CH185042A - Process for the preparation of an azo dye. - Google Patents
Process for the preparation of an azo dye.Info
- Publication number
- CH185042A CH185042A CH185042DA CH185042A CH 185042 A CH185042 A CH 185042A CH 185042D A CH185042D A CH 185042DA CH 185042 A CH185042 A CH 185042A
- Authority
- CH
- Switzerland
- Prior art keywords
- preparation
- azo dye
- dye
- naphthoquinoline
- dinitro
- Prior art date
Links
Landscapes
- Coloring (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Description
Verfahren zur Darstellung eines Azofarbstoffes. Nach dein im Hauptpatent beschriebenen Verfahren erhält man einen blauen Acetat seidenfarbstoff, wenn man dianotiertes 6-Broin- 2.4-dinitro-l-aminobenzol mit 1-Aminonaph- thalin kuppelt.
Wie nun weiter gefunden wurde, erhält man einen Farbstoff mit ganz ähnlichen Eigen schaften, wenn man 6-Brom-2.4-diniti,o-1- aminobenzol dianotiert und mit Tetrahydro- 3-oxy-a-naphthochinolin der Formel
EMI0001.0010
kuppelt. <I>Beispiel;</I> 26,2 Teile 6-Brom-2.4-dinitro-l-amino- beiizol werden in der üblichen Weise diano tiert und die mineralsäurehaltige Diazolösung wird in eine kalte Lösung von 22 Teilen Tetrahydro-3-oxy-a-naphthochinolin einlaufen gelassen. Man stumpft mit so viel Natrium acetat ab, bis die Kupplung beendet ist.
Der erhaltene Farbstoff färbt Acetatseide klar grünblau.
Process for the preparation of an azo dye. According to the process described in the main patent, a blue acetate silk dye is obtained when dianotated 6-broin-2,4-dinitro-1-aminobenzene is coupled with 1-aminonaphthalene.
As has now been found further, a dye with very similar properties is obtained if 6-bromo-2,4-diniti, o-1-aminobenzene is dianotized and tetrahydro-3-oxy-a-naphthoquinoline of the formula
EMI0001.0010
clutch. <I> Example; </I> 26.2 parts of 6-bromo-2,4-dinitro-1-amino-beiizol are diano-zol in the usual way and the mineral acid-containing diazo solution is in a cold solution of 22 parts of tetrahydro-3-oxy -a-naphthoquinoline run in. It is blunted with enough sodium acetate until the coupling is complete.
The dye obtained gives acetate silk a clear green-blue color.
Claims (1)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CH168144T | 1933-04-27 | ||
DE185042X | 1933-12-19 |
Publications (1)
Publication Number | Publication Date |
---|---|
CH185042A true CH185042A (en) | 1936-06-30 |
Family
ID=25718532
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CH185042D CH185042A (en) | 1933-04-27 | 1934-11-21 | Process for the preparation of an azo dye. |
Country Status (1)
Country | Link |
---|---|
CH (1) | CH185042A (en) |
-
1934
- 1934-11-21 CH CH185042D patent/CH185042A/en unknown
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