AU2001292154A1 - Method of preparing a modified corn steep liquor product - Google Patents
Method of preparing a modified corn steep liquor productInfo
- Publication number
- AU2001292154A1 AU2001292154A1 AU2001292154A AU9215401A AU2001292154A1 AU 2001292154 A1 AU2001292154 A1 AU 2001292154A1 AU 2001292154 A AU2001292154 A AU 2001292154A AU 9215401 A AU9215401 A AU 9215401A AU 2001292154 A1 AU2001292154 A1 AU 2001292154A1
- Authority
- AU
- Australia
- Prior art keywords
- product
- corn steep
- steep liquor
- inositol
- modified corn
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Abandoned
Links
- 240000008042 Zea mays Species 0.000 title abstract 5
- 235000005824 Zea mays ssp. parviglumis Nutrition 0.000 title abstract 5
- 235000002017 Zea mays subsp mays Nutrition 0.000 title abstract 5
- 235000005822 corn Nutrition 0.000 title abstract 5
- 238000000034 method Methods 0.000 title abstract 2
- 239000000047 product Substances 0.000 abstract 6
- IMQLKJBTEOYOSI-GPIVLXJGSA-N Inositol-hexakisphosphate Chemical compound OP(O)(=O)O[C@H]1[C@H](OP(O)(O)=O)[C@@H](OP(O)(O)=O)[C@H](OP(O)(O)=O)[C@H](OP(O)(O)=O)[C@@H]1OP(O)(O)=O IMQLKJBTEOYOSI-GPIVLXJGSA-N 0.000 abstract 2
- IMQLKJBTEOYOSI-UHFFFAOYSA-N Phytic acid Natural products OP(O)(=O)OC1C(OP(O)(O)=O)C(OP(O)(O)=O)C(OP(O)(O)=O)C(OP(O)(O)=O)C1OP(O)(O)=O IMQLKJBTEOYOSI-UHFFFAOYSA-N 0.000 abstract 2
- INAPMGSXUVUWAF-GCVPSNMTSA-N [(2r,3s,5r,6r)-2,3,4,5,6-pentahydroxycyclohexyl] dihydrogen phosphate Chemical compound OC1[C@H](O)[C@@H](O)C(OP(O)(O)=O)[C@H](O)[C@@H]1O INAPMGSXUVUWAF-GCVPSNMTSA-N 0.000 abstract 2
- CDAISMWEOUEBRE-GPIVLXJGSA-N inositol Chemical compound O[C@H]1[C@H](O)[C@@H](O)[C@H](O)[C@H](O)[C@@H]1O CDAISMWEOUEBRE-GPIVLXJGSA-N 0.000 abstract 2
- 229960000367 inositol Drugs 0.000 abstract 2
- 150000002605 large molecules Chemical class 0.000 abstract 2
- 239000002184 metal Substances 0.000 abstract 2
- 229940068041 phytic acid Drugs 0.000 abstract 2
- 235000002949 phytic acid Nutrition 0.000 abstract 2
- 239000000467 phytic acid Substances 0.000 abstract 2
- CDAISMWEOUEBRE-UHFFFAOYSA-N scyllo-inosotol Natural products OC1C(O)C(O)C(O)C(O)C1O CDAISMWEOUEBRE-UHFFFAOYSA-N 0.000 abstract 2
- 239000007787 solid Substances 0.000 abstract 2
- 108010011619 6-Phytase Proteins 0.000 abstract 1
- 108010051457 Acid Phosphatase Proteins 0.000 abstract 1
- 102000013563 Acid Phosphatase Human genes 0.000 abstract 1
- 239000002253 acid Substances 0.000 abstract 1
- 150000001768 cations Chemical class 0.000 abstract 1
- 239000002244 precipitate Substances 0.000 abstract 1
- 239000011347 resin Substances 0.000 abstract 1
- 229920005989 resin Polymers 0.000 abstract 1
- 238000000108 ultra-filtration Methods 0.000 abstract 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/10—Organic substances
- A23K20/142—Amino acids; Derivatives thereof
- A23K20/147—Polymeric derivatives, e.g. peptides or proteins
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23J—PROTEIN COMPOSITIONS FOR FOODSTUFFS; WORKING-UP PROTEINS FOR FOODSTUFFS; PHOSPHATIDE COMPOSITIONS FOR FOODSTUFFS
- A23J1/00—Obtaining protein compositions for foodstuffs; Bulk opening of eggs and separation of yolks from whites
- A23J1/16—Obtaining protein compositions for foodstuffs; Bulk opening of eggs and separation of yolks from whites from waste water of starch-manufacturing plant or like wastes
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/10—Organic substances
- A23K20/174—Vitamins
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J39/00—Cation exchange; Use of material as cation exchangers; Treatment of material for improving the cation exchange properties
- B01J39/04—Processes using organic exchangers
- B01J39/05—Processes using organic exchangers in the strongly acidic form
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J39/00—Cation exchange; Use of material as cation exchangers; Treatment of material for improving the cation exchange properties
