800

7.311
600
=====================================================================
400
Acq. Operator : SYSTEM Seq. Line : 6

8.982
6.848
200
Acq. Instrument : GC-02 Location : Vial 6
0
Injection Date 2 : 10/30/2023 3 9:13:29 4PM 5 Inj 6: 1 7 8 9 min
FID2 B, Back Signal (FA23_227_E7_LIDOCAINE_M-06_001.D)
Inj Volume : 0.2 µl
pA Volume from Sample Entry! Actual Inj Volume : 1 µl
Different 1800
Inj
Sequence
Use theFile
GC-FID
1600 : D:\DATA\FA23-CHEM225-227\DEF_GC
data below if your University N-Number ends in 0
2023-10-30 19-54-14\DEF_GC.S
Method 1400 : D:\DATA\FA23-CHEM225-227\DEF_GC 2023-10-30 19-54-14\ORGOLAB_2018-JTH-UPDATE
1200 .M (Sequence Method)
The following
1000
Last changed
GC-FID was collected after an attempt to synthesize and purify lidocaine according
: 10/30/2023 7:54:14 PM by SYSTEM
to the
procedure
Method Info800that you carried
: Orgolab Nov out2018-JTH
in Experiment #7A.
600
400
FID1 A, Front Signal (FA23_227_E7_LIDOCAINE_M-06_001.D)
200
pA
1800 0
2 3 4 5 6 7 8 9 min
1600
1400
=====================================================================
1200
Area Percent Report
1000
=====================================================================
800

7.311
600
Sorted By : Signal
400

8.982
6.848
Multiplier : 1.0000
200
Dilution : 1.0000
0
Do not
2 use Multiplier
3 & Dilution
4 Factor with
5 ISTDs 6 7 8 9 min
FID2 B, Back Signal (FA23_227_E7_LIDOCAINE_M-06_001.D)
pA
1800
Signal 1: FID1 A, Front Signal
1600
1400
Peak RetTime Type Width Area Height Area
1200
# [min] [min] [pA*s] [pA] %
1000
----|-------|----|-------|----------|----------|--------|
800
1 6.848 BB 0.0179 26.14561 23.24066 5.10994
600
2 7.311 BB 0.0190 447.44836 368.66861 87.44994
400
3 8.982 BB 0.0187 38.06832 31.94608 7.44013
200
0
Totals
2
: 3
511.66230
4
423.85535
5 6 7 8 9 min

===================================================================== Page 1 of 2
GC-02 10/30/2023 9:25:28 PM SYSTEM
Area Percent Report
=====================================================================

Sorted By : Signal
Multiplier : 1.0000
Dilution : 1.0000
Do not use Multiplier & Dilution Factor with ISTDs

Signal 1: FID1 A, Front Signal

Peak RetTime Type Width Area Height Area

# [min] [min] [pA*s] [pA] %
----|-------|----|-------|----------|----------|--------|
1 6.848 BB 0.0179 26.14561 23.24066 5.10994
2 7.311 BB 0.0190 447.44836 368.66861 87.44994
3 8.982 BB 0.0187 38.06832 31.94608 7.44013

Totals : 511.66230 423.85535

GC-02 10/30/2023 9:25:28 PM SYSTEM Page 1 of 2