CA2480327A1 - Liquid dish cleaning compositions having improved preservative system - Google Patents
Liquid dish cleaning compositions having improved preservative system Download PDFInfo
- Publication number
- CA2480327A1 CA2480327A1 CA002480327A CA2480327A CA2480327A1 CA 2480327 A1 CA2480327 A1 CA 2480327A1 CA 002480327 A CA002480327 A CA 002480327A CA 2480327 A CA2480327 A CA 2480327A CA 2480327 A1 CA2480327 A1 CA 2480327A1
- Authority
- CA
- Canada
- Prior art keywords
- composition
- preservative
- group
- surfactant
- disuccinate
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000000203 mixture Substances 0.000 title claims abstract 20
- 239000003755 preservative agent Substances 0.000 title claims abstract 12
- 230000002335 preservative effect Effects 0.000 title claims abstract 12
- 238000004140 cleaning Methods 0.000 title claims abstract 4
- 239000007788 liquid Substances 0.000 title claims abstract 4
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 claims abstract 3
- 239000002202 Polyethylene glycol Substances 0.000 claims abstract 3
- 239000011777 magnesium Substances 0.000 claims abstract 3
- 229910052749 magnesium Inorganic materials 0.000 claims abstract 3
- 229920001223 polyethylene glycol Polymers 0.000 claims abstract 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract 3
- 239000003945 anionic surfactant Substances 0.000 claims abstract 2
- 239000004094 surface-active agent Substances 0.000 claims 5
- 239000012188 paraffin wax Substances 0.000 claims 4
- BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 claims 4
- SOBHUZYZLFQYFK-UHFFFAOYSA-K trisodium;hydroxy-[[phosphonatomethyl(phosphonomethyl)amino]methyl]phosphinate Chemical compound [Na+].[Na+].[Na+].OP(O)(=O)CN(CP(O)([O-])=O)CP([O-])([O-])=O SOBHUZYZLFQYFK-UHFFFAOYSA-K 0.000 claims 4
- LVDKZNITIUWNER-UHFFFAOYSA-N Bronopol Chemical group OCC(Br)(CO)[N+]([O-])=O LVDKZNITIUWNER-UHFFFAOYSA-N 0.000 claims 3
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 claims 3
- 239000005977 Ethylene Substances 0.000 claims 3
- WSDISUOETYTPRL-UHFFFAOYSA-N dmdm hydantoin Chemical compound CC1(C)N(CO)C(=O)N(CO)C1=O WSDISUOETYTPRL-UHFFFAOYSA-N 0.000 claims 3
- JLHMJWHSBYZWJJ-UHFFFAOYSA-N 1,2-thiazole 1-oxide Chemical compound O=S1C=CC=N1 JLHMJWHSBYZWJJ-UHFFFAOYSA-N 0.000 claims 2
- 150000004996 alkyl benzenes Chemical class 0.000 claims 2
- -1 alkyl ether sulfate Chemical class 0.000 claims 2
- 150000002484 inorganic compounds Chemical class 0.000 claims 2
- 229910010272 inorganic material Inorganic materials 0.000 claims 2
- 159000000000 sodium salts Chemical class 0.000 claims 2
- 150000003871 sulfonates Chemical class 0.000 claims 2
- 229940080258 tetrasodium iminodisuccinate Drugs 0.000 claims 2
- GYBINGQBXROMRS-UHFFFAOYSA-J tetrasodium;2-(1,2-dicarboxylatoethylamino)butanedioate Chemical compound [Na+].[Na+].[Na+].[Na+].[O-]C(=O)CC(C([O-])=O)NC(C([O-])=O)CC([O-])=O GYBINGQBXROMRS-UHFFFAOYSA-J 0.000 claims 2
- 125000000129 anionic group Chemical group 0.000 claims 1
- 239000002736 nonionic surfactant Substances 0.000 claims 1
- 229910017053 inorganic salt Inorganic materials 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/04—Water-soluble compounds
- C11D3/046—Salts
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
- C11D1/14—Sulfonic acids or sulfuric acid esters; Salts thereof derived from aliphatic hydrocarbons or mono-alcohols
- C11D1/143—Sulfonic acid esters
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
- C11D1/22—Sulfonic acids or sulfuric acid esters; Salts thereof derived from aromatic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/83—Mixtures of non-ionic with anionic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/83—Mixtures of non-ionic with anionic compounds
