量极低,以至于这些元素的缺乏症常被忽略。Over the past fifty years, research on the biological functions of trace elements and related diseases caused by their deficiencies has progressed rapidly, and their importance has thus increased. Generally speaking, the lack of trace elements will cause health problems, such as anemia caused by iron deficiency and goiter caused by iodine deficiency are the most typical examples. Most people suffer from various pains due to unbalanced absorption of protein and calories, or various diseases due to insufficient intake of trace elements. Although malnutrition and muscle starvation are mainly found in some poor areas of Asia, Africa and Latin America, deficiencies of several trace elements, including zinc, copper, and selenium, have commonly occurred in various parts of the world (including rich areas. It is generally believed that Requirements for trace elements such as chromium, copper, manganese and selenium are so low that deficiencies of these elements are often overlooked.

以营养的角度而言,微量元素可以由自然食物中取得,不必额外补充。如果我们的土地是纯净天然、毫无任何污染,如果我们的水源与水质自然洁净,如果我们的空气清新怡人,那么,每天所需的营养素,包括微量元素都可以由食物、蔬果中供应。可惜的是,人为因素破坏整个大自然的物理化学与生物链,因此,在这种情况下,每天的食物与饮水则不能确保我们一天身体健康所需的营养。From a nutritional point of view, trace elements can be obtained from natural foods without additional supplementation. If our land is pure and natural without any pollution, if our water source and water quality are naturally clean, if our air is clean and pleasant, then the nutrients we need every day, including trace elements, can be supplied from food, vegetables and fruits. It is a pity that human factors destroy the physical, chemical and biological chains of the entire nature. Therefore, in this case, the daily food and drinking water cannot ensure the nutrition we need for a healthy day.

目前欲萃取水中的微量元素,皆是利用高温方式加以萃取,但以此方式萃取会使萃取出的微量元素物性不稳定,营养成份也极易流失,且物理架构(或其产生的药理活性也可能会被高温所破坏,因此,亦不完整。At present, the trace elements in the water are to be extracted by high temperature method, but the extraction in this way will make the extracted trace elements unstable in physical properties, and the nutrients are easily lost, and the physical structure (or the pharmacological activity produced by it) will also be affected. May be destroyed by heat and, therefore, incomplete.

发明内容 Contents of the invention

本发明人有鉴于以目前的环境因素,均衡的食物与饮水不能确保提供人们一天所需的微量元素,因此发明一种微量元素活性分析萃取方法及其装置,其利用臭氧及高压氧与水混合后,再配合超音波透热性,在常温下,利用其高分解能力与强迫渗透性,达到使萃取之物质物性稳定,营养素成份不易流失,萃取成份较高及药理活性完整为其发明目的。In view of the current environmental factors, balanced food and drinking water cannot ensure the supply of trace elements needed by people for a day, so the inventor invented a method for analyzing and extracting trace element activity and its device, which uses ozone and high pressure oxygen to mix with water Finally, combined with ultrasonic heat permeability, at room temperature, using its high decomposition ability and forced permeability, the physical properties of the extracted substances are stabilized, the nutrients are not easy to lose, the extracted components are high and the pharmacological activity is complete. This is the purpose of the invention.

为了可达到前述的发明目的,本发明所运用的技术手段在于提供一种微量元素活性分析萃取装置,其包括:In order to achieve the aforementioned object of the invention, the technical means used in the present invention is to provide a trace element activity analysis extraction device, which includes:

一过滤装置,将水源去离子化形成去离子水;A filter device to deionize the water source to form deionized water;

一预热装置,与过滤装置相连通,可将去离子水加热至25-50℃;A preheating device, connected with the filter device, can heat the deionized water to 25-50°C;

一萃取槽,与预热装置连通,其内置有物质材料,并可供上述加热后的水导入,并通以臭氧及高压氧形成萃取液;An extraction tank, which communicates with the preheating device, has a built-in material, and can be used for the introduction of the above-mentioned heated water, and is passed through ozone and high-pressure oxygen to form an extraction liquid;

一活化槽,与萃取槽连通,供上述通以臭氧与高压氧之萃取液导入,并通以臭氧加以活化成活化液;An activation tank, connected with the extraction tank, for the introduction of the above-mentioned extract solution fed with ozone and high pressure oxygen, and activated with ozone to form an activation solution;

一臭氧产生机,与萃取槽及活化槽相连通,提供臭氧源,并将产生之臭氧注入萃取槽及活化槽中;An ozone generator, connected to the extraction tank and the activation tank, provides an ozone source, and injects the generated ozone into the extraction tank and the activation tank;

