[go: up one dir, main page]

Skip to main content

Advertisement

Log in

Microstructural characterization of a modified 706-type Ni-Fe superalloy by small-angle neutron scattering and electron microscopy

  • Published:
Metallurgical and Materials Transactions A Aims and scope Submit manuscript

Abstract

The new Ni-Fe-based superalloy DT706, derived from INCONEL 706, is the object of studies for potential uses in turbine-disk applications at temperatures above 973 K. This alloy aims at improving the microstructural stability while preserving the excellent machinability and good mechanical properties of the base material. This article is the first of a two-part study concentrating on the characterization of the microstructure of the DT706 precipitates, depending on the heat-treatment conditions. Analyses were performed by means of ex-situ small-angle neutron scattering (SANS) measurements, together with conventional scanning electron microscopy (SEM) and transmission electron microscopy (TEM) microscopy, on experimentally-heat-treated samples. The results, when compared to a similar analysis previously made on INCONEL 706, showed that the precipitation characteristics of DT706 reflect compositional changes, but are still remarkably dependent on the cooling stages between the different heat-treatment steps.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Subscribe and save

Springer+ Basic
$34.99 /Month
  • Get 10 units per month
  • Download Article/Chapter or eBook
  • 1 Unit = 1 Article or 1 Chapter
  • Cancel anytime
Subscribe now

Buy Now

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Similar content being viewed by others

References

  1. J. Rösler, M. Götting, D. Del Genovese, B. Böttger, R. Kopp, M. Wolske, F. Schubert, H.-J. Penkalla, T. Seliga, A. Thoma, A. Scholz, and C. Berger: Adv. Eng. Mater., 2003, vol. 5 (7), pp. 469–83.

    Article  Google Scholar 

  2. J. Rösler, B. Böttger, M. Wsolske, H.J. Penkalla, and C. Berger: Materials for Advanced Power Engineering, J. Lecomte-Beckers, M. Carton, F. Schubert, and P.J. Ennis, eds., Forschungszentrum Jülich, Jülich, Germany, 2002, pp. 89–106.

    Google Scholar 

  3. “INCONEL 706,” Technical Brochure, Huntington Alloys Inc., Huntington WV, 1974, p. 3.

  4. P.W. Schilke and R.C. Schwant: Superalloys 718, 625, 706 and Various Derivatives, E.A. Loria, ed., TMS, Warrendale, PA, 2001, pp. 25–34.

    Google Scholar 

  5. R. Cozar and A. Pineau: Metall. Trans., 1973, vol. 4, pp. 47–59.

    CAS  Google Scholar 

  6. J. Rösler, S. Müller, D. Del Genovese, and M. Götting: Superalloys 718, 625, 706 and Various Derivatives, E.A. Loria, ed., TMS, Warrendale, PA, 2001, pp. 523–34.

    Google Scholar 

  7. C.T. Sims, N.S. Stoloff, and W.C. Hagel: Superalloys II, Chester Thomas, C.T. Sims, N.S. Stoloff, and W.C. Hagel, eds., Wiley Interscience Publication, New York, NY, 1987, pp. 178–80.

    Google Scholar 

  8. H.J. Penkalla, J. Wosik, W. Fischer, and F. Schubert: Superalloys 718, 625, 706 and Various Derivatives, E.A. Loria, ed., TMS, Warrendale, PA, 2001, pp. 279–90.

    Google Scholar 

  9. M. Durand-Charre: The Microstructure of Superalloys, Gordon and Breach Science Publishers, Amsterdam, The Netherlands, 1997, p. 47.

    Google Scholar 

  10. G. Härkegård, W. Ballach, K. Stärk, and J. Rösler: Superalloys 718, 625, 706 and Various Derivatives, E.A. Loria, ed., TMS, Warrendale, PA, 1997, pp. 425–30.

    Google Scholar 

  11. S. Müller and J. Rösler: Life Assessment of Hot Section Gas Turbine Components, R. Townsend, M. Winstone, M. Henderson, J.R. Nichols, A. Partridge, B. Nath, M. Wood, and R. Viswanathan, eds., Cambridge University Press, Cambridge, United Kingdom, 1999, pp. 49–60.

