[go: up one dir, main page]

BRPI0505212A - aperfeiçoamentos em processo de hidrólise ácida rápida de material lignocelulósico e em reator de hidrólise - Google Patents

aperfeiçoamentos em processo de hidrólise ácida rápida de material lignocelulósico e em reator de hidrólise

Info

Publication number
BRPI0505212A
BRPI0505212A BRPI0505212-2A BRPI0505212A BRPI0505212A BR PI0505212 A BRPI0505212 A BR PI0505212A BR PI0505212 A BRPI0505212 A BR PI0505212A BR PI0505212 A BRPI0505212 A BR PI0505212A
Authority
BR
Brazil
Prior art keywords
reactor
hydrolysis
liquid phase
levels
lignocellulosic material
Prior art date
Application number
BRPI0505212-2A
Other languages
English (en)
Inventor
Antonio Geraldo Proenca Hilst
Original Assignee
Dedini Sa Ind De Base
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Dedini Sa Ind De Base filed Critical Dedini Sa Ind De Base
Priority to BRPI0505212-2A priority Critical patent/BRPI0505212A/pt
Priority to ARP060104735A priority patent/AR057564A1/es
Priority to DE602006007374T priority patent/DE602006007374D1/de
Priority to CN2006800261306A priority patent/CN101223288B/zh
Priority to PCT/BR2006/000239 priority patent/WO2007051269A1/en
Priority to MX2008005647A priority patent/MX2008005647A/es
Priority to US11/916,617 priority patent/US7988788B2/en
Priority to ZA200711049A priority patent/ZA200711049B/xx
Priority to RU2008117424/13A priority patent/RU2008117424A/ru
Priority to CA002613745A priority patent/CA2613745A1/en
Priority to AU2006308733A priority patent/AU2006308733B2/en
Priority to EP06804597A priority patent/EP1945823B1/en
Publication of BRPI0505212A publication Critical patent/BRPI0505212A/pt

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C13SUGAR INDUSTRY
    • C13KSACCHARIDES OBTAINED FROM NATURAL SOURCES OR BY HYDROLYSIS OF NATURALLY OCCURRING DISACCHARIDES, OLIGOSACCHARIDES OR POLYSACCHARIDES
    • C13K1/00Glucose; Glucose-containing syrups
    • C13K1/02Glucose; Glucose-containing syrups obtained by saccharification of cellulosic materials
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08HDERIVATIVES OF NATURAL MACROMOLECULAR COMPOUNDS
    • C08H8/00Macromolecular compounds derived from lignocellulosic materials
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21CPRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
    • D21C3/00Pulping cellulose-containing materials
    • D21C3/04Pulping cellulose-containing materials with acids, acid salts or acid anhydrides
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21CPRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
    • D21C11/00Regeneration of pulp liquors or effluent waste waters
    • D21C11/0007Recovery of by-products, i.e. compounds other than those necessary for pulping, for multiple uses or not otherwise provided for
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21CPRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
    • D21C3/00Pulping cellulose-containing materials
    • D21C3/20Pulping cellulose-containing materials with organic solvents or in solvent environment
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21CPRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
    • D21C7/00Digesters
    • D21C7/14Means for circulating the lye

Landscapes

  • Chemical & Material Sciences (AREA)
  • Biochemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Materials Engineering (AREA)
  • General Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Emergency Medicine (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Polysaccharides And Polysaccharide Derivatives (AREA)
  • Furan Compounds (AREA)
  • Compounds Of Unknown Constitution (AREA)
  • Processing Of Solid Wastes (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

APERFEIçOAMENTOS EM PROCESSO DE HIDRóLISE áCIDA RáPIDA DE MATERIAL LIGNOCELULóSICO E EM REATOR DE HIDRóLISE, dito material lignocelulósico sendo alimentado em diferentes níveis de um reator (10) e contactado com fluxos de solvente orgânico de lignina, água e uma solução extremamente diluída de um ácido inogârnico forte, para obter uma fase líquida de extrato de hidrólise e uma fase sólida de material não reagido e não dissolvido. Um fluxo controlado de vapor é injetado nos diferentes níveis do reator, de modo a prover temperaturas adequadas de solvente orgânico e de ácido inorgânico forte e a formar os produtos (açúcares) desejados. Um fluxo da fase líquida é recirculado em diferentes níveis do reator. O remanescente da fase liquida é retirado do reator, resfriado bruscamente e submetido à evaporação do solvente para obter um concentrado dos produtos de reação, sendo a lignina transferida por decantação e sendo o concentrado transferido a etapas processuais subseqüentes.
BRPI0505212-2A 2005-11-01 2005-11-01 aperfeiçoamentos em processo de hidrólise ácida rápida de material lignocelulósico e em reator de hidrólise BRPI0505212A (pt)

