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Department of Textile Engineering
LAB REPORT
Course Name: Wet Processing II
Course Code: Tex-304
Section: 193[d2]
Date of Submission: 06th November 2021.
Submitted By: Submitted To:
Sadia Wasima Mr. Md. Mutasim Uddin
ID: 193003022 Lecturer
Department of Textile Eng. Department of Textile
(regular)
Green University of Green University of
Bangladesh Bangladesh
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Experiment No: 03 2
Experiment Name: Study on dyeing of cotton Polyester fabric with Disperse
Dey by carrier
Introduction:
Dey are colored, unsaturated organic chemical compound capable of giving color
to a substrate coloring or dyeing it.
The term “disperse dye” have been applied to the organic coloring substances
which are free from ionizing groups, are of low water solubility and are suitable for
dyeing hydrophobic fibers. Disperse dyes have substantivity for one or more
hydrophobic fibers e.g. cellulose acetate, nylon, polyester, acrylic and
other synthetic fibers.
The negative charge on the surface of hydrophobic fibers like polyester can not be
reduced by any means, so non-ionic dyes like disperse dyes are used which are not
influenced by that surface charge.
Properties of Disperse Dyes:
⮚ Disperse dyes are nonionic dyes. So they are free from ionizing group.
⮚ They are ready made dyes and are insoluble in water or have very low water
solubility.
⮚ They are organic coloring substances which are suitable for dyeing
hydrophobic fibers.
⮚ Disperse dyes are used for dyeing man made cellulose ester and synthetic
fibers specially acetate and polyester fibers and sometimes nylon and acrylic
fibers.
⮚ Carrier or dispersing agents are required for dyeing with disperse dyes.
⮚ Disperse dyes have fair to good light fastness with rating about 4-5.
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Objective of The Experiment: P
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1. To acquire knowledge about how to do Disperse dye process. G
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2. To get idea about chemicals. 2
3. To know about the type of chemicals & its functions.
4. To achieve practical knowledge about applying Disperse dye on
polyester fabric with carrier
5. To learn about the maintaining of the machine which we us
Apparatus:
1. Polyester.
2. Scissor
3. Electric balance
4. Dyeing pot
5. Biker
6. Pipet (0.1,0.2,0.5 ml)
7. Fresh water
8. Chemical
9. Glass cylinder
10. Dryer
11. Pedder
12. Stirrer
13. Steal Mug
14. Cotton Fabric
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Recipe: 2
Disperse Dye = 4% (OWF)
Dispersing Agent = 1 cc/l
Acetic Acid = 1.5 cc/l
Carrier = 1.5 cc/l
Levelling agent = 1. cc/l.
Wetting agent = 1.5g/l
Sequestering agent = 2.5
cc/l.
Time = 60 min
Temperature = 95°c - 100°c
PH = 4.5-5.5
M: L = 1:12
Sample weight = 11
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Calculation: A
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Total liquor = (11×12) ml
=132ml
Dispersing Dye = Material weight x shade %
Dispersing Dye = 11 x 4%
= 0.44 gm
1×132
Dispersing Agent = cc
1000
=0.132 cc
1.5×132
Acetic Acid = cc
1000
= 0.198 cc
1.5×132
Carrier = gm
1000
=0.198 cc
1×132
Leveling agent = CC
1000
= 0.132 cc
1.5×132
Wetting agent = CC
1000
= 0.198 cc
2.5×132
Sequestering agent is = CC
1000
=0.33 cc
Fresh water = Total Liquor - Other Elements
= {132 -(0.132+0.198+0.198+0.132+0.198+0.33)} cc
=130.812 cc
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After treatment Recipe: 2
For reduction Cleaning
Hydrose = 4 gm/l
Caustic = 5 gm/l
Time = 30 min
Temperature = 50 °c
Calculation:
Sample Weight =11 gm
Total Liquor= (11×12) cc
=132cc
4×132
Hydrose = gm
1000
=0.528 gm
5×132
Caustic = gm
1000
=0.66 gm
Fresh Water = Total Liquor - Other Elements
= {132(0.528+0.66)}cc
=130.812 cc
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Curve: 2
Temperature
90º C; 60-120 min
Dye
+Mtl+Chemicals
60º C 60-120 min
60º C
Wash off
15 min 15 min
40 º C
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Curve: G
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Temp
ºC 6
60 0
mc
90º
D. 50 D i
Dey agent n
A.A 4.5
40 ºC/min
30
20
S.A Carr
W.A
ier
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10 20 30 40 50 60 70 80 90
100
Time
(min)
Working procedure:
1. We took a cotton sample & weighted it on electric balance.
2. We took required apparatus & prepared for experiment.
3. Then we calculated the required amount of the chemicals & water.
4. We took water & chemicals in dyeing pot.
5. We put the sample into dyeing pot & shocked it.
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6. Then we put the pot into machine & set the program of the machine. G
7. After 45 min, we put out the fabric & poured it onto padder. E
8. Finally we ironed it & weighted it again. 2
9. We collected our Final sample.
Precaution:
1. We took wear glasses & gloves.
2. We should wear apron.
3. We should careful about using chemicals.
4. We should take the chemicals in accurate amount.
5. We should measure weight carefully.
6. We should do all the process very carefully.
Conclusion:
Dyes are absorbed evenly & the fabric looks nice for the even shade. By this
experiment we came to know the dyeing of cotton fabric with reactive dyes and
reactive dyes are of the least reactivity because they take more temperature and
more time for dyeing.
