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AU2002217211A1 - Method for preparing beta-phosphorus nitroxide radicals - Google Patents

Method for preparing beta-phosphorus nitroxide radicals

Info

Publication number
AU2002217211A1
AU2002217211A1 AU2002217211A AU1721102A AU2002217211A1 AU 2002217211 A1 AU2002217211 A1 AU 2002217211A1 AU 2002217211 A AU2002217211 A AU 2002217211A AU 1721102 A AU1721102 A AU 1721102A AU 2002217211 A1 AU2002217211 A1 AU 2002217211A1
Authority
AU
Australia
Prior art keywords
nitroxide radicals
preparing beta
aminophosphonate
beta
preparing
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Abandoned
Application number
AU2002217211A
Inventor
Jean-Luc Couturier
Olivier Guerret
Christophe Le Mercier
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Arkema France SA
Original Assignee
Atofina SA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Atofina SA filed Critical Atofina SA
Publication of AU2002217211A1 publication Critical patent/AU2002217211A1/en
Abandoned legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/28—Phosphorus compounds with one or more P—C bonds
    • C07F9/50—Organo-phosphines
    • C07F9/53—Organo-phosphine oxides; Organo-phosphine thioxides
    • C07F9/5304—Acyclic saturated phosphine oxides or thioxides
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/28—Phosphorus compounds with one or more P—C bonds
    • C07F9/38—Phosphonic acids [RP(=O)(OH)2]; Thiophosphonic acids ; [RP(=X1)(X2H)2(X1, X2 are each independently O, S or Se)]
    • C07F9/40—Esters thereof
    • C07F9/4003—Esters thereof the acid moiety containing a substituent or a structure which is considered as characteristic
    • C07F9/4006—Esters of acyclic acids which can have further substituents on alkyl

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Molecular Biology (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Polymerisation Methods In General (AREA)
  • Luminescent Compositions (AREA)

Abstract

The present invention relates to a process for the preparation of beta-phosphorated nitroxide radicals which consist in preparing, in a first step, an aminophosphonate by reaction of a carbonyl compound, of a primary amine and of a phosphorous compound in the presence of a Lewis acid and then, in a second step, in oxidizing the said crude aminophosphonate using nonhalogenated organic peracids in a water/organic solvent two-phase medium with an aqueous phase buffered at a pH ranging from 5 to 12.
AU2002217211A 2000-12-11 2001-12-07 Method for preparing beta-phosphorus nitroxide radicals Abandoned AU2002217211A1 (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
FR0016066A FR2817861B1 (en) 2000-12-11 2000-12-11 PROCESS FOR THE PREPARATION OF B-PHOSPHORUS NITROXIDE RADICALS
FR0016066 2000-12-11
PCT/FR2001/003876 WO2002048159A1 (en) 2000-12-11 2001-12-07 Method for preparing $g(b)-phosphorus nitroxide radicals

Publications (1)

Publication Number Publication Date
AU2002217211A1 true AU2002217211A1 (en) 2002-06-24

Family

ID=8857478

Family Applications (1)

Application Number Title Priority Date Filing Date
AU2002217211A Abandoned AU2002217211A1 (en) 2000-12-11 2001-12-07 Method for preparing beta-phosphorus nitroxide radicals

Country Status (14)

Country Link
US (1) US7126021B2 (en)
EP (1) EP1349862B1 (en)
JP (1) JP3988134B2 (en)
KR (1) KR100796961B1 (en)
CN (1) CN1247601C (en)
AT (1) ATE271559T1 (en)
AU (1) AU2002217211A1 (en)
DE (1) DE60104446T2 (en)
DK (1) DK1349862T3 (en)
ES (1) ES2225409T3 (en)
FR (1) FR2817861B1 (en)
MX (1) MXPA03005179A (en)
TR (1) TR200402798T4 (en)
WO (1) WO2002048159A1 (en)

Families Citing this family (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP1606259B1 (en) 2003-03-27 2014-06-25 Basf Se Process for the oxidation of secondary amines into the corresponding nitroxides
FR2870240B1 (en) * 2004-05-13 2006-07-07 Arkema Sa PROCESS FOR THE PREPARATION OF ALCOXYAMINE OR ITS SALTS COMPRISING A PHOTOLYSIS STEP
JP4912314B2 (en) 2004-10-26 2012-04-11 ジヤンセン・フアーマシユーチカ・ナームローゼ・フエンノートシヤツプ Factor Xa compound
FR2884517B1 (en) * 2005-04-19 2007-05-25 Arkema Sa PROCESS FOR THE PREPARATION OF ALCOXAMINES BY PHOTOLYSIS OF DITHIOCARBAMATES
FR2891841B1 (en) * 2005-10-11 2007-12-28 Arkema Sa ODORIZING MIXTURE FOR GASEOUS FUEL ODORLESS
WO2008079677A2 (en) * 2006-12-20 2008-07-03 Arkema Inc. Polymer encapsulation and/or binding
WO2013156356A2 (en) 2012-04-20 2013-10-24 Hilti Aktiengesellschaft Ss-phosphorylated nitroxide radicals as inhibitors for reactive resins, reactive resins containing said ss-phosphorylated nitroxide radicals, and use of said ss-phosphorylated nitroxide radicals
US10072032B2 (en) * 2016-09-19 2018-09-11 Afton Chemical Corporation AminoBisPhosphonate antiwear additives

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2730240A1 (en) * 1995-02-07 1996-08-09 Atochem Elf Sa STABILIZATION OF A POLYMER BY A STABLE FREE RADICAL
FR2730241B1 (en) 1995-02-07 1997-02-28 Atofina PROCESS FOR MANUFACTURING A COMPOSITION COMPRISING A VINYLAROMATIC POLYMER AND A RUBBER BY POLYMERIZATION IN THE PRESENCE OF A FREE STABLE RADICAL
FR2788270B1 (en) * 1999-01-08 2001-03-16 Atochem Elf Sa PROCESS FOR THE PREPARATION OF BETA-PHOSPHORUS NITROXIDE RADIALS
FR2788272B1 (en) * 1999-01-08 2001-03-16 Atochem Elf Sa PROCESS FOR THE PREPARATION OF NITROXIDES
FR2807439B1 (en) 2000-04-07 2003-06-13 Atofina MULTIMODAL POLYMERS BY CONTROLLED RADICAL POLYMERIZATION IN THE PRESENCE OF ALCOXYAMINES

Also Published As

Publication number Publication date
EP1349862B1 (en) 2004-07-21
FR2817861B1 (en) 2004-12-03
JP2004529863A (en) 2004-09-30
WO2002048159A1 (en) 2002-06-20
US20040077873A1 (en) 2004-04-22
ES2225409T3 (en) 2005-03-16
DE60104446T2 (en) 2005-07-28
DK1349862T3 (en) 2004-11-22
CN1489595A (en) 2004-04-14
KR20030060987A (en) 2003-07-16
US7126021B2 (en) 2006-10-24
JP3988134B2 (en) 2007-10-10
ATE271559T1 (en) 2004-08-15
TR200402798T4 (en) 2004-12-21
MXPA03005179A (en) 2003-09-10
KR100796961B1 (en) 2008-01-22
FR2817861A1 (en) 2002-06-14
EP1349862A1 (en) 2003-10-08
CN1247601C (en) 2006-03-29
DE60104446D1 (en) 2004-08-26

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