Z900 Series Manual 1.4

SciAps HH-LIBS Analyzers
Z900 Series User Manual

V1.4 2022
Contents
1. Contact Information 4
2. Technology 5
3. What’s in the Box? 6
4. Analyzer Overview 7
5. Safety 8
General Safety Warnings 8
Battery Safety 8
Laser Safety 8
Argon Safety 8
6. Model Overview 9
7. Start Up & User Interface 9
8. Calibration 18
Wavelength Calibration 18
Drift Correction 21
Type Standardization 29
9. Sample Preparation 33
10. Alloy(+) Mode 34
Alloy(+) Mode Overview 34
Element Suite 34
Taking a Test 35
Test Setup 42
Display Preferences 44
Test Info Fields 48
11. QuickSort(+) Mode 52
QuickSort(+) Mode Overview 52
Element Suite 52
Taking a Test 54
Test Setup 60
Test Info Fields 66
12. Carbon(+) Mode 70
Carbon(+) Mode Overview 70
Element Suite 71
Taking a Test 71
Test Setup 80
Test Info Fields 87
Formulas 92
13. Pipeline Mode 93
14. Results 114
Navigating Results 114
Data Management 118
Exporting Results 121
15. Analytical Settings 125
Force Base 125
Adjust User Factors 128
16. Formulas 133
17. System Features 138
Bluetooth 138
Wi-Fi 140
USB Connectivity 142
User Management 143
18. Instrument Ownership 147
Maintenance 147
Quartz Blast Shield 147
Argon 148
Li-Ion Batteries 148
Storage & Transportation 148
Software Updates 149
Appendix: Default Acquisition Settings 151
Appendix: Grade Library Management 152
Appendix: Sample PDF Report 153
1. Contact Information:
SciAps, Inc. Global Headquarters
7 Constitution Way, Woburn MA 01801
Phone: +1 339-927-9455
Sales: sales@sciaps.com
Support: support@sciaps.com
2. Technology
The Z is a handheld analyzer utilizing Laser Induced Breakdown Spectroscopy (LIBS), a type of atomic
optical emission spectroscopy (OES). Since the early 19th century, scientists have known that elements
emit specific colors of light. This combination of colors is a unique signature for each element. The
wavelength (color) of specific lines reveals the elements present, and the intensity of the light at a given
wavelength is related to the concentration of each element. Traditional OES has used sparks and flames
to generate a plasma. The invention and recent developments of laser technology allow lasers to be used
instead. This gives more precise control over the plasma formation. Unlike sparks and flames, the laser
can generate plasmas on the surface of non-conducting, unprepared samples, like soils, rocks, or liquids.
Sample analysis is broken down into five steps (fig 2.1):

1. A high energy pulsed laser is focused on the sample. The high temperature of the laser on the
sample results in ablation of a small volume of material (roughly 25 um: less than the thickness of a
dollar bill) in plasma plume. The plasma contains the sample’s excited atoms and ions.
2. As the plasma starts to cool, the electrons of the excited atoms and ions fall back down to their
ground states. As they return to their ground states, light of specific wavelengths is emitted from
the plasma and collected by the spectrometer.
3. The spectrometer separates all light emissions with high resolution optics to be detected by the
charge-coupled device (CCD).
4. The elements detected in the sample can be viewed in a graph or spectrum. The graph charts the
intensity of the emitted light as a function of the wavelength.
5. An on-board processor compares the height of specific peaks to a calibration. The calibrations are
built by testing a series of Certified Reference Materials (standards of known chemical composition).
This provides quantitative chemical results. Calibrations are added at the factory, or operators can
create their own calibration routines.
3. What’s in the Box?
1) 1x Hard Sided Instrument Case

2) 1x Instrument with Wrist Lanyard
3) 2x Li-ion Batteries
4) 1x Battery Charging Dock
5) 1x AC Power Adapter
6) 1x USB-C to USB-A Cable
7) 1x Laser Safety Glasses OD 5+ for 1064 nm Laser
8) Accessory Kit:
a. 1x M2 Allen Wrench
b. 2x Replacement Splatter Shield
c. 1x USB Drive; with Calibration Certificate
d. Digital Copy of Instrument Manual
e. Profile Builder Desktop Software (if included)
9) Drift Correction Standards (configuration specific)
10) 5x Argon Cylinders (applicable models only)
4. Analyzer Overview
5. Safety
General Safety Warnings
The main compartment contains high voltage electronics. Opening the main
compartment will void the warranty and could potentially be hazardous to a user.
Do not attempt to service the Z. If there is a malfunction, contact the factory for
assistance. Users may replace batteries, change the argon cylinder, and replace the
analyzer window, but all other maintenance and repair procedures must be done
with factory support or at the factory.
If the Z is damaged, do not attempt to operate it. Contact the factory for service.
Ensure that the correct external power source is used for operating the analyzer or
charging the battery. Voltage should be (100V-240 V/ 50-60 Hz). Do not overload an
electrical outlet.
Battery Safety
The Z-900 uses a 14.4V Li ion rechargeable battery pack. Care should be taken with this battery. Avoid
shorting it. Do not immerse it in water. Store in a cool, dry, and well-ventilated area. Avoid excessive
physical shock or vibration. Do not dispose of battery in fire.
Never use a damaged battery.

Only charge batteries in the approved charger or in the analyzer. Never use a
modified or damaged charger.
Laser Safety
All Z-900 Series models use an embedded CLASS 3B laser per requirements of the US Federal Laser
Product Performance Standard (FLPPS) contained in the regulations in 21 CFR Subchapter J except for
deviations specific to Notices issued by the Department of Health and Human Services including Laser
Notice No. 50, dated June 24, 2007. The maximum pulsed laser output is 7.5 mJ (50 Hz, 1064 nm).
The Nominal Ocular Hazard Distance (NOHD) describes the distance from the aperture where the laser
can be hazardous to the eye. For the Z-900 Series, a 1064nm Nd Yag laser, the NOHD for a 10 second
maximum permissible exposure (1.5mW/cm2) is 13.0 m.
The Z-900 Series uses fail-safe interlocks to function as engineering features to prevent the laser from
being fired without a sample present. With these engineering features active, the system may be used
as a CLASS 1M system following local Laser Safety Officer (LSO) approval.
Care should be taken to operate the instrument safely. Laser safety training is required for all operators.
Laser safety goggles with an optical density of 5+ @850-1080 nm are recommended but not required.
Extra laser safety goggles may be purchased through SciAps.
Argon Safety
Argon is an inert gas and not flammable, however, the heat of a fire can build
pressure in the cylinder and cause it to rupture. Do not expose the cylinder to
extreme heat or dispose of it in a fire. Recommended storage temperature: -30°C –
65° C.
6. Model Overview
Model Configuration Bases
Z-901 QuickSort Al, Ti, Fe, SS, Ni, Cu, Co, Pures (airburn)
Z-901 Alloy Al, Ti, Fe, SS, Ni, Cu, Co, Pures (argon)
Al, Ti, Fe, SS, Ni, Cu, Co, Pures (airburn)
Z-901 Dual Burn Al, Ti, Fe, SS, Ni, Cu, Co, Pures (argon)
Z-901 CSi Fe(C, Si), Stainless (C)
Z-902 QuickSort+ Al, Ti, Fe, SS, Ni, Cu, Co, Pures (airburn)
Z-902 Alloy+ Al, Ti, Fe, SS, Ni, Cu, Co, Pures (argon)
Al, Ti, Fe, SS, Ni, Cu, Co, Pures (airburn)
Z-902 Dual Burn+ Al, Ti, Fe, SS, Ni, Cu, Co, Pures (argon)
Z-902 Carbon Fe+C, Stainless+C
Z-902 Carbon PREMIUM Fe+C, Stainless+C, Al, Ti,, Ni, Cu, Co, Pures (argon)
Z-903 QuickSort+ Al, Ti, Fe, SS, Ni, Cu, Co, Pures (airburn)
Z-903 Alloy+ Al, Ti, Fe, SS, Ni, Cu, Co, Pures (argon)
Z-903 Carbon+ Fe+C, Stainless+C,
Z-903 Carbon+ PREMIUM Fe+C, Stainless+C, Al, Ti,, Ni, Cu, Co, Pures (argon)
Z-903 Geo Coming Fall 2021
Z-903 Empirical Coming Fall 2021
7. Start Up & User Interface

