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CA1041362A - Syrup and method of manufacturing same - Google Patents

Syrup and method of manufacturing same

Info

Publication number
CA1041362A
CA1041362A CA211,957A CA211957A CA1041362A CA 1041362 A CA1041362 A CA 1041362A CA 211957 A CA211957 A CA 211957A CA 1041362 A CA1041362 A CA 1041362A
Authority
CA
Canada
Prior art keywords
syrup
cmc
semi
preparing
concentrated
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
CA211,957A
Other languages
French (fr)
Inventor
Paul O. Carlson
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
General Foods Corp
Original Assignee
General Foods Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by General Foods Corp filed Critical General Foods Corp
Application granted granted Critical
Publication of CA1041362A publication Critical patent/CA1041362A/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C13SUGAR INDUSTRY
    • C13BPRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
    • C13B20/00Purification of sugar juices
    • C13B20/12Purification of sugar juices using adsorption agents, e.g. active carbon
    • C13B20/123Inorganic agents, e.g. active carbon
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
    • A23L29/00Foods or foodstuffs containing additives; Preparation or treatment thereof
    • A23L29/30Foods or foodstuffs containing additives; Preparation or treatment thereof containing carbohydrate syrups; containing sugars; containing sugar alcohols, e.g. xylitol; containing starch hydrolysates, e.g. dextrin

Landscapes

  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Biochemistry (AREA)
  • Organic Chemistry (AREA)
  • Molecular Biology (AREA)
  • Nutrition Science (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Jellies, Jams, And Syrups (AREA)

Abstract

ABSTRACT OF THE DISCLOSURE
A sucrose-based syrup is increased in viscosity to provide a preferred pourability and non-absorptive characteristic on pancakes and like porous comestibles to which it is applied by a method which employs a semi-refined sugar syrup which is mixed with CMC-thickened softened water operative to compensate for presence of ash and other flocculents in the semi-refined sugar syrup.

Description

1~34~36Z
This invention relates to a process for manufacture of syrup. Many users prefer a table syrup which is thickened to an extent such that the syrup remains on the pancake or like baked preparation, be it chemically- or yeast-leavened, and is less absorbed thereby to provide an improved organoleptic acceptance from standpoints of both taste and appearance;
sodium carboxymethylcellulose (CMC~ has been added to table :~
syrup preparations for such purposes. This addition renders more obvious the presence of discrete "floc" in some sugar 10 preparations after extended shelf storage, particularly those which are less refinecl, thereby reducing syrup clarity.
Although the practice of employing CMC to thicken a variety of table syrups and like topping compositions has been employed previously, the ability to provide an economical and reliably produced clear syrup containing CMC remains significantly dependent upon the absence in the syrup of such flocculents as ash, organic substances, and other matter which may contribute to a reduction in clarity.
Accordingly, there is a need to provide a table syrup ~ .
. .
process which is less dependent upon degree of purification or refinement of a given syrup and is less prone to the manifesta-tions of a "floc" appearance in thickened syrup preparations which employ CMC.
According to the invention there is provided a pro-cess for preparing a table syrup which employs semi-refined ~-sugar syrup as its principal constituent and which is thickened with CMC and comprises preparing a concentrated, pasteurized, . ~ . .
semi-refined sucrose syrup, said syrup containing naturally ~: occurring colloidal substances, filtering-said syrup through a '' .
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diatomaceous earth filter media to remove colloidally suspended mineral and organic residue contained therein, separately pre-~ paring a CMC solution from softened water having less than 5 `~ parts per million calcium and/or magnesium, admixing the latter solution with the concentrated syrup to dilute the concentrate and produce an ultimate .
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~ -la-syrup having a CMC level of C.15-0.25%,and pac~aging th~ diluted 3yrup in a transparent container.
Thus, a process is provided which meets these objects : by employing a diatomaceous earth filter a.i.d to partially clari~y a concentrated pasteurized semi-refined sucrose s~rup containing naturally occurring colloidal substances and combining this filtered syrup with a softened water containiny the CMC in amounts operative to rsduce Brix and increase viscosity the filtered syrup to the intended v.iscosity preparatory to bottling.
In accordance with its more specific aspects, a sem-refined syrup having an ash level exceeding that of ~ranulated sugar of commerce and typically having an ash content of about 0.30 and a polarization (dry basis) o 97.50 is admixed with corn syrup, maple syrup, flavor and color. The prepared syrup i8 ,...
, at an elevated Brix of at least 68 and preferably 71-72. The syrup is subjected to a pasteurization temperature, say, to a temperature of 180F. and at least 160F. and then is passed through a diatomaceous earth filter medium; this medium will typically be employed in a leaf-iype pressure filter known in the i ~ 20 art and will be continually developed and re.stored to maximal efficiency by building a substrate operative to re~ove impuritie3 in the syrup. In this respect a preferred practice will employ s regenerating levels of diatomaceous earth in the syrup solution which as it is introduced to the filter will continue to build iltration substrate and operatively result in partial removal - of colloidally suspended mineral and organic residue.
: Separately of the s~rup solution, a CMC solution is ~. ~ prepared at ambient Or only slightly elevated temperatures .~ employing a softened water which will have any chemical preserva-1. . .:! .
tives that may be employed in the finished table syrup present : ~ and into which CMC will be dispersed, say, at a level between !'';;'"' ' 1-5~ preferably 2.75% to provide the viscol.izing diluent solution. It has been ~ound essential in this respect to employ i ~ - 2 -, ; . ~ .