- C11D1/831—Mixtures of non-ionic with anionic compounds of sulfonates with ethers of polyoxyalkylenes without phosphates
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/26—Organic compounds containing nitrogen
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/26—Organic compounds containing nitrogen
- C11D3/32—Amides; Substituted amides
- C11D3/323—Amides; Substituted amides urea or derivatives thereof
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/26—Organic compounds containing nitrogen
- C11D3/33—Amino carboxylic acids
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/34—Organic compounds containing sulfur
- C11D3/349—Organic compounds containing sulfur additionally containing nitrogen atoms, e.g. nitro, nitroso, amino, imino, nitrilo, nitrile groups containing compounds or their derivatives or thio urea
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/37—Polymers
- C11D3/3703—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- C11D3/3707—Polyethers, e.g. polyalkyleneoxides
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/48—Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/72—Ethers of polyoxyalkylene glycols
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Life Sciences & Earth Sciences (AREA)
- Inorganic Chemistry (AREA)
- Detergent Compositions (AREA)
- Washing And Drying Of Tableware (AREA)
- Cleaning And De-Greasing Of Metallic Materials By Chemical Methods (AREA)
- Bidet-Like Cleaning Device And Other Flush Toilet Accessories (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
A liquid dish cleaning composition with desirable cleansing properties comprising at least one anionic surfactant, a magnesium containing inorganic salt, an improved preservative system, polyethylene glycol and water.</SDOAB >
Claims (12)
1. A liquid dish cleaning composition which comprises approximately by weight:
(a) 5% to 15% of at least one anionic surfactant selected from the group consisting of linear alkyl benzene sulfonates and paraffin sulfonates and mixtures thereof;
(b) 0.5% to 4% of a magnesium containing inorganic compound;
(c) 0.1 % to 4% of a polyethylene glycol;
(d) 0.0005% to 0.3% of a preservative;
(e) 0.01 % to 1.5% of a preservative potentiator which is selected from the group consisting of an optically pure isomer of trisodium S,S ethylene diamine-N,N~-disuccinate tetra sodium imino disuccinate; and (f) the balance being water.~
(a) 5% to 15% of at least one anionic surfactant selected from the group consisting of linear alkyl benzene sulfonates and paraffin sulfonates and mixtures thereof;
(b) 0.5% to 4% of a magnesium containing inorganic compound;
(c) 0.1 % to 4% of a polyethylene glycol;
(d) 0.0005% to 0.3% of a preservative;
(e) 0.01 % to 1.5% of a preservative potentiator which is selected from the group consisting of an optically pure isomer of trisodium S,S ethylene diamine-N,N~-disuccinate tetra sodium imino disuccinate; and (f) the balance being water.~
2. The composition of Claim 1, wherein at least one said sulfonate surfactant is said paraffin sulfonate.
3. The composition of Claim 2, wherein said preservative is 2-bromo-2-nitropropane-1,3-diol
4. The composition of Claim 2, wherein said preservative is selected from the group consisting of dimethylol dimethyl hydantoin, an isothiazolone mixture and 2-bromo-2-nitropropane-1,3-diol and mixtures thereof.
5. The composition of Claim 4, wherein said preservative potentiator is trisodium S,S ethylene diamine-N,N-disuccinate.
6. The composition of Claim 1 further including a sodium salt of an ethoxylated alkyl ether sulfate surfactant.
7. A liquid dish cleaning composition which comprises approximately by weight:
(a) 15% to 35% of at least one anionic sulfonated surfactant selected from the group consisting of a linear alkyl benzene sulfonates and paraffin sulfonates and mixtures thereof.