Inserting the battery
Batteries should be charged before use. A full

charge cycle takes approximately 3 hours.
Insert the keyed Li-ion battery into the handle of
the instrument.
Note: The tapered end of the battery should face

towards the nose of the instrument.
Inserting Argon
Screw argon canister into regulator on side of

instrument clockwise. The regulator will pierce
the single-use canister seal. Do not remove argon
canister until the system reports that the canister
is empty.
Each canister has enough argon for

approximately 600 tests (varies with acquisition
settings and averaged results).
Note 1 – Specific, carbon-grade argon is required

for accurate carbon analysis.
Note 2 – Argon canisters are single use and
cannot be refilled.
Do not remove canisters that are still under

pressure as it will cause premature
deterioration of the regulator gasket.
Powering on the system
Firmly press and release the power button on the

top of the analyzer. Power Button
LED Indicator Light:
OFF = Off
GREEN = On, laser has not been fired
RED = On, laser armed and ready to fire
To shut down the system, firmly press and hold

the power button for 3 seconds then release.
When prompted, select Power Off. Wait for the

LED light to turn off before removing the battery.
If required, hold the power button for 12 seconds

to perform a hard shutdown.
System Login
After the analyzer starts, you will need to login.
The default account is admin.
Simply press the > icon to continue.
Additional accounts may be generated when

logged into the account.
The Admin passcode is 1 2 3 4 5

Laser Safety Warning Message
After entering the passcode, you must accept the

laser safety warning message to continue. Use
should be limited to trained operators only.
The Z-900 Series analyzer utilizes an embedded

Class 3B laser with engineering features to
function as an interlock. This combination, with
local Laser Safety Officer approval, allows the
system to be operated under Class 1M
conditions.
Operation should be limited to trained operators

only, and the instrument should be controlled at
all times.
Launch Screen
Features 3 primary functions:

● Analyze
● Settings
● Results
Analyze is used for all analytical testing and data

collection.
Settings controls the analyzer settings. There are

additional settings in the Android Settings menu.
Results allows the user to view, review, export,

and manage previously captured data.
Swipe left to show additional features and
options.
Additional options include:
User Management: change password, manage

users
Android Settings: Access WiFi settings, Date and

Time, and other non-analytical system settings
Other Apps: Includes SciAps Updater, and 3rd

party apps such as Email or Contacts
Navigation Bar
Swiping up from the bottom will show the

navigation bar. In this bar, there are 3 options:
Back
Home
Open Apps
Back simply returns you to the previous screen.
Home returns you to the SciAps launch screen.
Open Apps shows all apps that are actively

running. This allows the user to quickly switch
between open apps or to close an app by swiping
the app icon in this view.
To start testing – select “Analyze” and select an

app.
Warm Up
The Z-900 Series has an optimal internal

temperature between 25° C and 40° C.
When an app is opened, if the internal

temperature is below 26° C, the system will
prompt for WARM UP. Simply pull the trigger or
tap Warm Up to continue.
In temperatures outside of the recommended

operation range, additional measures may be
required for optimal operation (e.g. reduced duty
cycle in high ambient temperatures).
By default, the system will run a 60 second warm

up cycle. The system does not emit any laser
pulses during warm up. A sample is not required
for warm up.
Repeat Warm Up
If the system does not reach the target

temperature before the cycle is completed, the
system will prompt the operator that the
minimum recommended operating temperature
has not been reached.
Warm up will repeat the protocol.
Cancel will take the operator to the testing

screen.
Factory recommendation is to repeat Warm Up

until the target temperature is reached. This is
when the instrument is being operated in the
recommended ambient temperature range.
Wavelength Calibration
When the analyzer reaches the target

temperature, the system will prompt for a
wavelength calibration.
This is indicated by the text “CALIBRATE” on the

button at the bottom of the screen.
When prompted to calibrate, simply tap the on-

screen “CALIBRATE” button or pull the trigger.
The system will shoot an internal standard. No

sample is required for Wavelength Calibration.
Wavelength Calibration corrects for any

wavelength drift in the spectrometer. Typically, a
Wavelength Calibration is recommended every
time the instrument is started, every four (4)
hours of use, or when the internal temperature
changes more than 7° C.
The instrument monitors time and temperature

for these changes.
After the WL Calibration is complete, the button

will read START. This indicates that the
instrument is ready for testing.
When the instrument is ready:

If equipped, argon pressure will be indicated in
the bottom left corner of the screen. It will
typically be between 10 and 12 PSI.
Internal instrument temperature will be indicated

in the bottom right corner of the screen. Ideal
operating temperature is between 25° and 40° C.
To take a test, pull the trigger or press the start
button.
Be sure to hold the sample flush to the laser

aperture and keep the sample still for the entire
test.
Result
Comprised of 6 primary components:

1. Test Number
2. Grade Match
3. Chemistry
4. Grade Compare
5. Camera
6. Test Info
Grade Match indicates the top match for the

measured chemistry compared to the instrument
grade library. The Grade Match Score indicates
the quality of the match. A score of 100 is
considered a perfect match, meaning that all
measured elements matching the alloy are
calculated by determining if each specified
element is in the specified range for the grade. If
it is out of range, a penalty is calculated based on
how far each element is out of range. The
calculated penalty for each element is summed
then subtracted from 100.
8. Calibration
Wavelength Calibrations are standard and recommended practice for the SciAps Z-900 Series. This
procedure verifies that the unit is operating properly and ensures that the wavelength scale is correct.
When a wavelength calibration is performed, the analyzer will fire the laser on a piece of metal inside
the laser. No sample is required for a Wavelength Calibration. The image will be visible on the screen.
When the procedure is complete, a message will appear on the screen indicating success.
When a Wavelength Calibration is required, the

START button will read CALIBRATE. Simply tap
CALIBRATE or pull the trigger to start the
Wavelength Calibration process. The process is
fully automated.
During Wavelength Calibration, the laser and LED

Spotlight will move to the top of the aperture and
fire a series of laser pulses. The test status bar
will read CALIBRATING…
If the Wavelength Calibration is successful, the
test status bar will read COMPLETED.
Manual Wavelength Calibration
Can be performed by opening the options menu

and selecting WL Calibration.
Wavelength Calibration Failure
In the event of a failure, the system will prompt:

Attention: WL Calibration Failed followed by a
specific error message.
Please contact SciAps Support if the WL

Calibration fails.
Basic Troubleshooting steps:

1. Repeat WL Calibration.
2. Confirm that the instrument is in the
proper operating temperature range.
3. Remove nose plate and clean the quartz
blast shield with a cotton swab.
4. Remove nose plate and clean the area
directly above the aperture with a cotton
swab.
Drift Correction
Similar to all Optical Emission Spectroscopy techniques, the Z-900 Series analyzers can experience
spectrometer drift due to temperature changes or other environmental and physical effects. Intensity
Drift can be corrected through the Drift Correction feature described below.
It is recommended that users test known check standards as part of their standard operating procedure.
If the instrument does not perform as expected on the check standards, then a Drift Correction can be
applied to correct for spectrometer drift.
Drift correction requires the specific set of drift correction standards that was delivered with the
instrument. Open the Drift Correction feature found in the three dots menu of the target testing app.
Follow the steps below to complete a drift correction.
Note – drift correction is specific to the testing mode.
Prior to Drift Correction, SciAps recommends:
1. Cleaning the Quartz blast shield with a cotton swab

2. Performing a Wavelength Calibration
For Drift Correction in Carbon(+), Carbon+Silicon, and Pipeline, proper sample preparation is required
prior to drift correction.
Access Drift Correction from the testing mode
options menu.
All available bases for drift correction will be

listed in the following screen.
Tap a base to perform a drift correction for that

base.
Some bases contain four standards. Simply scroll
down to see the additional standards.
To clear all drift correction values, tap the reset

button in the top corner of the drift correction
menu.
Then accept the prompt by tapping Reset Values.
To reset drift correction values for a specific base,

open that base then tap the reset button.
Then accept the prompt by tapping Reset Values.
This will not reset values for any other base.
This automated drift correction procedure calculates factors and offsets for elements within the base.
A factor is typically used for higher concentration elements.
An offset is typically used for lower concentration elements.