~ 4~3~Gi2 water of such softened condition as minimizes the flocculatio~
tendencies of the semi-refined sugar syrup described harein-above. The softened water will be characterized by the followin~
criteria~

Parts per ~illion Maximum _ (By Weiqht) _ _ Calcium and/or magnesium 5 The softened CMC solution, once prepared, will be hea~ed to a pasteurizing temperature of at least 160F. upon admixture with the filtered concentrate su~ar syrup solution and will be blended at a proportion operative to reduce Brix below 68 and typically to a preferred range of 65-67, a most preferred being about 66.5 and produce viscosity in the range of 600-1100 cps the blend will thereafter be repasteurized preparatory to bottling and packing, all in accordance with procedures well known to tho9e s~illed in the art.
The following is a typical syrup formulation and range ' ' for practicing the formulation of a syrup solution in accordance with this invention:

Range o~ Pr~ferred ~ -Ingredients % Level _ Semi-refined Liquid Sugar Syrup (67.5 Brix) 58 *

Corn Syrup (42 DE, 43 ~aume) 30 **

Sot ~ater (as specified herein) 8.7 Maple Sugar Syrup (67.50 Brix) 3.0 1-5***

CMC (Sodium carboxymethylcellulose) 0.20 0.15-0.75 Sodim Benzoate 0.05 Sorbic Acid 0.03 ~- Caramel Color 0.02 . .
*The range of liquid sugar syrup as a percent of the ini~hed product can vary depending upon formulary preference.
~`'! **The level of corn syrup employed as such may similarly vary depending upon formulary preference.
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. . .

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- ***The level of maple syrup forms no part of this invention and may be employed as cost and quality of the inishe~ product ' is required.
In the foregoing formulation the preerred form of ~ CMC will be one having a high degree of substitution of carboxy-; methyl groups on the cellulose ester polymer chain, the degree ~ of substitution being inversely related to the degree of stringi-,,i ness. Moreover, when the degree of substitution is less than optimal, the syrup as thickened will be found to have a non-smooth texture imparted thereto whereas at a high order of -substitution the syrup will have a smooth mouthfeel and less stringy. Accordingly, in accordance with its most preferred and ' specific aspects, the syrup will employ a CMC wherein the degree '' ,, of substitution is 0.9 carboxymeth"vl groups substituted per anhydro~lucose unit; a medium type viscosity ~800 to 3100 aps in a 2% solution at 25C LVF Brookfield 30 rpm ~3 ,~pindle) is preferred.
' As thus described the invention will be adaptable to a , -; variety of syrup manufacturers using less than refine~ sugar ~' syrups. 'Accordingly, the invention is to be interpreted with regard to the accompanying claims for construction thereof.

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Claims (2)

The embodiments of the invention in which an exclusive property or privilege is claimed are defined as follows:
1. Process for preparing a table syrup which employs semi-refined sugar syrup as its principal constituent and which is thickened with CMC and comprises preparing a concentrated, pas-teurized, semi-refined sucrose syrup, said syrup containing naturally occurring colloidal substances, filtering said syrup through a diatomaceous earth filter media to remove colloidally suspended mineral and organic residue contained therein, separate-ly preparing a CMC solution from softened water having less than 5 parts per million calcium and/or magnesium, admixing the latter solution with the concentrated syrup to dilute the concentrate and produce an ultimate syrup having a Brix below 68° and a CMC
level of 0.15-0.25%, and packaging the diluted syrup in a trans-parent container.
2. A process according to either of claims 1 and 2, where-in the CMC has an average of 0.9 carboxymethyl groups substituted per anhydroglucose unit.
CA211,957A 1973-11-23 1974-10-22 Syrup and method of manufacturing same Expired CA1041362A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US418330A US3897262A (en) 1973-11-23 1973-11-23 Syrup and method of manufacturing same

Publications (1)

Publication Number Publication Date
CA1041362A true CA1041362A (en) 1978-10-31

Family

ID=23657663

Family Applications (1)

Application Number Title Priority Date Filing Date
CA211,957A Expired CA1041362A (en) 1973-11-23 1974-10-22 Syrup and method of manufacturing same

Country Status (2)

Country Link
US (1) US3897262A (en)
CA (1) CA1041362A (en)

Families Citing this family (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4073963A (en) * 1976-12-27 1978-02-14 Cpc International Inc. Stable, homogeneous buttered table syrups
US4152466A (en) * 1978-06-27 1979-05-01 Deretchin Benjamin B Stable homogeneous peanut butter table syrup
US4394399A (en) * 1981-06-25 1983-07-19 The Quaker Oats Company Low calorie table syrup product
CA1294821C (en) * 1985-12-26 1992-01-28 Craig Joseph Bennett Aqueous table syrup with reduced sugar content
US5106646A (en) * 1991-01-08 1992-04-21 Kraft General Foods, Inc. Stabilized low calorie syrup with reduced sweetener solids content
US5478589A (en) * 1993-10-08 1995-12-26 The Quaker Oats Company Stable gum system for very low calorie table syrup applications
JP2013526267A (en) * 2010-05-11 2013-06-24 トリストラム プロプライエタリー リミテッド Flowable liquid composition
CA2814345C (en) * 2011-03-16 2014-01-14 Federation Des Producteurs Acericoles Du Quebec Apparatus and process for pasteurization of sap and product thereof

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2470202A (en) * 1947-04-19 1949-05-17 Wickenden Leonard Filtering process
US2935408A (en) * 1957-12-13 1960-05-03 American Food Lab Inc Stabilizer for non-frozen water-containing ingestible materials such, for instance, as foodstuffs and internal medicines

Also Published As

Publication number Publication date
US3897262A (en) 1975-07-29

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