(b) 0.5% to 4% of a magnesium containing inorganic compound;
(c) 0.1 % to 10% of at least one ethoxylated nonionic surfactant;
(d) 0.1 % to 4% of a polyethylene glycol;
(e) 0.0005% to 0.3% of a preservative;
(f) 0.01 % to 1.5%, more preferably 0.05% to 1.0% of a preservative potentiator which is selected from the group consisting of an optically pure isomer of trisodium S,S ethylene diamine-N,N~-disuccinate and tetra sodium iminodisuccinate;
and (g) the balance being water.
(a) 15% to 35% of at least one anionic sulfonated surfactant selected from the group consisting of a linear alkyl benzene sulfonates and paraffin sulfonates and mixtures thereof.
(b) 0.5% to 4% of a magnesium containing inorganic compound;
(c) 0.1 % to 10% of at least one ethoxylated nonionic surfactant;
(d) 0.1 % to 4% of a polyethylene glycol;
(e) 0.0005% to 0.3% of a preservative;
(f) 0.01 % to 1.5%, more preferably 0.05% to 1.0% of a preservative potentiator which is selected from the group consisting of an optically pure isomer of trisodium S,S ethylene diamine-N,N~-disuccinate and tetra sodium iminodisuccinate;
and (g) the balance being water.
8. The composition of Claim 7, wherein at least one said sulfonate surfactant is said paraffin sulfonate.
9. The composition of Claim 8, wherein said preservative is a dimethylol dimethyl hydantoin.
10. The composition of Claim 8, wherein said preservative is selected from the group consisting of dimethylol dimethyl hydantoin, an isothiazolone mixture and 2-bromo-2-nitropropane-1,3-diol and mixtures thereof.
11. The composition of Claim 7 further including a sodium salt of an ethoxylated alkyl ether sulfate surfactant.
12. The composition of claim 10, wherein said preservative potentiator is trisodium S,S ethylenediamine- N,N'-disuccinate
Applications Claiming Priority (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US10/108,136 | 2002-03-27 | ||
| US10/108,136 US6465406B1 (en) | 2002-03-27 | 2002-03-27 | Liquid dish cleaning compositions having improved preservative system comprising ethylene diamine-N,N-disuccinate |
| US10/231,927 US6537956B1 (en) | 2002-03-27 | 2002-08-30 | Liquid dish cleaning compositions having improved preservative system |
| US10/231,927 | 2002-08-30 | ||
| PCT/US2003/009038 WO2003083024A1 (en) | 2002-03-27 | 2003-03-26 | Liquid dish cleaning compositions having improved preservative system |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CA2480327A1 true CA2480327A1 (en) | 2003-10-09 |
| CA2480327C CA2480327C (en) | 2011-10-11 |
Family
ID=28677834
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA2480327A Expired - Fee Related CA2480327C (en) | 2002-03-27 | 2003-03-26 | Liquid dish cleaning compositions having improved preservative system |
Country Status (15)
| Country | Link |
|---|---|
| EP (1) | EP1487947B1 (en) |
| AT (1) | ATE327305T1 (en) |
| AU (1) | AU2003222062B2 (en) |
| CA (1) | CA2480327C (en) |
| DE (1) | DE60305463T2 (en) |
| DK (1) | DK1487947T3 (en) |
| EC (1) | ECSP045388A (en) |
| ES (1) | ES2262991T3 (en) |
| IL (1) | IL164305A0 (en) |
| MX (1) | MXPA04009295A (en) |
| NO (1) | NO20044541L (en) |
| NZ (1) | NZ535881A (en) |
| PL (1) | PL202766B1 (en) |
| PT (1) | PT1487947E (en) |
| WO (1) | WO2003083024A1 (en) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| ITCR20060016A1 (en) * | 2006-06-07 | 2007-12-08 | Silvia Palladini | DETERGENT FORMULATIONS AT LOW ENVIRONMENTAL IMPACT |