To drift correct the Aluminum base, select
aluminum from the main drift correction menu.
Tap a drift correction sample to select that

sample.
Hold the specific sample – confirming that both
the alloy (e.g. 3003) and the batch (e.g. 8) match
between the standard and the on screen display
– to the aperture.
Tap the START button or pull the trigger to start

the sequence.
In Alloy(+) and Quick Sort(+) mode, the system

will run 3 tests.
In Carbon+Silicon, Carbon(+), and Pipeline, the

system will run a Pre-Burn as set in the
Acquisition Settings menu then a series of 3 tests.
When testing, the test status bar will indicate

progress through the drift correction procedure.
For Aluminum and Copper bases, SciAps

recommends moving the sample between laser
bursts.
For all other bases, SciAps recommends leaving

the sample in the same location for all laser
bursts.
For Carbon based modes (C+Si, Carbon(+),

Pipeline), the sample must stay in the same
location for all tests.
When a standard is complete, the system will
return to the standard selection screen. The
standard will be updated with a blue check mark
and a time and date stamp.
Tap the next standard in the list to continue the

process.
When all standards in the list have a blue check
mark, tap Save Changes. If you exit without
saving changes, the correction values will not be
saved or applied to the chemistry.
After saving changes, the time and date stamp

will be updated for that base.
There is an internal check on the factors to
confirm that they are reasonable values. If a
standard is out of range, the system will prompt
the user.
In the event of an Out of Range message,

confirm:
1. The correct standard was shot
2. The standard is clean
3. The blast shield is clean
4. Instrument temperature is in the normal
operating range
5. If Argon is required, the canister did not
become empty during the test
If all of these basic criteria were met, reshoot the
standard. If the same out of range error is
produced, apply the factors and continue drift
correction. When the drift correction process is
complete, validate performance with a check
standard. If the chemistry is out of range, it may
be indicative of a hardware issue. In this case,
please contact SciAps Support for assistance.
Drift Correction Standards Bases and standards are model and mode specific
Aluminum Base 3003
6061
7050
356
Copper Base CDA 715
CDA 836
CDA 863
Iron Base CP Iron
1030
8620
LAS1
Stainless Base (Alloy*, QuickSort*) 317L
Custom 455
C350
Nitronic 60
Stainless Base (Carbon*) 316L
304
347H
Nickel Base Inconel 625
Rene 41
Type Standardization
Type Standardization is a single point calibration that allows users to automatically adjust the calibration
to match a particular Reference Material or Certified Reference Material. The Type Standardization will
adjust the slope or offset each element’s calibration curve so that the result will match the assay of the
standard. The slope is adjusted for high concentrations, and the offset is adjusted for trace levels.
Typically, the cutoff for slope versus offset is 0.2%.
Type Standardization should be used for improved accuracy on a small sample range when the
chemistry of the reference material, aka the Type Standard, is very similar to the material to be tested.
In order to perform a Type Standardization, you must have a Reference Material (RM) or Certified
Reference Material (CRM) entered into the system. To enter an RM or CRM, connect to the database in
Profile Builder, access the standards page, add your standard with assay values and designate the
standard for Type Standardization.
Type Standardization Setup
To access Type Standardization, open the options

menu and tap Type Standardization.
Select your RM or CRM
Select the Alloy Type, aka Base, that contains

your RM or CRM.
Then select the target RM or CRM from the
subsequent list.
Test the Sample
Prepare the sample and then shoot the sample

using the start button or the trigger. Pre-Burn
settings will be applied. The system will
automatically run 3 repeats on the sample.
When the acquisition is complete, review the
data and press save.
You are now ready to test. When a Type Standard

is applied, the selected standard will be listed in
the header, and there will be a target icon in the
top right corner.
Exiting Type Standardization
Tapping the target icon or pressing the back

button will exit that type standardization. Accept
the prompt to exit or press cancel to maintain the
Type Standardization.
9. Sample Preparation
While the Z-900 Series has effective cleaning protocols built into the system, LIBS is still fundamentally a
surface test. For a heavily corroded, dirty, or plated surface, sample preparation may be required.
Sample preparation is critical for carbon analysis.
If sample preparation is required, grind an area approximately 0.75 in/20 mm in diameter. The minimum
sample prep area is 0.15 in / 4 mm. Then use the camera to align the test location in the center of the
prepared area.
SciAps recommends the Milwaukee M12 Right Angle Die Grinder or the Milwaukee M12 Variable Speed
Polisher/Sander and the Norton Saint Gobain Blaze R980P Quick Change disc (2” or 3” diameter, 50 grit).
Proper grinding technique will result in a shiny surface with linear grind marks (not swirls).
10. Alloy(+) Mode
Alloy(+) Mode Overview

This testing app is used for quantitative analysis of alloys. The mode utilizes argon OptiPurge technology
to purge the testing chamber with argon – an inert gas. The argon environment increases the plasma
life, improving signal to noise ratio. Additionally, the argon atmosphere increases the overall intensity of
the plasma and limits impact of atmospheric absorption.
Alloy and Alloy+ share the same user interface and functions. Alloy uses a single spectrometer covering
200 – 420 nm. Alloy+ uses two spectrometers to achieve an expanded wavelength range of 190 – 610
nm.
Element Suite
Alloy Mode:
Alloy Family Elements Included

Aluminum Be, Mg, Al, Si, Ti, V, Cr, Mn, Fe, Ni, Cu, Zn, Zr, Pb, Bi, Ag
Titanium Al, Si, Ti, V, Cr, Mn, Fe, Ni, Zr, Nb, Mo, Sn
Low Alloy Steel (Fe) Al, Si, Ti, V, Cr, Mn, Fe, Co, Cu, Ni, Nb, Mo, W, Pb
Stainless Steel Al, Si, Ti, V, Cr, Mn, Fe, Co, Ni, Cu, Se, Nb, Mo, W
Nickel Al, Si, Ti, Cr, Mn, Fe, Co, Ni, Cu, Nb, Mo, W, Hf, Ta, Re
Copper Be, Al, Si, Cr, Mn, Fe, Co, Ni, Cu, Zn, Se, Ag, Sn, Pb, Bi
Cobalt Al, Si, Ti, Cr, Mn, Fe, Co, Ni, Cu, Nb, Mo, W
Specialty ** V, Cr, Mn, Ag, Ta, Hf, Re, Pb, Zr, Mg, Zn, Mo, W, Sn, Nb
Alloy+ Mode:

Aluminum Li, Be, Mg, Al, Si, Ti, V, Cr, Mn, Fe, Ni, Cu, Zn, Zr, Pb, Bi, Ag
** Identifies base only – no alloying or trace element analysis.
Additional bases or elements may be set up with factory support.
Taking a Test
Place sample over the laser aperture ensuring
that you completely cover the window.
Be sure to hold the sample square to the

instrument so that the laser LED Spotlight is in
clear focus on the sample.
Hold the sample still for the duration of the test.

The test will include 6 individual test points. The
system automatically moves through the full
raster pattern.
Raster pattern: 6 locations x 12 cleaning pulses x

16 data pulses
In alloy mode, we fire the laser 12 times in each

location to clean debris from the surface then 16
times in each location to collect data.
Rastering across the surface ensures a

representative sample is collected.
First Update
During a test, the system will deliver live updates

to the chemistry as data is collected and
processed.
This phase is indicated by the test status bar.

