CA1085685A - Methode de mise sous capsules de materiaux solubles dans l'eau - Google Patents

Methode de mise sous capsules de materiaux solubles dans l'eau

Info

Publication number: CA1085685A
Authority: CA; Canada
Prior art keywords: water; oil; soluble; soluble material; wall
Prior art date: 1976-05-12
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Expired

Application number

CA276,982A

Other languages

English (en)

Inventor

Abraham M. Rosengart

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Hercules LLC

Original Assignee

Hercules LLC

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1976-05-12

Filing date

1977-04-26

Publication date

1980-09-16

1977-04-26 Application filed by Hercules LLC filed Critical Hercules LLC

1980-09-16 Application granted granted Critical

1980-09-16 Publication of CA1085685A publication Critical patent/CA1085685A/fr

Status Expired legal-status Critical Current

Links

239000002195 soluble material Substances 0.000 title claims abstract description 28
238000000034 method Methods 0.000 title claims abstract description 27
239000000839 emulsion Substances 0.000 claims abstract description 16
IJCWFDPJFXGQBN-RYNSOKOISA-N [(2R)-2-[(2R,3R,4S)-4-hydroxy-3-octadecanoyloxyoxolan-2-yl]-2-octadecanoyloxyethyl] octadecanoate Chemical compound CCCCCCCCCCCCCCCCCC(=O)OC[C@@H](OC(=O)CCCCCCCCCCCCCCCCC)[C@H]1OC[C@H](O)[C@H]1OC(=O)CCCCCCCCCCCCCCCCC IJCWFDPJFXGQBN-RYNSOKOISA-N 0.000 claims abstract description 12
229920003171 Poly (ethylene oxide) Polymers 0.000 claims abstract description 11
229920002472 Starch Polymers 0.000 claims abstract description 11
-1 polyoxyethylene Polymers 0.000 claims abstract description 11
235000019698 starch Nutrition 0.000 claims abstract description 11
239000001589 sorbitan tristearate Substances 0.000 claims abstract description 10
235000011078 sorbitan tristearate Nutrition 0.000 claims abstract description 10
229960004129 sorbitan tristearate Drugs 0.000 claims abstract description 10
239000008107 starch Substances 0.000 claims abstract description 10
239000007864 aqueous solution Substances 0.000 claims abstract description 5
230000001804 emulsifying effect Effects 0.000 claims abstract description 5
239000000796 flavoring agent Substances 0.000 claims description 29
235000019634 flavors Nutrition 0.000 claims description 29
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 17
229920000642 polymer Polymers 0.000 claims description 13
239000007788 liquid Substances 0.000 claims description 10
238000001694 spray drying Methods 0.000 claims description 9
239000006185 dispersion Substances 0.000 claims description 4
239000003995 emulsifying agent Substances 0.000 claims description 4
235000019426 modified starch Nutrition 0.000 claims description 4
241000416162 Astragalus gummifer Species 0.000 claims description 3
WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 claims description 3
229920000084 Gum arabic Polymers 0.000 claims description 3
239000004368 Modified starch Substances 0.000 claims description 3
229920001615 Tragacanth Polymers 0.000 claims description 3
239000000205 acacia gum Substances 0.000 claims description 3
235000010489 acacia gum Nutrition 0.000 claims description 3
239000008121 dextrose Substances 0.000 claims description 3
OWEGMIWEEQEYGQ-UHFFFAOYSA-N 100676-05-9 Natural products OC1C(O)C(O)C(CO)OC1OCC1C(O)C(O)C(O)C(OC2C(OC(O)C(O)C2O)CO)O1 OWEGMIWEEQEYGQ-UHFFFAOYSA-N 0.000 claims description 2
229920002134 Carboxymethyl cellulose Polymers 0.000 claims description 2
GUBGYTABKSRVRQ-PICCSMPSSA-N Maltose Natural products O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@@H]1O[C@@H]1[C@@H](CO)OC(O)[C@H](O)[C@H]1O GUBGYTABKSRVRQ-PICCSMPSSA-N 0.000 claims description 2
CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 claims description 2
229930006000 Sucrose Natural products 0.000 claims description 2
WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 claims description 2
GUBGYTABKSRVRQ-QUYVBRFLSA-N beta-maltose Chemical compound OC[C@H]1O[C@H](O[C@H]2[C@H](O)[C@@H](O)[C@H](O)O[C@@H]2CO)[C@H](O)[C@@H](O)[C@@H]1O GUBGYTABKSRVRQ-QUYVBRFLSA-N 0.000 claims description 2
239000001768 carboxy methyl cellulose Substances 0.000 claims description 2