| WO2008101810A1 (en) * | 2007-02-20 | 2008-08-28 | Henkel Ag & Co. Kgaa | Use of urea derivatives in washing and cleaning compositions |
| ITMI20081255A1 (en) * | 2008-07-10 | 2010-01-11 | Mafra S P A | FOAM COMPOUND FOR THE CLEANING AND POLISHING OF BODYWORK, WITH EFFECT OF MAXIMUM GLOSS, USED IN TUNNEL CAR WASHES, IN THREE BRUSHES CAR WASHES, IN SELF SERVICES PLANTS WITH LANCE AND MANUALLY |
| EP2652107B1 (en) * | 2010-12-13 | 2019-03-27 | Colgate-Palmolive Company | Dilutable concentrated cleaning composition |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP1129173A2 (en) * | 1998-11-12 | 2001-09-05 | Colgate-Palmolive Company | Microemulsion liquid cleaning composition containing a short chain amphiphile |
| US6096701A (en) * | 1999-06-29 | 2000-08-01 | Colgate Palmolive Company | Antimicrobial multi purpose containing a cationic surfactant |
| US6511955B1 (en) * | 2001-12-10 | 2003-01-28 | Colgate-Palmolive Company | Light duty liquid cleaning compositions having improved preservative system |
| US6455481B1 (en) * | 2001-12-10 | 2002-09-24 | Colgate-Palmolive Company | Light duty liquid cleaning compositions having improved preservative system |
| US6489280B1 (en) * | 2002-08-26 | 2002-12-03 | Colgate-Palmolive Co. | Light duty liquid cleaning compositions having improved preservative system |
-
2003
- 2003-03-26 EP EP03718046A patent/EP1487947B1/en not_active Expired - Lifetime
- 2003-03-26 AT AT03718046T patent/ATE327305T1/en active
- 2003-03-26 PT PT03718046T patent/PT1487947E/en unknown
- 2003-03-26 DK DK03718046T patent/DK1487947T3/en active
- 2003-03-26 PL PL372575A patent/PL202766B1/en unknown
- 2003-03-26 DE DE60305463T patent/DE60305463T2/en not_active Expired - Lifetime
- 2003-03-26 NZ NZ535881A patent/NZ535881A/en not_active IP Right Cessation
- 2003-03-26 CA CA2480327A patent/CA2480327C/en not_active Expired - Fee Related
- 2003-03-26 ES ES03718046T patent/ES2262991T3/en not_active Expired - Lifetime
- 2003-03-26 WO PCT/US2003/009038 patent/WO2003083024A1/en not_active Application Discontinuation
- 2003-03-26 AU AU2003222062A patent/AU2003222062B2/en not_active Ceased
- 2003-03-26 MX MXPA04009295A patent/MXPA04009295A/en active IP Right Grant
- 2003-03-26 IL IL16430503A patent/IL164305A0/en active IP Right Grant
-
2004
- 2004-10-21 EC EC5388A patent/ECSP045388A/en unknown
- 2004-10-22 NO NO20044541A patent/NO20044541L/en not_active Application Discontinuation
Also Published As
| Publication number | Publication date |
|---|---|
| EP1487947B1 (en) | 2006-05-24 |
| NO20044541L (en) | 2004-10-22 |
| PL372575A1 (en) | 2005-07-25 |
| DK1487947T3 (en) | 2006-10-02 |
| DE60305463T2 (en) | 2007-05-03 |
| ATE327305T1 (en) | 2006-06-15 |
| MXPA04009295A (en) | 2005-01-25 |
| EP1487947A1 (en) | 2004-12-22 |
| NZ535881A (en) | 2007-11-30 |
| ECSP045388A (en) | 2005-11-22 |
| ES2262991T3 (en) | 2006-12-01 |
| DE60305463D1 (en) | 2006-06-29 |
| WO2003083024A1 (en) | 2003-10-09 |
| IL164305A0 (en) | 2005-12-18 |
| PL202766B1 (en) | 2009-07-31 |
| CA2480327C (en) | 2011-10-11 |
| AU2003222062B2 (en) | 2010-12-16 |
| AU2003222062A1 (en) | 2003-10-13 |
| PT1487947E (en) | 2006-10-31 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| EEER | Examination request | ||
| MKLA | Lapsed |
Effective date: 20220301 |
|
| MKLA | Lapsed |
Effective date: 20200831 |