While the status bar reads TESTING… the test is
still in progress. The sample should be kept in the
same location throughout this phase.
Test Complete
Each test is a test to completion. A complete test

is indicated on screen by the test status bar
turning GREEN and reading COMPLETED.
Alloy Result

1. Test Number
2. Grade Match
3. Chemistry
4. Grade Compare
5. Camera
6. Test Info

measured elements match the alloy specification.
The Grade Match Score is calculated by
determining if each specified element is in the
specified range for the grade. If it is out of range,
a penalty is calculated based on how far each
element is out of range. The calculated penalty
for each element is summed then subtracted
from 100.
Navigating Results
Swipe left to go to an earlier result or swipe right

to go to a more recent result.
Chemistry
Chemistry lives on the first page and lists all

measured elements including their
concentration, the precision of the measurement
(+/-), and, if there is a grade match, the grade
specification for each measured element.
ND indicates non-detect. This means that the

measured value failed to meet the criteria for a
valid measurement. In order for an element value
to be considered detected, the measured value
must be greater than the 3σ standard deviation.
See display preferences section for more
information about non-detects.
Grade Specification Comparison
Tap the grade specification column to expand the

grade specification (hiding the precision column).
Green indicates that the chemistry is within the

specified value for the grade.
Red indicates that the chemistry is outside of the

specified range.
Yellow indicates that, when considering the

precision of the measurement, the reported
chemistry may fall into the grade specification.
Compare Grade
The Grade Compare function lives on the second

page and allows the user to compare measured
chemistry against any grade in the active grade
library.
Tap the grade compare icon to see the top three

grade matches. The grade match score is listed
for each grade.
Tap Other… to see additional grade matches.
To compare with the non-top grade, tap another

entry in the list.
Compare Grade
Selecting a “compare with” grade will return the

system to the chemistry page.
Using the grade comparison feature, the system

will visually indicate what elements are out of
range for lower matches.
Camera
The Camera function lives on the third page and

allows the operator to capture and attach a micro
or macro image to a result for photo
documentation.
Tap the camera icon to enter the camera utility.

Simply tap Take a Photo to open the camera
view.
Camera
The camera opens in the micro view for capturing

an image of the test site. Tap the switch icon in
the top left corner to switch to the macro camera
for capturing an image of the entire sample.
Tap the white button to capture an image.
After capturing an image, the user may save the

image or retake the image.
Delete an Image
If an image is already present, the image will be

displayed in the camera page.
Tap the trash can icon to delete the image.
Test Info Page
The Test Info component lives on the fourth

page. This page includes test metadata including
date and time, calibration model used for
calculation, and the ability to enter test info for
record keeping.
Tap the icon to access the page.
Sample ID and, if activated, Test Info fields can be

populated after the test is taken.
Next Test
To take the next test, pull the trigger or tap the

back button to return to the targeting screen.
Position your sample and pull the trigger again or

tap START.
Test Setup
The Z-900 has factory default acquisition settings that are set at the factory level. Changing these
settings may impact the instrument calibration and should not be done without factory authorized
support. Beyond factory acquisition settings, the user or operator has the option to add in a Pre-Burn.
The Pre-Burn increases the cleaning of the sample prior to taking a test and may be used for dirty or
plated samples. For heavy corrosion or thick plating, grinding is recommended. When using Pre-Burn, it
is important to keep the sample in the same position until the test is completed.
Activating Pre-Burn
To activate Pre-Burn, select Acquisition Settings

from the options menu.
Tap Pre-Burn to open Pre-Burn options.
Pre-Burn Options
Off indicates no Pre-Burn.
Short indicates a single Pre-Burn (approximately

3 seconds).
Long indicates two back-to-back Pre-Burn cycles

(approximately 6 seconds).
The longer the Pre-Burn, the more surface

material is ablated or removed prior to collecting
data.
When testing with Pre-Burn, the test status bar
will indicate that the Pre-Burn is active.
Display Preferences
The Z-900 is designed to be customized to the operator's needs. One of the primary ways we allow
customization is the setup of the display preferences. This includes element display order, user
selectable confidence interval, and customizable limit of detection cutoffs.
To access display preferences, open the options

menu and tap display preferences.
Precision
The precision setting controls the number of

digits to display after the decimal point. This
setting is respected in both the onscreen display
and any exported report (CSV or PDF).
Chemistry
Set Elements allows the user to select what

elements should be displayed (if detected) on the
instrument screen.
Element Sort Order allows the operator to quickly

select the order of appearance for all elements.
Selecting Elements
To choose what elements are displayed, tap Set
Elements.
Elements highlighted with blue will be displayed

if measured. Use the select all elements and
deselect all elements to quickly make bulk
changes.
Element Sort Order
Determines the order of appearance on the

result screen.
Atomic Number will display elements based on

the specific element’s atomic number, or, more
simply, will rank the elements by their weight.
This will sort elements from the lightest element
to the heaviest element.
By Concentration sorts the elements by the

measured concentration from high to low
concentration.
By Symbol sorts elements alphabetically by

symbol.
Custom Order allows the user to determine the

preferred order of elements.
Creating a Custom Element Sort Order
To create a custom order, select Custom Order to

open the Reorder wizard.
Then tap the element you want to move and use

the up and down arrows in the top right corner to
move the element.
Grade Display Settings
Number of Grades to Display controls the

number of grades displayed in the Compare
Grade page and the number of grades displayed
in the PDF export.
Min Grade Match Number determines the cutoff

for No Grade Match response.
Closeness to Best Match screens for alloys that

are very similar in chemistry. Some alloys are so
similar that they cannot be sorted on chemistry
alone. If activated, this feature flags a result that
has more than one grade within the set value of
the top grade match.
Detected Elements
For an element to be considered detected, the

measured value must be greater than the 1 sigma
precision multiplied by the LOD Sigma. Thus, a
higher LOD Sigma will result in less detected
elements.
The system has the option to either hide or

display non-detect elements. It is highly
recommended to activate Show Chem < LOD as
ND when Show non detect elements is active.
The LOD Sigma is defined as 3.0. The user may

adjust this value if they desire.
The Display Sigma is a multiplier applied to the

calculated precision. It is expected that the result
will have analytical agreement with a certified
value approx. 95% of the time.
Correction Factors
Always show correction factors, when activated,

will list all calculated drift correction and type
standardization factors in the calibration
workflow.
This can be a powerful tool for advanced users or

for troubleshooting but is typically not
recommended for general usage.
Test Info Fields

Test Info Fields are a useful tool for attaching metadata or testing notes to a result.
Test Info Setup
Test Info setup is accessed through Test Info

Settings
Test Info Settings
Test Info is driven by a template. To customize

Test Info Fields, tap Template Setup.
Prompt for Test Info will prompt the user before

each test to populate the Test Info Fields.
Clear All will reset all Test Info fields except for
Sample ID.
Template Setup
Modify existing fields or add new fields. Users

may add a maximum of 8 fields.
To add a new field, tap Add New Field.
To modify an existing field, scroll through the list

and select the target field.
Sample ID is a factory enabled field and cannot

be deleted.
Enter Field Name
Each field must have a name. The name will

appear in the test info page and on exported
data.
Select Field Type
Free form is a general text entry.
Numeric field is numbers 0 – 9 only.
Selector gives the user a dropdown menu.
Selector Field
Add multiple options for the user to select from a

dropdown menu. This is a great option for
consistent descriptions.
Field Rules
After Selecting a Field Type, the user has the

option to apply a rule.
Auto-Increment will increment the input for a

field by +1 for each subsequent test.
Persist will maintain the input for a field until the

user changes that field.
Using Test Info
After configuring the Test Info Template, Test

Info Fields are ready to be used.
For training purposes, the following fields have

been setup:
Prompt For Test Info
To enter values prior to a test, activate Prompt

for Test Info in the Test Info Settings page.
When a test is started, the system will prompt

the user to input the test info values. Enter the
values then.
Review Values
The user may enter in all desired values.
Tap Start Test or Pull Trigger to start.
After the test is completed, the values may be

reviewed and edited in the Info tab.
11. QuickSort(+) Mode

QuickSort(+) Mode Overview
This testing app is used for quantitative analysis of alloys. This air-burn mode is designed for rapid alloy
analysis and alloy sorting.
QuickSort and QuickSort+ share the same user interface and functions. QuickSort uses a single
spectrometer covering 200 – 420 nm. QuickSort+ uses two spectrometers to achieve an expanded
wavelength range of 190 – 610 nm.
Element Suite
QuickSort Mode:

QuickSort+ Mode:


Taking a Test

clear focus on the sample.

The test will include 6 individual test points. The
system automatically moves through the full
raster pattern.
Raster pattern: 3 locations x 24 cleaning pulses x

32 data pulses
In QuickSort(+) mode, we fire the laser 24 times

in each location to clean debris from the surface
then 32 times in each location to collect data.

First Update
During a test, the system will deliver live updates

to the chemistry as data is collected and
processed.
This phase is indicated by the test status bar.

