AU2001242431A1 - Method for producing polyetherpolyols - Google Patents
Method for producing polyetherpolyolsInfo
- Publication number
- AU2001242431A1 AU2001242431A1 AU2001242431A AU4243101A AU2001242431A1 AU 2001242431 A1 AU2001242431 A1 AU 2001242431A1 AU 2001242431 A AU2001242431 A AU 2001242431A AU 4243101 A AU4243101 A AU 4243101A AU 2001242431 A1 AU2001242431 A1 AU 2001242431A1
- Authority
- AU
- Australia
- Prior art keywords
- polyetherpolyols
- oxide
- reaction
- mixture
- producing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Abandoned
Links
- 238000004519 manufacturing process Methods 0.000 title 1
- XFXPMWWXUTWYJX-UHFFFAOYSA-N Cyanide Chemical compound N#[C-] XFXPMWWXUTWYJX-UHFFFAOYSA-N 0.000 abstract 1
- IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 abstract 1
- GOOHAUXETOMSMM-UHFFFAOYSA-N Propylene oxide Chemical compound CC1CO1 GOOHAUXETOMSMM-UHFFFAOYSA-N 0.000 abstract 1
- WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 abstract 1
- 239000003054 catalyst Substances 0.000 abstract 1
- 150000002009 diols Chemical class 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- 229920005862 polyol Polymers 0.000 abstract 1
- 150000003077 polyols Chemical class 0.000 abstract 1
- 239000011541 reaction mixture Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
- C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
- C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
- C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
- C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
- C08G65/2696—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds characterised by the process or apparatus used
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
- C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
- C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
- C08G65/2642—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds characterised by the catalyst used
- C08G65/2645—Metals or compounds thereof, e.g. salts
- C08G65/2663—Metal cyanide catalysts, i.e. DMC's
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Toxicology (AREA)
- Polyethers (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Catalysts (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
- Crystals, And After-Treatments Of Crystals (AREA)
- Other Investigation Or Analysis Of Materials By Electrical Means (AREA)
Abstract
A process for the preparation of polyetherpolyols by reacting diols or polyols with ethylene oxide, propylene oxide, butylene oxide or a mixture thereof in the presence of a multimetal cyanide complex catalyst is proposed, the reaction being carried out in a stirred kettle reactor and the reaction mixture being circulated via an external heat exchanger by means of a pump.
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE10008635 | 2000-02-24 | ||
DE10008635A DE10008635A1 (en) | 2000-02-24 | 2000-02-24 | Process for the preparation of polyether polyols |
PCT/EP2001/002032 WO2001062825A1 (en) | 2000-02-24 | 2001-02-22 | Method for producing polyetherpolyols |
Publications (1)
Publication Number | Publication Date |
---|---|
AU2001242431A1 true AU2001242431A1 (en) | 2001-09-03 |
Family
ID=7632229
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
AU2001242431A Abandoned AU2001242431A1 (en) | 2000-02-24 | 2001-02-22 | Method for producing polyetherpolyols |
Country Status (18)
Country | Link |
---|---|
US (1) | US6664428B2 (en) |
EP (1) | EP1259560B2 (en) |
JP (1) | JP2003526714A (en) |
KR (1) | KR100721466B1 (en) |
CN (1) | CN1239571C (en) |
AT (1) | ATE266693T1 (en) |
AU (1) | AU2001242431A1 (en) |
BR (1) | BR0108651B1 (en) |
CA (1) | CA2401221A1 (en) |
CZ (1) | CZ20022868A3 (en) |
DE (2) | DE10008635A1 (en) |
ES (1) | ES2220739T5 (en) |
HU (1) | HUP0204267A2 (en) |
MX (1) | MX225794B (en) |
PL (1) | PL357018A1 (en) |
PT (1) | PT1259560E (en) |
RU (1) | RU2271370C2 (en) |
WO (1) | WO2001062825A1 (en) |
Families Citing this family (21)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE10137628A1 (en) * | 2001-08-03 | 2003-02-27 | Basf Ag | Process for the production of flexible polyurethane foams |
