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CH217980A - Process for the preparation of a new anthraquinone dye. - Google Patents

Process for the preparation of a new anthraquinone dye.

Info

Publication number
CH217980A
CH217980A CH217980DA CH217980A CH 217980 A CH217980 A CH 217980A CH 217980D A CH217980D A CH 217980DA CH 217980 A CH217980 A CH 217980A
Authority
CH
Switzerland
Prior art keywords
preparation
anthraquinone dye
new anthraquinone
dye
amino
Prior art date
Application number
Other languages
German (de)
Inventor
Sandoz A G
Original Assignee
Sandoz Ag
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Sandoz Ag filed Critical Sandoz Ag
Publication of CH217980A publication Critical patent/CH217980A/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B1/00—Dyes with anthracene nucleus not condensed with any other ring
    • C09B1/16—Amino-anthraquinones
    • C09B1/20—Preparation from starting materials already containing the anthracene nucleus
    • C09B1/26—Dyes with amino groups substituted by hydrocarbon radicals
    • C09B1/32—Dyes with amino groups substituted by hydrocarbon radicals substituted by aryl groups

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Description

  

  Verfahren zur Darstellung eines neuen     Anthrachinonfarbstoffes.       Das vorliegende Patent betrifft ein Ver  fahren zur     Darstellung    eines neuen     Anthra-          chinonfarbstoffes    und ist dadurch gekenn  zeichnet, dass man     1-amino-4-bromanthra-          5        chinon-2-sulfosaures    Natrium mit     3-Amino-6-          chlor-acetanilid    kondensiert.  



  Der neue     Farbstoff    besitzt die Formel  
EMI0001.0011     
    3 Er löst sich mit blauer Farbe in Wasser und  zieht auf Wolle in     grünstichig    blauen Tönen  von guten Echtheitseigenschaften. Er besitzt  ein     gutes        Egalisierungsvermögen.       <I>Beispiel:

  </I>    20     Gewichtsteile        1-amino-4-bromanthTa-          chinon-2-sulfosaures        Natrium    werden 150     Ge-          wichtsteilen    Wasser und 50     Gewichtsteilen     Alkohol mit 15     Gewichtsteilen        3-Amino-6-          chlor-acetanilid,    14 Gewichtsteilen     Natrium-          bicarbonat    und 0,8 Gewichtsteilen Kupfer  zirka 16     Stunden    bei 70   gerührt. Nach be  endeter     Kondensation    wird der Alkohol ab  getrieben.

   Der Farbstoff wird     abfiltriert    und  mit verdünnter     Kochsalzlösung    gewaschen  und getrocknet.    Der Farbstoff besitzt die Formel "  
EMI0001.0031     
      Er löst sich in     Wasser    mit blauer Farbe und  zieht auf Wolle     in        grünstichig    blauen Tönen  von     guten        Echtheitseigenschaften.    Er besitzt  ein gutes     Egalisiervermögen.  



  Process for the preparation of a new anthraquinone dye. The present patent relates to a process for the preparation of a new anthraquinone dye and is characterized in that 1-amino-4-bromoanthra-5-quinone-2-sulfonic acid sodium is condensed with 3-amino-6-chloroacetanilide.



  The new dye has the formula
EMI0001.0011
    3 It dissolves in water with a blue color and pulls onto wool in greenish blue tones with good fastness properties. He has a good ability to equalize. <I> example:

  </I> 20 parts by weight of 1-amino-4-bromoanthtaquinone-2-sulfonic acid sodium are 150 parts by weight of water and 50 parts by weight of alcohol with 15 parts by weight of 3-amino-6-chloroacetanilide, 14 parts by weight of sodium bicarbonate and 0 , 8 parts by weight of copper stirred at 70 for about 16 hours. After the condensation has ended, the alcohol is driven off.

   The dye is filtered off, washed with dilute sodium chloride solution and dried. The dye has the formula "
EMI0001.0031
      It dissolves in water with a blue color and pulls onto wool in greenish blue tones with good fastness properties. He has a good leveling ability.

Claims (1)

PATENTANSPRUCH: Verfahren zur Darstellung eines neuen Anthrachinonfarbstoffes, dadurch gekenn zeichnet, dass man 1-amino-4-bromanthra- chinon-2-sulfosaures Natrium mit 3-Amino- 6-chloracetanilid kondensiert. PATENT CLAIM: Process for the preparation of a new anthraquinone dye, characterized in that 1-amino-4-bromoanthraquinone-2-sulfonic acid sodium is condensed with 3-amino-6-chloroacetanilide. Der Farbstoff besitzt die Formel EMI0002.0014 Er löst sich mit blauer Farbe in Wasser und zieht auf Wolle in grünstichig blauen Tönen von guten Echtheitseigenschaften. Er besitzt ein gutes Egalisierungsvermögen. The dye has the formula EMI0002.0014 It dissolves in water with a blue color and pulls onto wool in greenish blue tones with good fastness properties. He has a good ability to equalize.
CH217980D 1939-12-09 1939-12-09 Process for the preparation of a new anthraquinone dye. CH217980A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
CH214909T 1939-12-09
CH217980T 1939-12-09

Publications (1)

Publication Number Publication Date
CH217980A true CH217980A (en) 1941-11-15

Family

ID=25725660

Family Applications (1)

Application Number Title Priority Date Filing Date
CH217980D CH217980A (en) 1939-12-09 1939-12-09 Process for the preparation of a new anthraquinone dye.

Country Status (1)

Country Link
CH (1) CH217980A (en)

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