While the status bar reads TESTING… the test is
still in progress. The sample should be kept in the
same location throughout this phase.
Test Complete
Each test is a test to completion. A complete test

is indicated on screen by the test status bar
turning GREEN and reading COMPLETED.
QuickSort Result

1. Test Number
2. Grade Match
3. Chemistry
4. Grade Compare
5. Camera
6. Test Info

measured elements match the alloy specification.
Grade Match Score is calculated by determining if
each specified element is in the specified range
for the grade. If it is out of range, a penalty is
calculated based on how far each element is out
of range. The calculated penalty for each element
is summed then subtracted from 100.
Navigating Results

Chemistry





specified range.

Compare Grade

library.

for each grade.

entry in the list.
Compare Grade


Camera

documentation.

view.
Camera


Delete an Image


Test Info Page

page. This page includes test metadata including
record keeping.

Next Test


tap START.
Test Setup
Activating Pre-Burn

Pre-Burn Options

3 seconds).


data.
Display Preferences
The Z-900 is designed to be customized to the operator’s needs. One of the primary ways we allow
customization is the setup of the display preferences. This includes element display order, user
selectable confidence interval, and customizable limit of detection cutoffs.

Precision

Chemistry

instrument screen.

Selecting Elements

Elements.

changes.
Element Sort Order

result screen.

the specific element’s atomic number, or, more
simply, will rank the elements by their weight.
This will sort elements from the lightest element
to the heaviest element.

concentration.

symbol.
Custom Order allows the user to determine the

To create a custom order, select custom order to


move the element.

in the PDF export.


Detected Elements

elements.



Correction Factors

workflow.

Test Info Fields

Test Info Setup

Settings.
Test Info Settings


Sample ID.
Template Setup



be deleted.
Enter Field Name

data.
Select Field Type
Selector Field

Field Rules

option of applying a rule.


Using Test Info


been setup:


values then.
Review Values

12. Carbon(+) Mode

Carbon(+) Mode Overview
The Carbon and Carbon+ apps are used for quantitative analysis of carbon as well as a broad range of
other alloying and trace elements for Positive Material Identification, the determination of Carbon
Equivalent value, and grading stainless steel. The mode utilizes argon OptiPurge technology to purge the
testing chamber with argon – an inert gas. The argon environment increases the plasma life improving
signal to noise ratio. An argon atmosphere is critical for carbon analysis to limit the impact of
atmospheric absorption. Additionally, this mode adds in Analysis Averaging to improve accuracy and
precision by averaging multiple tests with the added functionality of data rejection.
Carbon and Carbon+ share the same user interface and functions. Carbon uses 2 spectrometers covering
190 – 420 nm with a dedicated spectrometer for carbon analysis, delivering improved spectral
resolution for superior carbon performance. Carbon+ uses three spectrometers to achieve an expanded
wavelength range of 190 – 610 nm while maintaining a high resolution, dedicated carbon spectrometer.
Element Suite
Carbon Mode:

Low Alloy Steel (Fe) C, Al, Si, Ti, V, Cr, Mn, Fe, Co, Cu, Ni, Nb, Mo, W, Pb
Stainless Steel C, Al, Si, Ti, V, Cr, Mn, Fe, Co, Ni, Cu, Se, Nb, Mo, W
Additional Option Bases (included in Premium Model)
Carbon+ Mode:

Low Alloy Steel (Fe) C, Al, Si, Ti, V, Cr, Mn, Fe, Co, Cu, Ni, Nb, Mo, W, Pb
Stainless Steel C, Al, Si, Ti, V, Cr, Mn, Fe, Co, Ni, Cu, Se, Nb, Mo, W
Additional Option Bases (included in Premium Model)
Taking a Test
Carbon Mode User Interface:
Carbon(+) mode combines Pre-Burn, Multi-Shot averaging, and Data Rejection to provide quantitative
analysis of C and other alloying elements.
A carbon test is considered the average of multiple individual results. Each individual test is not
considered a result and should not be used for reporting or grading material.
Sample Preparation
Sample preparation is required for accurate

carbon analysis.
Grind a minimum area of approximately 0.75 in

(20 mm) in diameter. The minimum sample prep
area is 0.15 in / 4 mm. Then use the camera to
align the test location in the center of the
prepared area.
SciAps recommends the Milwaukee M12 Right

Angle Die Grinder or the Milwaukee M12
Variable Speed Polisher/Sander and the Norton
Saint Gobain Blaze R980P Quick Change disc (2”
or 3” diameter, 50 grit). Grinding discs should be
changed regularly to avoid cross-contamination.
Proper grinding technique will result in a shiny

surface with linear grind marks (not swirls).


clear focus on the ground portion of the sample.

The test will include pre-burn and multi-shot
average across 6 unique raster points. The system
automatically moves through the full raster
pattern.
Typical Raster pattern: 1-2 Pre-Burns, 3-5 shot

average, each individual test: 6 locations x 12
cleaning pulses x 16 data pulses

Pre-Burn
Pre-Burn is critical for removing any additional

contamination from the surface that is left after
grinding. The factory recommendation is to use a
Short Pre-Burn with 25 Pre-Burn pulses per
location.
Matrix View
After the Pre-Burn, the system will populate a

matrix with each individual test. All measured
elements will be reported in the matrix.
The Matrix view includes:

● Formulas (e.g. IIW) and elements (grey
column)
● the average of all selected tests (blue
column)
● Each individual test
Pan up and down by swiping on the screen.

Data Rejection
To account for outliers in the data (typically a

product of movement during the test or carbon
inclusions in the material), the user may tap a
column to reject that test from the average.
A rejected test will be greyed out and the number

will be replaced by an X.
Save Test
After qualifying the data and rejecting outliers,

press save to generate a Carbon Result.
Carbon Result

1. Average Indicator
2. Test Number
3. Grade Match
4. Chemistry
5. Grade Compare
6. Camera
7. Test Info

measured elements match the alloy. The Grade
Match Score is calculated by determining if each
specified element is in the specified range for the
grade. If it is out of range, a penalty is calculated
based on how far each element is out of range.
The calculated penalty for each element is
summed then subtracted from 100.
Navigating Results

Formulas
Any active formulas will be displayed at the top

of the result and color coded according to
configured action levels.
See formulas for more information. Available

factory formulas include:
● Dearden O’Neil CE
● AWS CE
● CSA Z662
● Critical Metal Parameter (Pcm)
Chemistry





specified range.

Compare Grade

library.

for each grade.

entry in the list.
Compare Grade


Camera

documentation.

view.
Camera


Delete an Image


Test Info Page

page. This page includes test metadata, including
record keeping.

Next Test


tap START.
Test Setup
Managing Pre-Burn

A minimum of a short Pre-Burn is recommended.
Pre-Burn Options

3 seconds).


data.
Analysis Averaging
Analysis Averaging is controlled from a dedicated

menu in the Options menu.
Analysis Averaging Options:
Max Number of Tests: Sets an upper bound for

the number of tests that can be included in a
Carbon Result.
Auto Repeat Test: When active, only one trigger

pull is required to run Pre-Burn and the Auto Shot
Number of tests. Essentially, 1 trigger pull to
collect all of the required tests.
Auto Shot Number: Target number of tests for

Carbon Result.
Display Preferences
The Z-900 is designed to be customized to the operator’s needs. One of the primary ways the user may
customize is the setup of the display preferences. This includes element display order, user selectable
confidence interval, and customizable limit of detection cutoffs.

Precision

Chemistry

instrument screen.

Selecting Elements

Elements.

changes.
Element Sort Order

result screen.

the number of protons in the element’s nucleus
or, more simply, will rank the elements by their
weight. This will sort elements from the lightest
element to the heaviest element.

concentration.

symbol.
Custom Order allows the user to determine their

To create a custom order, select custom order to


move the element.

in the PDF export.


Detected Elements

elements.



Correction Factors

workflow.

