BRPI0505212A - aperfeiçoamentos em processo de hidrólise ácida rápida de material lignocelulósico e em reator de hidrólise - Google Patents
aperfeiçoamentos em processo de hidrólise ácida rápida de material lignocelulósico e em reator de hidróliseInfo
- Publication number
- BRPI0505212A BRPI0505212A BRPI0505212-2A BRPI0505212A BRPI0505212A BR PI0505212 A BRPI0505212 A BR PI0505212A BR PI0505212 A BRPI0505212 A BR PI0505212A BR PI0505212 A BRPI0505212 A BR PI0505212A
- Authority
- BR
- Brazil
- Prior art keywords
- reactor
- hydrolysis
- liquid phase
- levels
- lignocellulosic material
- Prior art date
Links
- 230000007062 hydrolysis Effects 0.000 title abstract 3
- 238000006460 hydrolysis reaction Methods 0.000 title abstract 3
- 238000000034 method Methods 0.000 title abstract 3
- 238000005903 acid hydrolysis reaction Methods 0.000 title abstract 2
- 239000012978 lignocellulosic material Substances 0.000 title abstract 2
- 239000007791 liquid phase Substances 0.000 abstract 3
- 239000012141 concentrate Substances 0.000 abstract 2
- 229920005610 lignin Polymers 0.000 abstract 2
- 239000000463 material Substances 0.000 abstract 2
- 150000007522 mineralic acids Chemical class 0.000 abstract 2
- 239000003960 organic solvent Substances 0.000 abstract 2
- 239000007795 chemical reaction product Substances 0.000 abstract 1
- 238000010908 decantation Methods 0.000 abstract 1
- 239000000047 product Substances 0.000 abstract 1
- 239000007790 solid phase Substances 0.000 abstract 1
- 239000002904 solvent Substances 0.000 abstract 1
- 235000000346 sugar Nutrition 0.000 abstract 1
- 150000008163 sugars Chemical class 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13K—SACCHARIDES OBTAINED FROM NATURAL SOURCES OR BY HYDROLYSIS OF NATURALLY OCCURRING DISACCHARIDES, OLIGOSACCHARIDES OR POLYSACCHARIDES
- C13K1/00—Glucose; Glucose-containing syrups
- C13K1/02—Glucose; Glucose-containing syrups obtained by saccharification of cellulosic materials
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08H—DERIVATIVES OF NATURAL MACROMOLECULAR COMPOUNDS
- C08H8/00—Macromolecular compounds derived from lignocellulosic materials
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21C—PRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
- D21C3/00—Pulping cellulose-containing materials
- D21C3/04—Pulping cellulose-containing materials with acids, acid salts or acid anhydrides
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21C—PRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
- D21C11/00—Regeneration of pulp liquors or effluent waste waters
- D21C11/0007—Recovery of by-products, i.e. compounds other than those necessary for pulping, for multiple uses or not otherwise provided for
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21C—PRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
- D21C3/00—Pulping cellulose-containing materials
- D21C3/20—Pulping cellulose-containing materials with organic solvents or in solvent environment
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21C—PRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
- D21C7/00—Digesters
- D21C7/14—Means for circulating the lye
Landscapes
- Chemical & Material Sciences (AREA)
- Biochemistry (AREA)
- Health & Medical Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Materials Engineering (AREA)
- General Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Emergency Medicine (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
- Furan Compounds (AREA)
- Compounds Of Unknown Constitution (AREA)
- Processing Of Solid Wastes (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
APERFEIçOAMENTOS EM PROCESSO DE HIDRóLISE áCIDA RáPIDA DE MATERIAL LIGNOCELULóSICO E EM REATOR DE HIDRóLISE, dito material lignocelulósico sendo alimentado em diferentes níveis de um reator (10) e contactado com fluxos de solvente orgânico de lignina, água e uma solução extremamente diluída de um ácido inogârnico forte, para obter uma fase líquida de extrato de hidrólise e uma fase sólida de material não reagido e não dissolvido. Um fluxo controlado de vapor é injetado nos diferentes níveis do reator, de modo a prover temperaturas adequadas de solvente orgânico e de ácido inorgânico forte e a formar os produtos (açúcares) desejados. Um fluxo da fase líquida é recirculado em diferentes níveis do reator. O remanescente da fase liquida é retirado do reator, resfriado bruscamente e submetido à evaporação do solvente para obter um concentrado dos produtos de reação, sendo a lignina transferida por decantação e sendo o concentrado transferido a etapas processuais subseqüentes.
