[go: up one dir, main page]

BR9503835A - Process for removing impurities from the melting silicon - Google Patents

Process for removing impurities from the melting silicon

Info

Publication number
BR9503835A
BR9503835A BR9503835A BR9503835A BR9503835A BR 9503835 A BR9503835 A BR 9503835A BR 9503835 A BR9503835 A BR 9503835A BR 9503835 A BR9503835 A BR 9503835A BR 9503835 A BR9503835 A BR 9503835A
Authority
BR
Brazil
Prior art keywords
molten silicon
removing impurities
slag
silicon
continuously
Prior art date
Application number
BR9503835A
Other languages
Portuguese (pt)
Inventor
Anders Schei
Original Assignee
Elkem As
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Elkem As filed Critical Elkem As
Publication of BR9503835A publication Critical patent/BR9503835A/en

Links

Classifications

    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01LSEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
    • H01L21/00Processes or apparatus adapted for the manufacture or treatment of semiconductor or solid state devices or of parts thereof
    • H01L21/02Manufacture or treatment of semiconductor devices or of parts thereof
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00Silicon; Compounds thereof
    • C01B33/02Silicon
    • C01B33/037Purification

Landscapes

  • Organic Chemistry (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Inorganic Chemistry (AREA)
  • General Physics & Mathematics (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • Physics & Mathematics (AREA)
  • Manufacturing & Machinery (AREA)
  • Computer Hardware Design (AREA)
  • Microelectronics & Electronic Packaging (AREA)
  • Power Engineering (AREA)
  • Silicon Compounds (AREA)
  • Crystals, And After-Treatments Of Crystals (AREA)
  • Mechanical Treatment Of Semiconductor (AREA)

Abstract

The present invention relates to a process for removing impurities from molten silicon by treatment of molten silicon (4) contained in a vessel (2) with a slag (5) having the capability of removing the impurities, particularly boron, from molten silicon. The slag (5) is continuously or substantially continuously added to the molten silicon (4) and then continuously or substantially continuously inactivated or removed from the silicon melt (4) as soon as equilibrium between the slag (6) and molten silicon (4) is reached with respect to the impurity elements or element to be removed. <MATH>
BR9503835A 1994-09-01 1995-08-29 Process for removing impurities from the melting silicon BR9503835A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
NO943227A NO180532C (en) 1994-09-01 1994-09-01 Process for removing contaminants from molten silicon

Publications (1)

Publication Number Publication Date
BR9503835A true BR9503835A (en) 1996-09-10

Family

ID=19897360

Family Applications (1)

Application Number Title Priority Date Filing Date
BR9503835A BR9503835A (en) 1994-09-01 1995-08-29 Process for removing impurities from the melting silicon

Country Status (16)

Country Link
US (1) US5788945A (en)
EP (1) EP0699625B1 (en)
JP (1) JP2851257B2 (en)
KR (1) KR0178071B1 (en)
CN (1) CN1042821C (en)
AT (1) ATE178031T1 (en)
AU (1) AU682277B2 (en)
BR (1) BR9503835A (en)
DE (1) DE69508498T2 (en)
DK (1) DK0699625T3 (en)
ES (1) ES2130535T3 (en)
FI (1) FI114092B (en)
GR (1) GR3030154T3 (en)
NO (1) NO180532C (en)
RU (1) RU2098354C1 (en)
ZA (1) ZA956186B (en)