Test Info Fields

Test Info Setup

Settings.
Test Info Settings


Sample ID.
Template Setup



be deleted.
Enter Field Name

data.
Select Field Type
Selector Field

Field Rules



Using Test Info


been setup:


values then.
Review Values

Formulas
Factory Formulas
The Carbon(+) mode comes standard with the following Factory Formulas
American Welding
%𝑀𝑛 + %𝑆𝑖 %𝐶𝑟 + %𝑀𝑜 + %𝑉 %𝐶𝑢 + %𝑁𝑖
Society (AWS) 𝐴𝑊𝑆 = %𝐶 + + +
6 5 15
Dearden and O’Neill

%𝑀𝑛 %𝐶𝑟 + %𝑀𝑜 + %𝑉 %𝐶𝑢 + %𝑁𝑖
(IIW) 𝐼𝐼𝑊 = %𝐶 + + +
6 5 15
Critical Metal
Parameter (Pcm) 𝑃 = %𝐶 +
%𝑆𝑖 %𝑀𝑛 + %𝐶𝑢 + %𝐶𝑟 %𝑁𝑖 %𝑀𝑜 %𝑉
+ + + + + 5 × %𝐵
30 20 60 15 10
*B is a nominal value
of 0.007 per ASTM
415
CSA Z662 (CSA)
%𝑀𝑛 %𝑆𝑖 %𝐶𝑢 %𝑁𝑖 %𝐶𝑟 + %𝑀𝑜 + %𝑉 + %𝑁𝑏
𝐶𝑆𝐴 = %𝐶 + 𝐹 + + + + + 5 × %𝐵
*B is a nominal value 6 24 15 210 5
of 0.007 per ASTM
415
Seferian CE
𝑆𝑒𝑓 = %𝐶 + 0.111(%𝑀𝑛 + %𝐶𝑟) + 0.055(%𝑁𝑖) + 0.078(%𝑀𝑜)
API 5L
Hydrofluoric
Alkylation (API 751)
Schaeffler modified
Delong
13. Carbon + Silicon Mode

Carbon + Silicon (CSi) Mode Overview
The Carbon + Silicon apps is used for quantitative analysis of carbon and silicon in low alloy and stainless
steel. The mode utilizes argon OptiPurge technology to purge the testing chamber with argon – an inert
gas. The argon environment increases the plasma life improving signal to noise ratio. An argon
atmosphere is critical for carbon analysis to limit the impact of atmospheric absorption. Additionally,
this mode adds in Analysis Averaging to improve accuracy and precision by averaging multiple tests with
the added functionality of data rejection.
The Carbon + Silicon mode is only available on the Z901 CSi model. The system features a single
spectrometer with a range of 190 nm to 260 nm. The spectrometer offers ultra-high resolution for the
carbon and Silicon region.
The CSi is designed to accompany XRF. XRF may be used to determine the alloy and quantify the base
and alloying elements. The CSi will then provide C and Si content for the calculation of CE, grading
stainless steels into low, high or straight carbon grades.
Element Suite
Low Alloy Steel (Fe) C, Si
Stainless Steel C
Taking a Test
Carbon + Silicon User Interface:
Carbon(+) mode combines Pre-Burn, Multi-Shot averaging, and Data Rejection to provide quantitative
analysis of C and Si.
A carbon test is considered the average of multiple individual results. Each individual test is not
considered a result and should not be used for reporting or grading material.
Sample Preparation
Sample preparation is required for accurate

carbon analysis.
Grind a minimum area of approximately 0.75 in

(20 mm) in diameter. The minimum sample prep
area is 0.15 in / 4 mm. Then use the camera to
align the test location in the center of the
prepared area.
SciAps recommends the Milwaukee M12 Right

Angle Die Grinder or the Milwaukee M12
Variable Speed Polisher/Sander and the Norton
Saint Gobain Blaze R980P Quick Change disc (2”
or 3” diameter, 50 grit). Grinding discs should be
changed regularly to avoid cross-contamination.
Proper grinding technique will result in a shiny

surface with linear grind marks (not swirls).


clear focus on the ground portion of the sample.

The test will include pre-burn and multi-shot
average across 6 unique raster points. The system
automatically moves through the full raster
pattern.
Typical Raster pattern: 1-2 Pre-Burns, 3-5 shot

average, each individual test: 6 locations x 12
cleaning pulses x 16 data pulses

Pre-Burn
Pre-Burn is critical for removing any additional

contamination from the surface that is left after
grinding. The factory recommendation is to use a
Short Pre-Burn with 25 Pre-Burn pulses per
location.
Matrix View
After the Pre-Burn, the system will populate a

matrix with each individual test. All measured
elements will be reported in the matrix.
The Matrix view includes:
● The average of all selected tests (blue

column)
● Each individual test
● Chemistry for all calibrated elements
Scroll between results by swiping left or right on

the screen.
Data Rejection
To account for outliers in the data (typically a

product of movement during the test or carbon
inclusions in the material), the user may tap a
column to reject that test from the average.
A rejected test will be greyed out and the number

will be replaced by an X.
Save Test
After qualifying the data and rejecting outliers,

press save to generate a Carbon Result.
Carbon Result
Comprised of primary components:
1. Average Indicator and number of tests

included in the average
2. Test Number
3. Spectrum
4. Camera
5. Test Info
6. Chemistry
Unlike other SciAps analyzers, the CSi does not

provide grade match.
Navigating Results

Chemistry



View Spectrum
The View Spectrum allows the user to view the

collected spectrum from each individual test in a
carbon result.
Zoom and pan to investigate a specific peak.

Camera

documentation.

view.
Camera


Delete an Image

Test Info Page

page. This page includes test metadata, including
record keeping.

Next Test


tap START.
Test Setup
Managing Pre-Burn

A minimum of a short Pre-Burn is recommended.

Pre-Burn Options

3 seconds).


data.
Analysis Averaging
Analysis Averaging is controlled from a dedicated

menu in the Options menu.
Analysis Averaging Options:
Max Number of Tests: Sets an upper bound for

the number of tests that can be included in a
Carbon Result.
Auto Repeat Test: When active, only one trigger

pull is required to run Pre-Burn and the Auto Shot
Number of tests. Essentially, 1 trigger pull to
collect all of the required tests.
Auto Shot Number: Target number of tests for

Carbon Result.
Display Preferences
The Z-900 is designed to be customized to the operator’s needs. One of the primary ways the user may
customize is the setup of the display preferences. This includes element display order, user selectable
confidence interval, and customizable limit of detection cutoffs.

Precision

Detected Elements

elements.



Correction Factors

workflow.

Test Info Fields

Test Info Setup

Settings.
Test Info Settings


Sample ID.
Template Setup



be deleted.
Enter Field Name

data.
Select Field Type
Selector Field

Field Rules



Using Test Info


been setup:


values then.
Review Values

14. Pipeline Mode

Pipeline is a dedicated app for determining chemical composition and Carbon Equivalent value for
Pipeline Integrity Management in accordance with API 5L Specifications. In addition to the features
offered in Carbon(+) mode, the Pipeline mode offers:
Fixed Acquisition Settings
Pipeline mode standardizes the acquisition settings to:

 Pre-Burn = Long
 Number of Shots = 5
 Standard Carbon Raster Pattern
Automated Data Rejection
When the Pre-Burn and 5 intermediate tests

have been taken, the system will
automatically exclude the intermediate tests
with the highest and lowest C value from
the average.
Type Standardization Prompt
If CE value is between 0.4 and 0.5, the

system will prompt for a Type
Standardization.
If the CE value is 0.4 to 0.45, the system will

prompt the operator to perform a Type
Standardization with RM 1020 which has an
approximate CE value of 0.4.
If the CE value is 0.45 to 0.5, the system will

prompt the operator to perform a Type
Standardization with RM 1030 which has an
approximate CE value of 0.5.
This ensures the highest quality analysis

possible when a value is near the action
level.
Tapping Continue will take the user directly
to the Type Standardization Screen for the
appropriate standard.
After performing the Type Standardization,

the system is ready to retest the sample.
When Type Standardization is active, the
standard will be listed in the header.
Tap the Type Standardization icon in the top
right corner to exit Type Standardization.
Formulas
Pipeline mode requires that one CE formula

(IIW, AWS, Pcm, CSA) is selected. Additional
non-CE formulas may also be included.
15. Results
All results are stored in the Results App. Use Results to review data, generate PDF reports, export data
to CSV, delete data, and update Test Info.
Navigating Results
Access Results from the main home screen.
The header contains:

● Total number of tests in current view
● Multi-result selector tool
● Share Tool
● Options Menu
Results will be grouped under a header date.
Each result line will contain:

● A color-coded indicator for testing mode
● AVG icon for calculated average tests
● Camera icon for results with a photo
attached
● Grade Match & Grade Match Score
● Time Stamp
The Options may include:
● Templates Setup for customizing Excel
export option
● Filter by Date to filter results by a date or
date range
● A quick Export All Results key
● Function to Delete All Results
Filter by Date
Tap Set Date Range then select either a range or

a single date and tap okay.
This will limit results to those taken on the days
in the date range.
Once applied, the list will be limited to those

specific results.
Exporting all results or deleting all results from

the filtered view will only include tests in the
specified date range.
Data Management
To Delete all test results, open the options menu.
Then select Delete All Results.