Priority Applications (12)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
BRPI0505212-2A BRPI0505212A (pt) | 2005-11-01 | 2005-11-01 | aperfeiçoamentos em processo de hidrólise ácida rápida de material lignocelulósico e em reator de hidrólise |
ARP060104735A AR057564A1 (es) | 2005-11-01 | 2006-10-30 | Proceso de hidrolisis acida rapida de material lignocelulosico y un reactor de hidrolisis |
DE602006007374T DE602006007374D1 (de) | 2005-11-01 | 2006-10-31 | Verbesserung bei einem verfahren zur schnellen sauren hydrolyse von lignocellulosematerial und bei einem hydrolysereaktor |
CN2006800261306A CN101223288B (zh) | 2005-11-01 | 2006-10-31 | 改进的对木质纤维素材料快速酸水解的方法和水解反应器 |
PCT/BR2006/000239 WO2007051269A1 (en) | 2005-11-01 | 2006-10-31 | Improvements in a process for rapid acid hydrolysis of lignocellulosic material and in a hydrolysis reactor |
MX2008005647A MX2008005647A (es) | 2005-11-01 | 2006-10-31 | Mejoras en un procedimiento para hidrolisis acida rapida de material lignocelulosico y en un reactor de hidrolisis. |
US11/916,617 US7988788B2 (en) | 2005-11-01 | 2006-10-31 | Process for rapid acid hydrolysis of lignocellulosic material and in a hydrolysis reactor |
ZA200711049A ZA200711049B (en) | 2005-11-01 | 2006-10-31 | Improvements in a process for rapid acid hydrolysis of lignocellulosic material and in a hydrolysis reactor |
RU2008117424/13A RU2008117424A (ru) | 2005-11-01 | 2006-10-31 | Усовершенствования способа быстрого кислотного гидролиза лигноцеллюлозного материала и реактора гидролиза |
CA002613745A CA2613745A1 (en) | 2005-11-01 | 2006-10-31 | Improvements in a process for rapid acid hydrolysis of lignocellulosic material and in a hydrolysis reactor |
AU2006308733A AU2006308733B2 (en) | 2005-11-01 | 2006-10-31 | Improvements in a process for rapid acid hydrolysis of lignocellulosic material and in a hydrolysis reactor |
EP06804597A EP1945823B1 (en) | 2005-11-01 | 2006-10-31 | Improvements in a process for rapid acid hydrolysis of lignocellulosic material and in a hydrolysis reactor |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
BRPI0505212-2A BRPI0505212A (pt) | 2005-11-01 | 2005-11-01 | aperfeiçoamentos em processo de hidrólise ácida rápida de material lignocelulósico e em reator de hidrólise |
Publications (1)
Publication Number | Publication Date |
---|---|
BRPI0505212A true BRPI0505212A (pt) | 2007-08-07 |
Family
ID=37696763
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
BRPI0505212-2A BRPI0505212A (pt) | 2005-11-01 | 2005-11-01 | aperfeiçoamentos em processo de hidrólise ácida rápida de material lignocelulósico e em reator de hidrólise |
Country Status (12)
Country | Link |
---|---|
US (1) | US7988788B2 (pt) |
EP (1) | EP1945823B1 (pt) |
CN (1) | CN101223288B (pt) |
AR (1) | AR057564A1 (pt) |
AU (1) | AU2006308733B2 (pt) |
BR (1) | BRPI0505212A (pt) |
CA (1) | CA2613745A1 (pt) |
DE (1) | DE602006007374D1 (pt) |
MX (1) | MX2008005647A (pt) |
RU (1) | RU2008117424A (pt) |
WO (1) | WO2007051269A1 (pt) |
ZA (1) | ZA200711049B (pt) |
Families Citing this family (62)
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MY148779A (en) | 2006-05-08 | 2013-05-31 | Vertichem Corp | Integrated processing of plant biomass |
US9260818B2 (en) | 2007-05-23 | 2016-02-16 | Andritz Inc. | Single vessel reactor system for hydrolysis and digestion of wood chips with chemical enhanced wash method |
