CA2473224C - Process for the preparation of urea - Google Patents
Process for the preparation of urea Download PDFInfo
- Publication number
- CA2473224C CA2473224C CA2473224A CA2473224A CA2473224C CA 2473224 C CA2473224 C CA 2473224C CA 2473224 A CA2473224 A CA 2473224A CA 2473224 A CA2473224 A CA 2473224A CA 2473224 C CA2473224 C CA 2473224C
- Authority
- CA
- Canada
- Prior art keywords
- pressure
- condenser
- urea
- steam
- stripping
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 title claims abstract description 88
- 239000004202 carbamide Substances 0.000 title claims abstract description 88
- 238000000034 method Methods 0.000 title claims abstract description 48
- 238000002360 preparation method Methods 0.000 title claims abstract description 8
- 230000015572 biosynthetic process Effects 0.000 claims abstract description 39
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims abstract description 37
- 238000003786 synthesis reaction Methods 0.000 claims abstract description 36
- 238000000354 decomposition reaction Methods 0.000 claims abstract description 30
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims abstract description 28
- KXDHJXZQYSOELW-UHFFFAOYSA-N carbonic acid monoamide Natural products NC(O)=O KXDHJXZQYSOELW-UHFFFAOYSA-N 0.000 claims abstract description 22
- BVCZEBOGSOYJJT-UHFFFAOYSA-N ammonium carbamate Chemical group [NH4+].NC([O-])=O BVCZEBOGSOYJJT-UHFFFAOYSA-N 0.000 claims abstract description 21
- 229910021529 ammonia Inorganic materials 0.000 claims abstract description 17
- 229910002092 carbon dioxide Inorganic materials 0.000 claims abstract description 14
- 239000001569 carbon dioxide Substances 0.000 claims abstract description 11
- 238000009833 condensation Methods 0.000 claims description 12
- 230000005494 condensation Effects 0.000 claims description 12
- 239000007789 gas Substances 0.000 description 9
- KXDHJXZQYSOELW-UHFFFAOYSA-M Carbamate Chemical compound NC([O-])=O KXDHJXZQYSOELW-UHFFFAOYSA-M 0.000 description 7
- 239000000203 mixture Substances 0.000 description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
- 238000006243 chemical reaction Methods 0.000 description 4
- 239000002904 solvent Substances 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- 239000002826 coolant Substances 0.000 description 2
- 239000011261 inert gas Substances 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 229910000069 nitrogen hydride Inorganic materials 0.000 description 2
- 239000007795 chemical reaction product Substances 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 230000018044 dehydration Effects 0.000 description 1
- 238000006297 dehydration reaction Methods 0.000 description 1
- 230000001419 dependent effect Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000011552 falling film Substances 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 238000005201 scrubbing Methods 0.000 description 1
- 150000003672 ureas Chemical class 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C273/00—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups
- C07C273/02—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups of urea, its salts, complexes or addition compounds
- C07C273/04—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups of urea, its salts, complexes or addition compounds from carbon dioxide and ammonia
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0006—Controlling or regulating processes
- B01J19/0013—Controlling the temperature of the process
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00121—Controlling the temperature by direct heating or cooling
- B01J2219/0013—Controlling the temperature by direct heating or cooling by condensation of reactants
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| NL1019848A NL1019848C2 (nl) | 2002-01-28 | 2002-01-28 | Werkwijze voor de bereiding van ureum. |
| NL1019848 | 2002-01-28 | ||
| PCT/NL2002/000874 WO2003064379A1 (en) | 2002-01-28 | 2002-12-30 | Process for the preparation of urea |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CA2473224A1 CA2473224A1 (en) | 2003-08-07 |
| CA2473224C true CA2473224C (en) | 2012-09-25 |
Family
ID=27656498
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA2473224A Expired - Fee Related CA2473224C (en) | 2002-01-28 | 2002-12-30 | Process for the preparation of urea |
Country Status (8)
| Country | Link |
|---|---|
| CN (1) | CN1260209C (es) |
| AR (1) | AR038220A1 (es) |
| AU (1) | AU2002360227B2 (es) |
| CA (1) | CA2473224C (es) |
| MY (1) | MY140851A (es) |
| NL (1) | NL1019848C2 (es) |
| RU (1) | RU2301798C2 (es) |
| WO (1) | WO2003064379A1 (es) |
Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP1918273A1 (en) † | 2006-11-04 | 2008-05-07 | Urea Casale S.A. | Process for urea production and related plant |
| EA034717B1 (ru) * | 2012-05-03 | 2020-03-12 | Стамикарбон Б.В. | Способ производства мочевины из аммиака и диоксида углерода |
| GB201208312D0 (en) * | 2012-05-11 | 2012-06-27 | Afc Energy Plc | Fuel cell system |
| CN103570588A (zh) * | 2013-08-30 | 2014-02-12 | 北京丰汉工程技术有限公司 | 一种尿素合成装置及合成方法 |
| JP7088770B2 (ja) | 2018-07-26 | 2022-06-21 | 東洋エンジニアリング株式会社 | 尿素製造方法および装置 |
| JP7157684B2 (ja) | 2019-03-14 | 2022-10-20 | 東洋エンジニアリング株式会社 | 尿素製造方法および装置 |
| US12247002B2 (en) | 2019-03-14 | 2025-03-11 | Toyo Engineering Corporation | Process and apparatus for urea production |
| EP3736415A1 (en) * | 2019-05-10 | 2020-11-11 | Yara International ASA | Steam network assembly for a plant comprising an ammonia-producing unit and a urea-producing unit |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| IT1068268B (it) * | 1976-09-09 | 1985-03-21 | Snam Progetti | Procedimento per la produzione di urea e purificazione delle acque |
| NL1003923C2 (nl) * | 1996-08-30 | 1998-03-04 | Dsm Nv | Werkwijze voor de bereiding van ureum. |
-
2002
- 2002-01-28 NL NL1019848A patent/NL1019848C2/nl not_active IP Right Cessation
- 2002-12-30 AU AU2002360227A patent/AU2002360227B2/en not_active Ceased
- 2002-12-30 RU RU2004126243/04A patent/RU2301798C2/ru not_active IP Right Cessation
- 2002-12-30 CN CN 02827637 patent/CN1260209C/zh not_active Expired - Lifetime
- 2002-12-30 WO PCT/NL2002/000874 patent/WO2003064379A1/en not_active Application Discontinuation
- 2002-12-30 CA CA2473224A patent/CA2473224C/en not_active Expired - Fee Related
-
2003
- 2003-01-10 MY MYPI20030081 patent/MY140851A/en unknown
- 2003-01-24 AR ARP030100209 patent/AR038220A1/es not_active Application Discontinuation
Also Published As
| Publication number | Publication date |
|---|---|
| CA2473224A1 (en) | 2003-08-07 |
| RU2301798C2 (ru) | 2007-06-27 |
| NL1019848C2 (nl) | 2003-07-30 |
| MY140851A (en) | 2010-01-29 |
| AR038220A1 (es) | 2005-01-05 |
| CN1260209C (zh) | 2006-06-21 |
| RU2004126243A (ru) | 2006-01-27 |
| WO2003064379A1 (en) | 2003-08-07 |
| AU2002360227B2 (en) | 2009-02-26 |
| CN1617853A (zh) | 2005-05-18 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| EEER | Examination request | ||
| MKLA | Lapsed |
Effective date: 20181231 |