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BRPI0509353A - processo para a produção de um composto de 5-hidróxi-4-tiometilpirazol - Google Patents

processo para a produção de um composto de 5-hidróxi-4-tiometilpirazol

Info

Publication number
BRPI0509353A
BRPI0509353A BRPI0509353-8A BRPI0509353A BRPI0509353A BR PI0509353 A BRPI0509353 A BR PI0509353A BR PI0509353 A BRPI0509353 A BR PI0509353A BR PI0509353 A BRPI0509353 A BR PI0509353A
Authority
BR
Brazil
Prior art keywords
hydroxy
thiomethylpyrazole
compound
general formula
producing
Prior art date
Application number
BRPI0509353-8A
Other languages
English (en)
Inventor
Yukio Uchida
Original Assignee
Ihara Chemical Ind Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=35063690&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=BRPI0509353(A) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Ihara Chemical Ind Co filed Critical Ihara Chemical Ind Co
Publication of BRPI0509353A publication Critical patent/BRPI0509353A/pt
Publication of BRPI0509353A8 publication Critical patent/BRPI0509353A8/pt
Publication of BRPI0509353B1 publication Critical patent/BRPI0509353B1/pt

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
    • C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
    • C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D231/18—One oxygen or sulfur atom
    • C07D231/20—One oxygen atom attached in position 3 or 5
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
    • C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
    • C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D231/28—Two oxygen or sulfur atoms
    • C07D231/30—Two oxygen or sulfur atoms attached in positions 3 and 5
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D413/00—Heterocyclic compounds containing two or more hetero rings, at least one ring having nitrogen and oxygen atoms as the only ring hetero atoms
    • C07D413/02—Heterocyclic compounds containing two or more hetero rings, at least one ring having nitrogen and oxygen atoms as the only ring hetero atoms containing two hetero rings
    • C07D413/12—Heterocyclic compounds containing two or more hetero rings, at least one ring having nitrogen and oxygen atoms as the only ring hetero atoms containing two hetero rings linked by a chain containing hetero atoms as chain links

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Plural Heterocyclic Compounds (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

PROCESSO PARA A PRODUçãO DE UM COM POSTO DE 5-HIDRóXI-4-TIOMETILPIRAZOL. A presente invenção refere-se a um composto de pirazol repre sentado pela fórmula geral (1) que é reagido com um composto de enxofre representado pela fórmula geral (2) na presença de uma base e formaldeído, para produzir assim um composto de 5-hidróxi-4-tiometilpirazol representado pela fórmula geral (3). O composto de 5-hidróxi-4-tiometilpirazol pode ser facilmente produzido em um bom rendimento, através da utilização de tal processo. Ainda, este processo pode fornecer facilmente o composto de 5-hidróxi-4-tiometilpirazol sob uma condição suave em uma única etapa, sem utilizar um aparato especial, um catalisador ou um metal de transição dispendioso etc.Em adição, este processo pode ser realizado substancialmentesem produzir um rejeito prejudicial que pode ser derivado de um catalisador etc, e, portanto, este processo é inofensivo ao ambiente e tem valor industrial.
BRPI0509353A 2004-03-31 2005-03-31 processo para a produção de um composto de 5-hidróxi-4-tiometilpirazol BRPI0509353B1 (pt)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP2004102963A JP4621939B2 (ja) 2004-03-31 2004-03-31 ５−ヒドロキシ−４−チオメチルピラゾール化合物の製造方法
PCT/JP2005/006806 WO2005095352A1 (ja) 2004-03-31 2005-03-31 ５－ヒドロキシ－４－チオメチルピラゾール化合物の製造方法

Publications (3)

Publication Number Publication Date
BRPI0509353A true BRPI0509353A (pt) 2007-09-11
BRPI0509353A8 BRPI0509353A8 (pt) 2017-09-19
BRPI0509353B1 BRPI0509353B1 (pt) 2019-01-02

Family

ID=35063690

Family Applications (1)

Application Number Title Priority Date Filing Date
BRPI0509353A BRPI0509353B1 (pt) 2004-03-31 2005-03-31 processo para a produção de um composto de 5-hidróxi-4-tiometilpirazol

Country Status (19)

