AR104836A1 - Método de recuperación de productos químicos de la fabricación de pulpa a partir de ceniza disuelta con un alto contenido de carbonato - Google Patents
Método de recuperación de productos químicos de la fabricación de pulpa a partir de ceniza disuelta con un alto contenido de carbonatoInfo
- Publication number
- AR104836A1 AR104836A1 ARP160101590A ARP160101590A AR104836A1 AR 104836 A1 AR104836 A1 AR 104836A1 AR P160101590 A ARP160101590 A AR P160101590A AR P160101590 A ARP160101590 A AR P160101590A AR 104836 A1 AR104836 A1 AR 104836A1
- Authority
- AR
- Argentina
- Prior art keywords
- dissolved
- ash solution
- dissolved ash
- ash
- concentrated
- Prior art date
Links
- 238000000034 method Methods 0.000 title abstract 4
- 238000004519 manufacturing process Methods 0.000 title abstract 3
- 238000011084 recovery Methods 0.000 title abstract 2
- 239000000126 substance Substances 0.000 title abstract 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 title 1
- 229910052799 carbon Inorganic materials 0.000 title 1
- 238000002425 crystallisation Methods 0.000 abstract 4
- 230000008025 crystallization Effects 0.000 abstract 4
- CDBYLPFSWZWCQE-UHFFFAOYSA-L sodium carbonate Substances [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 abstract 4
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 abstract 2
- 229920001131 Pulp (paper) Polymers 0.000 abstract 2
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 abstract 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 abstract 2
- 229910000029 sodium carbonate Inorganic materials 0.000 abstract 2
- 229910052938 sodium sulfate Inorganic materials 0.000 abstract 2
- 235000011152 sodium sulphate Nutrition 0.000 abstract 2
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 abstract 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 abstract 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 abstract 1
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 abstract 1
- 239000012141 concentrate Substances 0.000 abstract 1
- 238000002156 mixing Methods 0.000 abstract 1
- 229910052700 potassium Inorganic materials 0.000 abstract 1
- 239000011591 potassium Substances 0.000 abstract 1
- 238000001556 precipitation Methods 0.000 abstract 1
- 238000010926 purge Methods 0.000 abstract 1
- 239000010802 sludge Substances 0.000 abstract 1
- 229910052708 sodium Inorganic materials 0.000 abstract 1
- 239000011734 sodium Substances 0.000 abstract 1
- 238000011144 upstream manufacturing Methods 0.000 abstract 1
Classifications
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21C—PRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
- D21C11/00—Regeneration of pulp liquors or effluent waste waters
- D21C11/12—Combustion of pulp liquors
- D21C11/14—Wet combustion ; Treatment of pulp liquors without previous evaporation, by oxidation of the liquors remaining at least partially in the liquid phase, e.g. by application or pressure
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21C—PRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
- D21C11/00—Regeneration of pulp liquors or effluent waste waters
- D21C11/06—Treatment of pulp gases; Recovery of the heat content of the gases; Treatment of gases arising from various sources in pulp and paper mills; Regeneration of gaseous SO2, e.g. arising from liquors containing sulfur compounds
- D21C11/063—Treatment of gas streams comprising solid matter, e.g. the ashes resulting from the combustion of black liquor
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
- C01D5/00—Sulfates or sulfites of sodium, potassium or alkali metals in general
- C01D5/16—Purification
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
- C01D7/00—Carbonates of sodium, potassium or alkali metals in general
- C01D7/22—Purification
- C01D7/24—Crystallisation
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21C—PRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
- D21C11/00—Regeneration of pulp liquors or effluent waste waters
- D21C11/0085—Introduction of auxiliary substances into the regenerating system in order to improve the performance of certain steps of the latter, the presence of these substances being confined to the regeneration cycle
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21C—PRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
- D21C11/00—Regeneration of pulp liquors or effluent waste waters
- D21C11/06—Treatment of pulp gases; Recovery of the heat content of the gases; Treatment of gases arising from various sources in pulp and paper mills; Regeneration of gaseous SO2, e.g. arising from liquors containing sulfur compounds
- D21C11/063—Treatment of gas streams comprising solid matter, e.g. the ashes resulting from the combustion of black liquor
- D21C11/066—Separation of solid compounds from these gases; further treatment of recovered products
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21C—PRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
- D21C11/00—Regeneration of pulp liquors or effluent waste waters
- D21C11/12—Combustion of pulp liquors
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P40/00—Technologies relating to the processing of minerals
- Y02P40/40—Production or processing of lime, e.g. limestone regeneration of lime in pulp and sugar mills
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Inorganic Chemistry (AREA)
- Paper (AREA)