235000010948 carboxy methyl cellulose Nutrition 0.000 claims description 2
239000008112 carboxymethyl-cellulose Substances 0.000 claims description 2
239000005720 sucrose Substances 0.000 claims description 2
241000978776 Senegalia senegal Species 0.000 claims 1
239000002304 perfume Substances 0.000 claims 1
239000007787 solid Substances 0.000 claims 1
239000000463 material Substances 0.000 abstract description 28
239000004094 surface-active agent Substances 0.000 abstract description 16
239000007921 spray Substances 0.000 abstract description 7
239000003921 oil Substances 0.000 description 37
235000019198 oils Nutrition 0.000 description 37
239000000047 product Substances 0.000 description 20
239000012071 phase Substances 0.000 description 13
239000000203 mixture Substances 0.000 description 11
239000000243 solution Substances 0.000 description 11
239000003240 coconut oil Substances 0.000 description 9
235000019864 coconut oil Nutrition 0.000 description 9
241000219198 Brassica Species 0.000 description 6
235000003351 Brassica cretica Nutrition 0.000 description 6
235000003343 Brassica rupestris Nutrition 0.000 description 6
QKSKPIVNLNLAAV-UHFFFAOYSA-N bis(2-chloroethyl) sulfide Chemical compound ClCCSCCCl QKSKPIVNLNLAAV-UHFFFAOYSA-N 0.000 description 6
235000010460 mustard Nutrition 0.000 description 6
238000005538 encapsulation Methods 0.000 description 5
238000013019 agitation Methods 0.000 description 4
238000002156 mixing Methods 0.000 description 4
239000000843 powder Substances 0.000 description 4
235000020046 sherry Nutrition 0.000 description 4
239000002904 solvent Substances 0.000 description 4
235000014101 wine Nutrition 0.000 description 4
241000208140 Acer Species 0.000 description 3
QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
229920000881 Modified starch Polymers 0.000 description 3
DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 3
238000005354 coacervation Methods 0.000 description 3
238000001035 drying Methods 0.000 description 3
239000008393 encapsulating agent Substances 0.000 description 3
239000011159 matrix material Substances 0.000 description 3
239000002245 particle Substances 0.000 description 3
229920000136 polysorbate Polymers 0.000 description 3
239000008158 vegetable oil Substances 0.000 description 3
JNYAEWCLZODPBN-JGWLITMVSA-N (2r,3r,4s)-2-[(1r)-1,2-dihydroxyethyl]oxolane-3,4-diol Chemical compound OC[C@@H](O)[C@H]1OC[C@H](O)[C@H]1O JNYAEWCLZODPBN-JGWLITMVSA-N 0.000 description 2
244000215068 Acacia senegal Species 0.000 description 2
101100536354 Drosophila melanogaster tant gene Proteins 0.000 description 2
IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 description 2
235000013361 beverage Nutrition 0.000 description 2
239000003795 chemical substances by application Substances 0.000 description 2
238000004945 emulsification Methods 0.000 description 2
238000002474 experimental method Methods 0.000 description 2
235000012907 honey Nutrition 0.000 description 2
239000002480 mineral oil Substances 0.000 description 2
239000002736 nonionic surfactant Substances 0.000 description 2
QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 description 2
229940100515 sorbitan Drugs 0.000 description 2
235000015112 vegetable and seed oil Nutrition 0.000 description 2
239000001606 7-[(2S,3R,4S,5S,6R)-4,5-dihydroxy-6-(hydroxymethyl)-3-[(2S,3R,4R,5R,6S)-3,4,5-trihydroxy-6-methyloxan-2-yl]oxyoxan-2-yl]oxy-5-hydroxy-2-(4-hydroxyphenyl)chroman-4-one Substances 0.000 description 1
240000008886 Ceratonia siliqua Species 0.000 description 1
235000013912 Ceratonia siliqua Nutrition 0.000 description 1
244000060011 Cocos nucifera Species 0.000 description 1
235000013162 Cocos nucifera Nutrition 0.000 description 1
229920002261 Corn starch Polymers 0.000 description 1
244000039154 Erica Species 0.000 description 1
108010010803 Gelatin Proteins 0.000 description 1
244000024873 Mentha crispa Species 0.000 description 1
235000014749 Mentha crispa Nutrition 0.000 description 1
244000061176 Nicotiana tabacum Species 0.000 description 1
235000002637 Nicotiana tabacum Nutrition 0.000 description 1
244000061456 Solanum tuberosum Species 0.000 description 1
235000002595 Solanum tuberosum Nutrition 0.000 description 1
235000019486 Sunflower oil Nutrition 0.000 description 1
