BR112017028433A2 - ?processo para preparação de um derivado de furfural? - Google Patents
?processo para preparação de um derivado de furfural?Info
- Publication number
- BR112017028433A2 BR112017028433A2 BR112017028433A BR112017028433A BR112017028433A2 BR 112017028433 A2 BR112017028433 A2 BR 112017028433A2 BR 112017028433 A BR112017028433 A BR 112017028433A BR 112017028433 A BR112017028433 A BR 112017028433A BR 112017028433 A2 BR112017028433 A2 BR 112017028433A2
- Authority
- BR
- Brazil
- Prior art keywords
- reaction mixture
- furfural derivative
- chemical formula
- acid reaction
- range
- Prior art date
Links
- HYBBIBNJHNGZAN-UHFFFAOYSA-N furfural Chemical class O=CC1=CC=CO1 HYBBIBNJHNGZAN-UHFFFAOYSA-N 0.000 title abstract 5
- 238000004519 manufacturing process Methods 0.000 title 1
- 239000011541 reaction mixture Substances 0.000 abstract 6
- 239000002253 acid Substances 0.000 abstract 4
- 239000000126 substance Substances 0.000 abstract 3
- 150000001875 compounds Chemical class 0.000 abstract 2
- 125000002887 hydroxy group Chemical group [H]O* 0.000 abstract 2
- 239000007788 liquid Substances 0.000 abstract 2
- 238000000034 method Methods 0.000 abstract 2
- 229930091371 Fructose Natural products 0.000 abstract 1
- RFSUNEUAIZKAJO-ARQDHWQXSA-N Fructose Chemical compound OC[C@H]1O[C@](O)(CO)[C@@H](O)[C@@H]1O RFSUNEUAIZKAJO-ARQDHWQXSA-N 0.000 abstract 1
- 239000005715 Fructose Substances 0.000 abstract 1
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 abstract 1
- 239000003377 acid catalyst Substances 0.000 abstract 1
- 125000002252 acyl group Chemical group 0.000 abstract 1
- 125000000217 alkyl group Chemical group 0.000 abstract 1
- 239000008103 glucose Substances 0.000 abstract 1
- 229910052739 hydrogen Inorganic materials 0.000 abstract 1
- 239000001257 hydrogen Substances 0.000 abstract 1
- 125000004435 hydrogen atom Chemical group [H]* 0.000 abstract 1
- 239000000463 material Substances 0.000 abstract 1
- 239000007858 starting material Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
- C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
- C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
- C07D307/38—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
- C07D307/40—Radicals substituted by oxygen atoms
- C07D307/46—Doubly bound oxygen atoms, or two oxygen atoms singly bound to the same carbon atom
- C07D307/48—Furfural
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
- C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
- C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
- C07D307/38—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
- C07D307/40—Radicals substituted by oxygen atoms
- C07D307/46—Doubly bound oxygen atoms, or two oxygen atoms singly bound to the same carbon atom
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Furan Compounds (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
um derivado de furfural tendo a fórmula química (1) em que r representa hidrogênio, um grupo alquila ou um grupo acila, é preparado em um processo, tal processo compreende reagir uma material iniciador contendo frutose e/ou glicose com um composto contendo grupo hidroxila líquido da fórmula r-oh na presença de um catalisador ácido em uma temperatura de reação na faixa de 150 a 300 °c para produzir uma mistura de reação ácida primária compreendendo o derivado de furfural da fórmula química (1); separar parte do composto contendo grupo hidroxila líquido da mistura de reação ácida primária para render uma mistura de reação ácida secundária; neutralizar a mistura de reação ácida secundária para um valor de ph na faixa de pelo menos 3 para obter uma mistura de reação neutralizada e purificar a mistura de reação parcialmente neutralizada para recuperar o derivado de furfural da fórmula química (1).