Abstract
Un método de recuperación de productos químicos de la fabricación de pulpa de madera a partir de un licor negro producido en un proceso de fabricación de pulpa de madera en donde el proceso involucra quemar el licor negro en una caldera de recuperación para formar ceniza que contiene altos niveles de carbonato así como también sodio, potasio y cloruro. La ceniza es disuelta para formar una solución de ceniza disuelta que se dirige hacia una unidad de primera etapa de cristalización que concentra la solución de ceniza disuelta y que da lugar a la precipitación de sulfato de sodio y carbonato de sodio. A continuación la solución de ceniza disuelta concentrada se dirige hacia una unidad de segunda etapa de cristalización que enfría adiabáticamente la solución de ceniza disuelta concentrada para formar un lodo de glaserita y una corriente de purga que resulta rica en cloruro. Con el objetivo de reducir la tendencia a cristalizar del carbonato de sodio y la burkeita en la unidad de segunda etapa de cristalización y para inducir la cristalización de glaserita pura en el cristalizador, el método involucra mezclar una fuente de sulfato, tal como sulfato de sodio o ácido sulfúrico, con la solución de ceniza disuelta concentrada corriente arriba del cristalizador.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201562169031P | 2015-06-01 | 2015-06-01 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| AR104836A1 true AR104836A1 (es) | 2017-08-16 |
Family
ID=57399632
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ARP160101590A AR104836A1 (es) | 2015-06-01 | 2016-05-31 | Método de recuperación de productos químicos de la fabricación de pulpa a partir de ceniza disuelta con un alto contenido de carbonato |
Country Status (10)
| Country | Link |
|---|---|
| US (1) | US9574303B2 (es) |
| JP (1) | JP6556264B2 (es) |
| CN (1) | CN107660245B (es) |
| AR (1) | AR104836A1 (es) |
| AU (1) | AU2016271293B2 (es) |
| BR (1) | BR112017025523B1 (es) |
| CA (1) | CA2988081C (es) |
| CL (1) | CL2017003054A1 (es) |
| WO (1) | WO2016196430A1 (es) |
| ZA (1) | ZA201707870B (es) |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107902677A (zh) | 2016-12-12 | 2018-04-13 | 威立雅水处理技术公司 | 从废水中生产硫酸钾和氯化钠的方法 |
| FI130066B (en) * | 2019-02-13 | 2023-01-31 | Andritz Oy | A method for replacing sodium losses in a pulp mill and a method for producing bleached cellulose pulp |
| CN113998712A (zh) * | 2021-11-18 | 2022-02-01 | 江苏力波兴水务科技有限公司 | 一种碱灰析滤液脱除氯离子并回收硫酸钠与碳酸钠的方法 |
| WO2024151589A1 (en) | 2023-01-10 | 2024-07-18 | Veolia Water Technologies, Inc. | System and process for reducing chemical losses in treating ash produced in a recovery boiler of a wood pulping process |
| AT527522A1 (de) * | 2023-09-12 | 2025-03-15 | Mondi Ag | Verfahren zum Kompaktieren eines Materials |
Family Cites Families (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS4943482B2 (es) * | 1971-11-02 | 1974-11-21 | ||
| CH572867A5 (es) * | 1972-12-15 | 1976-02-27 | Escher Wyss Ag | |
| JPS5673620A (en) * | 1979-11-19 | 1981-06-18 | Tokuyama Soda Co Ltd | Separation of sodium sulfate and sodium chloride from mixed solution of sodium chloride and sodium sulfate |
| DD273427A1 (de) | 1988-06-28 | 1989-11-15 | Kali Veb K | Verfahren zur erhoehung der wertstoffausbeute bei der glaseritkristallisation |
| JPH04146284A (ja) * | 1990-10-08 | 1992-05-20 | Babcock Hitachi Kk | アルカリ金属塩含有灰からぼう硝の回収方法およびその装置 |
| JPH09234302A (ja) * | 1996-03-04 | 1997-09-09 | Mitsubishi Heavy Ind Ltd | パルプ蒸解薬品中のカリウム塩除去装置及びその温度調節方法 |
| CN100528752C (zh) * | 2007-09-17 | 2009-08-19 | 长沙理工大学 | 一种从蒸煮黑液中回收木素和碱的方法 |
| JP5079631B2 (ja) * | 2008-08-11 | 2012-11-21 | 株式会社ダイセキ | 廃液の減量方法及び廃液の処理方法 |
| CN101831826B (zh) * | 2010-06-22 | 2012-05-23 | 永州湘江纸业有限责任公司 | 一种造纸制浆黑液结晶蒸发方法 |
| US8721837B2 (en) * | 2012-07-26 | 2014-05-13 | Veolia Water Solutions & Technologies North America, Inc. | Method for recovering pulping chemicals and reducing the concentration of potassium and chloride therein |
-
2016
- 2016-05-26 US US15/165,332 patent/US9574303B2/en active Active
- 2016-05-31 JP JP2017562328A patent/JP6556264B2/ja active Active
- 2016-05-31 AR ARP160101590A patent/AR104836A1/es active IP Right Grant
- 2016-05-31 WO PCT/US2016/034957 patent/WO2016196430A1/en active Application Filing
- 2016-05-31 BR BR112017025523-5A patent/BR112017025523B1/pt active IP Right Grant
- 2016-05-31 CA CA2988081A patent/CA2988081C/en active Active
- 2016-05-31 AU AU2016271293A patent/AU2016271293B2/en not_active Ceased
- 2016-05-31 CN CN201680031822.3A patent/CN107660245B/zh active Active
-
2017
- 2017-11-20 ZA ZA2017/07870A patent/ZA201707870B/en unknown
- 2017-11-30 CL CL2017003054A patent/CL2017003054A1/es unknown
Also Published As
| Publication number | Publication date |
|---|---|
| BR112017025523B1 (pt) | 2022-05-24 |
| AU2016271293A1 (en) | 2017-12-07 |
| CN107660245B (zh) | 2020-09-08 |
| CL2017003054A1 (es) | 2018-04-13 |
| JP2018524484A (ja) | 2018-08-30 |
| CN107660245A (zh) | 2018-02-02 |
| ZA201707870B (en) | 2019-05-29 |
| US9574303B2 (en) | 2017-02-21 |
| CA2988081C (en) | 2021-01-12 |
| WO2016196430A1 (en) | 2016-12-08 |
| US20160348310A1 (en) | 2016-12-01 |
| JP6556264B2 (ja) | 2019-08-07 |
| AU2016271293B2 (en) | 2018-10-04 |
| CA2988081A1 (en) | 2016-12-08 |
| BR112017025523A2 (pt) | 2018-08-07 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FG | Grant, registration |