Country Link
US (1) US7488831B2 (pt)
EP (1) EP1767528B1 (pt)
JP (1) JP4621939B2 (pt)
KR (1) KR101205731B1 (pt)
CN (1) CN1938278B (pt)
AU (1) AU2005228017B2 (pt)
BR (1) BRPI0509353B1 (pt)
CA (1) CA2560936C (pt)
CR (1) CR8640A (pt)
ES (1) ES2508765T3 (pt)
IL (1) IL178233A (pt)
IN (1) IN2006DE05581A (pt)
MX (1) MX280092B (pt)
NZ (1) NZ550143A (pt)
PL (1) PL1767528T3 (pt)
RU (1) RU2386619C2 (pt)
TW (1) TWI357899B (pt)
UA (1) UA83910C2 (pt)
WO (1) WO2005095352A1 (pt)

Families Citing this family (25)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CA2579091A1 (en) 2004-10-05 2006-04-13 Syngenta Limited Isoxazoline derivatives and their use as herbicides
NZ554870A (en) * 2004-12-20 2009-09-25 Ihara Chemical Ind Co Process for production of (4,5-dihydroisoxazol-3-Yl)thio- carboxamidine salts
JP2007031342A (ja) * 2005-07-27 2007-02-08 Ihara Chem Ind Co Ltd ５−ヒドロキシ−１−アルキルピラゾール誘導体の製造方法
NZ570495A (en) * 2006-02-14 2011-10-28 Ihara Chemical Ind Co Process for production of 5-alkoxy-4-hydroxymethylpyrazole compound
EP2167464B1 (en) * 2007-05-25 2014-12-03 AbbVie Deutschland GmbH & Co KG Heterocyclic compounds as positive modulators of metabotropic glutamate receptor 2 (mglu2 receptor)
GB0916267D0 (en) 2009-09-16 2009-10-28 Syngenta Ltd Herbicidal compounds
CN102666502B (zh) 2009-11-26 2015-01-07 巴斯夫欧洲公司 生产5,5-二取代的4,5-二氢异噁唑-3-硫基甲脒盐的方法
WO2011063843A1 (de) 2009-11-26 2011-06-03 Basf Se Verfahren zur herstellung 5,5-disubstituierter 2-isoxazoline
ES2528646T3 (es) * 2010-05-20 2015-02-11 Bayer Intellectual Property Gmbh Procedimiento para la fabricación de 1-alquil-3-difluorometil-5-hidroxipirazoles
CA2843415C (en) 2011-07-29 2019-12-31 University Of Saskatchewan Polymer-based resonator antennas
CN103387541B (zh) * 2012-05-10 2016-02-10 中国中化股份有限公司 一种取代吡唑醚类化合物的制备方法
WO2017084995A1 (en) 2015-11-16 2017-05-26 Lonza Ltd Method for preparation of 1-methyl-3-(trifluoromethyl)-1hpyrazol-5-ol
TW201835036A (zh) 2017-02-27 2018-10-01 瑞士商隆薩有限公司 製備1-甲基-3-(三氟甲基)-1h-吡唑-5-醇的方法
CN111542514B (zh) * 2017-12-27 2021-09-03 组合化学工业株式会社 硫基甲脒盐化合物的制造方法
CN112135814B (zh) * 2018-05-31 2021-09-28 组合化学工业株式会社 含氟吡唑衍生物的制造方法及其中间体
CA3149137A1 (en) 2019-07-30 2021-02-04 Adama Agan Ltd. Process and intermediates for the preparation of pyroxasulfone
MY197145A (en) 2019-10-31 2023-05-26 Kumiai Chemical Industry Co Process for producing herbicide and intermediate thereof
BR112022017794A2 (pt) 2020-03-05 2022-10-25 Adama Agan Ltd Processo e intermediários para a preparação de piroxassulfona
CN111574511A (zh) * 2020-06-28 2020-08-25 安徽久易农业股份有限公司 一种砜吡草唑的合成方法及其应用
EP3936503A1 (en) 2020-07-10 2022-01-12 Adama Agan Ltd. Process and intermediates for the preparation of pyroxasulfone, fenoxasulfone and various sulfone analogs of 5,5-dimethyl-4h-1,2-oxazole
CN112110912B (zh) * 2020-07-31 2022-07-05 绍兴贝斯美化工股份有限公司 一种合成硫醚类中间体的方法
TW202334128A (zh) 2021-10-29 2023-09-01 日商組合化學工業股份有限公司 二硫化物化合物、多硫化物化合物及其用途
AR127776A1 (es) 2021-11-28 2024-02-28 Adama Agan Ltd Composiciones de concentrado en suspensión de alta carga
CN114716428B (zh) * 2022-05-06 2024-02-06 山东潍坊润丰化工股份有限公司 制备砜吡草唑中间体的方法
CN115850178B (zh) * 2022-12-28 2025-04-04 宁夏格瑞精细化工有限公司 一种1-甲基-3-(三氟甲基)-1h-吡唑-5-醇的制备方法