一高压氧产生机,与萃取槽相连通,提供高压氧源,并将产生的高压氧与上述臭氧混合注入萃取槽中;A hyperbaric oxygen generator, connected with the extraction tank, providing a high-pressure oxygen source, and injecting the generated hyperbaric oxygen into the extraction tank mixed with the above-mentioned ozone;

一过滤储存槽,与活化槽相连通,供活化液导入,其内设有一过滤装置,将活化液加以过滤,并可供此过滤液储存;A filter storage tank, connected with the activation tank, for the introduction of the activation solution, with a filter device inside to filter the activation solution and store the filtrate;

一封装设备,与过滤储存槽相连通,将过滤液加以封装。An encapsulation device communicates with the filter storage tank and encapsulates the filtrate.

所述的装置,其物质材料为矿石、海藻、灵芝、蒲公英或薏苡仁。The material of the device is ore, seaweed, ganoderma lucidum, dandelion or coix seed.

一种分析萃取微量元素的方法,包括有:A method for analyzing and extracting trace elements, comprising:

取得一水源;obtain a source of water;

将其去离子化,形成去离子化的纯水;Deionize it to form deionized pure water;

将此纯水加温成25-50℃的加热水;Warm the pure water into heated water at 25-50°C;

将加热水加入物质材料成为混合液;Add heated water to the substance material to form a mixed liquid;

将该混合液通以臭氧与高压氧成为携带有微量元素之萃取液;The mixture is passed through ozone and high pressure oxygen to become an extract carrying trace elements;

将此萃取液以臭氧加以活化成活化水;Activating the extract with ozone into activated water;

将此活化水再次与物质材料接触并通以臭氧及高压氧后,再以臭氧加以活化,重复此一步骤;Contact the activated water with the material again and pass it through ozone and high pressure oxygen, then activate it with ozone, and repeat this step;

将此活化水过滤成滤清液;Filter this activated water into a filtrate;

将滤清液加以装瓶。The filtrate is bottled.

所述的方法,其物质材料为矿石、海藻、灵芝、蒲公英或薏苡仁。In the method, the material is ore, seaweed, ganoderma lucidum, dandelion or coix seed.

所述的方法,其加热水与物质材料混合比为2∶3。In the method, the mixing ratio of heating water to material is 2:3.

所述的方法,将活化水再次与物质材料接触并通以臭氧及高压氧后,再以臭氧加以活化,重复此一步骤最少五小时。In the method described above, the activated water is contacted with the material again and passed through ozone and high-pressure oxygen, and then activated with ozone, and this step is repeated for at least five hours.

附图说明 Description of drawings

图1是本发明的示意图。Figure 1 is a schematic diagram of the present invention.

10:过滤装置    20:预热装置10: Filtration device 20: Preheating device

30:萃取槽        31:高压氧产生机30: Extraction tank 31: Hyperbaric oxygen generator

32:臭氧产生机    40:活化槽32: Ozone generator 40: Activation tank

50:过滤储存槽    60:封装设备50: Filtration storage tank 60: Packaging equipment

本发明的微量元素活性分析萃取装置,参看图1所示,其包括:一过滤装置10,将水源去离子化形成去离子水;一预热装置20,与上述过滤装置10相连通,可将去离子水加热至25-50℃;一萃取槽30,与前述的预热装置20相连通,其内置有物质材料31,并可供上述加热后的水导入,并通以臭氧及高压氧形成萃取液;一活化槽40,与上述萃取槽30相连通,可供上述通以臭氧与高压氧的萃取液导入,并通以臭氧加以活化成活化液;一臭氧产生机32,与上述萃取槽30及活化槽40相连通,提供臭氧源,并将产生的臭氧注入萃取槽30及活化槽40中;一高压氧产生机31,与上述萃取槽30相连通,提供高压氧源,并将产生的高压氧与上述臭氧混合注入萃取槽30中;一过滤储存槽50,与活化槽40相连通,供活化液导入,其内设有一过滤装置,将活化液加以过滤,并可供此过滤液储存;一封装设备60,与过滤储存槽相连通,将过滤液加以封装。The trace element activity analysis and extraction device of the present invention is shown in Fig. 1, and it comprises: a filter device 10, deionizes water source and forms deionized water; A preheating device 20, communicates with above-mentioned filter device 10, can The deionized water is heated to 25-50°C; an extraction tank 30 is connected with the aforementioned preheating device 20, and has a built-in material 31, which can be introduced into the heated water and passed through ozone and high-pressure oxygen to form Extraction solution; an activation tank 40, which communicates with the above-mentioned extraction tank 30, can be used for the introduction of the above-mentioned extraction solution with ozone and high pressure oxygen, and is activated with ozone to become an activation solution; an ozone generator 32, connected with the above-mentioned extraction tank 30 and activation tank 40 are communicated to provide an ozone source, and inject the ozone produced in the extraction tank 30 and activation tank 40; a high-pressure oxygen generator 31 communicates with the above-mentioned extraction tank 30 to provide a high-pressure oxygen source and generate The high pressure oxygen and the above-mentioned ozone are mixed and injected into the extraction tank 30; a filter storage tank 50 is connected with the activation tank 40 for the introduction of the activation solution, and a filter device is arranged in it to filter the activation solution and provide the filtrate Storage: an encapsulation device 60 communicated with the filter storage tank for encapsulating the filtrate.