Families Citing this family (36)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6368403B1 (en) * 1997-08-28 2002-04-09 Crystal Systems, Inc. Method and apparatus for purifying silicon
NO316020B1 (en) * 2001-10-10 2003-12-01 Elkem Materials Device for continuous slag treatment of silicon
AU2003208106A1 (en) * 2002-02-04 2003-09-02 Sharp Kabushiki Kaisha Silicon purifying method, slag for purifying silicon, and purified silicon
NO318092B1 (en) * 2002-05-22 2005-01-31 Elkem Materials Calcium-silicate-based slag, process for the preparation of calcium-silicate-based slag, and application for slag treatment of molten silicon
JP4354265B2 (en) * 2003-12-11 2009-10-28 新日鉄マテリアルズ株式会社 Slag separation method in silicon refining
NO333319B1 (en) * 2003-12-29 2013-05-06 Elkem As Silicon material for the production of solar cells
JP4766837B2 (en) * 2004-03-03 2011-09-07 新日鉄マテリアルズ株式会社 Method for removing boron from silicon
JP4632769B2 (en) 2004-12-09 2011-02-16 シャープ株式会社 Silicon purification method
JP4782428B2 (en) * 2005-01-11 2011-09-28 新日鉄マテリアルズ株式会社 Silicon refining method
JP4511957B2 (en) * 2005-01-24 2010-07-28 新日鉄マテリアルズ株式会社 Silicon refining method
JP4966560B2 (en) * 2005-03-07 2012-07-04 新日鉄マテリアルズ株式会社 Manufacturing method of high purity silicon
JP5140835B2 (en) * 2005-03-07 2013-02-13 新日鉄住金マテリアルズ株式会社 Manufacturing method of high purity silicon
JP4689373B2 (en) * 2005-07-04 2011-05-25 シャープ株式会社 How to reuse silicon
JP4671872B2 (en) * 2006-01-18 2011-04-20 新日鉄マテリアルズ株式会社 Silicon refining method
US7820126B2 (en) * 2006-08-18 2010-10-26 Iosil Energy Corporation Method and apparatus for improving the efficiency of purification and deposition of polycrystalline silicon
UA97488C2 (en) * 2006-09-14 2012-02-27 Силисиум Беканкур Инк. Process for purifying of low-purity silicon material, use of rotary drum furnace in it, melt of silicon material, off-gases and solid polycrystalline silicon produced by the process
CN101868422B (en) * 2007-09-13 2013-10-09 费罗索勒硅业公司 Process for producing medium and high purity silicon from metallurgical grade silicon
SG10201402045WA (en) * 2008-04-11 2014-10-30 Iosil Energy Corp Methods And Apparatus For Recovery Of Silicon And Silicon Carbide From Spent Wafer-Sawing Slurry
US20110305619A1 (en) * 2008-05-27 2011-12-15 Spawnt Private S.A.R.L Silicon Containing Halogenide, Method for Producing the Same, and Use of the Same
DE102008036143A1 (en) 2008-08-01 2010-02-04 Berlinsolar Gmbh Process for removing nonmetallic impurities from metallurgical silicon
US8329133B2 (en) * 2008-11-03 2012-12-11 Gt Crystal Systems, Llc Method and apparatus for refining metallurgical grade silicon to produce solar grade silicon
WO2010056350A2 (en) * 2008-11-14 2010-05-20 Carnegie Mellon University Methods for casting by a float process and associated appratuses
NO330928B1 (en) * 2009-01-13 2011-08-22 Elkem Solar As Apparatus and method for the treatment of immiscible liquids
IT1394029B1 (en) 2009-05-12 2012-05-25 Raysolar S R L METHOD FOR THE PURIFICATION OF SILICON AND APPARATUS WITH WHICH TO REALIZE IT
CN101955186A (en) * 2010-09-19 2011-01-26 江西盛丰新能源科技有限公司 Method for preparing polycrystalline silicon by physically removing boron
KR101222175B1 (en) * 2011-03-31 2013-01-14 연세대학교 산학협력단 Refining method of impurities from MG-Si by utilizing the density difference between molten Si and reducing slags
CN103011169B (en) * 2012-12-14 2014-05-07 厦门大学 A kind of preparation method of sheet silicon
NO339608B1 (en) 2013-09-09 2017-01-09 Elkem Solar As Multicrystalline silicon ginger, silicon master alloy, process for increasing the yield of multicrystalline silicon ginger for solar cells
CN103754882B (en) * 2013-12-27 2015-07-08 福建兴朝阳硅材料股份有限公司 Purifying method of slag-making agent with boron removal
RU2600055C1 (en) * 2015-05-26 2016-10-20 Общество с ограниченной ответственностью "Современные химические и металлургические технологии" (ООО "СХИМТ") Method and device for refining technical silicon
CN105063749B (en) * 2015-06-08 2017-07-18 朱超 A kind of method for preparing high-purity polycrystalline silicon
GB201621609D0 (en) * 2016-12-19 2017-02-01 Norwegian Univ Of Science And Tech (Ntnu) Process for the production of commercial grade silicon
TWI640473B (en) 2017-12-07 2018-11-11 財團法人工業技術研究院 Method and apparatus for removing boron
WO2020192870A1 (en) * 2019-03-22 2020-10-01 Wacker Chemie Ag Method for producing technical silicon
WO2020192913A1 (en) * 2019-03-27 2020-10-01 Wacker Chemie Ag Method for producing technical silicon
CN113748086B (en) * 2019-04-30 2024-02-06 瓦克化学股份公司 Method for refining crude silicon melt using particulate media

