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CH200526A - Process for the preparation of an acidic wool azo dye. - Google Patents

Process for the preparation of an acidic wool azo dye.

Info

Publication number
CH200526A
CH200526A CH200526DA CH200526A CH 200526 A CH200526 A CH 200526A CH 200526D A CH200526D A CH 200526DA CH 200526 A CH200526 A CH 200526A
Authority
CH
Switzerland
Prior art keywords
preparation
azo dye
wool
acidic
acidic wool
Prior art date
Application number
Other languages
German (de)
Inventor
Aktiengesellsc Farbenindustrie
Original Assignee
Ig Farbenindustrie Ag
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ig Farbenindustrie Ag filed Critical Ig Farbenindustrie Ag
Publication of CH200526A publication Critical patent/CH200526A/en

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09BORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B29/00Monoazo dyes prepared by diazotising and coupling
    • C09B29/24Monoazo dyes prepared by diazotising and coupling from coupling components containing both hydroxyl and amino directing groups
    • C09B29/28Amino naphthols
    • C09B29/30Amino naphtholsulfonic acid
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09BORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B29/00Monoazo dyes prepared by diazotising and coupling
    • C09B29/34Monoazo dyes prepared by diazotising and coupling from other coupling components
    • C09B29/36Monoazo dyes prepared by diazotising and coupling from other coupling components from heterocyclic compounds
    • C09B29/3604Monoazo dyes prepared by diazotising and coupling from other coupling components from heterocyclic compounds containing only a nitrogen as heteroatom
    • C09B29/3647Monoazo dyes prepared by diazotising and coupling from other coupling components from heterocyclic compounds containing only a nitrogen as heteroatom containing a five-membered ring with two nitrogen atoms as heteroatoms
    • C09B29/3652Monoazo dyes prepared by diazotising and coupling from other coupling components from heterocyclic compounds containing only a nitrogen as heteroatom containing a five-membered ring with two nitrogen atoms as heteroatoms containing a 1,2-diazoles or hydrogenated 1,2-diazoles
    • C09B29/366Monoazo dyes prepared by diazotising and coupling from other coupling components from heterocyclic compounds containing only a nitrogen as heteroatom containing a five-membered ring with two nitrogen atoms as heteroatoms containing a 1,2-diazoles or hydrogenated 1,2-diazoles containing hydroxy-1,2-diazoles, e.g. pyrazolone

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Coloring (AREA)

Description

  

  Verfahren zur Herstellung eines sauren     Wollazofarbstoffes.            Vorliegendes    Patent bezieht sich auf ein  Verfahren zur     Herstellung        eines    sauren       Wollazofarbstoffes,    dadurch     gekennzeichnet,          dass        man,diazotiertes        1-(N-Acetyl-sec.-butyl-          amino)-4-aminobenzol        in    essigsaurem     Medium     mit     1-Benzoylamino-5-naphthol-7=s.ulfosäume     kuppelt.  



  Der so erhaltene Farbstoff     bildet    nach  dem Trocknen ein ziegelrotes, wasserlösliches  Pulver und färbt Wolle und Seide in leb  haften     gelbstichigroten    Tönen von sehr       gutem        Egalisiervermögen    und     guten    Echt  heitseigenschaften.  



  <I>Beispiel:</I>  20,6     Teile        1-(N-Aoetyl-sec.-buty1,amino)-          4-aminobenzol    werden     in.    der     üblichen    Weise       ,diazotiert.    Die erhaltene     Diazolösung    lässt  man in eine mit     überschüssigem    Natrium  acetat versetzte Lösung von<B>36,</B> Teilen         1-Benzoylamino-5-naphthol-7-sulfonsäure    ein  laufen. Nach beendeter Kupplung     wird    der  Farbstoff abgeschieden und     ,getrocknet.  



  Process for the preparation of an acidic wool azo dye. The present patent relates to a process for the preparation of an acidic wool azo dye, characterized in that diazotized 1- (N-acetyl-sec.-butyl-amino) -4-aminobenzene in acetic acid medium with 1-benzoylamino-5-naphthol- 7 = s.ulfo seams domes.



  The dye thus obtained forms a brick-red, water-soluble powder after drying and dyes wool and silk in lively yellow-tinged red shades with very good leveling properties and good fastness properties.



  <I> Example: </I> 20.6 parts of 1- (N-aoetyl-sec.-buty1, amino) -4-aminobenzene are diazotized in the usual way. The diazo solution obtained is poured into a solution of 36 parts of 1-benzoylamino-5-naphthol-7-sulfonic acid to which excess sodium acetate has been added. After the coupling has ended, the dye is deposited and dried.

 

Claims (1)

PATENTANSPRUCH: Verfahren zur Herstellung eines sauren Wollazofarbstoffes,dadurch gekennzeichnet, daB man diazotiertes 1-N-Acetyl-sec.-butyl- amino)-4-aminobenzol in essigsaurem Me dium mit 1-Ben:zoylamino-5-naphthod-7-sulfo- säure kuppelt. Claim: Process for the preparation of an acid wool azo dye, characterized in that diazotized 1-N-acetyl-sec.-butyl-amino) -4-aminobenzene in acetic acid medium with 1-ben: zoylamino-5-naphthod-7-sulfo - acid coupling. Der so erhaltene Farbstoff bildet nach dem Trocknen ein ziegelrotes, wasserlösliehes Pulver und färbt Wolle und Seide in leb haften gelbstichigroten Tönen von sehr gutem EgalisiervermÖgen und guten Echt- heitseigenschaften. After drying, the dyestuff thus obtained forms a brick-red, water-soluble powder and dyes wool and silk in lively yellow-tinged red shades with very good leveling power and good fastness properties.
CH200526D 1935-10-02 1936-09-17 Process for the preparation of an acidic wool azo dye. CH200526A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE200526X 1935-10-02
CH195654T 1936-09-17

Publications (1)

Publication Number Publication Date
CH200526A true CH200526A (en) 1938-10-15

Family

ID=25722776

Family Applications (1)

Application Number Title Priority Date Filing Date
CH200526D CH200526A (en) 1935-10-02 1936-09-17 Process for the preparation of an acidic wool azo dye.

Country Status (1)

Country Link
CH (1) CH200526A (en)

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