本发明分析萃取微量元素的方法,包括有:取得一水源;将其于过滤装置10中去离子化,形成去离子化的纯水;将此纯水导入预热装置20中加温成25-50℃的加热水;将此加热水加入置有物质材料的萃取槽30中使其成为混合液;将该混合液于萃取槽30中,再通以臭氧产生机32所产生的臭氧与高压氧产生机31所产生的高压氧,使其成为携带有微量元素的萃取液;再将此萃取液导入活化槽40中,再以臭氧产生机32产生的臭氧加以活化成活化水;继续将此活化水导入萃取槽30中,在此萃取槽30中通以臭氧及高压氧,再将其导入活化槽40中,以臭氧加以活化,重复此一步骤五小时以上,且皆于常温的环境下进行,使活化水提高其内的微量元素含量;将此活化水导入过滤储存槽50中过滤成滤清液并加以储存;最后将滤清液利用封装设备60加以装瓶。The method for analyzing and extracting trace elements of the present invention includes: obtaining a water source; deionizing it in the filter device 10 to form deionized pure water; introducing the pure water into the preheating device 20 and heating it to 25- Heated water at 50°C; add this heated water into the extraction tank 30 with the material material to make it a mixed solution; put the mixed solution in the extraction tank 30, and then pass through the ozone and high-pressure oxygen produced by the ozone generator 32 The high-pressure oxygen produced by the generator 31 makes it an extract containing trace elements; then the extract is introduced into the activation tank 40, and then activated by the ozone produced by the ozone generator 32 to become activated water; continue to activate this Water is introduced into the extraction tank 30, ozone and high pressure oxygen are passed through the extraction tank 30, and then introduced into the activation tank 40, activated with ozone, and this step is repeated for more than five hours, and all are carried out at room temperature , to increase the trace element content in the activated water; introduce the activated water into the filter storage tank 50 to filter into a filtrate and store it;

上述置于萃取槽30中的物质材料可为矿石、海藻、灵芝、蒲公英或薏苡仁等,另,其加热水与物质材料混合比为2∶3,如水40%、物质材料60%,在常温下,利用高压氧及臭氧产生的超音波透热方式,将上述物质材料中含有的微量元素萃取出来,并溶入水中,使水中含有微量元素,其使用物质材料的比例可为矿石40%、灵芝10%、海藻20%、蒲公英15%、薏苡仁15%。The above-mentioned material material placed in the extraction tank 30 can be ore, seaweed, Ganoderma lucidum, dandelion or coix seed, etc. In addition, the mixing ratio of the heating water and the material material is 2:3, such as 40% water, 60% material material, at normal temperature Under the condition of using hyperbaric oxygen and ozone to produce ultrasonic diathermy, the trace elements contained in the above materials are extracted and dissolved in water to make the water contain trace elements. The ratio of the materials used can be 40% ore, Ganoderma lucidum 10%, seaweed 20%, dandelion 15%, coix seed 15%.

而实施时,上述萃取槽30的容量为30公吨,而萃取液的臭氧浓度为0.08ppm至0.13ppm,且臭氧的出气压力为3.5公斤,另高压氧流量为700公升/分钟;另,活化槽40的容量为10公吨,而其内的臭氧浓度为0.3ppm至0.5ppm,且其臭氧的出气压力为3.5公斤至5公斤。And during implementation, the capacity of above-mentioned extraction tank 30 is 30 metric tons, and the ozone concentration of extraction liquid is 0.08ppm to 0.13ppm, and the gas outlet pressure of ozone is 3.5 kilograms, and other hyperbaric oxygen flow rate is 700 liters/minute; In addition, activation tank The capacity of 40 is 10 metric tons, and the ozone concentration in it is 0.3ppm to 0.5ppm, and the outlet pressure of its ozone is 3.5kg to 5kg.