- B01J39/26—Cation exchangers for chromatographic processes
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
- C12P7/00—Preparation of oxygen-containing organic compounds
- C12P7/02—Preparation of oxygen-containing organic compounds containing a hydroxy group
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12Y—ENZYMES
- C12Y301/00—Hydrolases acting on ester bonds (3.1)
- C12Y301/03—Phosphoric monoester hydrolases (3.1.3)
- C12Y301/03008—3-Phytase (3.1.3.8)
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Organic Chemistry (AREA)
- Polymers & Plastics (AREA)
- Engineering & Computer Science (AREA)
- Zoology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Wood Science & Technology (AREA)
- Food Science & Technology (AREA)
- Biochemistry (AREA)
- Genetics & Genomics (AREA)
- Bioinformatics & Cheminformatics (AREA)
- General Health & Medical Sciences (AREA)
- General Engineering & Computer Science (AREA)
- Animal Husbandry (AREA)
- Proteomics, Peptides & Aminoacids (AREA)
- Health & Medical Sciences (AREA)
- Microbiology (AREA)
- General Chemical & Material Sciences (AREA)
- Biotechnology (AREA)
- Analytical Chemistry (AREA)
- Preparation Of Compounds By Using Micro-Organisms (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Fodder In General (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
- Cereal-Derived Products (AREA)
- Preventing Corrosion Or Incrustation Of Metals (AREA)
- Paper (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
- Noodles (AREA)
Abstract
A method of preparing a modified corn steep liquor product from a corn steep liquor which includes suspended solids, high molecular weight compounds, phytic acid, and metal values includes the steps of: subjecting the corn steep liquor to ultrafiltration to remove the suspended solids and high molecular weight compounds; treating the product of step (a) with a phytase enzyme to convert the phytic acid to inositol-mono-phosphate; treating the product of step (b) with an acid phosphatase enzyme to convert the inositol-mono-phosphate to myo-inositol; adjusting the pH of the product of step (c) to from 7 to 9 inclusive using a soluble base which causes most or all of the Mg values to precipitate, and removing the precipitate; and contacting the product of step (d) with a strong acid cation chromatographic resin to produce a first fraction containing most of the remaining metal values and a second fraction containing most of the myo-inositol, the second fraction being the modified corn steep liquor product.
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| ZA200005371 | 2000-10-03 | ||
| ZA2000/5371 | 2000-10-03 | ||
| PCT/IB2001/001827 WO2002029077A2 (en) | 2000-10-03 | 2001-10-03 | Method of preparing a modified corn steep liquor product |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| AU2001292154A1 true AU2001292154A1 (en) | 2002-04-15 |
Family
ID=25588930
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AU2001292154A Abandoned AU2001292154A1 (en) | 2000-10-03 | 2001-10-03 | Method of preparing a modified corn steep liquor product |
| AU2001294077A Abandoned AU2001294077A1 (en) | 2000-10-03 | 2001-10-03 | Modified corn steep liquor product |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AU2001294077A Abandoned AU2001294077A1 (en) | 2000-10-03 | 2001-10-03 | Modified corn steep liquor product |
Country Status (7)
| Country | Link |
|---|---|
| US (2) | US20040071820A1 (en) |
| EP (2) | EP1324669B1 (en) |
| CN (2) | CN1474655A (en) |
| AT (2) | ATE321458T1 (en) |
| AU (2) | AU2001292154A1 (en) |
| DE (2) | DE60117158T2 (en) |
| WO (2) | WO2002029077A2 (en) |
Families Citing this family (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2003061403A1 (en) * | 2002-01-24 | 2003-07-31 | Cargill, Incorporated | Low phosphorus animal feed and method for making same |
