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(Reversible) Hydrocolloid

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AGAR

(reversible)
hydrocolloid

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DEFINITION
• An aqueous impression material used for
recording maximum detail; e.g. as required in
the production of dies for fixed restorations.
• An organic hydrophilic colloid (polysaccharide)
extracted from certain types of seaweed.

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COMPOSITION OF COMMERCIAL
REVERSIBLE HYDROCOLLOID
IMPRESSION MATERIALS
component function composition(%)
agar brush-heap structure 13-17

borate strength 0.2-0.5


sulfate gypsum hardener 1.0-2.0

wax, hard filler 0.5-1.0


thixotropic materials thickener 0.3-0.5

water reaction medium balance


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CLASSIFICATION
(ISO 1564: 2001)
• TYPE I – high consistency (for use as tray
material)
• TYPE II – medium consistency (for use as tray
or syringe material)
• TYPE III – low consistency (for syringe use
only)

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USES
• For cast duplication (e.g. during fabrication of
cast metal removable partial dentures, etc.)
• For full mouth impressions without deep
undercuts.
• Previously used for FPD impressions prior to
elastomers.
• As a tissue conditioner.

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SUPPLIED AS
• Two forms:
 Syringe material
 Tray material
• Tubes are used to fill the water-cooled trays
and cartridges for use with the syringes.
• Differences between two forms are the color
and a greater fluidity of the syringe material.

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CARTRIDGE OF AGAR HYDROCOLLOID AND SYRINGES
USED FOR INJECTING ONTO THE PREPARED TOOTH.
ALSO SHOWN IS THE HOLDER FOR CARRYING THE
AGAR INTO THE CONDITIONING UNIT.
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MANIPULATION
• Manipulation includes:
 liquefying the gel
 placing it in the impression tray
 tempering it to a lower temperature that the
patient can tolerate
 maintenance of fluid state to capture details of
oral structures
 once in the mouth, material is cooled below
mouth temperature to ensure gelation

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• The process requires proper equipment.
• Three compartments in conditioning unit
make it possible to simultaneously liquefy,
store, and temper the hydrocolloid.
• Temperatures in each of the step are critical.
• Equipment should be calibrated weekly.

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CONDITIONING UNIT FOR AGAR HYDROCOLLOID
IMPRESSION MATERIALS. THE THREE COMPARTMENTS ARE
USED FOR LIQUEFYING THE MATERIAL, STORING AFTER
BOILING, AND TEMPERING THE TRAY HYDROCOLLOID.
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Step 1: Preparation and conditioning of the
agar material

• First step is to liquefy the hydrocolloid gel in boiling


water for at least 10 minutes.
• After liquefaction, the material may be stored in the
sol condition at 65⁰C until needed for injection into
prepared tooth or for filling a tray.
• The material can be stored for several days,
therefore, a number of tubes and syringes can be
prepared for use throughout a week or so.

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Step 2: Tempering of the material
• 65⁰C is too hot for the oral tissues, therefore, the
material used to fill the tray must be tempered.
• For immediate preparation step : hydrocolloid sol
removed from storage bath, tray filled with sol, gauze
pad placed over it, placed in water filled tempering
container at 45⁰C.
• Tempering time 3-10 minutes.
• To ensure that agar temperature is <55⁰C.

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• Tempering increases viscosity.
• Syringe material is never tempered but always
maintained in a fluid state to enhance adaptation to
tissues.

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Step 3: Making the agar impression
• Just before completion of tempering for tray material, low
viscosity material syringed directly from storage compartment
is applied to prepared tooth (first applied to the base, then
rest of the preparation covered).
• Gauze pack and outer layer of agar is removed from
tempering bath, transferred into stock tray and seated with
light pressure.
• Gelation is accelerated by circulating cool water (18-21⁰C)
through the tray for 3-5 min.
• Lower the temperature, more rapid is the gelation and
stronger the material.
• Impression removed suddenly with snap (viscoelastic
behavior).
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AGAR HYDROCOLLOID IMPRESSION
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LAMINATE TECHNIQUE
• Recent modification to traditional agar procedure.
• Hydrocolloid in the tray is replaced with a mix of
chilled alginate that bonds with the agar
expressed from a syringe.
• Alginate gels by a chemical reaction, whereas,
agar gels by means of contact with the cool
alginate.
• Since agar is in contact with the prepared teeth,
maximum detail is reproduced.

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PROPERTIES OF AGAR HYDROCOLLOID
IMPRESSION MATERIALS

Gelation Elastic Flexibility** Compressive Tear


(⁰C) recovery* (%) strength*** strength
(%) (MPa) (kN/m)

agar 37-45 99.0 4-15 0.78 0.8-0.9

* At 10% compression for 30 sec.


** At a stress of 1000 g/cm²
*** At a loading rate of 10 kg/min.

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Other properties
• Accuracy:
 Highly accurate at the time of removal from the
mouth, but shrinks in air and expands in water.
• Viscosity of the sol:
 Sufficiently viscous to record every detail of the
teeth and soft tissues if correctly manipulated.

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• Compatibility with gypsum:
 More compatible with gypsum model materials than
alginates.
 Washed of saliva or blood.
 Excess liquid blown with an air syringe.
• Dimensional stability:
 If stored in air, lose water and contract.
 Replacement in water leads to absorption and
swelling.
 Best stored in 100% relative humidity.

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ADVANTAGES DISADVANTAGES
• Accurate dies can be • Does not flow well.
prepared. • Cannot be electroplated.
• Good elastic properties help • Thermal discomfort on
reproduce most undercut insertion or gelation.
areas. • Dimensional instability.
• Has good recovery from • Tears easily.
distortion.
• Only one model can be
• Hydrophilic. poured.
• Palatable and well • Needs special equipment
tolerated. and technique.
• Economical. • Risk of contamination and
• Reusable. deterioration of properties
• Cost effective. on reuse.
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