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| NL2015066 | 2015-07-01 | ||
| NL2015066 | 2015-07-01 | ||
| PCT/NL2016/050470 WO2017003294A1 (en) | 2015-07-01 | 2016-07-01 | Process for the preparation of a furfural derivative comprising neutralizing an acid reaction mixture |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| BR112017028433A2 true BR112017028433A2 (pt) | 2018-08-28 |
| BR112017028433B1 BR112017028433B1 (pt) | 2022-02-08 |
Family
ID=53783874
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| BR112017028433-2A BR112017028433B1 (pt) | 2015-07-01 | 2016-07-01 | Processo para preparação de um derivado de furfural |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US10266508B2 (pt) |
| EP (1) | EP3317262B1 (pt) |
| CN (1) | CN107848996B (pt) |
| BR (1) | BR112017028433B1 (pt) |
| CA (1) | CA2990588C (pt) |
| ES (1) | ES2806988T3 (pt) |
| MX (1) | MX2018000198A (pt) |
| WO (1) | WO2017003294A1 (pt) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2017003293A1 (en) * | 2015-07-01 | 2017-01-05 | Furanix Technologies B.V. | Process for the preparation of a furfural derivative |
| CN118119604A (zh) | 2021-10-21 | 2024-05-31 | 福兰尼克斯科技公司 | 用于制备糠醛衍生物的工艺 |
Family Cites Families (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3290263A (en) * | 1962-08-02 | 1966-12-06 | Colonial Sugar Refining Co | Process of reacting sugars with reagents wherein the sugar is dissolved in monohydric alcohols containing grouping |
| DE3601281A1 (de) * | 1986-01-17 | 1987-07-23 | Sueddeutsche Zucker Ag | Verfahren zur herstellung von 5-hydroxymethylfurfural einschliesslich eines kristallinen produktes unter ausschliesslicher verwendung von wasser als loesungsmittel |
| US7317116B2 (en) * | 2004-12-10 | 2008-01-08 | Archer-Daniels-Midland-Company | Processes for the preparation and purification of hydroxymethylfuraldehyde and derivatives |
| EP1834950A1 (en) | 2006-03-10 | 2007-09-19 | Avantium International B.V. | Method for the synthesis of 5-alkoxymethylfurfural ethers and their use |
| EP1834951A1 (en) * | 2006-03-10 | 2007-09-19 | Avantium International B.V. | Method for the synthesis of organic acid esters of 5-hydroxymethylfurfural and their use |
| EP2197867B1 (en) | 2007-09-07 | 2016-03-02 | Furanix Technologies B.V | Hydroxymethylfurfural ethers from sugars or hmf and branched alcohols |
| NL2005928C2 (en) * | 2010-12-28 | 2012-07-02 | Furanix Technologies Bv | Process for the conversion of a carbohydrate-containing feedstock. |
| CN103857664B (zh) * | 2011-09-23 | 2016-08-24 | 新加坡科技研究局 | 由碳水化合物制备5-羟甲基糠醛的方法 |
| CN103159707A (zh) * | 2011-12-09 | 2013-06-19 | 中国科学院大连化学物理研究所 | 一种生物质催化转化制备呋喃衍生物的方法 |
| WO2016207025A1 (de) * | 2015-06-24 | 2016-12-29 | Basf Se | Verfahren zum herstellen und abtrennen von hmf |
| WO2017003293A1 (en) * | 2015-07-01 | 2017-01-05 | Furanix Technologies B.V. | Process for the preparation of a furfural derivative |
-
2016
- 2016-07-01 CA CA2990588A patent/CA2990588C/en active Active
- 2016-07-01 WO PCT/NL2016/050470 patent/WO2017003294A1/en active Application Filing
- 2016-07-01 MX MX2018000198A patent/MX2018000198A/es unknown
- 2016-07-01 ES ES16745529T patent/ES2806988T3/es active Active
- 2016-07-01 EP EP16745529.4A patent/EP3317262B1/en active Active
- 2016-07-01 CN CN201680039049.5A patent/CN107848996B/zh active Active
- 2016-07-01 US US15/736,037 patent/US10266508B2/en active Active
- 2016-07-01 BR BR112017028433-2A patent/BR112017028433B1/pt active IP Right Grant
Also Published As
| Publication number | Publication date |
|---|---|
| CA2990588C (en) | 2020-04-14 |
| EP3317262B1 (en) | 2020-04-22 |
| US10266508B2 (en) | 2019-04-23 |
| WO2017003294A1 (en) | 2017-01-05 |
| MX2018000198A (es) | 2018-04-11 |
| ES2806988T3 (es) | 2021-02-19 |
| EP3317262A1 (en) | 2018-05-09 |
| CN107848996B (zh) | 2021-07-27 |
| US20180186761A1 (en) | 2018-07-05 |
| CN107848996A (zh) | 2018-03-27 |
| BR112017028433B1 (pt) | 2022-02-08 |
| CA2990588A1 (en) | 2017-01-05 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| B06U | Preliminary requirement: requests with searches performed by other patent offices: procedure suspended [chapter 6.21 patent gazette] | ||
| B25A | Requested transfer of rights approved |
Owner name: FURANIX TECHNOLOGIES B.V. (NL) |
|
| B09A | Decision: intention to grant [chapter 9.1 patent gazette] | ||
| B16A | Patent or certificate of addition of invention granted [chapter 16.1 patent gazette] |
Free format text: PRAZO DE VALIDADE: 20 (VINTE) ANOS CONTADOS A PARTIR DE 01/07/2016, OBSERVADAS AS CONDICOES LEGAIS. |