Priority Applications (12)

Application Number Priority Date Filing Date Title
BRPI0505212-2A BRPI0505212A (pt) 2005-11-01 2005-11-01 aperfeiçoamentos em processo de hidrólise ácida rápida de material lignocelulósico e em reator de hidrólise
ARP060104735A AR057564A1 (es) 2005-11-01 2006-10-30 Proceso de hidrolisis acida rapida de material lignocelulosico y un reactor de hidrolisis
DE602006007374T DE602006007374D1 (de) 2005-11-01 2006-10-31 Verbesserung bei einem verfahren zur schnellen sauren hydrolyse von lignocellulosematerial und bei einem hydrolysereaktor
CN2006800261306A CN101223288B (zh) 2005-11-01 2006-10-31 改进的对木质纤维素材料快速酸水解的方法和水解反应器
PCT/BR2006/000239 WO2007051269A1 (en) 2005-11-01 2006-10-31 Improvements in a process for rapid acid hydrolysis of lignocellulosic material and in a hydrolysis reactor
MX2008005647A MX2008005647A (es) 2005-11-01 2006-10-31 Mejoras en un procedimiento para hidrolisis acida rapida de material lignocelulosico y en un reactor de hidrolisis.
US11/916,617 US7988788B2 (en) 2005-11-01 2006-10-31 Process for rapid acid hydrolysis of lignocellulosic material and in a hydrolysis reactor
ZA200711049A ZA200711049B (en) 2005-11-01 2006-10-31 Improvements in a process for rapid acid hydrolysis of lignocellulosic material and in a hydrolysis reactor
RU2008117424/13A RU2008117424A (ru) 2005-11-01 2006-10-31 Усовершенствования способа быстрого кислотного гидролиза лигноцеллюлозного материала и реактора гидролиза
CA002613745A CA2613745A1 (en) 2005-11-01 2006-10-31 Improvements in a process for rapid acid hydrolysis of lignocellulosic material and in a hydrolysis reactor
AU2006308733A AU2006308733B2 (en) 2005-11-01 2006-10-31 Improvements in a process for rapid acid hydrolysis of lignocellulosic material and in a hydrolysis reactor
EP06804597A EP1945823B1 (en) 2005-11-01 2006-10-31 Improvements in a process for rapid acid hydrolysis of lignocellulosic material and in a hydrolysis reactor

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
BRPI0505212-2A BRPI0505212A (pt) 2005-11-01 2005-11-01 aperfeiçoamentos em processo de hidrólise ácida rápida de material lignocelulósico e em reator de hidrólise

Publications (1)

Publication Number Publication Date
BRPI0505212A true BRPI0505212A (pt) 2007-08-07

Family

ID=37696763

Family Applications (1)

Application Number Title Priority Date Filing Date
BRPI0505212-2A BRPI0505212A (pt) 2005-11-01 2005-11-01 aperfeiçoamentos em processo de hidrólise ácida rápida de material lignocelulósico e em reator de hidrólise

Country Status (12)

Country Link
US (1) US7988788B2 (pt)
EP (1) EP1945823B1 (pt)
CN (1) CN101223288B (pt)
AR (1) AR057564A1 (pt)
AU (1) AU2006308733B2 (pt)
BR (1) BRPI0505212A (pt)
CA (1) CA2613745A1 (pt)
DE (1) DE602006007374D1 (pt)
MX (1) MX2008005647A (pt)
RU (1) RU2008117424A (pt)
WO (1) WO2007051269A1 (pt)
ZA (1) ZA200711049B (pt)