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
AR035912A1 (es) * 2000-03-02 2004-07-28 Aventis Cropscience Sa Compuestos de 4-tiometilpirazol, composicion plaguicida, metodo para el control de plagas en un lugar, semillas tratadas o recubiertas,uso de estos compuestos o composiciones para el control de plagas, uso de estos compuestos para preparar un medicamento veterinario, y,proceso para la preparacion de
JP4465133B2 (ja) * 2001-02-08 2010-05-19 クミアイ化学工業株式会社 イソオキサゾリン誘導体及びこれを有効成分とする除草剤
WO2003000686A1 (fr) * 2001-06-21 2003-01-03 Kumiai Chemical Industry Co., Ltd. Dérivés d'isoxazoline et herbicides
RS53725B1 (sr) * 2002-08-01 2015-06-30 Ihara Chemical Industry Co. Ltd. Derivati pirazola i postupak njihovog dobijanja
UA78071C2 (en) * 2002-08-07 2007-02-15 Kumiai Chemical Industry Co Herbicidal composition

Also Published As

Publication number Publication date
CR8640A (es) 2007-08-28
PL1767528T3 (pl) 2015-03-31
AU2005228017B2 (en) 2010-09-30
TWI357899B (en) 2012-02-11
EP1767528A4 (en) 2010-04-21
CA2560936C (en) 2013-01-08
ES2508765T3 (es) 2014-10-16
IL178233A (en) 2014-02-27
KR101205731B1 (ko) 2012-11-28
WO2005095352A1 (ja) 2005-10-13
RU2386619C2 (ru) 2010-04-20
CN1938278A (zh) 2007-03-28
RU2006138241A (ru) 2008-05-10
UA83910C2 (ru) 2008-08-26
BRPI0509353A8 (pt) 2017-09-19
CA2560936A1 (en) 2005-10-13
KR20070003964A (ko) 2007-01-05
IN2006DE05581A (pt) 2007-08-31
EP1767528A1 (en) 2007-03-28
NZ550143A (en) 2010-04-30
EP1767528B1 (en) 2014-09-17
BRPI0509353B1 (pt) 2019-01-02
MXPA06011130A (es) 2007-01-25
US7488831B2 (en) 2009-02-10
IL178233A0 (en) 2006-12-31
JP2005289824A (ja) 2005-10-20
US20070185334A1 (en) 2007-08-09
MX280092B (es) 2010-10-18
JP4621939B2 (ja) 2011-02-02
AU2005228017A1 (en) 2005-10-13
CN1938278B (zh) 2012-12-12
TW200536832A (en) 2005-11-16

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Legal Events

Date Code Title Description
B06F Objections, documents and/or translations needed after an examination request according [chapter 6.6 patent gazette]
B07D Technical examination (opinion) related to article 229 of industrial property law [chapter 7.4 patent gazette]
B25A Requested transfer of rights approved

Owner name: KUMIAI CHEMICAL INDUSTRY CO., LTD. (JP)

B07G Grant request does not fulfill article 229-c lpi (prior consent of anvisa) [chapter 7.7 patent gazette]
B06A Patent application procedure suspended [chapter 6.1 patent gazette]
B06A Patent application procedure suspended [chapter 6.1 patent gazette]
B09A Decision: intention to grant [chapter 9.1 patent gazette]
B16A Patent or certificate of addition of invention granted [chapter 16.1 patent gazette]

Free format text: PRAZO DE VALIDADE: 10 (DEZ) ANOS CONTADOS A PARTIR DE 02/01/2019, OBSERVADAS AS CONDICOES LEGAIS.