AU722916B2 - Shell solution and fabrication method thereof - Google Patents
Shell solution and fabrication method thereof Download PDFInfo
- Publication number
- AU722916B2 AU722916B2 AU75425/96A AU7542596A AU722916B2 AU 722916 B2 AU722916 B2 AU 722916B2 AU 75425/96 A AU75425/96 A AU 75425/96A AU 7542596 A AU7542596 A AU 7542596A AU 722916 B2 AU722916 B2 AU 722916B2
- Authority
- AU
- Australia
- Prior art keywords
- shell
- solution
- shell solution
- acetic acid
- acid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Ceased
Links
- 238000000034 method Methods 0.000 title claims description 14
- 238000004519 manufacturing process Methods 0.000 title claims description 12
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims description 57
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 30
- 229920001661 Chitosan Polymers 0.000 claims description 9
- 239000002253 acid Substances 0.000 claims description 8
- 229910052500 inorganic mineral Inorganic materials 0.000 claims description 7
- 239000011707 mineral Substances 0.000 claims description 7
- 240000007594 Oryza sativa Species 0.000 claims description 3
- 235000007164 Oryza sativa Nutrition 0.000 claims description 3
- 235000009566 rice Nutrition 0.000 claims description 3
- 239000002245 particle Substances 0.000 claims description 2
- 239000000243 solution Substances 0.000 description 53
- 239000002699 waste material Substances 0.000 description 14
- 235000013305 food Nutrition 0.000 description 10
- 239000007788 liquid Substances 0.000 description 7
- 241000196324 Embryophyta Species 0.000 description 6
- 239000011575 calcium Substances 0.000 description 6
- 238000010411 cooking Methods 0.000 description 6
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 5
- 229910052791 calcium Inorganic materials 0.000 description 5
- 230000003750 conditioning effect Effects 0.000 description 5
- 241000251468 Actinopterygii Species 0.000 description 4
- 235000019688 fish Nutrition 0.000 description 4
- 239000002689 soil Substances 0.000 description 4
- 235000013599 spices Nutrition 0.000 description 4
- 235000010469 Glycine max Nutrition 0.000 description 3
- 230000034303 cell budding Effects 0.000 description 3
- 201000010099 disease Diseases 0.000 description 3
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 3
- XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Substances [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 239000000843 powder Substances 0.000 description 3
- QJZYHAIUNVAGQP-UHFFFAOYSA-N 3-nitrobicyclo[2.2.1]hept-5-ene-2,3-dicarboxylic acid Chemical compound C1C2C=CC1C(C(=O)O)C2(C(O)=O)[N+]([O-])=O QJZYHAIUNVAGQP-UHFFFAOYSA-N 0.000 description 2
- 241000238876 Acari Species 0.000 description 2
- 235000009024 Ceanothus sanguineus Nutrition 0.000 description 2
- 244000068988 Glycine max Species 0.000 description 2
- 241000238631 Hexapoda Species 0.000 description 2
- 240000003553 Leptospermum scoparium Species 0.000 description 2
- 235000015459 Lycium barbarum Nutrition 0.000 description 2
- 241000237502 Ostreidae Species 0.000 description 2
- 239000004952 Polyamide Substances 0.000 description 2
- 241000206607 Porphyra umbilicalis Species 0.000 description 2
- 238000007792 addition Methods 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 230000003247 decreasing effect Effects 0.000 description 2
- 239000004021 humic acid Substances 0.000 description 2
- 239000011777 magnesium Substances 0.000 description 2
- 235000020636 oyster Nutrition 0.000 description 2
- 229920002647 polyamide Polymers 0.000 description 2
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- 235000007688 Lycopersicon esculentum Nutrition 0.000 description 1
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 1
- PWHULOQIROXLJO-UHFFFAOYSA-N Manganese Chemical compound [Mn] PWHULOQIROXLJO-UHFFFAOYSA-N 0.000 description 1
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- KEAYESYHFKHZAL-UHFFFAOYSA-N Sodium Chemical compound [Na] KEAYESYHFKHZAL-UHFFFAOYSA-N 0.000 description 1
- 240000003768 Solanum lycopersicum Species 0.000 description 1
- 244000061456 Solanum tuberosum Species 0.000 description 1
- 235000002595 Solanum tuberosum Nutrition 0.000 description 1
- 240000008042 Zea mays Species 0.000 description 1
- 235000005824 Zea mays ssp. parviglumis Nutrition 0.000 description 1
- 235000002017 Zea mays subsp mays Nutrition 0.000 description 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 235000013527 bean curd Nutrition 0.000 description 1
- 235000012970 cakes Nutrition 0.000 description 1
- 239000002361 compost Substances 0.000 description 1
- 235000013409 condiments Nutrition 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 239000010949 copper Substances 0.000 description 1
- 235000005822 corn Nutrition 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 238000009313 farming Methods 0.000 description 1
- 239000003337 fertilizer Substances 0.000 description 1
- 239000013505 freshwater Substances 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 238000003306 harvesting Methods 0.000 description 1