Families Citing this family (62)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
MY148779A (en) 2006-05-08 2013-05-31 Vertichem Corp Integrated processing of plant biomass
US9260818B2 (en) 2007-05-23 2016-02-16 Andritz Inc. Single vessel reactor system for hydrolysis and digestion of wood chips with chemical enhanced wash method
US8734610B2 (en) * 2007-05-23 2014-05-27 Andritz Inc. Two vessel reactor system and method for hydrolysis and digestion of wood chips with chemical enhanced wash method
CN101121735B (zh) * 2007-07-06 2011-04-06 陈培豪 植物纤维原料水解液及利用该水解液预处理植物纤维原料的方法
DK2185734T3 (da) * 2007-07-25 2011-07-18 Haarslev As Fremgangsmåde og apparat til forbehandling af lignocellulosisk materiale
BRPI0815822A2 (pt) 2007-08-31 2017-05-16 Biojoule Ltd lignina e outros produtos a partir de material de planta, e métodos e composições para estes.
US8057639B2 (en) 2008-02-28 2011-11-15 Andritz Inc. System and method for preextraction of hemicellulose through using a continuous prehydrolysis and steam explosion pretreatment process
US9187571B2 (en) 2008-04-03 2015-11-17 Cellulose Sciences International, Inc. Nano-deaggregated cellulose
WO2009124240A1 (en) * 2008-04-03 2009-10-08 Cellulose Sciences International, Inc. Highly disordered cellulose
US8192549B2 (en) 2008-06-10 2012-06-05 Andritz Inc. Apparatus and method for hydrolysis of cellulosic material in a two-step process
US20090308383A1 (en) 2008-06-10 2009-12-17 Andritz Inc. Apparatus and method for hydrolysis of cellulosic material in a multi-step process to produce c5 and c6 sugars using a single vessel
GB0819406D0 (en) 2008-10-22 2008-11-26 Weyland As Process
US8353989B2 (en) 2008-11-10 2013-01-15 Andritz Inc. Apparatus and method for treating, pressing and washing biomass
US8304213B2 (en) 2008-12-19 2012-11-06 E I Du Pont De Nemours And Company Organic solvent pretreatment of biomass to enhance enzymatic saccharification
US8241873B2 (en) * 2008-12-19 2012-08-14 E I Du Pont De Nemours And Company Organic solvent pretreatment of biomass to enhance enzymatic saccharification
US8216809B2 (en) 2008-12-19 2012-07-10 E I Du Pont De Nemours And Company Organic solvent pretreatment of biomass to enhance enzymatic saccharification
US8278070B2 (en) 2008-12-19 2012-10-02 E I Du Pont De Nemours And Company Organic solvent pretreatment of biomass to enhance enzymatic saccharification
BRPI0916498B1 (pt) 2008-12-19 2019-05-07 E.I. Du Pont De Nemours And Company Método para produção de biomassa enriquecida com carboidratos
US20120329116A1 (en) * 2009-04-20 2012-12-27 Greenfield Ethanol Inc. Pretreatment of lignocellulosic biomass through removal of inhibitory compounds
BRPI1007109A2 (pt) * 2009-04-20 2018-02-20 Greenfield Ethanol Inc "pré- tratamento de biomassa lignocelulósica através da remoção de compostos inibitórios"
GB0907879D0 (en) 2009-05-07 2009-06-24 Weyland As Process
AP2011006029A0 (en) 2009-05-20 2011-12-31 Xyleco Inc Processing biomass.
WO2010135377A1 (en) 2009-05-20 2010-11-25 Xyleco, Inc. Bioprocessing
US8636402B2 (en) 2009-05-20 2014-01-28 Xyleco, Inc. Processing biomass
WO2010135804A1 (en) * 2009-05-28 2010-12-02 Lignol Innovations Ltd. Derivatives of native lignin
US8597431B2 (en) 2009-10-05 2013-12-03 Andritz (Usa) Inc. Biomass pretreatment
WO2011073253A1 (en) 2009-12-16 2011-06-23 Shell Internationale Research Maatschappij B.V. Method for producing furfural from lignocellulosic biomass material
CA2785801A1 (en) 2010-01-20 2011-07-28 Xyleco, Inc. Dispersing feedstocks and processing materials