239000002253 acid Substances 0.000 description 1
125000003342 alkenyl group Chemical group 0.000 description 1
239000010775 animal oil Substances 0.000 description 1
239000008346 aqueous phase Substances 0.000 description 1
125000003710 aryl alkyl group Chemical group 0.000 description 1
AEMOLEFTQBMNLQ-DTEWXJGMSA-N beta-D-galacturonic acid Chemical compound O[C@@H]1O[C@H](C(O)=O)[C@H](O)[C@H](O)[C@H]1O AEMOLEFTQBMNLQ-DTEWXJGMSA-N 0.000 description 1
239000005018 casein Substances 0.000 description 1
BECPQYXYKAMYBN-UHFFFAOYSA-N casein, tech. Chemical compound NCCCCC(C(O)=O)N=C(O)C(CC(O)=O)N=C(O)C(CCC(O)=N)N=C(O)C(CC(C)C)N=C(O)C(CCC(O)=O)N=C(O)C(CC(O)=O)N=C(O)C(CCC(O)=O)N=C(O)C(C(C)O)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=O)N=C(O)C(CCC(O)=O)N=C(O)C(COP(O)(O)=O)N=C(O)C(CCC(O)=N)N=C(O)C(N)CC1=CC=CC=C1 BECPQYXYKAMYBN-UHFFFAOYSA-N 0.000 description 1
235000021240 caseins Nutrition 0.000 description 1
229940112822 chewing gum Drugs 0.000 description 1
235000015218 chewing gum Nutrition 0.000 description 1
238000000975 co-precipitation Methods 0.000 description 1
239000012612 commercial material Substances 0.000 description 1
150000001875 compounds Chemical class 0.000 description 1
230000002844 continuous effect Effects 0.000 description 1
239000013068 control sample Substances 0.000 description 1
235000005687 corn oil Nutrition 0.000 description 1
239000002285 corn oil Substances 0.000 description 1
239000008120 corn starch Substances 0.000 description 1
239000002537 cosmetic Substances 0.000 description 1
239000003599 detergent Substances 0.000 description 1
150000001990 dicarboxylic acid derivatives Chemical class 0.000 description 1
238000004090 dissolution Methods 0.000 description 1
230000000694 effects Effects 0.000 description 1
239000003792 electrolyte Substances 0.000 description 1
150000002148 esters Chemical class 0.000 description 1
239000003205 fragrance Substances 0.000 description 1
229920000159 gelatin Polymers 0.000 description 1
239000008273 gelatin Substances 0.000 description 1
235000019322 gelatine Nutrition 0.000 description 1
235000011852 gelatine desserts Nutrition 0.000 description 1
239000007970 homogeneous dispersion Substances 0.000 description 1
238000002386 leaching Methods 0.000 description 1
239000007791 liquid phase Substances 0.000 description 1
239000012263 liquid product Substances 0.000 description 1
235000013575 mashed potatoes Nutrition 0.000 description 1
235000010446 mineral oil Nutrition 0.000 description 1
125000000896 monocarboxylic acid group Chemical group 0.000 description 1
DFPMSGMNTNDNHN-ZPHOTFPESA-N naringin Chemical compound O[C@@H]1[C@H](O)[C@@H](O)[C@H](C)O[C@H]1O[C@H]1[C@H](OC=2C=C3O[C@@H](CC(=O)C3=C(O)C=2)C=2C=CC(O)=CC=2)O[C@H](CO)[C@@H](O)[C@@H]1O DFPMSGMNTNDNHN-ZPHOTFPESA-N 0.000 description 1
229940052490 naringin Drugs 0.000 description 1
229930019673 naringin Natural products 0.000 description 1
239000001814 pectin Substances 0.000 description 1
235000010987 pectin Nutrition 0.000 description 1
229960000292 pectin Drugs 0.000 description 1
239000000575 pesticide Substances 0.000 description 1
239000000825 pharmaceutical preparation Substances 0.000 description 1
229940127557 pharmaceutical product Drugs 0.000 description 1
238000005191 phase separation Methods 0.000 description 1
230000001376 precipitating effect Effects 0.000 description 1
238000002360 preparation method Methods 0.000 description 1
230000001681 protective effect Effects 0.000 description 1
239000011343 solid material Substances 0.000 description 1
239000000126 substance Substances 0.000 description 1
239000002600 sunflower oil Substances 0.000 description 1
239000000725 suspension Substances 0.000 description 1
CYRMSUTZVYGINF-UHFFFAOYSA-N trichlorofluoromethane Chemical compound FC(Cl)(Cl)Cl CYRMSUTZVYGINF-UHFFFAOYSA-N 0.000 description 1
229940029284 trichlorofluoromethane Drugs 0.000 description 1
125000003258 trimethylene group Chemical group [H]C([H])([*:2])C([H])([H])C([H])([H])[*:1] 0.000 description 1
235000013311 vegetables Nutrition 0.000 description 1
239000011782 vitamin Substances 0.000 description 1
229940088594 vitamin Drugs 0.000 description 1
229930003231 vitamin Natural products 0.000 description 1
235000013343 vitamin Nutrition 0.000 description 1