综上所述,本发明的微量元素活性分析萃取方法及其装置,其利用臭氧及高压氧与水混合后,再配合超音波透热性,在常温下,利用其高分解能力与强迫渗透性,为一可使萃取的物质物性稳定,营养素成份不易流失,萃取成份较高及药理活性完整的发明。In summary, the trace element activity analysis and extraction method and its device of the present invention use ozone and high pressure oxygen to mix with water, and then cooperate with ultrasonic heat permeability, and use its high decomposition ability and forced permeability at room temperature , is an invention that can stabilize the physical properties of the extracted substance, prevent the loss of nutrients, have high extraction components and complete pharmacological activity.

Claims (6)

1. a micro-activity analysis extraction equipment is characterized in that, comprising:
One filter forms deionized water with the water source deionization;
One preheating device is connected with filter, deionized water can be heated to 25-50 ℃;
One extraction tank is communicated with preheating device, and it is built-in with material, and can import for the water after the above-mentioned heating, and passes to ozone and hyperbaric oxygen formation extract;
One activated bath is communicated with extraction tank, for the above-mentioned extract importing that passes to ozone and hyperbaric oxygen, and passes to ozone and is activated into activating solution;
One ozone generating machine is connected with extraction tank and activated bath, and ozone source is provided, and the ozone that produces is injected extraction tank and activated bath;
One hyperbaric oxygen produces machine, with extraction trough, provides the high pressure oxygen source, and the hyperbaric oxygen that produces is mixed the injection extraction tank with above-mentioned ozone;
One filters accumulator tank, is connected with activated bath, imports for activating solution, is provided with a filter in it, activating solution is filtered, and can store for this filtered fluid;
One sealed in unit is connected with the filtration accumulator tank, and filtered fluid is encapsulated.
2. device as claimed in claim 1 is characterized in that, material is ore, marine alga, glossy ganoderma, dandelion or coix seed.
3. the method for an analytical extraction trace element is characterized in that, this method includes:
Obtain a water source;
With its deionization, form the pure water of deionization;
This pure water heated into 25-50 ℃ the hot water that adds;
To add hot water admixture material and become mixed liquor;
This mixed liquor is passed to ozone and hyperbaric oxygen become the extract that carries trace element;
This extract is activated into activated water with ozone;
After this activated water contacted and pass to ozone and hyperbaric oxygen with material once more, activated with ozone again, repeated this step;
This activated water is filtered into cleaner liquid;
Cleaner liquid is bottled.
4. method as claimed in claim 3 is characterized in that, material is ore, marine alga, glossy ganoderma, dandelion or coix seed.
5. method as claimed in claim 3 is characterized in that, adding hot water and material mixing ratio is 2: 3.
6. method as claimed in claim 3 is characterized in that, activated water is contacted and passes to ozone and hyperbaric oxygen with material once more after, activated with ozone again, repeated this step minimum five hours.
CNB2004100481436A 2004-06-16 2004-06-16 Trace element activity analysis and extraction method and device Expired - Fee Related CN100409917C (en)

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Citations (5)

* Cited by examiner, † Cited by third party
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CN1243760A (en) * 1998-07-30 2000-02-09 吕胜一 Multifunctional Rapid Extraction and Fusion Device
US6051421A (en) * 1996-09-09 2000-04-18 Air Liquide America Corporation Continuous processing apparatus and method for cleaning articles with liquified compressed gaseous solvents
TW497980B (en) * 2001-01-09 2002-08-11 Jle Engineering Corp Method for extracting useful material from waste acid liquid and device therefor
WO2002074886A1 (en) * 2001-03-20 2002-09-26 Naturol Limited Refining of crude extracts and mixtures
TW574152B (en) * 2002-08-16 2004-02-01 Ind Tech Res Inst Chemistry mechanism of high concentration ozone/reaction liquid generation system and method

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6051421A (en) * 1996-09-09 2000-04-18 Air Liquide America Corporation Continuous processing apparatus and method for cleaning articles with liquified compressed gaseous solvents
CN1243760A (en) * 1998-07-30 2000-02-09 吕胜一 Multifunctional Rapid Extraction and Fusion Device
TW497980B (en) * 2001-01-09 2002-08-11 Jle Engineering Corp Method for extracting useful material from waste acid liquid and device therefor
WO2002074886A1 (en) * 2001-03-20 2002-09-26 Naturol Limited Refining of crude extracts and mixtures
TW574152B (en) * 2002-08-16 2004-02-01 Ind Tech Res Inst Chemistry mechanism of high concentration ozone/reaction liquid generation system and method

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