US8734610B2 (en) * | 2007-05-23 | 2014-05-27 | Andritz Inc. | Two vessel reactor system and method for hydrolysis and digestion of wood chips with chemical enhanced wash method |
CN101121735B (zh) * | 2007-07-06 | 2011-04-06 | 陈培豪 | 植物纤维原料水解液及利用该水解液预处理植物纤维原料的方法 |
DK2185734T3 (da) * | 2007-07-25 | 2011-07-18 | Haarslev As | Fremgangsmåde og apparat til forbehandling af lignocellulosisk materiale |
BRPI0815822A2 (pt) | 2007-08-31 | 2017-05-16 | Biojoule Ltd | lignina e outros produtos a partir de material de planta, e métodos e composições para estes. |
US8057639B2 (en) | 2008-02-28 | 2011-11-15 | Andritz Inc. | System and method for preextraction of hemicellulose through using a continuous prehydrolysis and steam explosion pretreatment process |
US9187571B2 (en) | 2008-04-03 | 2015-11-17 | Cellulose Sciences International, Inc. | Nano-deaggregated cellulose |
WO2009124240A1 (en) * | 2008-04-03 | 2009-10-08 | Cellulose Sciences International, Inc. | Highly disordered cellulose |
US8192549B2 (en) | 2008-06-10 | 2012-06-05 | Andritz Inc. | Apparatus and method for hydrolysis of cellulosic material in a two-step process |
US20090308383A1 (en) | 2008-06-10 | 2009-12-17 | Andritz Inc. | Apparatus and method for hydrolysis of cellulosic material in a multi-step process to produce c5 and c6 sugars using a single vessel |
GB0819406D0 (en) | 2008-10-22 | 2008-11-26 | Weyland As | Process |
US8353989B2 (en) | 2008-11-10 | 2013-01-15 | Andritz Inc. | Apparatus and method for treating, pressing and washing biomass |
US8304213B2 (en) | 2008-12-19 | 2012-11-06 | E I Du Pont De Nemours And Company | Organic solvent pretreatment of biomass to enhance enzymatic saccharification |
US8241873B2 (en) * | 2008-12-19 | 2012-08-14 | E I Du Pont De Nemours And Company | Organic solvent pretreatment of biomass to enhance enzymatic saccharification |
US8216809B2 (en) | 2008-12-19 | 2012-07-10 | E I Du Pont De Nemours And Company | Organic solvent pretreatment of biomass to enhance enzymatic saccharification |
US8278070B2 (en) | 2008-12-19 | 2012-10-02 | E I Du Pont De Nemours And Company | Organic solvent pretreatment of biomass to enhance enzymatic saccharification |
BRPI0916498B1 (pt) | 2008-12-19 | 2019-05-07 | E.I. Du Pont De Nemours And Company | Método para produção de biomassa enriquecida com carboidratos |
US20120329116A1 (en) * | 2009-04-20 | 2012-12-27 | Greenfield Ethanol Inc. | Pretreatment of lignocellulosic biomass through removal of inhibitory compounds |
BRPI1007109A2 (pt) * | 2009-04-20 | 2018-02-20 | Greenfield Ethanol Inc | "pré- tratamento de biomassa lignocelulósica através da remoção de compostos inibitórios" |
GB0907879D0 (en) | 2009-05-07 | 2009-06-24 | Weyland As | Process |
AP2011006029A0 (en) | 2009-05-20 | 2011-12-31 | Xyleco Inc | Processing biomass. |
WO2010135377A1 (en) | 2009-05-20 | 2010-11-25 | Xyleco, Inc. | Bioprocessing |
US8636402B2 (en) | 2009-05-20 | 2014-01-28 | Xyleco, Inc. | Processing biomass |
WO2010135804A1 (en) * | 2009-05-28 | 2010-12-02 | Lignol Innovations Ltd. | Derivatives of native lignin |
US8597431B2 (en) | 2009-10-05 | 2013-12-03 | Andritz (Usa) Inc. | Biomass pretreatment |
WO2011073253A1 (en) | 2009-12-16 | 2011-06-23 | Shell Internationale Research Maatschappij B.V. | Method for producing furfural from lignocellulosic biomass material |