- BHEPBYXIRTUNPN-UHFFFAOYSA-N hydridophosphorus(.) (triplet) Chemical compound [PH] BHEPBYXIRTUNPN-UHFFFAOYSA-N 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 235000015094 jam Nutrition 0.000 description 1
- 229910052749 magnesium Inorganic materials 0.000 description 1
- 229910052748 manganese Inorganic materials 0.000 description 1
- 239000011572 manganese Substances 0.000 description 1
- 235000010746 mayonnaise Nutrition 0.000 description 1
- 239000008268 mayonnaise Substances 0.000 description 1
- 239000011259 mixed solution Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 235000012149 noodles Nutrition 0.000 description 1
- 239000011574 phosphorus Substances 0.000 description 1
- 229910052698 phosphorus Inorganic materials 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 235000012015 potatoes Nutrition 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- 238000002791 soaking Methods 0.000 description 1
- 235000014214 soft drink Nutrition 0.000 description 1
- 239000003516 soil conditioner Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 241001478887 unidentified soil bacteria Species 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B09—DISPOSAL OF SOLID WASTE; RECLAMATION OF CONTAMINATED SOIL
- B09B—DISPOSAL OF SOLID WASTE NOT OTHERWISE PROVIDED FOR
- B09B3/00—Destroying solid waste or transforming solid waste into something useful or harmless
- B09B3/80—Destroying solid waste or transforming solid waste into something useful or harmless involving an extraction step
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A40/00—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production
- Y02A40/80—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production in fisheries management
- Y02A40/81—Aquaculture, e.g. of fish
Landscapes
- Engineering & Computer Science (AREA)
- Environmental & Geological Engineering (AREA)
- Fertilizers (AREA)
- Processing Of Solid Wastes (AREA)
- Soil Conditioners And Soil-Stabilizing Materials (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
- General Preparation And Processing Of Foods (AREA)
Description
AUSTRALIA
Patents Act 1990 INTERNATIONAL ASTRA CO., LTD.
ORIGINAL
COMPLETE SPECIFICATION STANDARD PATENT Invention Title: 4, C
C.
I. 44fl t4.t 0 *9 I 4*
C
0* *eIe..
C
Shell solution and fabrication method thereof The following statement is a fuill description of this invention including the best method of performing it known to us:- SHELL SOLUTIO? AND FFRCATONMETHOD THEREQF BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to a shell solution and a fabrication method thereof; and more particularly to a shell solution and a fabrication method thereof by which it is possible -0 to' prevent the formation of shell waste by dissolving the shells.
2. Description of the Conventional Art Generally, shell waste, which occurs at seaside on farms, or the like, may be classified into pearl shell waste at a pearl farm or at seaside, oyster shell waste at an oyster farm or at seaside, of sea shell waste at seaside or on a shell farm.
The conventional shell waste disposal method involves grinding the shell waste and disposing it in the sea or using it as soil conditioning material. In general, shell waste has not been used for practical purposes. when shells are disposed as waste at or near seaside, or near sea villages, waste problems result at the shore.
It is desirable therefore to provide a shell solution and a fabrication method thereof, which overcomes the problems encountered in the conventional shell disposal method.
1/1 It is also desirable to provide a shell solution and a fabrication method thereof by which it is possible to prevent the formation of shell waste by dissolving the shells.
It is also desirable to provide a shell solution and a fabrication method thereof which is capable of effectively overcoming shell waste problems by fabricating a shell solution by dissolving the shells, at a low cost, and by using the shell solution as a food cooking liquid, as cooking spices, as a soil conditioning liquid, as a conditioning liquid at farms, and for other practical purposes.
Summary of the Invention In one aspect the present invention is directed to a shell solution containing a mineral component, which is helpful for a human body, in an amount of over 1.5 weight wherein the shell solution is fabricated by dissolving shell in an acetic acid solution containing 1-3 weight citric acid.
Preferably, a chitosan acid solution is added to the shell solution.
In aspect, the present invention is directed to a method of fabricating a 0°0' shell solution wherein particles of shell are dissolved in acetic acid containing 1-3 weight of citric acid until a pH of 6.8 7.0 is reached.
Preferably, the method further includes the addition of a chitosan acid solution.
DETAILED DESCRIPTTON OF THE INVENTION The present invention is directed to methods of fabricating a shell solution by extracting a mineral component of the shells, which is beneficial for the human body, by dissolving the shells into acetic acid in which citric acid is contained.