EP1295902A1 (en) * | 2001-09-20 | 2003-03-26 | Shell Internationale Researchmaatschappij B.V. | Process for preparing polyoxyalkylene polyether products. |
CN1310998C (en) * | 2002-01-22 | 2007-04-18 | 旭硝子株式会社 | Method for continuously producing a polyether |
DE102004013408A1 (en) * | 2004-03-18 | 2005-10-06 | Basf Ag | Polyether alcohols and process for the preparation of polyether alcohols for polyurethane synthesis |
DE102004031836A1 (en) * | 2004-06-30 | 2006-01-19 | Basf Ag | Process for the preparation of polyether alcohols |
CN1320029C (en) * | 2005-05-31 | 2007-06-06 | 抚顺佳化聚氨酯有限公司 | Method for preparing polyether glycol |
DE102005034001A1 (en) | 2005-07-18 | 2007-01-25 | Basf Ag | Process for the preparation of polyether alcohols |
US7547801B2 (en) * | 2006-06-26 | 2009-06-16 | Bayer Materialscience Llc | Process for the continuous preparation of isocyanates |
US20080132729A1 (en) * | 2006-12-01 | 2008-06-05 | Mcdaniel Kenneth G | Continuous process for the production of ethoxylates |
DE102007057146A1 (en) | 2007-11-28 | 2009-06-04 | Evonik Goldschmidt Gmbh | Process for the preparation of polyether alcohols with DMC catalysts using special additives with aromatic hydroxy functionalization |
DE102007057145A1 (en) | 2007-11-28 | 2009-06-04 | Evonik Goldschmidt Gmbh | Process for the preparation of polyether alcohols with DMC catalysts using compounds bearing SiH groups as additives |
CN101225159B (en) * | 2008-01-04 | 2011-08-31 | 张国忠 | Method for producing polyether-type defoaming agent |
CN101220145B (en) * | 2008-01-24 | 2011-03-16 | 中国石油技术开发公司 | Method for producing low interfacial tension polyalcohol polyether |
DE102008043343A1 (en) | 2008-10-31 | 2010-05-06 | Evonik Goldschmidt Gmbh | Silicone polyether block copolymers with defined polydispersity in the polyoxyalkylene part and their use as stabilizers for the production of polyurethane foams |
DE102009002371A1 (en) | 2009-04-15 | 2010-10-21 | Evonik Goldschmidt Gmbh | Process for the preparation of odorless polyether alcohols by means of DMC catalysts and their use in cosmetic and / or dermatological preparations |
SG181448A1 (en) | 2010-01-15 | 2012-08-30 | Basf Se | "process for the dmc-catalyzed preparation of polyols" |
EP2542612B1 (en) * | 2010-03-02 | 2014-04-30 | Basf Se | Process for preparing polyether alcohols |
DE102013215664A1 (en) | 2013-08-08 | 2015-02-12 | Evonik Industries Ag | Apparatus for carrying out a ring-opening polymerization process |
US9879114B2 (en) | 2015-12-22 | 2018-01-30 | Covestro Llc | Process for the production of low molecular weight polyoxyalkylene polyols |
US10258953B2 (en) | 2016-08-05 | 2019-04-16 | Covestro Llc | Systems and processes for producing polyether polyols |
CN114433098B (en) * | 2020-10-20 | 2024-03-29 | 中国石油化工股份有限公司 | Catalyst, preparation method thereof and method for reducing aldehyde content in polyether polyol |
Family Cites Families (20)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3900518A (en) † | 1967-10-20 | 1975-08-19 | Gen Tire & Rubber Co | Hydroxyl or thiol terminated telomeric ethers |
US3894093A (en) † | 1969-07-16 | 1975-07-08 | Hoechst Ag | Process for the manufacture of addition products of ethylene oxide and compounds containing mobile hydrogen |
DE1936046C3 (en) * | 1969-07-16 | 1982-09-02 | Hoechst Ag, 6000 Frankfurt | Process for the production of addition products of ethylene oxide with compounds containing mobile hydrogen |
US3829505A (en) † | 1970-02-24 | 1974-08-13 | Gen Tire & Rubber Co | Polyethers and method for making the same |
US3941849A (en) † | 1972-07-07 | 1976-03-02 | The General Tire & Rubber Company | Polyethers and method for making the same |
JPH05320209A (en) * | 1992-05-19 | 1993-12-03 | Shin Etsu Chem Co Ltd | Apparatus for producing vinyl chloride polymer |
CH686117A5 (en) | 1993-07-08 | 1996-01-15 | Biazzi Sa | gas-liquid reaction apparatus. |
DE4323687A1 (en) † | 1993-07-15 | 1995-01-19 | Bayer Ag | Continuous process for the production of aromatic amines |
JPH09504031A (en) † | 1993-10-22 | 1997-04-22 | ザ・ダウ・ケミカル・カンパニー | Alkylene glycol with high primary hydroxyl content |