Tapping Delete will permanently delete the
selected results.
To Delete a subset of results, use the selector

button in the header row.
Select the results to delete by tapping the row
then tap the delete icon.
To permanently delete those results, tap Delete.

Exporting Results
Tap the share icon to export results.
You may select a subset of the results using the

Filter by Date feature or the Selector function.
There are two options for exporting results:
A formatted PDF report (see appendix for

example)
PDF Export will respect display settings for:

● Active formulas
● Elements to display
● Precision
● Limits of Detection and Detected
element display rules
An Excel (.csv) file for additional data handling or

multiple tests in a single file
PDF Export
To set up PDF Export, tap PDF from the format

selection screen.
Customize Output
Select what fields to include then tap Start

Export.
Export to CSV
Tap Excel.
Select export template.

Custom Templates
Select Template Setup from the Options menu.
Create a new template or modify an existing

template.
Name template and select setup fields.
Select Fields to include, Elements to include,

Formulas, and Arrange order.
Additionally, may include uncertainty for each

element and test info for each result.
All reports are saved to This PC\NGL\SD card\export in either the PDF or csv folder.
16. Analytical Settings

Force Base
All quantitative modes on the SciAps Z-900 Series have built-in automated base identification. However,
some alloys or custom bases may cause issues for the automated base identification system. Take
manual control over the system with Force Base.
Standard Operation
When Force Base is not active, the top bar will

display the name of the active mode.
Activating Force Base
To activate Force Base, open the options menu

and select Analytical Settings.
Select Force Base
Select target base (e.g. Al [Aluminum]) and then

click back to the testing screen.
When Force Base is active, the header will display
the selected base (e.g. Al) and an icon will appear
in the top right corner of the camera view.
At this stage, no matter what material type is

tested, the system will use the aluminum models
to determine chemistry.
Tapping the icon will return the system to the

Force Base menu. Select Auto base ID to return
to standard, automated base identification.
Adjust User Factors

Adjust User Factors allows the user to apply factors and offsets on a base and element specific basis to
adjust chemistry. All adjustments are made to the final result. Adjust User Factors should be limited to
advanced users only but can be a powerful way to adjust repeatable but biased data.
Activating Adjust User Factors
From the target testing mode, select the options

menu and select analytical settings.
Select Adjust User Factors.

Tap Customize Models.
Tap Add New Model.

Name Model and tap Create Model.
To customize, select the new model (e.g. Z900

MANUAL).
Select Base and Order to filter factors. Order is
used for split curves where Order 1 is standard
and Order 2 is used for low concentrations. Most
elements only have Order 1. Split curves address
large concentration ranges (e.g. Zn in Copper
alloys).
Adjust factors, offsets, LOD sigma and %

threshold. Then return to the Adjust User Factors
Home Screen.
To activate your new adjusted user factors, select
the new model from Selected Model dropdown
menu.
17. Formulas
Create or load formulas to elevate your instrument functionality. Set single element formulas to screen
for hazardous materials, load Carbon Equivalent or other complex formulas to save time on calculations.
With the added ability of action levels, take the guesswork out of analysis.
Formulas
The software supports adding custom formulas
or importing formulas from the Factory Library.
Adding Factory Formulas
Select Options and tap Add from Library.

Select all formulas to be added and return to the
previous screen.
The formulas will now be available.

To activate a formula in the app, check the box to
the right of the formula.
Multiple formulas may be selected at the same

time.
To deactivate a formula, simply uncheck the box.
Adding a Custom Formula
Tap + Add Formula

Enter a Formula Name & Enter the formula.
Addition, Subtraction, Multiplication, and Division

are supported for multi-element formulas.
Single element formulas are also supported.
If you’d like to include an action level, enter a

minimum or maximum passing level.
For a simple Pass/Fail setup, only enter a Passing

threshold.
Less than or equal to 1: Pass

Greater than 1: Fail
Greater than or equal to 1: Pass

Less than 1: Fail
If you’d like to include an inclusive zone, include both a maximum and a minimum.
Less than or equal to 1: Pass
Greater than 2: Fail
Between 1 and 2: Inconclusive
Greater than or equal to 2: Pass

Less than 1: Fail
Between 2 and 1: Inconclusive
18. System Features

Bluetooth
Activating Bluetooth
Open Android Settings.

Select Bluetooth.
Ensure the slider is turned on.

Select your device from the list of Available
Devices.
Wi-Fi
Activating Wi-Fi
Open Android Settings.

Select Wi-Fi.
Turn on Wi-Fi by tapping the slider.

Select your target network.
If required, enter Password then click connect.
If the system will not connect, try setting a static

IP in the Advanced Options Menu.
USB Connectivity
Connecting by USB is the simplest way to transfer data from your system to a computer. Connect the
provided USB-C to USB-A cable to both the analyzer and the target computer. The device will appear
under /This PC/ NGL/ SD Card.
User Management
User Management allows the admin to create additional accounts, manage permissions, and reset
passwords. Only an Admin can create and manage accounts unless specific permissions are given to an
account.
Accessing User Management
Navigate to the settings page and tap the user

icon.
Tap Manage Users to create or manage
additional user profiles.
Tap Create or Load Users.

Tap Create New User.
Select Operator or Admin then press > to

continue.
Enter Operator Name then press > to continue.
Optional: Enter Email then press > to continue.

Enter 5-digit PIN then press > to continue.
Select Permissions and click the save button.
19. Instrument Ownership

Maintenance
The Z-900 Series requires basic periodic maintenance.
Quartz Blast Shield

Primarily, the quartz blast shield requires regular cleaning. Frequency varies with the number of
tests taken. On systems with argon purge, typically the window should be cleaned every 500-
1000 tests. This will vary with environment and material tested. For air-burn systems, the blast
shield should be cleaned every 100-500 tests. For low melting point materials, e.g. tin or lead
solder, more frequent cleaning may be required.
To clean the blast shield, shutdown the system and remove the two nose plate screws. Using a
cotton swab, thoroughly wipe the quartz surface. Note – the black foam gasket should be
towards the outside of the system.
The purchase of a Z-900 includes two spare blast shields in addition to the blast shield in the
system. If there is significant buildup of debris or pitting to this blast shield, it may need to be
replaced. Frequent cleaning extends the life of the blast shield.
Note – do not use alcohol or other similar cleaning agents to clean the blast shield on units used
for measuring and quantifying carbon. Using alcohol may result in contamination to the system.
Argon
The argon canister (if equipped) should be replaced when prompted.
In addition to replacing the argon canister, there is a gasket in the regulator that may wear with
time and usage. If the system is not delivering the expected number of tests per canister,
contact SciAps support – you may need a new argon regulator gasket.
Li-Ion Batteries
Given normal storage and usage, users can expect the battery to deliver 80% or more of its
initial capacity after 300 charge/discharge cycles.
Drift Correction Standards (Reference Materials and Certified Reference Materials)

Drift Correction samples should be re-surfaced as required. For non-carbon applications, re-
surfacing is only required when there is no longer room to run tests on a fresh area. For carbon
applications, surface preparation should be done regularly. With the frequent re-surfacing
required for carbon applications, it is common to develop “cupping” of the drift correction
standard over time. That is, the center of the standard is lower than the outer edge. This can be
checked by holding a straight edge across the standard. The straight edge should appear to
touch the sample across the straight edge. If there is separation between the two edges, use a
belt sander, disc, or mill to flatten the standard.
Storage & Transportation

The SciAps Z-900 Series should always be stored, transported, and shipped in the included protective
case with form-fitting foam. Always shutdown the system and remove the battery before putting the
instrument into the case. For extended storage, keep the system in an ambient temperature of 50° F –
95°F 10° C – 65° C and humidity between 0 and 95%.
Check travel and shipping restrictions for details about proper handling of Li-ion batteries and argon
canisters. Regulations vary by location and vendor.
Note – some airlines have restrictions on argon canisters. Check with your airline for specific policy.
Software Updates
SciAps periodically releases software updates that add features, fix software bugs, and offer other
general improvements. Some updates may require the instrument to be returned to the factory, but
generally, software updates can be completed remotely.
When a compatible software update is available, SciAps will reach out with an updater file in a .sup
format. To run the update, copy the file to the analyzer’s SD Card then follow the directions below:
Software updates are driven through the SciAps

Updater app. This app can be accessed through
Other Apps option.
Scroll to the bottom and select SciAps Updater.

