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CH204449A - Process for the production of a new azo dye. - Google Patents

Process for the production of a new azo dye.

Info

Publication number
CH204449A
CH204449A CH204449DA CH204449A CH 204449 A CH204449 A CH 204449A CH 204449D A CH204449D A CH 204449DA CH 204449 A CH204449 A CH 204449A
Authority
CH
Switzerland
Prior art keywords
mol
dye
azo dye
new azo
diazotized
Prior art date
Application number
Other languages
German (de)
Inventor
Gesellschaft Fuer Chemis Basel
Original Assignee
Chem Ind Basel
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Chem Ind Basel filed Critical Chem Ind Basel
Publication of CH204449A publication Critical patent/CH204449A/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B29/00—Monoazo dyes prepared by diazotising and coupling
    • C09B29/24—Monoazo dyes prepared by diazotising and coupling from coupling components containing both hydroxyl and amino directing groups
    • C09B29/28—Amino naphthols
    • C09B29/30—Amino naphtholsulfonic acid
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B29/00—Monoazo dyes prepared by diazotising and coupling
    • C09B29/34—Monoazo dyes prepared by diazotising and coupling from other coupling components
    • C09B29/36—Monoazo dyes prepared by diazotising and coupling from other coupling components from heterocyclic compounds
    • C09B29/3604—Monoazo dyes prepared by diazotising and coupling from other coupling components from heterocyclic compounds containing only a nitrogen as heteroatom
    • C09B29/3647—Monoazo dyes prepared by diazotising and coupling from other coupling components from heterocyclic compounds containing only a nitrogen as heteroatom containing a five-membered ring with two nitrogen atoms as heteroatoms
    • C09B29/3652—Monoazo dyes prepared by diazotising and coupling from other coupling components from heterocyclic compounds containing only a nitrogen as heteroatom containing a five-membered ring with two nitrogen atoms as heteroatoms containing a 1,2-diazoles or hydrogenated 1,2-diazoles
    • C09B29/366—Monoazo dyes prepared by diazotising and coupling from other coupling components from heterocyclic compounds containing only a nitrogen as heteroatom containing a five-membered ring with two nitrogen atoms as heteroatoms containing a 1,2-diazoles or hydrogenated 1,2-diazoles containing hydroxy-1,2-diazoles, e.g. pyrazolone
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B31/00—Disazo and polyazo dyes of the type A->B->C, A->B->C->D, or the like, prepared by diazotising and coupling
    • C09B31/02—Disazo dyes
    • C09B31/08—Disazo dyes from a coupling component "C" containing directive hydroxyl and amino groups

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Coloring (AREA)

Description

  

  Zusatzpatent zum Hauptpatent     Nr.   <B>200672.</B>    Verfahren zur Herstellung eines neuen     Azofarbstoffes.       Es wurde gefunden,     dass    man einen neuen       Azofarbstoff,    erhält, wenn man<B>1</B>     Mol   <B>2-(3-</B>       [4"-Aminol-betizoylamino-5'-amino)-berizoyl-          amino-5-oxyiiaphthalin-7-sulfonsäuremitIMol     des     diazotierten        Monoazofarbstoffes,

      erhalten  durch Kuppeln von<B>1</B>     Mol        diazotierter        2-Amino-          iiaphthalin-4.        8-disulfonsäure    mit<B>1</B>     Mol        1-          Aminonaphthalin    und     Weiterdiazotieren,    ver  einigt.

   Der so erhaltene Farbstoff bildet ein  graues Pulver, das sich in Wasser mit     violett-          blauer    Farbe löst und Baumwolle in violetten  Tönen färbt, die durch     Weiterdiazotieren    auf  der Faser und Entwickeln mit     1-Phenyl-3-          methyl-5-pyrazolon    stumpfgrün werden.    <I>Beispiel:</I>         303        Teilo        2-Aminonaphthalin-4.8-disulfon-          säure    werden in     ühlicher    Weise     diazotiert     und mit 143 Teilen     1-Aminonaphthalin    ge  kuppelt.