    Google Scholar 

  12. S. Müller and J. Rösler: Steels and Materials for Power Plants, P. Neumann, D. Allen, and E. Tenckhoff, eds., Wiley-VCH-Verlag, Gmbh, Weinheim, Germany, 2000, pp. 352–58.

    Chapter  Google Scholar 

  13. E. Andrieu, N. Wang, R. Molins, and A. Pineau: Superalloys 718, 625, 706 and Various Derivatives, E.A. Loria, ed., TMS, Warrendale, PA, 1994, pp. 695–710.

    Google Scholar 

  14. C.T. Sims, N.S. Stoloff, and W.C. Hagel: Superalloys II, Chester Thomas, C.T. Sims, N.S. Stoloff, and W.C. Hagel, eds., Wiley Interscience Publication, New York, NY, 1987, p. 170.

    Google Scholar 

  15. S. Mannan, S. Patel, and J. deBarbadillo: Superalloys 2000, K.A. Green, T.M. Pollock, R.D. Kissinger, and R.R. Bowmann, eds., TMS, Warrendale, PA, 2000, pp. 449–58.

    Google Scholar 

  16. X. Xie, Q. Liang, J. Dong, W. Meng, Z. Xu, M. Chan, F. Wang, E. Andrieu, and A. Pineau: Superalloys 718, 625, 706 and Various Derivatives, E.A. Loria, ed., TMS, Warrendale, PA, 1994, pp. 711–20.

    Google Scholar 

  17. D. Mukherji, P. Strunz, D. Del Genovese, R. Gilles, J. Rösler, and A. Wiedenmann: Metall. Mater. Trans. A, 2003, vol. 34A, pp. 2781–92.

    CAS  Google Scholar 

  18. D. Del Genovese, P. Strunz, D. Mukherji, R. Gilles, and J. Rösler: IFW, Technical University of Braunschweig, 2004–2005, unpublished research.

  19. T. Shibata, T. Takahashi, Y. Shudo, M. Kusuhashi, J. Taira, and T. Ishiguro: Superalloys 718, 625, 706 and Various Derivatives, E.A. Loria, ed., TMS, Warrendale, PA, 1997, pp. 379–88.

    Google Scholar 

  20. Petzow Günter: Metallographisches, Keramographisches, Plastographisches Ätzen, 6th ed., Gebrüder Bornträger, ed., Berlin, 1994, p. 241.

  21. Leszek Wojmar: Image Analysis: Applications in Material Engineering, CRC Press LLC, Boca Raton, FL, 1998, pp. 123–28.

    Google Scholar 

  22. P. Strunz, K. Mortensen, and S. Janssen: Physica B, 2004, vol. 350, p. e783.

  23. P. Strunz, R. Gilles, D. Mukherji, and A. Wiedenmann: J. Appl. Cryst., 2003, vol. 36, pp. 854–59.

    Article  CAS  Google Scholar 

  24. G. Kostorz: Neutron Scattering, G. Kostorz, ed., Academic Press, New York, NY, 1979, pp. 227–89.

    Google Scholar 

  25. N. Saunders, M. Fahrmann, and C.J. Small: Superalloys 2000, K.A. Green, R.D. Kissinger, T.M. Pollock, and R.R. Bowmann, eds., TMS, Warrendale, PA, 2000, pp. 803–11.

    Google Scholar 

  26. D.F. Paulonis, J.M. Oblak, and D.S. Duvall: Trans. ASM, 1969, vol. 62, pp. 611–22.

    CAS  Google Scholar 

  27. E. Andrieu, R. Cozar, and A. Pineau: Superalloys 718, 625, 706 and Various Derivatives, E.A. Loria, ed., TMS, Warrendale, PA, 1989, pp. 241–56.

    Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Rights and permissions

Reprints and permissions

About this article

Cite this article

Del Genovese, D., Rösler, J., Strunz, P. et al. Microstructural characterization of a modified 706-type Ni-Fe superalloy by small-angle neutron scattering and electron microscopy. Metall Mater Trans A 36, 3439–3450 (2005). https://doi.org/10.1007/s11661-005-0017-3

Download citation

  • Received:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s11661-005-0017-3

Keywords

Navigation