Tiki Tar and Shell India Pvt Ltd

Website: wwww.tkitarshel com

CIN No.: U23300MH2019PTC33I592

Certification Certificate of Quality (Quality Assurance)

Product Shell Cariphalte PG 70E-10 as per IS 15462 2019

Location Taloja
Testtype Quality Assurance

Sample Receipt Date 03/03/2023

Batch/Sample No. 2023/TL/SAM/PMB 70E-10/5621

Truck No. MH 46 BM 6433

Report No. FG/PMB 70E-10/Q4 TL/2023/14958

Laboratory Taloja
Involce No. TSTWSI222300582

Test Property Test method Units Results

Specification Comments

(A) Tests to be Carried out on Original

Binder

Softening point (R&B). "C, Min IS: 1205 265 75.4 PASS

Elastic recovery of half thread in IS 15462:2019

270% 76 PASS
ductilometer at 15°C, percent, Min Annex A

Flash point, COC, °C, Min S 1209 C 2 230 C 338 PASS

Viscosity at 150"C, Pa.s, Max ASTM D 4402 Pa.s s12 Pas 1.17 PASS

Complex modulus (G") divided by Sin

delta (G*/sin 6) as Min 1.0 kPa, 25mm IS 15462:2019
Plate, 1mm Gap, at 10 rad/s, at a
kpa 21 kpa 4.34 PASS
Annex B
temperature, 70'C

IS 15462 2019
Phase Angle (6), degree, Max degree 75 degree 58.2 PASS
Annex B

Separation, difference in softening IS 15462:2019

s3 C 1.7 PASS
point (R&B), "C, Max Annex C

FRAASS breaking point, "C, Max IS 9381 C S-10 C 14 PASS

(8) Tests to be Carried out on Rolling

Thin Film Oven (RTFO) Residue

Loss in mass, percent, Max Is 9382 s10% 0.04 PASS

Complex modulus (G*/sin 5) as Min

IS 15462.2019
2.2 kPa, at 10 rad/s, at a temperature, kpa 222 kpa 8.45 PASS
Annex B
70°C

MSCR Test

IS 15462:2019
Jnr3.2, Test Temperature, 70°C
Annex D
KPa-1 s0.5 kPa-1 0.29 PASS

IS 15462:2019
Jnrdiff, Test Temperature, 70°C s75 % 38.88 PASS
Annex D

(C) Tests to be Carried out on Pressure

Aging Vessel (PAV) Residue

Complex modulus (G) multiplied by

Sin delta (G*sin 6) as Max 6000 kPa, 8 IS 15462:2019
s 6000 kpa 3968 PASS
mm Plate, 2 mm Gap, at 10 rad/s at a Annex DA PRIy
temperature, 34°C PRIVATE
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BEST BITUMEN FOR BEST ROADS

Date: 06/03/2023
ViGN
 Tiki Tar and Shell India Pvt ltd
Website: vwww.tkitarshell corm
CIN No. U2330OMH2019PTC331592

Certificate of Quality (Quality Assurance)

Certification
Shell Cariphalte PG 76E-10 as per IS 15462 2019
Product

Location Taloja

Quality Assurance
Test type

Sample Receipt Date 07/03/2023

Batch/Sample No.
2023/TL/SAM/PMB 76E-10/5635

. MH 01 DR 4199
Truck No.

Report No. FG/PMB 76E-10/Q4 TL/2023/14987

Laboratory Taloja

Invoice No. TSTWS1222300587

Test method Units Specification Results Comments

Test Property

(A) Tests to be Carried out on Original

Binder

270 77 6 PASS
Softening point (R&B), "C, Min IS 1205

Elastic recovery of half thread in IS 15462 2019 76 PASS

2 70%
ductlometer at 15'C, percent, Min Annex A

2 230 C 338 PASS

Flash point, COC, "C, Min S 1209

ASTM D 4402 Pa.s .18 PASS

Viscosity at 150"C, Pa.s, Max S1.2 Pa.s
Complex modulus (G*) divided by Sin
delta (G/Sin 6) as Min 1.0kPa, 25mm IS 15462 2019 4 86 PASS
Kpa 21kkpa
Plate, 1mm Gap, at 10 rad/s, at a Annex B