Classifications

- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J13/00—Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
- B01J13/02—Making microcapsules or microballoons
- B01J13/06—Making microcapsules or microballoons by phase separation
- B01J13/12—Making microcapsules or microballoons by phase separation removing solvent from the wall-forming material solution
- B01J13/125—Making microcapsules or microballoons by phase separation removing solvent from the wall-forming material solution by evaporation of the solvent
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
- A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
- A23L27/70—Fixation, conservation, or encapsulation of flavouring agents
- A23L27/72—Encapsulation

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Health & Medical Sciences (AREA)
Nutrition Science (AREA)
Life Sciences & Earth Sciences (AREA)
Engineering & Computer Science (AREA)
Food Science & Technology (AREA)
Polymers & Plastics (AREA)
Dispersion Chemistry (AREA)
Chemical Kinetics & Catalysis (AREA)
Manufacturing Of Micro-Capsules (AREA)

CA276,982A 1976-05-12 1977-04-26 Methode de mise sous capsules de materiaux solubles dans l'eau Expired CA1085685A (fr)

Applications Claiming Priority (2)

Application Number	Priority Date	Filing Date	Title
US68587376A	1976-05-12	1976-05-12
US685,873		1976-05-12

Publications (1)

Publication Number	Publication Date
CA1085685A true CA1085685A (fr)	1980-09-16

Family

ID=24754028

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
CA276,982A Expired CA1085685A (fr)	1976-05-12	1977-04-26	Methode de mise sous capsules de materiaux solubles dans l'eau

Country Status (10)

Country	Link
JP (1)	JPS52136890A (fr)
AU (1)	AU2507477A (fr)
BE (1)	BE853873A (fr)
CA (1)	CA1085685A (fr)
DE (1)	DE2720477A1 (fr)
FR (1)	FR2350875A1 (fr)
GB (1)	GB1535470A (fr)
IL (1)	IL51928A (fr)
IT (1)	IT1193167B (fr)
NL (1)	NL7705214A (fr)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US4382813A (en) *	1980-10-30	1983-05-10	The United States Of America As Represented By The Secretary Of Agriculture	Encapsulation by entrapment within starch adduct matrix
DE4330958A1 (de) *	1993-09-09	1995-03-16	Schering Ag	Neue wirkstoffhaltige Mikropartikel, diese enthaltende Mittel, deren Verwendung zur ultraschallgesteuerten Freisetzung von Wirkstoffen sowie Verfahren zu deren Herstellung
GB201107221D0 (en) *	2011-05-03	2011-06-15	Givaudan Sa	Process

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JPS5214234B2 (fr) *	1971-07-30	1977-04-20
JPS528795B2 (fr) *	1971-12-30	1977-03-11