CA2785801A1 (en) | 2010-01-20 | 2011-07-28 | Xyleco, Inc. | Dispersing feedstocks and processing materials |
US8691526B2 (en) | 2010-01-20 | 2014-04-08 | Xyleco, Inc. | Processing materials |
BR112012030819A2 (pt) * | 2010-06-03 | 2018-03-13 | Virdia Ltd | composições de lignina, sistemas e métodos para processar lignina e/ou hcl |
ES2862178T3 (es) | 2010-06-26 | 2021-10-07 | Virdia Llc | Métodos de producción de mezclas de azúcares |
IL206678A0 (en) | 2010-06-28 | 2010-12-30 | Hcl Cleantech Ltd | A method for the production of fermentable sugars |
IL207329A0 (en) | 2010-08-01 | 2010-12-30 | Robert Jansen | A method for refining a recycle extractant and for processing a lignocellulosic material and for the production of a carbohydrate composition |
IL207945A0 (en) | 2010-09-02 | 2010-12-30 | Robert Jansen | Method for the production of carbohydrates |
US20130236392A1 (en) * | 2010-09-03 | 2013-09-12 | Greg Naterer | Thermochemical Reactors and Processes for Hydrolysis of Cupric Chloride |
PT106039A (pt) | 2010-12-09 | 2012-10-26 | Hcl Cleantech Ltd | Processos e sistemas para o processamento de materiais lenhocelulósicos e composições relacionadas |
MY164999A (en) | 2011-02-14 | 2018-02-28 | Xyleco Inc | Processing paper feedstocks |
WO2012137201A1 (en) | 2011-04-07 | 2012-10-11 | Hcl Cleantech Ltd. | Lignocellulose conversion processes and products |
CA2838560A1 (en) * | 2011-07-15 | 2013-01-24 | Frank A. Dottori | Conditioning of biomass for improved c5/c6 sugar release prior to fermentation |
US9228243B2 (en) | 2011-08-24 | 2016-01-05 | Red Shield Acquistion, LLC | System and method for conditioning a hardwood pulp liquid hydrolysate |
WO2013055785A1 (en) | 2011-10-10 | 2013-04-18 | Virdia Ltd | Sugar compositions |
GB2496001A (en) * | 2011-10-24 | 2013-05-01 | Virdia Ltd | Hydrolysis systems and methods |
US9493851B2 (en) | 2012-05-03 | 2016-11-15 | Virdia, Inc. | Methods for treating lignocellulosic materials |
CA2872510C (en) | 2012-05-03 | 2019-12-24 | Virdia Ltd | Methods for treating lignocellulosic materials |
CN102816877A (zh) * | 2012-08-29 | 2012-12-12 | 上海交通大学 | 一种纤维素类生物质水热糖化方法及装置 |
US9657146B2 (en) | 2013-03-14 | 2017-05-23 | Virdia, Inc. | Methods for treating lignocellulosic materials |
US9255187B2 (en) * | 2013-03-15 | 2016-02-09 | Synergy Horizon Limited | Method for production of dry hydrolytic lignin |
JP6666242B2 (ja) | 2013-05-03 | 2020-03-13 | ヴァーディア, インコーポレイテッド | リグノセルロース系材料処理の方法 |
KR20160007537A (ko) | 2013-05-03 | 2016-01-20 | 버디아, 인크. | 열안정성 리그닌 분획물의 제조 방법 |
EP4477306A3 (en) | 2014-05-01 | 2024-12-25 | Renmatix, Inc. | Upgrading lignin from lignin-containing residues through reactive extraction |
JP6687594B2 (ja) | 2014-07-09 | 2020-04-22 | ヴァーディア, インコーポレイテッド | 黒液からリグニンを分離および精製する方法ならびにその組成物 |
WO2016112134A1 (en) | 2015-01-07 | 2016-07-14 | Virdia, Inc. | Methods for extracting and converting hemicellulose sugars |
US11091815B2 (en) | 2015-05-27 | 2021-08-17 | Virdia, Llc | Integrated methods for treating lignocellulosic material |
US11365454B2 (en) | 2017-09-26 | 2022-06-21 | Poet Research, Inc. | Systems and methods for processing lignocellulosic biomass |
WO2020112701A1 (en) | 2018-11-26 | 2020-06-04 | Board Of Trustees Of Michigan State University | Methods for cellulose hydrolysis using sulfonated polyaromatic catalysts |
