CH280062A - Process for the preparation of a nitro dye. - Google Patents
Process for the preparation of a nitro dye.Info
- Publication number
- CH280062A CH280062A CH280062DA CH280062A CH 280062 A CH280062 A CH 280062A CH 280062D A CH280062D A CH 280062DA CH 280062 A CH280062 A CH 280062A
- Authority
- CH
- Switzerland
- Prior art keywords
- nitro dye
- preparation
- dinitrobenzophenone
- dibromo
- amino
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B51/00—Nitro or nitroso dyes
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Coloring (AREA)
Description
<B>Zusatzpatent</B> zum Hauptpatent Nr.274851. Verfahren zur Herstellung eines Nitrofarbstoffes. Gegenstand des vorliegenden Zusatzpaten tes ist ein Verfahren zur Herstellung eines Nitrofarbstoffes, welches dadurch gekenn zeichnet ist, dass man 4,4'-Dibrom-3,3'-dinitro- benzophenon mit 1.-Amino-3,4-dimethj>lbenzol- 6-sulfonsäure kondensiert.
<I>Beispiel:</I> 50 Gewichtsteile 4,4'-Dibrom-3,3'-dinitro- benzophenon und 1.20 Gewichtsteile des Am moniumsalzes der 1-Amino-3,4-dimethylbenzol.- 6-sulfonsäure werden bei Gegenwart von 30 Gewichtsteilen Natriumacetat in 500 Gewichts teilen Wasser suspendiert; die Mischung wird 5 Stunden bei 130 im Autoklaven gerührt. Nach Beendigung der Reaktion wird die Lö sung geklärt und der gebildete Farbstoff aus gesalzen.
Das so erhaltene Produkt stellt ein orange farbenes Pulver dar, das sieh in Wasser mit gelber Farbe löst und Wolle aueh aus neutra lem Bade in gelben Tönen von guten Echt heitseigenschaften, insbesondere guter Licht- eehtheit, färbt.
<B> Additional patent </B> to main patent number 274851. Process for the preparation of a nitro dye. The subject of the present additional patent is a process for the production of a nitro dye, which is characterized in that 4,4'-dibromo-3,3'-dinitrobenzophenone with 1.-amino-3,4-dimethj> lbenzene- 6-sulfonic acid condensed.
<I> Example: </I> 50 parts by weight of 4,4'-dibromo-3,3'-dinitrobenzophenone and 1.20 parts by weight of the ammonium salt of 1-amino-3,4-dimethylbenzene-6-sulfonic acid are present in the presence suspended by 30 parts by weight of sodium acetate in 500 parts by weight of water; the mixture is stirred in the autoclave at 130 for 5 hours. After the reaction has ended, the solution is clarified and the dye formed is salted out.
The product thus obtained is an orange-colored powder which dissolves in water with a yellow color and also dyes wool from neutral bath in yellow shades of good fastness properties, in particular good lightfastness.
Claims (1)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE280062X | 1948-12-31 | ||
CH274851T | 1949-05-09 |
Publications (1)
Publication Number | Publication Date |
---|---|
CH280062A true CH280062A (en) | 1951-12-31 |
Family
ID=25731583
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CH280062D CH280062A (en) | 1948-12-31 | 1949-05-09 | Process for the preparation of a nitro dye. |
Country Status (1)
Country | Link |
---|---|
CH (1) | CH280062A (en) |
-
1949
- 1949-05-09 CH CH280062D patent/CH280062A/en unknown
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