US5811595A (en) | 1994-07-08 | 1998-09-22 | Ellis; Vincent Simon | Process for preparing alkylene oxide reaction products |
NL9401302A (en) † | 1994-08-11 | 1996-03-01 | Scantech Bv | Barcode scanner. |
US5482908A (en) † | 1994-09-08 | 1996-01-09 | Arco Chemical Technology, L.P. | Highly active double metal cyanide catalysts |
JPH08188603A (en) * | 1995-01-11 | 1996-07-23 | Mitsui Toatsu Chem Inc | Polymerization equipment |
US5767323A (en) † | 1995-12-22 | 1998-06-16 | Arco Chemical Technology, L.P. | Process for preparing polyoxyalkylene polyether polyols having low levels of transition metals through double metal cyanide complex polyoxyalkylation |
EP0850954A1 (en) * | 1996-12-27 | 1998-07-01 | CP TECH S.r.l. | A method for the production of polyadducts of alkylene oxides with a liquid in a gas dispersion reactor |
EP0853975A1 (en) † | 1997-01-20 | 1998-07-22 | CP TECH S.r.l. | Apparatus for the production of polyadducts of alkylene oxides with a combined liquid-in-gas and gas-in-liquid dispersion reactor |
DE19742978A1 (en) * | 1997-09-29 | 1999-04-01 | Basf Ag | Multimetal cyanide complexes as catalysts |
DE19809539A1 (en) † | 1998-03-05 | 1999-09-09 | Basf Ag | Process for the preparation of double metal cyanide catalysts |
DE10008630A1 (en) * | 2000-02-24 | 2001-09-06 | Basf Ag | Production of polyether polyols comprises use of a multi-metal cyanide complex catalyst in a tall cylindrical reactor having a downward facing spray nozzle in the upper reactor portion. |
JP2002043319A (en) | 2000-07-19 | 2002-02-08 | Mitsubishi Electric Corp | Semiconductor device |
-
2000
- 2000-02-24 DE DE10008635A patent/DE10008635A1/en not_active Withdrawn
-
2001
- 2001-02-22 PT PT01915290T patent/PT1259560E/en unknown
- 2001-02-22 AU AU2001242431A patent/AU2001242431A1/en not_active Abandoned
- 2001-02-22 BR BRPI0108651-0A patent/BR0108651B1/en not_active IP Right Cessation
- 2001-02-22 KR KR1020027011055A patent/KR100721466B1/en not_active Expired - Lifetime
- 2001-02-22 WO PCT/EP2001/002032 patent/WO2001062825A1/en active IP Right Grant
- 2001-02-22 CN CNB018051545A patent/CN1239571C/en not_active Expired - Lifetime
- 2001-02-22 EP EP01915290A patent/EP1259560B2/en not_active Expired - Lifetime
- 2001-02-22 CZ CZ20022868A patent/CZ20022868A3/en unknown
- 2001-02-22 HU HU0204267A patent/HUP0204267A2/en unknown
- 2001-02-22 ES ES01915290T patent/ES2220739T5/en not_active Expired - Lifetime
- 2001-02-22 DE DE50102264T patent/DE50102264D1/en not_active Expired - Lifetime
- 2001-02-22 PL PL01357018A patent/PL357018A1/en not_active Application Discontinuation
- 2001-02-22 AT AT01915290T patent/ATE266693T1/en not_active IP Right Cessation
- 2001-02-22 JP JP2001562604A patent/JP2003526714A/en active Pending
- 2001-02-22 RU RU2002125667/04A patent/RU2271370C2/en not_active IP Right Cessation
- 2001-02-22 CA CA002401221A patent/CA2401221A1/en not_active Abandoned
- 2001-02-22 MX MXPA02008166 patent/MX225794B/en active IP Right Grant
- 2001-02-22 US US10/204,293 patent/US6664428B2/en not_active Expired - Lifetime
Also Published As
Publication number | Publication date |
---|---|
WO2001062825A1 (en) | 2001-08-30 |
ES2220739T5 (en) | 2011-07-18 |
MXPA02008166A (en) | 2003-05-23 |
PL357018A1 (en) | 2004-07-12 |
HUP0204267A2 (en) | 2003-05-28 |
ATE266693T1 (en) | 2004-05-15 |
CZ20022868A3 (en) | 2002-11-13 |
PT1259560E (en) | 2004-10-29 |
EP1259560A1 (en) | 2002-11-27 |
RU2002125667A (en) | 2004-01-10 |
BR0108651B1 (en) | 2010-12-28 |
ES2220739T3 (en) | 2004-12-16 |
BR0108651A (en) | 2002-12-17 |
EP1259560B1 (en) | 2004-05-12 |
CN1239571C (en) | 2006-02-01 |
DE50102264D1 (en) | 2004-06-17 |
KR20020095183A (en) | 2002-12-20 |
MX225794B (en) | 2005-01-25 |
US6664428B2 (en) | 2003-12-16 |
KR100721466B1 (en) | 2007-05-25 |
DE10008635A1 (en) | 2001-09-06 |
EP1259560B2 (en) | 2011-04-27 |
RU2271370C2 (en) | 2006-03-10 |
US20030013921A1 (en) | 2003-01-16 |
CA2401221A1 (en) | 2001-08-30 |
CN1400982A (en) | 2003-03-05 |
JP2003526714A (en) | 2003-09-09 |
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