   Daraus wird nach gewohnter Art die       Diazoverbindung    hergestellt und gereinigt.  Die     Diazosuspension    wird in eine kalte Lö  sung aus etwa 400 Teilen 2-(3'-[4"-Amino]  benzoylamino-5'-amino)-benzoylamino-5-oxy-         naphthaliii-7-sulfonsäure,   <B>300</B> Teilen     Natrium-          earbonat    und<B>5000</B> Teilen Wasser eingerührt.  Nach beendeter Kupplung wird der Farbstoff,  gegebenenfalls nach     Aussalzen,        abfiltriert    und  getrocknet.



  Additional patent to main patent no. <B> 200672. </B> Process for the production of a new azo dye. It has been found that a new azo dye is obtained if <B> 1 </B> mol <B> 2- (3- </B> [4 "-aminol-betizoylamino-5'-amino) -berizoyl] - amino-5-oxyiiaphthalene-7-sulfonic acid with 1 mol of the diazotized monoazo dye,

      obtained by coupling <B> 1 </B> mol of diazotized 2-amino-iiaphthalene-4. 8-disulfonic acid with <B> 1 </B> mol 1-aminonaphthalene and further diazotization, united.

   The dye thus obtained forms a gray powder which dissolves in water with a violet-blue color and dyes cotton in violet tones which become dull green when the fibers are further diazotized and developed with 1-phenyl-3-methyl-5-pyrazolone. <I> Example: </I> 303 parts of 2-aminonaphthalene-4.8-disulfonic acid are diazotized in the usual way and coupled with 143 parts of 1-aminonaphthalene.

   From this the diazo compound is produced and cleaned in the usual way. The diazo suspension is dissolved in a cold solution of about 400 parts of 2- (3 '- [4 "-amino] benzoylamino-5'-amino) -benzoylamino-5-oxynaphthaliii-7-sulfonic acid, <B> 300 </ B> parts of sodium carbonate and 5000 parts of water are stirred in. After coupling has ended, the dyestuff, optionally after salting out, is filtered off and dried.

Claims (1)

PATENTANSPRUCH. Verfahren zur Herstellung ei<B>,</B> nes neuen Azofarbstoffes, dadurch gekennzeichnet, dass man<B>1</B> Mol 2-(3'-[4"-Amiiio]-benzoylamino-5' amino)-benzoylamino-5-oxynaphtbalin-7-stil- fonsäure mit<B>1</B> Mol des diazotierten Monoazo- farbstoffes, PATENT CLAIM. Process for the preparation of a new azo dye, characterized in that <B> 1 </B> mol of 2- (3 '- [4 "-Amiiio] -benzoylamino-5' amino) - benzoylamino-5-oxynaphthbalin-7-nitric acid with <B> 1 </B> mol of the diazotized monoazo dye, erhalten durch Kuppeln von<B>1</B> Mol diazotierter 2 -Aminonaphthaliii-4. 8-disulfon- säure mit<B>1</B> Mol 1-An-iinonaphthalin und Weiterdiazotieren, vereinigt. Der so erhaltene Farbstoff bildet ein graues Pulver, das sich in Wasser mit violettblauer Farbe löst und Baumwolle in violetten Tönen färbt, die durch Weiterdiazotieren auf der Faser und Ent wickeln mit 1-Phenyl-3-methyl-5-pyrazolon stumpfgrün werden. obtained by coupling <B> 1 </B> moles of diazotized 2-aminonaphthalene-4. 8-disulfonic acid with <B> 1 </B> mol 1-aninonaphthalene and further diazotization, combined. The dye thus obtained forms a gray powder that dissolves in water with a violet-blue color and dyes cotton in violet tones that are dull green by further diazotizing on the fiber and developing with 1-phenyl-3-methyl-5-pyrazolone.
CH204449D 1937-02-10 1937-02-10 Process for the production of a new azo dye. CH204449A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
CH204449T 1937-02-10
CH200672T 1938-10-31

Publications (1)

Publication Number Publication Date
CH204449A true CH204449A (en) 1939-04-30

Family

ID=25723553

Family Applications (1)

Application Number Title Priority Date Filing Date
CH204449D CH204449A (en) 1937-02-10 1937-02-10 Process for the production of a new azo dye.

Country Status (1)

Country Link
CH (1) CH204449A (en)

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