| AR047658A1 (en) | 2004-02-03 | 2006-02-01 | Cargill Inc | CONCENTRATE OF PROTEINS AND WATER CURRENT WITH HYDROSOLUBBLE CARBOHYDRATES |
| CN102373247B (en) * | 2010-08-25 | 2013-07-10 | 中粮生物化学（安徽）股份有限公司 | Preparation method of improved corn steep liquor for amino acid fermented broth and application thereof |
| CN102443658B (en) * | 2011-10-14 | 2013-05-15 | 广州双桥股份有限公司 | Preparation method of refined corn steep liquor and nitrogen-containing starch syrup for fermentation |
| CN102603487A (en) * | 2012-02-20 | 2012-07-25 | 河南鑫源食品有限公司 | Method for preparing inositol from corn steep liquor |
| JP6262186B2 (en) * | 2015-03-09 | 2018-01-17 | 長谷川香料株式会社 | Method for producing taste beverage ingredient extract |
| CN108101744B (en) * | 2017-12-14 | 2018-12-11 | 四川安益生物科技有限公司 | Inositol extraction method |
| CN112409132B (en) * | 2020-11-30 | 2022-11-04 | 诸城市浩天药业有限公司 | Method for separating inositol and by-products |
| CN116554002B (en) * | 2023-04-17 | 2025-01-28 | 诸城市浩天药业有限公司 | A method for recovering inositol and amino acid substances from inositol crystallization mother liquor |
| CN118221084B (en) * | 2024-05-23 | 2024-08-20 | 诸城市浩天药业有限公司 | Method for producing monopotassium phosphate by using corn soaking water |
Family Cites Families (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB740205A (en) * | 1953-09-03 | 1955-11-09 | Corn Prod Refining Co | Process for recovery of inositol |
| FR2483749A1 (en) * | 1980-06-06 | 1981-12-11 | Roquette Freres | INTERMEDIATE MOISTURE FOOD, PARTICULARLY FOR ANIMALS, AND THE PROCESS AND AGENT FOR PREPARING THE SAME |
| NL8702735A (en) * | 1987-11-17 | 1989-06-16 | Dorr Oliver Inc | METHOD FOR SOAKING CEREALS WITH A NEW ENZYME PREPARATION. |
| US5626847A (en) * | 1990-12-20 | 1997-05-06 | Agrawal; Pramod | Method of purifying cyclitols |
| JPH04365489A (en) * | 1991-06-12 | 1992-12-17 | Mitsui Toatsu Chem Inc | Production of myoinositol |
| JP3950185B2 (en) * | 1996-09-04 | 2007-07-25 | 王子コーンスターチ株式会社 | Production method of inositol |
| JPH11266846A (en) * | 1998-03-19 | 1999-10-05 | Morinaga & Co Ltd | Antioxidant food |
-
2001
- 2001-10-03 CN CNA018191258A patent/CN1474655A/en active Pending
- 2001-10-03 AU AU2001292154A patent/AU2001292154A1/en not_active Abandoned
- 2001-10-03 AT AT01974563T patent/ATE321458T1/en not_active IP Right Cessation
- 2001-10-03 AT AT01972383T patent/ATE317447T1/en not_active IP Right Cessation
- 2001-10-03 DE DE60117158T patent/DE60117158T2/en not_active Expired - Fee Related
- 2001-10-03 EP EP01974563A patent/EP1324669B1/en not_active Expired - Lifetime
- 2001-10-03 WO PCT/IB2001/001827 patent/WO2002029077A2/en active IP Right Grant
- 2001-10-03 AU AU2001294077A patent/AU2001294077A1/en not_active Abandoned
- 2001-10-03 CN CNB018191266A patent/CN1279173C/en not_active Expired - Fee Related
- 2001-10-03 US US10/398,261 patent/US20040071820A1/en not_active Abandoned
- 2001-10-03 US US10/398,292 patent/US20040058421A1/en not_active Abandoned
- 2001-10-03 WO PCT/IB2001/001822 patent/WO2002028196A2/en active IP Right Grant
- 2001-10-03 EP EP01972383A patent/EP1330533B1/en not_active Expired - Lifetime
- 2001-10-03 DE DE60118413T patent/DE60118413T2/en not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| CN1474655A (en) | 2004-02-11 |
| ATE317447T1 (en) | 2006-02-15 |
| DE60118413D1 (en) | 2006-05-18 |
| WO2002028196A3 (en) | 2002-06-13 |
| DE60117158D1 (en) | 2006-04-20 |
| DE60118413T2 (en) | 2006-08-24 |
| ATE321458T1 (en) | 2006-04-15 |
| US20040071820A1 (en) | 2004-04-15 |
| AU2001294077A1 (en) | 2002-04-15 |
| DE60117158T2 (en) | 2006-07-20 |
| EP1324669A2 (en) | 2003-07-09 |
| EP1324669B1 (en) | 2006-03-29 |
| WO2002029077A3 (en) | 2002-05-30 |
| EP1330533A2 (en) | 2003-07-30 |
| US20040058421A1 (en) | 2004-03-25 |
| WO2002028196A2 (en) | 2002-04-11 |
| EP1330533B1 (en) | 2006-02-08 |
| WO2002029077A2 (en) | 2002-04-11 |
| CN1279173C (en) | 2006-10-11 |
| CN1527884A (en) | 2004-09-08 |
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