CH208289A - Process for the preparation of a wetting agent. - Google Patents
Process for the preparation of a wetting agent.Info
- Publication number
- CH208289A CH208289A CH208289DA CH208289A CH 208289 A CH208289 A CH 208289A CH 208289D A CH208289D A CH 208289DA CH 208289 A CH208289 A CH 208289A
- Authority
- CH
- Switzerland
- Prior art keywords
- wetting agent
- preparation
- wetting effect
- ammonium base
- trimethylamine
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims description 4
- 239000000080 wetting agent Substances 0.000 title description 3
- 238000002360 preparation method Methods 0.000 title description 2
- GETQZCLCWQTVFV-UHFFFAOYSA-N trimethylamine Chemical compound CN(C)C GETQZCLCWQTVFV-UHFFFAOYSA-N 0.000 claims description 6
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 claims description 4
- 150000003839 salts Chemical class 0.000 claims description 4
- 238000009736 wetting Methods 0.000 claims description 4
- ZVHAANQOQZVVFD-UHFFFAOYSA-N 5-methylhexan-1-ol Chemical compound CC(C)CCCCO ZVHAANQOQZVVFD-UHFFFAOYSA-N 0.000 claims description 3
- 229940106681 chloroacetic acid Drugs 0.000 claims description 3
- -1 chloroacetic acid ester Chemical class 0.000 claims description 3
- HGWAKQDTQVDVRP-OKULMJQMSA-N butyl (z,12r)-12-hydroxyoctadec-9-enoate Chemical compound CCCCCC[C@@H](O)C\C=C/CCCCCCCC(=O)OCCCC HGWAKQDTQVDVRP-OKULMJQMSA-N 0.000 claims description 2
- 239000007788 liquid Substances 0.000 claims description 2
- 238000006277 sulfonation reaction Methods 0.000 claims description 2
- 235000002639 sodium chloride Nutrition 0.000 description 4
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 125000001309 chloro group Chemical group Cl* 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 125000004108 n-butyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 description 1
- 239000011780 sodium chloride Substances 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
- D06M13/46—Compounds containing quaternary nitrogen atoms
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Emulsifying, Dispersing, Foam-Producing Or Wetting Agents (AREA)
- Detergent Compositions (AREA)
Description
Verfahren zur Herstellung eines Netzmittels. Vorliegendes Patent bezieht sich auf ein Verfahren zur Herstellung eines Netzmittels, dadurch gekennzeichnet, dass man das Sul- fonierungsprodukt des Rizirrolsäure-n-butyl- esters mit einer Ammoniumbase umsetzt, welche durch Vereinigung des Chloressig- säureesters des Isoheptylalkohols der Formel
EMI0001.0009
mit Trimethylamin gewonnen wird.
Das so erhaltene Salz stellt eine dick flüssige, gelbe Masse von hervorragender Netzwirkung dar, die die schon an sich sehr gute Netzwirkung der ersten Komponente noch erheblich übertrifft.
<I>Beispiel:</I> 100 Teile einer Lösung von sulfiertem Rizinolsäure-n-butylester von 40 % Fettge- halt werden mit 10 Teilen einer Ammonium- Base gemischt, welche durch Vereinigung des Chloressigsäureesters des Isoheptylalkohols der Formel
EMI0001.0023
mit Trimethylamin gewonnen wurde. Durch Zusatz von Kochsalz kann das Salz der Ammoniumbase ausgeschieden und gegebenenfalls durch Aufnehmen in Chloro form und Abdampfen desselben salz- und wasserfrei erhalten werden.
Process for the preparation of a wetting agent. The present patent relates to a process for the production of a wetting agent, characterized in that the sulfonation product of rizirrolic acid n-butyl ester is reacted with an ammonium base which is obtained by combining the chloroacetic acid ester of isoheptyl alcohol of the formula
EMI0001.0009
is obtained with trimethylamine.
The salt thus obtained is a thick, liquid, yellow mass with an excellent wetting effect, which considerably exceeds the wetting effect of the first component, which is already very good.
<I> Example: </I> 100 parts of a solution of sulfated ricinoleic acid n-butyl ester with 40% fat content are mixed with 10 parts of an ammonium base, which is obtained by combining the chloroacetic acid ester of isoheptyl alcohol of the formula
EMI0001.0023
was obtained with trimethylamine. By adding common salt, the salt of the ammonium base can be excreted and optionally obtained free of salt and anhydrous by taking it up in chlorine form and evaporating it.
Claims (1)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DEI58385A DE730520C (en) | 1937-06-24 | 1937-06-24 | Process for the neutralization of sulfonic acids with organic ammonium bases |
| CH205892T | 1938-06-20 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CH208289A true CH208289A (en) | 1940-01-15 |
Family
ID=89835276
Family Applications (3)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CH208288D CH208288A (en) | 1937-06-24 | 1938-06-20 | Process for the preparation of a wetting agent. |
| CH208289D CH208289A (en) | 1937-06-24 | 1938-06-20 | Process for the preparation of a wetting agent. |
| CH208290D CH208290A (en) | 1937-06-24 | 1938-06-20 | Process for the preparation of a wetting agent. |
Family Applications Before (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CH208288D CH208288A (en) | 1937-06-24 | 1938-06-20 | Process for the preparation of a wetting agent. |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CH208290D CH208290A (en) | 1937-06-24 | 1938-06-20 | Process for the preparation of a wetting agent. |
Country Status (1)
| Country | Link |
|---|---|
| CH (3) | CH208288A (en) |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2781391A (en) * | 1956-03-06 | 1957-02-12 | Hans S Mannheimer | Detergent sulphonic acid and sulphate salts of certain amphoteric detergents |
| US2781388A (en) * | 1956-03-06 | 1957-02-12 | Hans S Mannheimer | Detergent sulphonic acid and sulphate salts of certain amphoteric detergents |
| US2781390A (en) * | 1956-05-24 | 1957-02-12 | Hans S Mannheimer | Detergent sulphonic acid and sulphate salts of certain amphoteric detergents |
| US2781392A (en) * | 1956-05-24 | 1957-02-12 | Hans S Mannheimer | Detergent sulphonic acid and sulphate salts of certain amphoteric detergents |
| US2781389A (en) * | 1956-06-13 | 1957-02-12 | Hans S Mannheimer | Detergent sulphonic acid and sulphate salts of certain amphoteric detergents |
-
1938
- 1938-06-20 CH CH208288D patent/CH208288A/en unknown
- 1938-06-20 CH CH208289D patent/CH208289A/en unknown
- 1938-06-20 CH CH208290D patent/CH208290A/en unknown
Also Published As
| Publication number | Publication date |
|---|---|
| CH208288A (en) | 1940-01-15 |
| CH208290A (en) | 1940-01-15 |
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