US8691526B2 (en) 2010-01-20 2014-04-08 Xyleco, Inc. Processing materials
BR112012030819A2 (pt) * 2010-06-03 2018-03-13 Virdia Ltd composições de lignina, sistemas e métodos para processar lignina e/ou hcl
ES2862178T3 (es) 2010-06-26 2021-10-07 Virdia Llc Métodos de producción de mezclas de azúcares
IL206678A0 (en) 2010-06-28 2010-12-30 Hcl Cleantech Ltd A method for the production of fermentable sugars
IL207329A0 (en) 2010-08-01 2010-12-30 Robert Jansen A method for refining a recycle extractant and for processing a lignocellulosic material and for the production of a carbohydrate composition
IL207945A0 (en) 2010-09-02 2010-12-30 Robert Jansen Method for the production of carbohydrates
US20130236392A1 (en) * 2010-09-03 2013-09-12 Greg Naterer Thermochemical Reactors and Processes for Hydrolysis of Cupric Chloride
PT106039A (pt) 2010-12-09 2012-10-26 Hcl Cleantech Ltd Processos e sistemas para o processamento de materiais lenhocelulósicos e composições relacionadas
MY164999A (en) 2011-02-14 2018-02-28 Xyleco Inc Processing paper feedstocks
WO2012137201A1 (en) 2011-04-07 2012-10-11 Hcl Cleantech Ltd. Lignocellulose conversion processes and products
CA2838560A1 (en) * 2011-07-15 2013-01-24 Frank A. Dottori Conditioning of biomass for improved c5/c6 sugar release prior to fermentation
US9228243B2 (en) 2011-08-24 2016-01-05 Red Shield Acquistion, LLC System and method for conditioning a hardwood pulp liquid hydrolysate
WO2013055785A1 (en) 2011-10-10 2013-04-18 Virdia Ltd Sugar compositions
GB2496001A (en) * 2011-10-24 2013-05-01 Virdia Ltd Hydrolysis systems and methods
US9493851B2 (en) 2012-05-03 2016-11-15 Virdia, Inc. Methods for treating lignocellulosic materials
CA2872510C (en) 2012-05-03 2019-12-24 Virdia Ltd Methods for treating lignocellulosic materials
CN102816877A (zh) * 2012-08-29 2012-12-12 上海交通大学 一种纤维素类生物质水热糖化方法及装置
US9657146B2 (en) 2013-03-14 2017-05-23 Virdia, Inc. Methods for treating lignocellulosic materials
US9255187B2 (en) * 2013-03-15 2016-02-09 Synergy Horizon Limited Method for production of dry hydrolytic lignin
JP6666242B2 (ja) 2013-05-03 2020-03-13 ヴァーディア, インコーポレイテッド リグノセルロース系材料処理の方法
KR20160007537A (ko) 2013-05-03 2016-01-20 버디아, 인크. 열안정성 리그닌 분획물의 제조 방법
EP4477306A3 (en) 2014-05-01 2024-12-25 Renmatix, Inc. Upgrading lignin from lignin-containing residues through reactive extraction
JP6687594B2 (ja) 2014-07-09 2020-04-22 ヴァーディア, インコーポレイテッド 黒液からリグニンを分離および精製する方法ならびにその組成物
WO2016112134A1 (en) 2015-01-07 2016-07-14 Virdia, Inc. Methods for extracting and converting hemicellulose sugars
US11091815B2 (en) 2015-05-27 2021-08-17 Virdia, Llc Integrated methods for treating lignocellulosic material
US11365454B2 (en) 2017-09-26 2022-06-21 Poet Research, Inc. Systems and methods for processing lignocellulosic biomass
WO2020112701A1 (en) 2018-11-26 2020-06-04 Board Of Trustees Of Michigan State University Methods for cellulose hydrolysis using sulfonated polyaromatic catalysts
SE542991C2 (en) * 2019-03-29 2020-09-22 Valmet Oy A method and a system for extracting hydrolyzate in a continuous cooking process for producing pulp
CN110541320B (zh) * 2019-09-12 2021-12-17 武汉轻工大学 从木质纤维素原料中分离木质素和纤维素的方法
CN113304671B (zh) * 2021-05-28 2022-02-01 江西海尔思药业股份有限公司 一种含乳果糖的口服溶液制备用装置及其使用方法
LU102852B1 (en) * 2021-08-02 2023-02-02 Technische Univ Hamburg Process for continuous extraction of lignocellulosic material
KR20240035817A (ko) * 2021-08-02 2024-03-18 머쉬랩스 게엠베하 리그노셀룰로오스 재료의 연속 추출 방법
CN114029022B (zh) * 2021-12-01 2023-05-16 合肥智慧环境研究院 一种木质素分离系统及其方法
TW202338080A (zh) 2022-02-24 2023-10-01 德商菌絲科技有限公司 有色真菌菌絲體之生產