That is, it is possible to obtain a shell solution in which the mineral component, which is beneficial for the human body, is contained at 1.5 weight-percent by dissolving the shells in acetic acid in which citric acid- is contained at 1-3 weightpercent. The mineral components contained in the shells include Na(Natrium), K(Potassium), Ca(Calcium), Fe(Iron), P(Phosphorus), Mg(Magnesium), and the like.
In accordance with a further embodiment of the invention, a shell solution is fabricated in which a chitosan acid is contained. The chitosan acid is dissolved into the acetic acid by 5-10 weight-percent. The weight percent of the shell solution and the chitosan acid solution can be selected within a range of 1:99 through 99:1.
The present invention is directed to a method of fabricating a shell solution by dissolving -ground shells into acetic acid until the pH of the acetic acid containing citric acid at 1-3 weight percent reaches 6.8 S. In addition, the present invention is directed to dissolving ground shells into acetic acid, and mixing a chitosan solution into the solution until the pH of the acetic acid containing citric acid by 1-3 weight percent reaches 6.8 The shell solution of the present invention is used as a food cooking liquid, as cooking spices, as a soil conditioning liquid, as a conditioning liquid at various farms, and for other practical purposes. The acetic acid is used because it is safe as a food. As the acetic acid, artificially-made acetic acid or chemically-made acetic acid may be used.
The citric acid contained in the shell solution serves to expedite solution operation of carbonic calcium of the shells.
When the citric acid is absorbed in the human body it also serves to increase absorption of calcium into the body, thereby making it preferable for the shell solution.
The embodiments of the present invention will now be described in more detail.
First Embodimet In order to fabricate a shell solution according to the present invention, oyster shells are substantially cleaned using fresh water, dried, and ground to a powder. Thereafter, 2 kg of the shell powder is added to 20 1 of the artificially-made acetic acid containing two weight percent of citric acid in a polyamide container, and then stirred using an electrical stirrer having a magnetic bar for about 12 to about 48 hours at a speed of about 150 to about 250 rpm. After stirring, the mixed materials are filtered using a Buchner funnel and a vacuum filter flask connected to an aspirator, thus obtaining the shell solution of the present invention. The remaining shell powder after fabricating the shell solution can be used again. If after 12-48 hours the pH of the 4 shell solution is still below 6.8B-7. 0, the shell solution is not dissolved up to the saturated state. in this case, the dissolution of the shell solution is preferably be repeated until the pH reaches 6. 8-7. 0.
The mineral components provided in the resulting shell solution, which are useful in the human body, are as follows: Components Amouznt contained Calcium 1.629/1009 Natium ai. 4mg/lbag .0 Kallum 1.m/10 Magneflium 9. 78mg/lbOg Phosphorous 9.2mq/bog9 Iran 0.34mg/bOOg Copper 0.O6ppm zinc 0.66ppm Manganese 1. 1Sppm Second Embodizent The shell solution which is fabricated in accordance with 0 the f irst embodiment of the present invention is diluted by 50-200 times, and when it is used as f ood conditioner, it is possible to get 600mg of calcium for one person from about 40g of shell solution.
That is, the shell solution obtained by the second ermbodiment of the present invention can be used as food conditioner for rice, rice cake, noodles, bean-curd, soy-soaked food, saltsoaked fish, grilled fish, jam, soft drinks, food conditioners (such as soy bean paste, soy, spices and condiments, mayonnaise, the like), material for fried food, seasoned soy bean paste, and any other appropriate foods.
In a polyamide container, 20 1 of the artificially-made acetic acid and 1kg of chitosan acid are well mixed. After 48 hours in the container with a lid, a gel-type solution is obtained.
6kg of the above-mentioned gel-type solution is substantially mixed with 3.2 1 of the shell solution which is obtained by the f irst embodiment. In addition, if necessary, 2 kg humic acid may be mixed with the thusly mixed solution, thus obtaining a shell solution of this embodiment of the present invention. The humic acid prevents gathering of mold in the artificially-made acetic acid.
Thereafter, the shell solution obtained by the second embodiment is diluted with water by 50-200 times. The diluted solution may be used as a coil conditioner, as a liquid for seeds or young plants, as a plant growing conditioner, as artificial food for fish, or for any other appropriate purpose.
soil asndi ioner.* At an area of the ground to be seeded, tons of well-seasoned compost is applied over the ground per unit area of 10 hectares, and then the shell solution of the present invention i1s applied over the g-round per unit area of 6 hectares. Thereafter, the plant appeared to have grown better. in addition, the mineral components were increased in its amount.
Balance against soil bacteria was recovered. Anti-disease strength was increased. Improved quality plants were obtained.