temperature, 76°C

IS 15462.2019
degree $75 degree 57.6 PASS
Phase Angle (6), degree, Max
AnnexIB

Separation, difference in softening9 IS 15462 2019 C 4 PASS

C
point (R&B), 'C, Max Annex C

C -10 C PASS
FRAASS breaking point, "C, Max IS 9381

(B) Tests to be Carried out on Rolling

Thin Film Oven (RTFO) Residue

S1.0% 0.04 PASS

Loss in mass, percent, Max IS 9382

Complex modulus (G*) div1ded by Sin

delta (G/sin 6) as Min 2 2 kPa, 25mm IS 15462 2019 4.88 PASS
Plate, 1mm Gap, at 10 rad/s, at a Annex B
kpa 222 kpa
temperature, 76'C

MSCR Test
IS 15462 2019 PASS
kPa-1 sO5 kPa-1 0.26
Jnr3 2, Test Temperature, 76°C
Annex D

IS 15462:2019 s 75 % 58.3 PASS

Jnrdiff, Test Temperature, 76°C
Annex D

(C) Tests to be Carried out on Pressure

Aging Vessel (PAV) Residue

Complex modulus (G") multiplied by

Sin delta (G*sin 8) as Max 6000 kPa,8 IS 15462.2019 s 6000 kpa 4134 PASS
kpa
mm Plate, 2 mm Gap, at 10 rad/s at a Annex C
DAPRIV N
temperature, 37"C

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BEST BITUMEN FOR BEST ROADS

Date 09/03/2023 VIGH

 Tiki Tar and Shell India Pvt Ltd
Website: www.tkitarshell.corn
CIN No.: U2330OMH2019PTC331592

Certification :Certificate of Quality (Quality Assurance)

: Shell Bitumen VG 40 as per IS 73 : 2013

Product

Location : Taloja

Test type :QualityAssurance

Sample Receipt Date :01/03/2023

Batch/Sample No. 2023/TL/SAM/VG40/5598

Truck No. MH 14 KA 7802

Report No. :FG/VG40/QA-TL/2023/14901

Laboratory Taloja

Invoice No. : TSTWSI222300578

Test method Units Specification Results Comments

Test Property

IS: 1205 C 250 52.6 Pass

Softening Point (R&B), °C, Min

IS 1206 (Part 4136 Pass

Absolute Viscosity@ 60 °C poises 3200 to 4800
2)
Penetration at 25°C,100g, 5s IS: 1203 dmm 235 42 Pass

IS 1206 (Part
Kinematic Viscosity @135°C CSt 2400 579 Pass
3)
IS 1448 (P
Flash Point, COC, °C, Min C 2220 316 Pass
69
Solubility in Trichloroethylene IS: 1216 299 99.42 Pass

Tests on residue

IS 1206 (Part
Viscosity Ratio@60 "C poises s4 poises 2.4 Pass
2)
IS: 1208 Cm 2 25 cm 76 Pass
Ductility@ 25°C

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Date: 02/03/2023

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 Tiki Tar and Shell India Pvt Ltd
Website: www.tikitarshell com
CIN No.: U23300MH2019PTC331592

Certification f toboratty use nty

Certificate of Quality (Quality Assurance)

Product Shell Mexphalte CRMB 60 as per IS 17079 2019

Location Taloja

Test type
:Quality Assurance
Sample Receipt Date 26/02/2023

Batch/Sample No.
2023/TL/SAM/CRMB 60/5570
Truck No. :MH 04
GR 4766
Report No. : FG/CRMB 60/QA-TL/2023/14846

Laboratory Taloja
Invoice No. TSTWSI222300570

Test Property Test method Units Specification Results Comments

(A) Tests to be Carried out on Original
Binder

enetration at 25°C, 0.1 mm, 1000 g.