Family Cites Families (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
IT1100218B (en) * 1978-11-09 1985-09-28 Montedison Spa SILICON PURIFICATION PROCEDURE
US4247528A (en) * 1979-04-11 1981-01-27 Dow Corning Corporation Method for producing solar-cell-grade silicon
US4312848A (en) * 1979-05-24 1982-01-26 Aluminum Company Of America Boron removal in silicon purification
DE2945072A1 (en) * 1979-11-08 1981-06-04 Heliotronic Forschungs- und Entwicklungsgesellschaft für Solarzellen-Grundstoffe mbH, 8263 Burghausen METHOD FOR CLEANING RAW SILICON
US4388286A (en) * 1982-01-27 1983-06-14 Atlantic Richfield Company Silicon purification
FR2556333A1 (en) * 1983-12-09 1985-06-14 Hanna Mining Co Process for purifying silicon for applications requiring high purity
US4643833A (en) * 1984-05-04 1987-02-17 Siemens Aktiengesellschaft Method for separating solid reaction products from silicon produced in an arc furnace
US4612179A (en) * 1985-03-13 1986-09-16 Sri International Process for purification of solid silicon
SE460287B (en) * 1987-09-15 1989-09-25 Casco Nobel Ab PROCEDURE FOR PURIFICATION OF SILICONE FROM BORN
NO901150L (en) * 1987-09-15 1990-03-12 Casco Nobel Ab PROCEDURE FOR CLEANING SILICONE.
JP2856839B2 (en) * 1990-05-11 1999-02-10 川崎製鉄株式会社 Silicon purification method
JP2846408B2 (en) * 1990-05-30 1999-01-13 川崎製鉄株式会社 Silicon purification method
JP3205352B2 (en) * 1990-05-30 2001-09-04 川崎製鉄株式会社 Silicon purification method and apparatus
US5208001A (en) * 1991-06-20 1993-05-04 Texas Instruments Incorporated Method for silicon purification
DE4122190C2 (en) * 1991-07-04 1995-07-06 Wacker Chemie Gmbh Method and apparatus for continuous treatment of silicon
CN1080264A (en) * 1993-03-01 1994-01-05 吴旺河 Industrial silicon slag-cleaning and calcium-removing device and process for purification thereof

Also Published As

Publication number Publication date
AU682277B2 (en) 1997-09-25
FI954108A0 (en) 1995-09-01
JP2851257B2 (en) 1999-01-27
EP0699625B1 (en) 1999-03-24
AU3036295A (en) 1996-03-14
ZA956186B (en) 1997-01-27
FI954108A (en) 1996-03-02
DK0699625T3 (en) 1999-05-25
NO180532C (en) 1997-05-07
RU2098354C1 (en) 1997-12-10
JPH0873209A (en) 1996-03-19
CN1042821C (en) 1999-04-07
KR960012284A (en) 1996-04-20
NO943227L (en) 1996-03-04
FI114092B (en) 2004-08-13
CN1133262A (en) 1996-10-16
ES2130535T3 (en) 1999-07-01
EP0699625A1 (en) 1996-03-06
KR0178071B1 (en) 1999-04-15
ATE178031T1 (en) 1999-04-15
US5788945A (en) 1998-08-04
DE69508498T2 (en) 1999-11-18
NO943227D0 (en) 1994-09-01
GR3030154T3 (en) 1999-08-31
DE69508498D1 (en) 1999-04-29
NO180532B (en) 1997-01-27

Similar Documents

Publication Publication Date Title
BR9503835A (en) Process for removing impurities from the melting silicon
BR0211195B1 (en) medium purity silencing process for use as raw material in the production of silicon of photovoltaic or electronic quality.
RU95114671A (en) METHOD FOR REMOVING SILICON MELT IMPURITIES
DE69231742D1 (en) Method and device for vitrifying asbestos-containing waste, infected waste, toxic materials and radioactive waste
SE8207238D0 (en) PROCEDURE FOR PURIFICATION OF SILICONE
AU562231B2 (en) Removal of ca, al as impurities from silicon and ferrosilicon with acid slag
ATE35293T1 (en) METHOD AND DEVICE FOR LITHIUM REFINING.
UA27030A1 (en) Method for magnesium and its alloys fining and device for realization thereof
FI934862A0 (en) Foerfarande Foer quantitative rening of glycolipid
DE3361823D1 (en) Process for the removal of the slag from molten mixtures of slag and silicon
CA2153932A1 (en) Method for Refining of Silicon
SE8003840L (en) PROCEDURE FOR PURIFICATION OF SILICONE
EP0390671A3 (en) Process for determination of concentrations of metal impurities in czochralski single crystal silicon
ES2097148T3 (en) ELEMENTAL SULFUR PURIFICATION.
EP0172913A4 (en) Process and device for removing impurities contained in melted iron flowing from shaft furnace.
GB9216227D0 (en) Improvements in or relating to removal of contaminants from molten metals
ATE50972T1 (en) SURFACE MELTING AND REFRACTORY CLOTHING.
DE69103825D1 (en) Process for removing silicon compounds from pickling baths and device therefor.
JPS6456311A (en) Production of high-purity silicon
Kramer Phosphorus Removal in Silicon Purification
RU93039916A (en) METHOD FOR PROCESSING TECHNICALLY PURE METAL
JPS5635708A (en) Refining method of molten iron alloy
SU1776064A1 (en) Method of rough copper refinement
CS802488A1 (en) Method of impurities removal from upper part of crystal drawn from crucible
JPS57104613A (en) Production of as cast ferrite type spheroidal graphite cast iron

Legal Events

Date Code Title Description
FF Decision: intention to grant
FG9A Patent or certificate of addition granted
B21A Patent or certificate of addition expired [chapter 21.1 patent gazette]

Free format text: PATENTE EXTINTA EM 29/08/2015