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
AR227462A1 (es) 1981-03-26 1982-10-29 Thermoform Bau Forschung Procedimiento mejorado para la produccion de hidrolizados de carbohidratos a partir de material celulosico triturado
CA1225636A (en) * 1984-07-13 1987-08-18 Robert P. Chang Method for continuous countercurrent organosolv saccharification of wood and other lignocellulosic materials
BR9600672A (pt) * 1996-03-08 1997-12-30 Dedini S A Administracao E Par Processo de hidrólise ácido de material lignocelulósico e reator de hidrólise

Also Published As

Publication number Publication date
EP1945823B1 (en) 2009-06-17
DE602006007374D1 (de) 2009-07-30
AU2006308733A1 (en) 2007-05-10
US20080202504A1 (en) 2008-08-28
AU2006308733B2 (en) 2011-02-03
RU2008117424A (ru) 2009-11-20
WO2007051269A1 (en) 2007-05-10
CN101223288B (zh) 2011-12-14
EP1945823A1 (en) 2008-07-23
US7988788B2 (en) 2011-08-02
MX2008005647A (es) 2008-10-03
ZA200711049B (en) 2009-04-29
AR057564A1 (es) 2007-12-05
CA2613745A1 (en) 2007-05-10
CN101223288A (zh) 2008-07-16

Similar Documents

Publication Publication Date Title
BRPI0505212A (pt) aperfeiçoamentos em processo de hidrólise ácida rápida de material lignocelulósico e em reator de hidrólise
Zhang et al. Transforming lignocellulosic biomass into biofuels enabled by ionic liquid pretreatment
Huang et al. Facilitating enzymatic hydrolysis with a novel guaiacol-based deep eutectic solvent pretreatment
Mellmer et al. Effects of γ-valerolactone in hydrolysis of lignocellulosic biomass to monosaccharides
Hou et al. Pretreatment of lignocellulosic biomass with ionic liquids and ionic liquid-based solvent systems
BR112021023121A2 (pt) Processo para tratamento de biomassa
Liu et al. The effect of flow rate of compressed hot water on xylan, lignin, and total mass removal from corn stover
BR112015015524A2 (pt) processo para fracionamento de biomassa lignocelulósica
BR112013024183A2 (pt) estrutura de folha termoplástica e artigos formados a partir desta
BRPI0500534A (pt) processo de hidrólise ácida de materiais celulósicos e lignocelulósicos, vaso de digestão e reator de hidrólise
BR112016000954A8 (pt) processo para fracionamento da biomassa lignocelulósica; líquor, polpa ou hidrolisado enzimático de organossolve; e uso de um líquido de tratamento para fracionamento de biomasssa lignocelulósica
Mok et al. Uncatalyzed solvolysis of whole biomass hemicellulose by hot compressed liquid water
Qian et al. Ab initio molecular dynamics simulations of β-D-glucose and β-D-xylose degradation mechanisms in acidic aqueous solution
Ingram et al. Comparison of different pretreatment methods for lignocellulosic materials. Part I: Conversion of rye straw to valuable products
Xu et al. Enhanced production of glucose and xylose with partial dissolution of corn stover in ionic liquid, 1-ethyl-3-methylimidazolium acetate
BR112015029688A2 (pt) processo para fracionamento da biomassa lignocelulósica em celulose, hemicelulose e lignina
BR112012007026A2 (pt) método e sistema para fracionamento de biomassa lignocelulósica
Liu et al. Periodic peristalsis enhancing the high solids enzymatic hydrolysis performance of steam exploded corn stover biomass
Wang et al. Exploration of the interaction mechanism of lignocellulosic hybrid systems based on deep eutectic solvents
BR112014014415A2 (pt) processo para produção de produto de degradação de lignina
BRPI0906378A8 (pt) Processo para produzir bioetanol a partir de uma matéria-prima vegetal lignocelulósica
BR112015014411A2 (pt) processo para fracionar biomassa lignocelulósica
BR112015015589A2 (pt) processo para produzir celulose purificada
BRPI0919856A2 (pt) processo para a produção de álcool
Lamminpää et al. Acid-catalysed xylose dehydration into furfural in the presence of kraft lignin

Legal Events

Date Code Title Description
B06F Objections, documents and/or translations needed after an examination request according [chapter 6.6 patent gazette]
B06A Patent application procedure suspended [chapter 6.1 patent gazette]
B08F Application dismissed because of non-payment of annual fees [chapter 8.6 patent gazette]

Free format text: REFERENTE A 10A ANUIDADE.

B08K Patent lapsed as no evidence of payment of the annual fee has been furnished to inpi [chapter 8.11 patent gazette]

Free format text: EM VIRTUDE DO ARQUIVAMENTO PUBLICADO NA RPI 2331 DE 08-09-2015 E CONSIDERANDO AUSENCIA DE MANIFESTACAO DENTRO DOS PRAZOS LEGAIS, INFORMO QUE CABE SER MANTIDO O ARQUIVAMENTO DO PEDIDO DE PATENTE, CONFORME O DISPOSTO NO ARTIGO 12, DA RESOLUCAO 113/2013.