Seed _culivation licid: After soaking seeds to be cultivated and young plants to be planted in the shell solution of the present invention, seed budding time was reduced, and the growing state after budding was made better. Anti-disease strength was high.
yro canditi nor: 200-600 1 of the shell solution was applied over a unit area of 10 hectares over the leafsa and roots of plant one week after budding. Thereafter, once every two weeks, and in the case of potatoes, tomatoes, and 'corn, 3-4 times every two weeks, the shell solution is applied thereto. As a result, anti-insects ef fect was increased with respect to insects such as ticks, and the like. When applying the shell solution of the present invention to fruit trees or tea trees, it was not necessary to apply fertilizer. In case of tea trees, the harvest of f resh leaf thereof was increased by 30% by preventing insects such as 0 ticks.
Fis farming onditioner: After f eeding sliced f ish to f ish fry as f ood, together with the shell solution by 3 weight percent, the death rate of the fry was decreased. in addition, when applying 3-4 1 of the shell solution over per unit area of 1 2 with respect to layer in a layer f arm at full tide, the layer 0. 0 disease occuzrenci rate was substantially decreased. in addition, 7 when a laver cultivation net was soaked with the solution of the present invention, and then was used at sea, the growing state of laver improved.
As described above, the shell solution and a fabrication method thereof of the present invention is directed to effectively treating shell waste, and utilizing the shell solution as food cooking conditioner, cooking spice, crop growing conditioner, soil conditioner, fish farm conditioner, and the like. In addition, it is possible to effectively resolving the shell waste problem by utilizing it for practical purposes.
Although the present invention have been described with respect to particular embodiments of the invention, it will be appreciated that the invention relates generally to the dissolving of shells in acetic acid so as to extract useful components from the shells. Those skilled in the art will appreciate that the invention may be practiced more broadly than described in the preferred embodiments herein so as to enable shells to be dissolved for other purposes. More broadly, although the preferred embodiments of the present invention have been disclosed for illustrative purposes, those skilled in the art will appreciate that various modifications, additions and substitutions are possible, without departing from the scope and spirit of the invention as described in the accompanying claims.
°oo*o
Claims (4)
1. A shell solution containing a mineral component, which is helpful for a human body, in an amount of over 1.5 weight wherein the shell solution is fabricated by dissolving shell in an acetic acid solution containing 1-3 weight citric acid.
2. The shell solution of claim 1, wherein a chitosan acid solution is added to the shell solution.
3. A method of fabricating a shell solution wherein particles of shell are dissolved in acetic acid containing 1-3 weight of citric acid until a pH of
6.8 7.0 is reached. 4. A method of fabricating a shell solution according to claim 3 wherein the method further includes the addition of a chitosan acid solution. Dated this ninth day of June 2000 INTERNATIONAL ASTRA CO., LTD. Patent Attorneys for the Applicant: F B RICE CO f
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| KR1019960008296A KR0173556B1 (en) | 1996-03-26 | 1996-03-26 | Shell solution and its manufacturing method |
| KR96/8296 | 1996-03-26 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| AU7542596A AU7542596A (en) | 1997-10-16 |
| AU722916B2 true AU722916B2 (en) | 2000-08-17 |
Family
ID=19453928
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AU75425/96A Ceased AU722916B2 (en) | 1996-03-26 | 1996-12-17 | Shell solution and fabrication method thereof |
Country Status (4)
| Country | Link |
|---|---|
| KR (1) | KR0173556B1 (en) |
| AU (1) | AU722916B2 (en) |
| NZ (1) | NZ314055A (en) |
| TW (1) | TW360499B (en) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR101357078B1 (en) | 2012-09-18 | 2014-02-03 | 주식회사 서진바이오텍 | Process for seperation of cutoffs having anti-inflamentary or osteoarthritis inhibition effects using oyster shells |
| CN103651223B (en) * | 2014-01-03 | 2015-08-05 | 鲁东大学 | A kind of appraisal procedure of long oyster soft body weight in wet base |
-
1996
- 1996-03-26 KR KR1019960008296A patent/KR0173556B1/en not_active IP Right Cessation
- 1996-11-21 TW TW085114318A patent/TW360499B/en active
- 1996-12-17 AU AU75425/96A patent/AU722916B2/en not_active Ceased
-
1997
- 1997-01-10 NZ NZ314055A patent/NZ314055A/en unknown
Also Published As
| Publication number | Publication date |
|---|---|
| KR970064756A (en) | 1997-10-13 |
| AU7542596A (en) | 1997-10-16 |
| KR0173556B1 (en) | 1999-02-01 |
| TW360499B (en) | 1999-06-11 |
| NZ314055A (en) | 1997-03-24 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FGA | Letters patent sealed or granted (standard patent) |