IS: 1203 dmm 20 to 50 dmm 25
5s Pass

Softening point (R&B), °C, Min IS: 1205 C 260 C 65.8 Pass
Flash point, COc, "C, Min IS1209 2220 C 322 Pass
Elastic recovery of half thread in IS 17079:2019
ductilometer at 15°C, percent, Min % 260% 55 Pass
Annex A

Complex modulus (G*/sin 6) as Min

IS 15462:2019
1.0 kPa, at 10 rad/s, at a temperature, kpa 1 kpa 4.22
Annex B Pass
70'C

Separation, difference in softening IS 15462:2019

C s4 C 2.4 Pass
point (R&B), °C, Max Annex C

IS 1206 (Part
Viscosity at 150°C, Poise, Max poises 6 to 12 poises 11.1 Pass
)

Test to be carried out on Thin Film Oven

Residue

Loss in mass, percent, Max S 9382

$1% 0.033 Pass

Change in Softening Point S 1205 C s5*C 2.8 Pass

Reduction in penetration of residue, atIS 1203 s 35% 28.6 Pass

25°C, percent, Max

Elastic recovery of half thread in IS 17079:2019

235 % 55.2 Pass
ductilometer at 25°C. percent, Min Annex A

Complex modulus (G*) divided by Sin IS 15462:2019

delta (G/sin 6) as Min 2.2 kPa at 2 2.2 kpa 7.69 VATE Rass
Kpa
Annex B
10rad/s, at a temperature 70°C

This is auto generated report does not require signature.

BEST BITUMEN FOR BEST ROADS

Date: 28/02/2023
 Tiki Tar and Shell India Pvt
Ltd
Website: www.tkitarshell.com
CIN No.: U23300MH2019PTC331592

for lcboratory wse only

Certification
:Certificate of Quality
(Quality Assurance)
Product : Shell Bitumen VG 10 as per IS 73: 2013
Location : Taloja

Test type
:Quality Assurance
Sample Receipt Date :06/12/2022

Batch/Sample No. : 2022/TL/SAM/VG 10/4903

Truck No.
: KA 11 B 9413

Report No. : FG/VG 10/QA-TL/2022/13230

Laboratory : Taloja

Invoice No.
TSTWSI222300375

Test Property Test method Units Specification Results Comments

(A) Tests to be Carried out on Original
Binder

Softening point (R&B), 'C, Min IS: 1205 C 240°C 45.8 Pass
Penetration at 25°C, 0.1 mm, 100 g, 5s IS: 1203 dmm 280 dmm 88 Pass

IS 1206 (Part
Absolute Viscosity at 60°C poises 800 to 1200 poises 1080 Pass
2)
IS 1206 (Part
Kinematic Viscosity at 135°C CSt 250 cSt 315 Pass
3)
IS 1448 [P
Flash point, COC, °C, Min C 220 C 308 Pass
69
Solubility in Tricholoethylene 299 % 99.7 Pass

(8) Tests to be Carried out on Rolling Thin

Film Oven (RTFO) Residue

IS 1206 (Part
Viscosity ratio at 60'C % s4% 2.12 Pass
2)
Ductility at 25°C IS: 1208 Cm 275 cmm 93 Pass

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E L L IuIA PRI

Date: 07/12/2022 (O)

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 Tiki Tar and Shell India Pvt ltd
Website wwwtvnuh yr
CIN No 123300M 2019PT 31592

Certification Certificate of Quality (Quality Assurance)

Product Shell Bitumen VG 30 as per IS 73: 2013

Location Taloja
Test type Quality Assurance
Sai 1ple Receipt Date 29/04/2022

Batch/Sample No. : 2022/TL/SAM/VG30/3692

Truck No. MH 06 BW 7557

Report No. FG/VG30/QATL/2022/10127

Laboratory Taloja
Invoice No. :TSTWSI222300037

Test Property Test method Units Specification Results Comments

Softening Point (R&B), 'C, Min IS: 1205 C 247 49.8 Pass

IS 1206 (Part
Absolute Viscosity@ 60 °C poises 2400 to 3600 2934 Pass
2)
Penetration at 25°C,100g, 5s IS: 1203 dmm 2 45 52 Pass

IS 1206 (Part
Kinematic Viscosity @ 135°C cSt 2350 508 Pass
3)

Flash Point, COC, "C, Min

IS 1448 (P:
C 2220 316 Pass
69
Solubility in Trichloroethylene IS: 1216 % 299 99.72 Pass
Tests on residue

IS 1206 (Part
Viscosity Ratio @60 °C poises s4 poises 2.8
2) Pass

Ductility @ 25°C IS: 1208 cm 2 40 cm 79 Pass

This is auto generated report does not require signature.

iDiAP

O
Date: 30/04/2022 BEST BITUMEN FOR BEST ROADS