1977
- 1977-04-20 FR FR7711828A patent/FR2350875A1/fr not_active Withdrawn
- 1977-04-22 BE BE176943A patent/BE853873A/fr unknown
- 1977-04-22 IL IL51928A patent/IL51928A/xx unknown
- 1977-04-26 CA CA276,982A patent/CA1085685A/fr not_active Expired
- 1977-05-06 DE DE19772720477 patent/DE2720477A1/de active Pending
- 1977-05-11 NL NL7705214A patent/NL7705214A/xx not_active Application Discontinuation
- 1977-05-11 IT IT23440/77A patent/IT1193167B/it active
- 1977-05-11 GB GB19783/77A patent/GB1535470A/en not_active Expired
- 1977-05-11 AU AU25074/77A patent/AU2507477A/en not_active Expired
- 1977-05-12 JP JP5481877A patent/JPS52136890A/ja active Pending

Also Published As

Publication number	Publication date
BE853873A (fr)	1977-10-24
DE2720477A1 (de)	1977-12-01
NL7705214A (nl)	1977-11-15
GB1535470A (en)	1978-12-13
JPS52136890A (en)	1977-11-15
IT1193167B (it)	1988-06-02
FR2350875A1 (fr)	1977-12-09
IL51928A (en)	1979-03-12
IL51928A0 (en)	1977-06-30
AU2507477A (en)	1978-11-16

Publication	Publication Date	Title
US3971852A (en)	1976-07-27	Process of encapsulating an oil and product produced thereby
US3780195A (en)	1973-12-18	Encapsulation process
US3664963A (en)	1972-05-23	Encapsulation process
US4389419A (en)	1983-06-21	Vitamin encapsulation
CA1220098A (fr)	1987-04-07	Methode de preparation de microspheres pour liberation intravasculaire
Bodmeier et al.	1988	Solvent selection in the preparation of poly (DL-lactide) microspheres prepared by the solvent evaporation method
DE69726446T2 (de)	2004-08-26	Verfahren zur herstellung eines perlförmigen nahrungsmittelzusatzes
EP0070719B1 (fr)	1985-12-11	Encapsulation de liquides volatils
JP3313114B2 (ja)	2002-08-12	乳化剤及び乳化組成物並びに粉末化組成物
JP2001252013A (ja)	2001-09-18	複合物質
US20120034284A1 (en)	2012-02-09	Microencapsulation Product and Process
US20040247664A1 (en)	2004-12-09	Gel capsules containing active ingredients and use thereof
US20080277812A1 (en)	2008-11-13	Wax Encapsulation
WO1997013416A1 (fr)	1997-04-17	Procede de double encapsulation et compositions aromatisantes ainsi preparees
WO1998018338A1 (fr)	1998-05-07	Compositions d'encapsulation permettant d'obtenir des revetements gras et procede de preparation de ces compositions
WO1991017821A1 (fr)	1991-11-28	Procede de preparation de microcapsules contenant un agent aromatique incorpore dans une substance matrice et produits ainsi prepares
Bodmeier et al.	1992	Process and formulation variables in the preparation of wax microparticles by a melt dispersion technique. II. W/O/W multiple emulsion technique for water-soluble drugs
DE60003646T2 (de)	2004-06-17	Aromatisierung eines aufgusses
EP0523184A1 (fr)	1993-01-20	Emulsion proteinique filmogene
EP2654737A1 (fr)	2013-10-30	Nouvelle préparation d'un système de libération entérique
PL174160B1 (pl)	1998-06-30	Środek zastępujący tłuszcz w produktach spożywczych lub kosmetycznych i sposób wytwarzania środka zastępującego tłuszcz w produktach spożywczych lub kosmetycznych
CA1085685A (fr)	1980-09-16	Methode de mise sous capsules de materiaux solubles dans l'eau
CN111074674A (zh)	2020-04-28	一种缓释香精成型纸
KR100457251B1 (ko)	2004-11-16	마이크로캡슐 형태의 살충제 및 이의 제조방법
Kristmundsdottir et al.	1994	Influence of emulsifying agents on the properties of cellulose acetate butyrate and ethylcellulose microcapsules

Legal Events

Date	Code	Title	Description
1997-09-16	MKEX	Expiry