SE542991C2 (en) * | 2019-03-29 | 2020-09-22 | Valmet Oy | A method and a system for extracting hydrolyzate in a continuous cooking process for producing pulp |
CN110541320B (zh) * | 2019-09-12 | 2021-12-17 | 武汉轻工大学 | 从木质纤维素原料中分离木质素和纤维素的方法 |
CN113304671B (zh) * | 2021-05-28 | 2022-02-01 | 江西海尔思药业股份有限公司 | 一种含乳果糖的口服溶液制备用装置及其使用方法 |
LU102852B1 (en) * | 2021-08-02 | 2023-02-02 | Technische Univ Hamburg | Process for continuous extraction of lignocellulosic material |
KR20240035817A (ko) * | 2021-08-02 | 2024-03-18 | 머쉬랩스 게엠베하 | 리그노셀룰로오스 재료의 연속 추출 방법 |
CN114029022B (zh) * | 2021-12-01 | 2023-05-16 | 合肥智慧环境研究院 | 一种木质素分离系统及其方法 |
TW202338080A (zh) | 2022-02-24 | 2023-10-01 | 德商菌絲科技有限公司 | 有色真菌菌絲體之生產 |
Family Cites Families (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
AR227462A1 (es) | 1981-03-26 | 1982-10-29 | Thermoform Bau Forschung | Procedimiento mejorado para la produccion de hidrolizados de carbohidratos a partir de material celulosico triturado |
CA1225636A (en) * | 1984-07-13 | 1987-08-18 | Robert P. Chang | Method for continuous countercurrent organosolv saccharification of wood and other lignocellulosic materials |
BR9600672A (pt) * | 1996-03-08 | 1997-12-30 | Dedini S A Administracao E Par | Processo de hidrólise ácido de material lignocelulósico e reator de hidrólise |
-
2005
- 2005-11-01 BR BRPI0505212-2A patent/BRPI0505212A/pt not_active IP Right Cessation
-
2006
- 2006-10-30 AR ARP060104735A patent/AR057564A1/es unknown
- 2006-10-31 MX MX2008005647A patent/MX2008005647A/es unknown
- 2006-10-31 DE DE602006007374T patent/DE602006007374D1/de active Active
- 2006-10-31 EP EP06804597A patent/EP1945823B1/en not_active Expired - Fee Related
- 2006-10-31 AU AU2006308733A patent/AU2006308733B2/en not_active Expired - Fee Related
- 2006-10-31 RU RU2008117424/13A patent/RU2008117424A/ru not_active Application Discontinuation
- 2006-10-31 WO PCT/BR2006/000239 patent/WO2007051269A1/en active Application Filing
- 2006-10-31 CA CA002613745A patent/CA2613745A1/en not_active Abandoned
- 2006-10-31 US US11/916,617 patent/US7988788B2/en not_active Expired - Fee Related
- 2006-10-31 ZA ZA200711049A patent/ZA200711049B/xx unknown
- 2006-10-31 CN CN2006800261306A patent/CN101223288B/zh not_active Expired - Fee Related
Also Published As
Publication number | Publication date |
---|---|
EP1945823B1 (en) | 2009-06-17 |
DE602006007374D1 (de) | 2009-07-30 |
AU2006308733A1 (en) | 2007-05-10 |
US20080202504A1 (en) | 2008-08-28 |
AU2006308733B2 (en) | 2011-02-03 |
RU2008117424A (ru) | 2009-11-20 |
WO2007051269A1 (en) | 2007-05-10 |
CN101223288B (zh) | 2011-12-14 |
EP1945823A1 (en) | 2008-07-23 |
US7988788B2 (en) | 2011-08-02 |
MX2008005647A (es) | 2008-10-03 |
ZA200711049B (en) | 2009-04-29 |
AR057564A1 (es) | 2007-12-05 |
CA2613745A1 (en) | 2007-05-10 |
CN101223288A (zh) | 2008-07-16 |
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Legal Events
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B06F | Objections, documents and/or translations needed after an examination request according [chapter 6.6 patent gazette] | ||
B06A | Patent application procedure suspended [chapter 6.1 patent gazette] | ||
B08F | Application dismissed because of non-payment of annual fees [chapter 8.6 patent gazette] |
Free format text: REFERENTE A 10A ANUIDADE. |
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