Scroll through the list to find the provided file.
Select the file and tap SELECT.
The SciAps Updater app will give a brief summary

of the contents of the update. Click UPDATE
NOW to continue.
The system will often automatically restart after a

software update.
Appendix: Default Acquisition Settings
Z901 Z902 Z902 Z902 Z902 Z903 Z903 Z903 Z903
Z901 Z901 Z902 Z902
Model QuickSor QuickSort Alloy QuickSor Pipelin QuickSort Alloy Carbon Pipelin
Alloy CSi Alloy Carbon
t + + t e + + + e
Argon
OFF ON ON OFF ON OFF ON ON ON OFF ON ON ON
Enabled
Argon Pre-
n/a 300 300 n/a 300 n/a 300 300 300 n/a 300 300 300
Flush Time
Raster
3 6 6 3 6 3 6 6 6 3 6 6 6
Positions
Cleaning
24 12 12 24 12 24 12 12 12 24 12 12 12
Pulses
Data
32 16 16 32 16 32 16 16 16 32 16 16 16
Pulses
Data Pulse
16 16 16 16 16 16 16 16 16 16 16 16 16
Averaging
Laser Pulse 20 or 50 20 or 20 or 20 or 50 20 or 20 or 50 20 or 20 or 20 or 20 or 50 20 or 20 or 50 20 or
Rate Hz 50 Hz 50 Hz Hz 50 Hz Hz 50 Hz 50 Hz 50 Hz Hz 50 Hz Hz 50 Hz
SHOR SHOR
Pre-Burn OFF OFF OFF OFF OFF OFF LONG OFF OFF SHORT LONG
T T
Number
Pre-burn 25 25 25 25 25 25 25 25 25 25 25 25 25
Pulses
Argon
Pressure n/a 5 5 n/a 5 n/a 5 5 5 n/a 5 5 5
Threshold
Low Argon
n/a ON ON n/a ON n/a ON ON ON n/a ON ON ON
Warning
CCD
Integration 19 35 19 19 19 19 19 19 19 19 19 19 19
Delay
CCD
Integration 0 0 0 0 0 0 0 0 0 0 0 0 0
Period
Appendix: Grade Library Management
The Z-900 Series uses a highly user-friendly CSV file format. In the Z-900 Series, the grade library is saved as a csv
file. Each library will be app specific and stored in:
SD Card/ sciaps/ App Name e.g. quicksort/ gradetables
The naming convention is:
appname_LibraryName.csv
App Filename Location
Alloy alloy_Master.csv SD Card\sciaps\alloy\gradetables
QuickSort quicksort_Master.csv SD Card\sciaps\quicksort\gradetables
CSi carbonsi_Master.csv SD Card\sciaps\carbonsi\gradetables
Alloy+ alloyplus_Master.csv SD Card\sciaps\alloyplus\gradetables
QuickSort+ quicksortplus_Master.csv SD Card\sciaps\quicksortplus\gradetables
Carbon carbon_Master.csv SD Card\sciaps\carbon\gradetables
Carbon+ carbonplus_Master.csv SD Card\sciaps\carbonplus\gradetables
Note 1 – file and folder names are case sensitive.
Note 2 – Only the LibraryName (e.g. Master) will appear in the system UI.
Note 3 – The system only supports csv files – not excel files.
The format of the csv file uses the following approach:

Element Element
Alloy Alloy Standard Eligible abbrev.* abbrev.** Match
name family* source* Personal notes* for GM * * Weight*
Referenc
name base e Comments enabled Z_min H_max H__MW
1100 Al A91100 Upd 2020-01-13 TRUE
2014 Al Upd 2020-01-13 TRUE
2024 Al A92024 Upd 2020-01-13 TRUE
CDA 197 Cu C 19700 TRUE
316 SS TRUE
317 SS TRUE
*optional
** A min value should be included if there is a max value
***If no max value specified, sw assumes 0
Note 1: Must include a specification for the base element. Simply set from 0 to 100 or calculate by:
Min=100-SUM(maxall other elements)
Max=100-SUM(min all other elements)
In practice, it is a good idea to add a buffer to base elements.

Appendix: Sample PDF Report
Appendix: Instrument Operating Temperature
LIBS performs best when it is operated at a consistent, stable temperature. As a general guideline, the Z-
900 will operate at:
Duty Cycle High Medium Low

Ambient temperature + 10°C + 5°C + 2°C
Laser Firing > 30 seconds+ / minute 20 seconds / minute < 10 seconds
To ameliorate the impacts of temperature change, Wavelength Calibration and Warm Up should be
performed anytime the system prompts. On the Z-900 series, Warm Up utility actively raises the
temperature of the instrument by generating heat with the laser. No laser pulses are emitted from the
laser during this process.
When warming up the instrument from a cold start, it is good to practice to warm up the instrument to
the target temperature and then wait for a couple of minutes to allow the system to reach equilibrium.
In the first few minutes after target temperature is achieved, the instrument temperature may quickly
drop back down below the target temperature as heat is transferred from the laser to the
spectrometers and the heat syncs.
If the target temperature needs to be adjusted from its default setting, contact the factory or your local
support contact for support. The target temperature and maximum session time are controlled in
Settings > Factory Settings > Warm Up
Appendix: Hot Samples - Maximum Temperature

The Z-900 series can reliably achieve accurate chemistry on samples that are up to 150°C (300°F). The
system may be used to measure samples up to 500°C (900°F) without damaging the instrument.
However, at temperatures greater than 150°C (300°F), elements such as C and Si will tend to read high
due to accelerated reactivity of the sample with the environment.
Maximum recommended duty cycle: 15 seconds on, 45 seconds off (approximately 1 full carbon test w/
short pre-burn and 5 shots to average per minute).

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SciAps HH-LIBS Analyzers

Z900 Series User Manual

SciAps, Inc. Global Headquarters

7 Constitution Way, Woburn MA 01801

Sample analysis is broken down into five steps (fig 2.1):

1) 1x Hard Sided Instrument Case

Never use a damaged battery.

7. Start Up & User Interface

Batteries should be charged before use. A full

Note: The tapered end of the battery should face

Screw argon canister into regulator on side of

Each canister has enough argon for

Note 1 – Specific, carbon-grade argon is required

Do not remove canisters that are still under

Powering on the system

Firmly press and release the power button on the

To shut down the system, firmly press and hold

When prompted, select Power Off. Wait for the

If required, hold the power button for 12 seconds

After the analyzer starts, you will need to login.

The default account is admin.

Simply press the > icon to continue.

Additional accounts may be generated when

The Admin passcode is 1 2 3 4 5

After entering the passcode, you must accept the

The Z-900 Series analyzer utilizes an embedded

Operation should be limited to trained operators

Features 3 primary functions:

Analyze is used for all analytical testing and data

Settings controls the analyzer settings. There are

Results allows the user to view, review, export,

Additional options include:

User Management: change password, manage

Android Settings: Access WiFi settings, Date and

Other Apps: Includes SciAps Updater, and 3rd

Swiping up from the bottom will show the

Back simply returns you to the previous screen.

Home returns you to the SciAps launch screen.

Open Apps shows all apps that are actively

To start testing – select “Analyze” and select an

The Z-900 Series has an optimal internal

When an app is opened, if the internal

In temperatures outside of the recommended

By default, the system will run a 60 second warm

If the system does not reach the target

Warm up will repeat the protocol.

Cancel will take the operator to the testing

Factory recommendation is to repeat Warm Up

When the analyzer reaches the target

This is indicated by the text “CALIBRATE” on the

When prompted to calibrate, simply tap the on-

The system will shoot an internal standard. No

Wavelength Calibration corrects for any

The instrument monitors time and temperature

After the WL Calibration is complete, the button

When the instrument is ready:

Internal instrument temperature will be indicated

Be sure to hold the sample flush to the laser

Comprised of 6 primary components: